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EP0172965A1 - Continuous pan crystallizer - Google Patents

Continuous pan crystallizer Download PDF

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Publication number
EP0172965A1
EP0172965A1 EP84305974A EP84305974A EP0172965A1 EP 0172965 A1 EP0172965 A1 EP 0172965A1 EP 84305974 A EP84305974 A EP 84305974A EP 84305974 A EP84305974 A EP 84305974A EP 0172965 A1 EP0172965 A1 EP 0172965A1
Authority
EP
European Patent Office
Prior art keywords
pan
massecuite
baffles
cross
compartment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP84305974A
Other languages
German (de)
French (fr)
Other versions
EP0172965B1 (en
Inventor
Peter William Rein
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TONGAAT-HULETT GROUP Ltd
Tongaat Hulett Group Ltd
Original Assignee
TONGAAT-HULETT GROUP Ltd
Tongaat Hulett Group Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to ZA835372A priority Critical patent/ZA846920B/xx
Application filed by TONGAAT-HULETT GROUP Ltd, Tongaat Hulett Group Ltd filed Critical TONGAAT-HULETT GROUP Ltd
Priority to EP84305974A priority patent/EP0172965B1/en
Priority to DE8484305974T priority patent/DE3477495D1/en
Priority to AT84305974T priority patent/ATE41788T1/en
Publication of EP0172965A1 publication Critical patent/EP0172965A1/en
Application granted granted Critical
Publication of EP0172965B1 publication Critical patent/EP0172965B1/en
Expired legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C13SUGAR INDUSTRY
    • C13BPRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B30/00Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
    • C13B30/02Crystallisation; Crystallising apparatus
    • C13B30/022Continuous processes, apparatus therefor
    • CCHEMISTRY; METALLURGY
    • C13SUGAR INDUSTRY
    • C13BPRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B25/00Evaporators or boiling pans specially adapted for sugar juices; Evaporating or boiling sugar juices

Definitions

  • This invention relates to continuous vacuum pan crystallizers.
  • One of the objects of the present invention is to provide a system for massecuite to pass from one compartment to another in such a way as to eliminate problems experienced with other types of continuous pans, such as:
  • Another object of the invention is to eliminate encrustation of sugar on baffles and other surfaces inside the pan. Such encrustation can lead to the formation of lumps or the dislodging of large pieces of encrustation which can block heating tubes or massecuite outlets.
  • a further object is to provide a condenser integral with the pan to reduce the cost of the continuous vacuum pan system.
  • a continuous pan crystalliser includes a plurality of compartments, baffles being provided on either or both sides of the cross-over ports and arranged for the massecuite moving in the direction of the cross-over ports to pass up through the tubes between the baffles and the walls of the compartments.
  • the massecuite must, therefore, have had at least one pass through the tubes before leaving a compartment. Massecuite which passes through the cross-over port is directed into the downtake area of the next compartment.
  • the cross-over ports are preferably located immediately above the calandria, and the turbulence and vigorous flow obtained in these zones keeps the cross-over ports free of encrustation.
  • a further aspect of the invention is the provision of very fine water sprays onto all surfaces extending above the normal massecuite operating level. This eliminates any build-up or encrustation on these surfaces, which can otherwise lead to the formation of lumps. Because the quantity of water sprayed through the sprays is very small, it does not affect the control of the supersaturation of the mother liquor in the massecuite and the crystallisation process in not affected.
  • the continuous pan is provided with an integral condenser. This has the advantage of eliminating the costly steelwork and large diameter vapour piping required for conventional separate condensers.
  • a continuous pan crystallizer includes a plurality of compartments (in this case 12) as shown. Seed massecuite enters the first compartment and syrup or molasses enters the crystallizer through ports 100. The massecuite passes anti-clockwise from one compartment to the next around the apparatus and leaves it through the outlet 102 (see Figure 3).
  • the cross-over ports 104,105 between adjacent compartments ( 1 to 12) each have a pair of baffles 106, 108 which are located a short distance from the ports and above the level of the top of the tubes 110. One vertical edge of the baffles abuts the wall of the apparatus and the other is located a short distance away from the vertical edge of the ports.
  • the massecuite leaving a compartment flows up the tubes between the baffle 108 and the compartment wall, and then through the port 105. It passes through the port and then has to negotiate the second baffle 106 on the downstream side of the compartment 109, which directs the massecuite into the downtake .
  • baffles will differ according to the various parameters of the crystallizer and will have to be determined with a view to obtaining optimum plug flow and direction according to pan capacity and evaporation rate.
  • the second aspect of the invention involves the installation of fine water sprays, positioned above the normal massecuite level. These sprays are so positioned as to direct a fine spray of water onto some or all of the surfaces of the compartment 109, the deflection baffles 106 and 108, and the internal surfaces of the shell of the vessel.
  • the third aspect of the invention is the provision of an integral condenser generally indicated by reference 112.
  • the condenser is attached to the top wall of the crystallizer and thereby obviates the expense of the complicated support means which would otherwise be necessary.
  • the condenser has an injection water inlet 114 and a vacuum connection 116 and an injection water outlet 118.
  • the condenser is conventional, preceded by an entrainment separator 126.
  • the rising vapour is contacted in the condenser with a downwardly directed spray of cooling water for collection in a collector 128 for removal through outlet 118.

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The invention concerns a continuous pan crystallizer which is conventional in that it has a number of interleading compartments with cross-over ports through which the massecuite passes from compartment to compartment. The cross-over ports have baffles on one or both sides thereof to direct the massecuite up the tubes between the baffles and the walls of the compartments in order to avoid short-circuiting or by pass of massecuite from one compartment to another.

Description

  • This invention relates to continuous vacuum pan crystallizers.
  • Most continuous pans are divided into a number of compartments in an attempt to promote plug flow through the system. It is important that the flow system approach plug flow as closely as possible, so that crystal residence times in the continuous pan are uniform, leading to equal growth on all crystals and a uniform crystal size in the product massecuite leaving the pan.
  • One of the objects of the present invention is to provide a system for massecuite to pass from one compartment to another in such a way as to eliminate problems experienced with other types of continuous pans, such as:
    • (a) short-circuiting or by-passing of massecuite from one compartment to another.
    • (b) elimination of encrustation in the opening between compartments.
  • In order to overcome the latter problem, steam blowers needed to be installed in some pans at the cross-over ports, to prevent encrustation in the ports. This is expensive and detrimental to thermal economy.
  • Another object of the invention is to eliminate encrustation of sugar on baffles and other surfaces inside the pan. Such encrustation can lead to the formation of lumps or the dislodging of large pieces of encrustation which can block heating tubes or massecuite outlets.
  • A further object is to provide a condenser integral with the pan to reduce the cost of the continuous vacuum pan system.
  • According to the invention a continuous pan crystalliser includes a plurality of compartments, baffles being provided on either or both sides of the cross-over ports and arranged for the massecuite moving in the direction of the cross-over ports to pass up through the tubes between the baffles and the walls of the compartments.
  • The massecuite must, therefore, have had at least one pass through the tubes before leaving a compartment. Massecuite which passes through the cross-over port is directed into the downtake area of the next compartment. The cross-over ports are preferably located immediately above the calandria, and the turbulence and vigorous flow obtained in these zones keeps the cross-over ports free of encrustation.
  • A further aspect of the invention is the provision of very fine water sprays onto all surfaces extending above the normal massecuite operating level. This eliminates any build-up or encrustation on these surfaces, which can otherwise lead to the formation of lumps. Because the quantity of water sprayed through the sprays is very small, it does not affect the control of the supersaturation of the mother liquor in the massecuite and the crystallisation process in not affected.
  • In a further aspect of the invention, the continuous pan is provided with an integral condenser. This has the advantage of eliminating the costly steelwork and large diameter vapour piping required for conventional separate condensers.
  • An embodiment of the invention is described below with reference to the accompanying drawings, in which:-
    • Figure 1 is a plan view, partly in section of a continuous pan crystalliser according to the invention;
    • Figure 2 is a side view of the same crystallizer;
    • Figure 3 is an end view of the crystallizer; and
    • Figure 1A is a detailed plan of heating tubes in one compartment.
  • In the drawings a continuous pan crystallizer includes a plurality of compartments (in this case 12) as shown. Seed massecuite enters the first compartment and syrup or molasses enters the crystallizer through ports 100. The massecuite passes anti-clockwise from one compartment to the next around the apparatus and leaves it through the outlet 102 (see Figure 3). The cross-over ports 104,105 between adjacent compartments ( 1 to 12) each have a pair of baffles 106, 108 which are located a short distance from the ports and above the level of the top of the tubes 110. One vertical edge of the baffles abuts the wall of the apparatus and the other is located a short distance away from the vertical edge of the ports. Thus the massecuite leaving a compartment flows up the tubes between the baffle 108 and the compartment wall, and then through the port 105. It passes through the port and then has to negotiate the second baffle 106 on the downstream side of the compartment 109, which directs the massecuite into the downtake .
  • It will be appreciated that the dimensions and location of the baffles will differ according to the various parameters of the crystallizer and will have to be determined with a view to obtaining optimum plug flow and direction according to pan capacity and evaporation rate.
  • The second aspect of the invention involves the installation of fine water sprays, positioned above the normal massecuite level. These sprays are so positioned as to direct a fine spray of water onto some or all of the surfaces of the compartment 109, the deflection baffles 106 and 108, and the internal surfaces of the shell of the vessel.
  • The third aspect of the invention is the provision of an integral condenser generally indicated by reference 112.
  • The condenser is attached to the top wall of the crystallizer and thereby obviates the expense of the complicated support means which would otherwise be necessary. The condenser has an injection water inlet 114 and a vacuum connection 116 and an injection water outlet 118.
  • The condenser is conventional, preceded by an entrainment separator 126. The rising vapour is contacted in the condenser with a downwardly directed spray of cooling water for collection in a collector 128 for removal through outlet 118.

Claims (6)

1. A continuous pan crystalliser including a plurality of compartments having calandria and cross-over ports, characterised by the provision of baffles located on either or both sides of the cross-over ports, and spaced away therefrom to provide a passage for the massecuite moving in the direction of the cross-over ports to pass up the tubes of the calandria between the baffles and the walls of the compartments.
2. The pan of claim 1 characterised in that the baffles are arranged for the massecuite to have at least one pass through the tubes before leaving a compartment.
3. The pan of claim 1 or claim 2 characterised in that the cross-over ports and baffles are arranged for massecuite which enters a compartment to be directed towards the downtake of the compartment.
4. The pan of any of the above claims characterised in that the cross-over ports are located in an area of vigorous boiling just above the tube-plate.
5. The pan of any of the above claims characterised in that it includes water sprays located and adapted to overcome encrustation on the baffles and sides of the pan.
6. The pan of any of the above claims characterised in that a condenser is located integral with the pan and in direct communication with the compartments.
EP84305974A 1983-07-22 1984-08-31 Continuous pan crystallizer Expired EP0172965B1 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
ZA835372A ZA846920B (en) 1983-07-22 1983-07-22
EP84305974A EP0172965B1 (en) 1983-07-22 1984-08-31 Continuous pan crystallizer
DE8484305974T DE3477495D1 (en) 1984-08-31 1984-08-31 Continuous pan crystallizer
AT84305974T ATE41788T1 (en) 1984-08-31 1984-08-31 CONTINUOUS CRYSTALLIZATION COOKING APPARATUS.

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
ZA835372A ZA846920B (en) 1983-07-22 1983-07-22
EP84305974A EP0172965B1 (en) 1983-07-22 1984-08-31 Continuous pan crystallizer
ZA846920 1984-09-04

Publications (2)

Publication Number Publication Date
EP0172965A1 true EP0172965A1 (en) 1986-03-05
EP0172965B1 EP0172965B1 (en) 1989-03-29

Family

ID=27227239

Family Applications (1)

Application Number Title Priority Date Filing Date
EP84305974A Expired EP0172965B1 (en) 1983-07-22 1984-08-31 Continuous pan crystallizer

Country Status (2)

Country Link
EP (1) EP0172965B1 (en)
ZA (1) ZA846920B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001091875A1 (en) * 2000-06-01 2001-12-06 The Tongaat-Hulett Group Limited Continuous vacuum pan
WO2009095873A3 (en) * 2008-01-30 2010-01-14 Tongaat Hulett Limited Structure for use in a sugar making process
WO2013068934A1 (en) * 2011-11-11 2013-05-16 Tongaat Hulett Limited Evaporator arrangement incorporating a condenser

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB378341A (en) * 1931-02-28 1932-08-11 Werkspoor Nv Apparatus for crystallizing sugar and other solutions by evaporation or cooling
GB1141639A (en) * 1966-07-28 1969-01-29 Fives Lillie Cail Soc Prevention of encrustation on the internal surfaces of crystallizers of the evaporator type
FR2329317A1 (en) * 1975-10-29 1977-05-27 Skyring Alan Crystallising evaporator, e.g. for sugar prodn. - with natural recirculation
AU527620B2 (en) * 1977-06-20 1983-03-17 Evans Deakin Industries Limited Continuous crystalliser

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB378341A (en) * 1931-02-28 1932-08-11 Werkspoor Nv Apparatus for crystallizing sugar and other solutions by evaporation or cooling
GB1141639A (en) * 1966-07-28 1969-01-29 Fives Lillie Cail Soc Prevention of encrustation on the internal surfaces of crystallizers of the evaporator type
FR2329317A1 (en) * 1975-10-29 1977-05-27 Skyring Alan Crystallising evaporator, e.g. for sugar prodn. - with natural recirculation
AU527620B2 (en) * 1977-06-20 1983-03-17 Evans Deakin Industries Limited Continuous crystalliser

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001091875A1 (en) * 2000-06-01 2001-12-06 The Tongaat-Hulett Group Limited Continuous vacuum pan
US6991708B2 (en) 2000-06-01 2006-01-31 The Tongaat-Hulett Group Limited Continuous vacuum pan
WO2009095873A3 (en) * 2008-01-30 2010-01-14 Tongaat Hulett Limited Structure for use in a sugar making process
WO2013068934A1 (en) * 2011-11-11 2013-05-16 Tongaat Hulett Limited Evaporator arrangement incorporating a condenser

Also Published As

Publication number Publication date
ZA846920B (en) 1985-03-05
EP0172965B1 (en) 1989-03-29

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