EA200800635A1 - Способ производства диалкилкарбоната и диола - Google Patents
Способ производства диалкилкарбоната и диолаInfo
- Publication number
- EA200800635A1 EA200800635A1 EA200800635A EA200800635A EA200800635A1 EA 200800635 A1 EA200800635 A1 EA 200800635A1 EA 200800635 A EA200800635 A EA 200800635A EA 200800635 A EA200800635 A EA 200800635A EA 200800635 A1 EA200800635 A1 EA 200800635A1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- diol
- carbonate
- cyclic carbonate
- dialkyl carbonate
- production
- Prior art date
Links
- 150000002009 diols Chemical class 0.000 title abstract 5
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 3
- 150000005676 cyclic carbonates Chemical class 0.000 abstract 3
- 238000004821 distillation Methods 0.000 abstract 3
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 1
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 238000005809 transesterification reaction Methods 0.000 abstract 1
- 238000002834 transmittance Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C68/00—Preparation of esters of carbonic or haloformic acids
- C07C68/06—Preparation of esters of carbonic or haloformic acids from organic carbonates
- C07C68/065—Preparation of esters of carbonic or haloformic acids from organic carbonates from alkylene carbonates
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C27/00—Processes involving the simultaneous production of more than one class of oxygen-containing compounds
- C07C27/26—Purification; Separation; Stabilisation
- C07C27/28—Purification; Separation; Stabilisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/18—Polyhydroxylic acyclic alcohols
- C07C31/20—Dihydroxylic alcohols
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Представлен процесс производства диалкилкарбоната и диола из циклического карбоната и одноатомного алифатического спирта, в котором циклический карбонат может быть преобразован с высокой степенью конверсии, диалкилкарбонат и диол могут быть получены с высокой селективностью, любая усложненная обработка (например, добавление воды в ходе процесса дистилляции/очистки) не требуется, и может быть получен диол высокой чистоты, имеющий высокий коэффициент УФ-пропускания и низкое содержание альдегида. Процесс производства диалкилкарбоната и диола, включающий стадию реакции циклического карбоната с одноатомным алифатическим спиртом в присутствии катализатора в реакторе для переэтерификации, оборудованном колонной для непрерывной многоступенчатой дистилляции тарельчатого типа, в котором реакция в дистилляционной колонне выполняется при заранее заданных условиях (время пребывания, температура).
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2005272557 | 2005-09-20 | ||
| PCT/JP2006/317492 WO2007034669A1 (ja) | 2005-09-20 | 2006-09-05 | ジアルキルカーボネートとジオールの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EA200800635A1 true EA200800635A1 (ru) | 2008-06-30 |
| EA013128B1 EA013128B1 (ru) | 2010-02-26 |
Family
ID=37888722
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EA200800635A EA013128B1 (ru) | 2005-09-20 | 2006-09-05 | Способ производства диалкилкарбоната и диола |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US7799939B2 (ru) |
| EP (1) | EP1927583B1 (ru) |
| JP (1) | JP4272686B2 (ru) |
| KR (1) | KR100895602B1 (ru) |
| CN (1) | CN101268030B (ru) |
| BR (1) | BRPI0616303B1 (ru) |
| EA (1) | EA013128B1 (ru) |
| TW (1) | TWI311987B (ru) |
| WO (1) | WO2007034669A1 (ru) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102010006657A1 (de) * | 2010-02-03 | 2011-08-04 | Bayer MaterialScience AG, 51373 | Verfahren zur Herstellung von Dialkylcarbonaten |
| CN102304050A (zh) * | 2011-07-25 | 2012-01-04 | 屈强好 | 连续精馏碳酸二甲酯和1，2-丙二醇的方法 |
| CN111116330A (zh) * | 2019-12-30 | 2020-05-08 | 山西中科惠安化工有限公司 | 一种酯交换生产碳酸酯过程中碳化工艺过滤后滤液的分离装置和方法 |
| JP6916366B1 (ja) * | 2020-11-16 | 2021-08-11 | 株式会社日本触媒 | ジオールの製造方法 |
| KR102644181B1 (ko) * | 2020-11-27 | 2024-03-05 | 롯데케미칼 주식회사 | 염기성 이온교환수지를 이용한 이종 선형 카보네이트의 제조 방법 |
| KR20240046762A (ko) | 2021-10-05 | 2024-04-09 | 아사히 가세이 가부시키가이샤 | 고순도 디아릴카르보네이트의 제조 방법 |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3642858A (en) * | 1969-02-12 | 1972-02-15 | Dow Chemical Co | Carbonate synthesis from alkylene carbonates |
| US3803201A (en) * | 1971-02-22 | 1974-04-09 | Dow Chemical Co | Synthesis of dimethyl carbonate |
| IT1034961B (it) * | 1975-04-09 | 1979-10-10 | Snam Progetti | Procedimento per la preparazione di dialchilcarbonati |
| DE2740243A1 (de) * | 1977-09-07 | 1979-03-15 | Bayer Ag | Verfahren zur herstellung von dialkylcarbonaten |
| DE2740251A1 (de) | 1977-09-07 | 1979-03-22 | Bayer Ag | Verfahren zur herstellung von dialkylcarbonaten |
| JPS5463023A (en) | 1977-10-26 | 1979-05-21 | Mitsubishi Chem Ind Ltd | Ester exchange of carbonate |
| JPS6022697B2 (ja) | 1978-05-16 | 1985-06-03 | 日曹油化工業株式会社 | ジアルキル炭酸エステルの製造法 |
| JPS6022698B2 (ja) | 1978-11-08 | 1985-06-03 | 日曹油化工業株式会社 | ジアルキル炭酸エステルの製法 |
| JPS5564551A (en) | 1978-11-08 | 1980-05-15 | Nisso Yuka Kogyo Kk | Preparation of dialkyl carbonate |
| JPS5610144A (en) | 1979-07-05 | 1981-02-02 | Showa Denko Kk | Preparation of dialkyl carbonate |
| US4691041A (en) * | 1986-01-03 | 1987-09-01 | Texaco Inc. | Process for production of ethylene glycol and dimethyl carbonate |
| US4661609A (en) | 1986-07-31 | 1987-04-28 | Texaco Inc. | Process for cosynthesis of ethylene glycol and dimethyl carbonate |
| US4734518A (en) * | 1987-01-12 | 1988-03-29 | Texaco Inc. | Process for cosynthesis of ethylene glycol and dimethyl carbonate |
| JPH0737422B2 (ja) | 1987-03-26 | 1995-04-26 | 旭化成工業株式会社 | ジアルキルカ−ボネ−トの製造方法 |
| JPS6431737U (ru) | 1987-08-20 | 1989-02-27 | ||
| DE4129316A1 (de) | 1991-09-03 | 1993-03-04 | Bayer Ag | Verfahren zur kontinuierlichen herstellung von dialkylcarbonaten |
| DE4216121A1 (de) | 1992-05-15 | 1993-11-18 | Bayer Ag | Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonaten |
| EP0889025B1 (en) | 1995-12-22 | 2002-04-03 | Asahi Kasei Kabushiki Kaisha | Process for continuously preparing dialkyl carbonates and diols |
| CN1145600C (zh) | 1998-06-10 | 2004-04-14 | 旭化成株式会社 | 连续生产碳酸二烷基酯和二醇的方法 |
| WO2000051954A1 (en) * | 1999-03-03 | 2000-09-08 | Asahi Kasei Kabushiki Kaisha | Process for continuously producing dialkyl carbonate and diol |
| JP4467204B2 (ja) | 2001-04-13 | 2010-05-26 | 旭化成ケミカルズ株式会社 | ジアルキルカーボネートおよびジオールの製造方法 |
| JP2002371037A (ja) * | 2001-06-12 | 2002-12-26 | Mitsubishi Chemicals Corp | 高純度ジメチルカーボネートの製造方法 |
| JP4424898B2 (ja) | 2002-10-08 | 2010-03-03 | 旭化成ケミカルズ株式会社 | ジアルキルカーボネートおよびジオールを製造する方法 |
| JP4192587B2 (ja) | 2002-12-16 | 2008-12-10 | 東ソー株式会社 | 光透過性容器の中の液体の有無を検知する装置 |
| JP3853295B2 (ja) | 2003-01-29 | 2006-12-06 | 電気化学工業株式会社 | 噴霧方法及び装置 |
-
2006
- 2006-09-05 BR BRPI0616303A patent/BRPI0616303B1/pt active IP Right Grant
- 2006-09-05 EA EA200800635A patent/EA013128B1/ru not_active IP Right Cessation
- 2006-09-05 CN CN2006800346304A patent/CN101268030B/zh active Active
- 2006-09-05 EP EP06783181A patent/EP1927583B1/en active Active
- 2006-09-05 JP JP2007536438A patent/JP4272686B2/ja active Active
- 2006-09-05 US US11/990,913 patent/US7799939B2/en active Active
- 2006-09-05 KR KR1020087006638A patent/KR100895602B1/ko active Active
- 2006-09-05 WO PCT/JP2006/317492 patent/WO2007034669A1/ja not_active Ceased
- 2006-09-19 TW TW095134670A patent/TWI311987B/zh active
Also Published As
| Publication number | Publication date |
|---|---|
| EP1927583A4 (en) | 2010-09-08 |
| JP4272686B2 (ja) | 2009-06-03 |
| KR100895602B1 (ko) | 2009-05-06 |
| TWI311987B (en) | 2009-07-11 |
| WO2007034669A1 (ja) | 2007-03-29 |
| EA013128B1 (ru) | 2010-02-26 |
| BRPI0616303A2 (pt) | 2012-05-22 |
| EP1927583A1 (en) | 2008-06-04 |
| US7799939B2 (en) | 2010-09-21 |
| TW200726740A (en) | 2007-07-16 |
| CN101268030A (zh) | 2008-09-17 |
| KR20080037727A (ko) | 2008-04-30 |
| CN101268030B (zh) | 2011-05-11 |
| JPWO2007034669A1 (ja) | 2009-03-19 |
| EP1927583B1 (en) | 2012-05-02 |
| BRPI0616303B1 (pt) | 2015-12-01 |
| US20090149669A1 (en) | 2009-06-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s) |
Designated state(s): AM AZ BY KZ KG MD TJ TM |
|
| PD4A | Registration of transfer of a eurasian patent in accordance with the succession in title |