EP0172965A1 - Continuous pan crystallizer - Google Patents
Continuous pan crystallizer Download PDFInfo
- Publication number
- EP0172965A1 EP0172965A1 EP84305974A EP84305974A EP0172965A1 EP 0172965 A1 EP0172965 A1 EP 0172965A1 EP 84305974 A EP84305974 A EP 84305974A EP 84305974 A EP84305974 A EP 84305974A EP 0172965 A1 EP0172965 A1 EP 0172965A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- pan
- massecuite
- baffles
- cross
- compartment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000007921 spray Substances 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 238000009835 boiling Methods 0.000 claims 1
- 239000013078 crystal Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 235000013379 molasses Nutrition 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 235000020357 syrup Nutrition 0.000 description 1
- 239000006188 syrup Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
- C13B30/02—Crystallisation; Crystallising apparatus
- C13B30/022—Continuous processes, apparatus therefor
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B25/00—Evaporators or boiling pans specially adapted for sugar juices; Evaporating or boiling sugar juices
Definitions
- This invention relates to continuous vacuum pan crystallizers.
- One of the objects of the present invention is to provide a system for massecuite to pass from one compartment to another in such a way as to eliminate problems experienced with other types of continuous pans, such as:
- Another object of the invention is to eliminate encrustation of sugar on baffles and other surfaces inside the pan. Such encrustation can lead to the formation of lumps or the dislodging of large pieces of encrustation which can block heating tubes or massecuite outlets.
- a further object is to provide a condenser integral with the pan to reduce the cost of the continuous vacuum pan system.
- a continuous pan crystalliser includes a plurality of compartments, baffles being provided on either or both sides of the cross-over ports and arranged for the massecuite moving in the direction of the cross-over ports to pass up through the tubes between the baffles and the walls of the compartments.
- the massecuite must, therefore, have had at least one pass through the tubes before leaving a compartment. Massecuite which passes through the cross-over port is directed into the downtake area of the next compartment.
- the cross-over ports are preferably located immediately above the calandria, and the turbulence and vigorous flow obtained in these zones keeps the cross-over ports free of encrustation.
- a further aspect of the invention is the provision of very fine water sprays onto all surfaces extending above the normal massecuite operating level. This eliminates any build-up or encrustation on these surfaces, which can otherwise lead to the formation of lumps. Because the quantity of water sprayed through the sprays is very small, it does not affect the control of the supersaturation of the mother liquor in the massecuite and the crystallisation process in not affected.
- the continuous pan is provided with an integral condenser. This has the advantage of eliminating the costly steelwork and large diameter vapour piping required for conventional separate condensers.
- a continuous pan crystallizer includes a plurality of compartments (in this case 12) as shown. Seed massecuite enters the first compartment and syrup or molasses enters the crystallizer through ports 100. The massecuite passes anti-clockwise from one compartment to the next around the apparatus and leaves it through the outlet 102 (see Figure 3).
- the cross-over ports 104,105 between adjacent compartments ( 1 to 12) each have a pair of baffles 106, 108 which are located a short distance from the ports and above the level of the top of the tubes 110. One vertical edge of the baffles abuts the wall of the apparatus and the other is located a short distance away from the vertical edge of the ports.
- the massecuite leaving a compartment flows up the tubes between the baffle 108 and the compartment wall, and then through the port 105. It passes through the port and then has to negotiate the second baffle 106 on the downstream side of the compartment 109, which directs the massecuite into the downtake .
- baffles will differ according to the various parameters of the crystallizer and will have to be determined with a view to obtaining optimum plug flow and direction according to pan capacity and evaporation rate.
- the second aspect of the invention involves the installation of fine water sprays, positioned above the normal massecuite level. These sprays are so positioned as to direct a fine spray of water onto some or all of the surfaces of the compartment 109, the deflection baffles 106 and 108, and the internal surfaces of the shell of the vessel.
- the third aspect of the invention is the provision of an integral condenser generally indicated by reference 112.
- the condenser is attached to the top wall of the crystallizer and thereby obviates the expense of the complicated support means which would otherwise be necessary.
- the condenser has an injection water inlet 114 and a vacuum connection 116 and an injection water outlet 118.
- the condenser is conventional, preceded by an entrainment separator 126.
- the rising vapour is contacted in the condenser with a downwardly directed spray of cooling water for collection in a collector 128 for removal through outlet 118.
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
Description
- This invention relates to continuous vacuum pan crystallizers.
- Most continuous pans are divided into a number of compartments in an attempt to promote plug flow through the system. It is important that the flow system approach plug flow as closely as possible, so that crystal residence times in the continuous pan are uniform, leading to equal growth on all crystals and a uniform crystal size in the product massecuite leaving the pan.
- One of the objects of the present invention is to provide a system for massecuite to pass from one compartment to another in such a way as to eliminate problems experienced with other types of continuous pans, such as:
- (a) short-circuiting or by-passing of massecuite from one compartment to another.
- (b) elimination of encrustation in the opening between compartments.
- In order to overcome the latter problem, steam blowers needed to be installed in some pans at the cross-over ports, to prevent encrustation in the ports. This is expensive and detrimental to thermal economy.
- Another object of the invention is to eliminate encrustation of sugar on baffles and other surfaces inside the pan. Such encrustation can lead to the formation of lumps or the dislodging of large pieces of encrustation which can block heating tubes or massecuite outlets.
- A further object is to provide a condenser integral with the pan to reduce the cost of the continuous vacuum pan system.
- According to the invention a continuous pan crystalliser includes a plurality of compartments, baffles being provided on either or both sides of the cross-over ports and arranged for the massecuite moving in the direction of the cross-over ports to pass up through the tubes between the baffles and the walls of the compartments.
- The massecuite must, therefore, have had at least one pass through the tubes before leaving a compartment. Massecuite which passes through the cross-over port is directed into the downtake area of the next compartment. The cross-over ports are preferably located immediately above the calandria, and the turbulence and vigorous flow obtained in these zones keeps the cross-over ports free of encrustation.
- A further aspect of the invention is the provision of very fine water sprays onto all surfaces extending above the normal massecuite operating level. This eliminates any build-up or encrustation on these surfaces, which can otherwise lead to the formation of lumps. Because the quantity of water sprayed through the sprays is very small, it does not affect the control of the supersaturation of the mother liquor in the massecuite and the crystallisation process in not affected.
- In a further aspect of the invention, the continuous pan is provided with an integral condenser. This has the advantage of eliminating the costly steelwork and large diameter vapour piping required for conventional separate condensers.
- An embodiment of the invention is described below with reference to the accompanying drawings, in which:-
- Figure 1 is a plan view, partly in section of a continuous pan crystalliser according to the invention;
- Figure 2 is a side view of the same crystallizer;
- Figure 3 is an end view of the crystallizer; and
- Figure 1A is a detailed plan of heating tubes in one compartment.
- In the drawings a continuous pan crystallizer includes a plurality of compartments (in this case 12) as shown. Seed massecuite enters the first compartment and syrup or molasses enters the crystallizer through
ports 100. The massecuite passes anti-clockwise from one compartment to the next around the apparatus and leaves it through the outlet 102 (see Figure 3). The cross-over ports 104,105 between adjacent compartments ( 1 to 12) each have a pair of 106, 108 which are located a short distance from the ports and above the level of the top of thebaffles tubes 110. One vertical edge of the baffles abuts the wall of the apparatus and the other is located a short distance away from the vertical edge of the ports. Thus the massecuite leaving a compartment flows up the tubes between thebaffle 108 and the compartment wall, and then through theport 105. It passes through the port and then has to negotiate thesecond baffle 106 on the downstream side of thecompartment 109, which directs the massecuite into the downtake . - It will be appreciated that the dimensions and location of the baffles will differ according to the various parameters of the crystallizer and will have to be determined with a view to obtaining optimum plug flow and direction according to pan capacity and evaporation rate.
- The second aspect of the invention involves the installation of fine water sprays, positioned above the normal massecuite level. These sprays are so positioned as to direct a fine spray of water onto some or all of the surfaces of the
compartment 109, the 106 and 108, and the internal surfaces of the shell of the vessel.deflection baffles - The third aspect of the invention is the provision of an integral condenser generally indicated by
reference 112. - The condenser is attached to the top wall of the crystallizer and thereby obviates the expense of the complicated support means which would otherwise be necessary. The condenser has an
injection water inlet 114 and avacuum connection 116 and aninjection water outlet 118. - The condenser is conventional, preceded by an
entrainment separator 126. The rising vapour is contacted in the condenser with a downwardly directed spray of cooling water for collection in acollector 128 for removal throughoutlet 118.
Claims (6)
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ZA835372A ZA846920B (en) | 1983-07-22 | 1983-07-22 | |
| EP84305974A EP0172965B1 (en) | 1983-07-22 | 1984-08-31 | Continuous pan crystallizer |
| DE8484305974T DE3477495D1 (en) | 1984-08-31 | 1984-08-31 | Continuous pan crystallizer |
| AT84305974T ATE41788T1 (en) | 1984-08-31 | 1984-08-31 | CONTINUOUS CRYSTALLIZATION COOKING APPARATUS. |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ZA835372A ZA846920B (en) | 1983-07-22 | 1983-07-22 | |
| EP84305974A EP0172965B1 (en) | 1983-07-22 | 1984-08-31 | Continuous pan crystallizer |
| ZA846920 | 1984-09-04 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EP0172965A1 true EP0172965A1 (en) | 1986-03-05 |
| EP0172965B1 EP0172965B1 (en) | 1989-03-29 |
Family
ID=27227239
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP84305974A Expired EP0172965B1 (en) | 1983-07-22 | 1984-08-31 | Continuous pan crystallizer |
Country Status (2)
| Country | Link |
|---|---|
| EP (1) | EP0172965B1 (en) |
| ZA (1) | ZA846920B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2001091875A1 (en) * | 2000-06-01 | 2001-12-06 | The Tongaat-Hulett Group Limited | Continuous vacuum pan |
| WO2009095873A3 (en) * | 2008-01-30 | 2010-01-14 | Tongaat Hulett Limited | Structure for use in a sugar making process |
| WO2013068934A1 (en) * | 2011-11-11 | 2013-05-16 | Tongaat Hulett Limited | Evaporator arrangement incorporating a condenser |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB378341A (en) * | 1931-02-28 | 1932-08-11 | Werkspoor Nv | Apparatus for crystallizing sugar and other solutions by evaporation or cooling |
| GB1141639A (en) * | 1966-07-28 | 1969-01-29 | Fives Lillie Cail Soc | Prevention of encrustation on the internal surfaces of crystallizers of the evaporator type |
| FR2329317A1 (en) * | 1975-10-29 | 1977-05-27 | Skyring Alan | Crystallising evaporator, e.g. for sugar prodn. - with natural recirculation |
| AU527620B2 (en) * | 1977-06-20 | 1983-03-17 | Evans Deakin Industries Limited | Continuous crystalliser |
-
1983
- 1983-07-22 ZA ZA835372A patent/ZA846920B/xx unknown
-
1984
- 1984-08-31 EP EP84305974A patent/EP0172965B1/en not_active Expired
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB378341A (en) * | 1931-02-28 | 1932-08-11 | Werkspoor Nv | Apparatus for crystallizing sugar and other solutions by evaporation or cooling |
| GB1141639A (en) * | 1966-07-28 | 1969-01-29 | Fives Lillie Cail Soc | Prevention of encrustation on the internal surfaces of crystallizers of the evaporator type |
| FR2329317A1 (en) * | 1975-10-29 | 1977-05-27 | Skyring Alan | Crystallising evaporator, e.g. for sugar prodn. - with natural recirculation |
| AU527620B2 (en) * | 1977-06-20 | 1983-03-17 | Evans Deakin Industries Limited | Continuous crystalliser |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2001091875A1 (en) * | 2000-06-01 | 2001-12-06 | The Tongaat-Hulett Group Limited | Continuous vacuum pan |
| US6991708B2 (en) | 2000-06-01 | 2006-01-31 | The Tongaat-Hulett Group Limited | Continuous vacuum pan |
| WO2009095873A3 (en) * | 2008-01-30 | 2010-01-14 | Tongaat Hulett Limited | Structure for use in a sugar making process |
| WO2013068934A1 (en) * | 2011-11-11 | 2013-05-16 | Tongaat Hulett Limited | Evaporator arrangement incorporating a condenser |
Also Published As
| Publication number | Publication date |
|---|---|
| ZA846920B (en) | 1985-03-05 |
| EP0172965B1 (en) | 1989-03-29 |
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