EA200300020A1 - METHOD AND DEVICE FOR EXTRACTING TUNGSTEN AND MOLYBDENE FROM POOR LOW-SORT ORE RAW MATERIALS - Google Patents
METHOD AND DEVICE FOR EXTRACTING TUNGSTEN AND MOLYBDENE FROM POOR LOW-SORT ORE RAW MATERIALSInfo
- Publication number
- EA200300020A1 EA200300020A1 EA200300020A EA200300020A EA200300020A1 EA 200300020 A1 EA200300020 A1 EA 200300020A1 EA 200300020 A EA200300020 A EA 200300020A EA 200300020 A EA200300020 A EA 200300020A EA 200300020 A1 EA200300020 A1 EA 200300020A1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- tungsten
- condenser
- molybdenum
- raw materials
- condensed
- Prior art date
Links
Landscapes
- Manufacture And Refinement Of Metals (AREA)
Abstract
Изобретение относится к неорганической химии и химической технологии, а именно к редкометальной металлургии, конкретнее к извлечению и очистке вольфрамовых и молибденовых соединений газофазным методом. Целью настоящего изобретения является извлечение вольфрама и молибдена в низкотемпературном режиме хлорирования (НТХ) путем переработки низкосортного сырья поточно-селективным методом. Поставленная цель достигается созданием способа низкотемпературного режима хлорирования (НТХ) бедного рудного сырья для извлечения вольфрама и молибдена и устройства для его осуществления с установкой системы раздельной конденсации возгонов с обеспечением непрерывности ее функционирования и дальнейшего совершенного разделения твердофазных конденсатов в виде индивидуальных продуктов. Установка состоит из гранулятора шихты (1), контейнеров (2), сушильной камеры (3) горячим воздухом, затем контейнеры сверху тельфером (7) при помощи подъемника контейнеров (8) погружаются в реактор (6), в который пропускается хлористая сера (4), полученная ранее пропусканием хлора через жидкую серу (5). В конденсаторе (9) конденсируется основная доля паров хлорного железа; в конденсаторе (11) конденсируется основная масса паров оксотетрахлорида вольфрама; в конденсаторе (13) конденсируется молибден, если он присутствует в вольфрамовом рудном сырье, что бывает нередко. Из конденсатора (13) выходит сернистый газ с микропримесью паров хлоридов титана, рения, мышьяка и других возможных элементов. Для отделения этих примесей сернистый газ проходит через промывную башню (14), орошаемую оборотной водой, подаваемой насосом (15); очищенный от примесей сернистый газ из промывной башниThe invention relates to inorganic chemistry and chemical technology, namely, rare-metal metallurgy, more specifically to the extraction and purification of tungsten and molybdenum compounds by the gas-phase method. The aim of the present invention is the extraction of tungsten and molybdenum in the low-temperature chlorination mode (STC) by processing low-grade raw materials by the flow-selective method. This goal is achieved by creating a method of low-temperature chlorination (NTX) mode of poor ore raw materials for the extraction of tungsten and molybdenum and a device for its implementation with the installation of a separate sublimation condensation system ensuring continuity of its operation and further perfect separation of solid-phase condensates in the form of individual products. The installation consists of a granulator charge (1), containers (2), a drying chamber (3) with hot air, then the containers on top of the hoist (7) with the help of a container lift (8) are immersed in a reactor (6), into which sulfuric chloride (4 , previously obtained by passing chlorine through liquid sulfur (5). In the condenser (9) the main fraction of ferric chloride vapor is condensed; in the condenser (11) the bulk of the tungsten oxotetrachloride vapor is condensed; molybdenum is condensed in condenser (13) if it is present in a tungsten ore material, which is not uncommon. Sulfur dioxide escapes from the condenser (13) with a micronutrient vapor of titanium chloride, rhenium, arsenic and other possible elements. To separate these impurities, sulfur dioxide passes through a wash tower (14), irrigated with circulating water supplied by a pump (15); purified sulfur dioxide from the wash tower
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EA200300020A EA004480B1 (en) | 2002-12-10 | 2002-12-10 | Method and device for recovery tungsten and molybdenum from low grade ore material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EA200300020A EA004480B1 (en) | 2002-12-10 | 2002-12-10 | Method and device for recovery tungsten and molybdenum from low grade ore material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EA200300020A1 true EA200300020A1 (en) | 2004-04-29 |
| EA004480B1 EA004480B1 (en) | 2004-04-29 |
Family
ID=32405642
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EA200300020A EA004480B1 (en) | 2002-12-10 | 2002-12-10 | Method and device for recovery tungsten and molybdenum from low grade ore material |
Country Status (1)
| Country | Link |
|---|---|
| EA (1) | EA004480B1 (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018219417A1 (en) * | 2017-06-02 | 2018-12-06 | Общество С Ограниченной Ответственностью "Редметпром" | Method and device for extracting molybdenum from low-grade crude ore |
| US10287177B1 (en) | 2018-05-08 | 2019-05-14 | Robert Ten | Method and apparatus for extracting high-purity molybdenum oxide powders and nanopowders from low-grade concentrates |
| US10612111B2 (en) | 2018-08-21 | 2020-04-07 | Robert Ten | Method and apparatus for extracting high-purity gold from ore |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6780137B2 (en) | 2018-07-25 | 2020-11-04 | Ｊｘ金属株式会社 | Manufacturing method of high bulk density molybdenum oxychloride |
-
2002
- 2002-12-10 EA EA200300020A patent/EA004480B1/en not_active IP Right Cessation
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018219417A1 (en) * | 2017-06-02 | 2018-12-06 | Общество С Ограниченной Ответственностью "Редметпром" | Method and device for extracting molybdenum from low-grade crude ore |
| US10287177B1 (en) | 2018-05-08 | 2019-05-14 | Robert Ten | Method and apparatus for extracting high-purity molybdenum oxide powders and nanopowders from low-grade concentrates |
| WO2019215563A1 (en) * | 2018-05-08 | 2019-11-14 | Makhnitskaya, Elena | Method and apparatus for extracting high-purity molibdenium oxide powders |
| US10612111B2 (en) | 2018-08-21 | 2020-04-07 | Robert Ten | Method and apparatus for extracting high-purity gold from ore |
Also Published As
| Publication number | Publication date |
|---|---|
| EA004480B1 (en) | 2004-04-29 |
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| MM4A | Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s) |
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| NF4A | Restoration of lapsed right to a eurasian patent |
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| MM4A | Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s) |
Designated state(s): RU |