EA199900753A1 - Усовершенствованный способ синтеза мочевины и устройство для его осуществления - Google Patents
Усовершенствованный способ синтеза мочевины и устройство для его осуществленияInfo
- Publication number
- EA199900753A1 EA199900753A1 EA199900753A EA199900753A EA199900753A1 EA 199900753 A1 EA199900753 A1 EA 199900753A1 EA 199900753 A EA199900753 A EA 199900753A EA 199900753 A EA199900753 A EA 199900753A EA 199900753 A1 EA199900753 A1 EA 199900753A1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- synthesis
- urea
- condensate
- pipes
- contact
- Prior art date
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
- C07C273/04—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0003—Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/002—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by condensation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
- B01J10/002—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/006—Baffles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0073—Sealings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/04—Pressure vessels, e.g. autoclaves
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00078—Fingers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00083—Coils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00761—Details of the reactor
- B01J2219/00763—Baffles
- B01J2219/00765—Baffles attached to the reactor wall
- B01J2219/00777—Baffles attached to the reactor wall horizontal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
- B01J2219/0277—Metal based
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/18—Details relating to the spatial orientation of the reactor
- B01J2219/182—Details relating to the spatial orientation of the reactor horizontal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/18—Details relating to the spatial orientation of the reactor
- B01J2219/185—Details relating to the spatial orientation of the reactor vertical
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/19—Details relating to the geometry of the reactor
- B01J2219/194—Details relating to the geometry of the reactor round
- B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
- B01J2219/1943—Details relating to the geometry of the reactor round circular or disk-shaped cylindrical
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/10—Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Настоящим изобретением является усовершенствованный способ синтеза мочевины из аммиака и двуокиси углерода, предотвращающий коррозию участков соединений плиты для труб и охлаждающих труб, находящихся в контакте с конденсатом, в конденсаторе, установленном вертикально или горизонтально. В соответствии с этим способом участки, находящиеся в контакте с конденсатом, соединений плиты для труб и охлаждающих труб в конденсаторе защищают от коррозии путем покрытия участков жидким аммиаком или раствором, обогащенным аммиаком, в процессе синтеза мочевины, включающем отделение не прореагировавшего аммиака и не прореагировавшей двуокиси углерода в виде их газообразной смеси от раствора для синтеза мочевины при давлении, по существу равном давлению синтеза мочевины, контакт газообразной смеси с абсорбирующей средой в конденсаторе для образования конденсата и рециркуляцию конденсата в колонну синтеза.Международная заявка была опубликована вместе с отчетом о международном поиске.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP34934097A JP4112056B2 (ja) | 1997-12-18 | 1997-12-18 | 改良された尿素の合成方法および装置 |
| PCT/JP1998/005698 WO1999031053A1 (en) | 1997-12-18 | 1998-12-17 | Improved process for the synthesis of urea and equipment therefor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EA199900753A1 true EA199900753A1 (ru) | 2000-02-28 |
| EA001299B1 EA001299B1 (ru) | 2000-12-25 |
Family
ID=18403117
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EA199900753A EA001299B1 (ru) | 1997-12-18 | 1998-12-17 | Усовершенствованный способ синтеза мочевины и устройство для его осуществления |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US6093850A (ru) |
| EP (1) | EP0976724B1 (ru) |
| JP (1) | JP4112056B2 (ru) |
| CN (1) | CN1071742C (ru) |
| BR (1) | BR9806081B1 (ru) |
| CA (1) | CA2268974C (ru) |
| DE (1) | DE69829556T2 (ru) |
| EA (1) | EA001299B1 (ru) |
| ES (1) | ES2238777T3 (ru) |
| ID (1) | ID23791A (ru) |
| UA (1) | UA57064C2 (ru) |
| WO (1) | WO1999031053A1 (ru) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4292835B2 (ja) * | 2003-03-13 | 2009-07-08 | 沖電気工業株式会社 | 秘密再構成方法、分散秘密再構成装置、及び秘密再構成システム |
| US7922065B2 (en) * | 2004-08-02 | 2011-04-12 | Ati Properties, Inc. | Corrosion resistant fluid conducting parts, methods of making corrosion resistant fluid conducting parts and equipment and parts replacement methods utilizing corrosion resistant fluid conducting parts |
| WO2006083250A1 (en) * | 2005-02-03 | 2006-08-10 | Stepan Company | Continuous segmented plug flow reactor |
| WO2006083251A1 (en) * | 2005-02-03 | 2006-08-10 | Stepan Company | Method for performing chemical reactions in a continuous segmented plug flow reactor |
| CN101166714B (zh) | 2005-04-27 | 2011-11-30 | 东洋工程株式会社 | 尿素合成装置 |
| EP1876171B1 (en) | 2005-04-27 | 2011-12-07 | Toyo Engineering Corporation | Apparatus for urea synthesis and method of improving the same |
| EA019803B1 (ru) * | 2006-12-08 | 2014-06-30 | Стамикарбон Б.В. | Способ получения мочевины |
| EP2399669A1 (en) | 2010-06-24 | 2011-12-28 | Borealis Agrolinz Melamine GmbH | Horizontal high-pressure melamine reactor |
| US10118259B1 (en) | 2012-12-11 | 2018-11-06 | Ati Properties Llc | Corrosion resistant bimetallic tube manufactured by a two-step process |
| GB2530447B (en) | 2013-05-28 | 2020-02-26 | Toyo Engineering Corp | Urea synthesis method |
| EP3248962A1 (de) * | 2016-05-24 | 2017-11-29 | Linde Aktiengesellschaft | Prozess und anlagenverbund zur herstellung von harnstoff |
| JP6862612B2 (ja) | 2017-10-27 | 2021-04-21 | スタミカーボン・ベー・フェー | 高圧カルバメート凝縮器 |
| WO2021170391A1 (en) | 2020-02-25 | 2021-09-02 | Casale Sa | Process and plant for the synthesis of urea |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL164328C (nl) * | 1970-04-02 | 1980-12-15 | Stamicarbon | Werkwijze voor het verhogen van de weerstand tegen cor- rosie van austenitische chroom-nikkelstalen, alsmede werkwijze voor de bereiding van ureum in apperatuur waarvan de weerstand tegen corrosie aldus is verhoogd. |
| US4173615A (en) * | 1974-07-08 | 1979-11-06 | Mitsui Toatsu Chemicals, Incorporated | Chemical apparatus for corrosive materials |
| US5223238A (en) * | 1992-01-16 | 1993-06-29 | The M. W. Kellogg Company | Method for treating ammonia and urea condensates |
| ZA96686B (en) * | 1995-02-01 | 1996-08-16 | Urea Casale Sa | Process and plant for the production of urea with high conversion yield and low energy consumption |
| IT1274362B (it) * | 1995-02-16 | 1997-07-17 | Snam Progetti | Procedimento ad alta resa per la sintesi dell'urea |
| JPH08291130A (ja) * | 1995-04-25 | 1996-11-05 | Toyo Eng Corp | 尿素製造方法 |
| JPH08301834A (ja) * | 1995-05-02 | 1996-11-19 | Toyo Eng Corp | 尿素の合成方法 |
| JPH08301835A (ja) * | 1995-05-09 | 1996-11-19 | Toyo Eng Corp | 尿素合成方法 |
| JPH08311008A (ja) * | 1995-05-16 | 1996-11-26 | Toyo Eng Corp | 尿素製造方法 |
| JPH08325222A (ja) * | 1995-06-02 | 1996-12-10 | Toyo Eng Corp | 尿素の製造方法 |
| JPH08325221A (ja) * | 1995-06-02 | 1996-12-10 | Toyo Eng Corp | 尿素製造方法 |
| US5523483A (en) * | 1995-06-16 | 1996-06-04 | The M. W. Kellogg Company | Integrated urea/ammonia process |
| IT1275451B (it) * | 1995-06-30 | 1997-08-07 | Snam Progetti | Procedimento per la sintesi dell'urea comprendente due separate zone di reazione |
| US5744009A (en) * | 1995-07-07 | 1998-04-28 | The M. W. Kellogg Company | Method and apparatus for recovering condensables in vapor from a urea vacuum evaporator |
| EP0822181B1 (en) * | 1996-08-01 | 2001-05-02 | Urea Casale S.A. | Process and plant for the production of urea with high conversion yield and low energy consumption |
| JP3987607B2 (ja) * | 1996-10-07 | 2007-10-10 | 東洋エンジニアリング株式会社 | 改良された尿素合成方法および装置 |
| JPH10120643A (ja) * | 1996-10-24 | 1998-05-12 | Toyo Eng Corp | 改良された尿素合成方法 |
-
1997
- 1997-12-18 JP JP34934097A patent/JP4112056B2/ja not_active Expired - Lifetime
-
1998
- 1998-12-17 EA EA199900753A patent/EA001299B1/ru not_active IP Right Cessation
- 1998-12-17 EP EP98961376A patent/EP0976724B1/en not_active Expired - Lifetime
- 1998-12-17 ES ES98961376T patent/ES2238777T3/es not_active Expired - Lifetime
- 1998-12-17 CA CA002268974A patent/CA2268974C/en not_active Expired - Fee Related
- 1998-12-17 ID IDW990135D patent/ID23791A/id unknown
- 1998-12-17 DE DE69829556T patent/DE69829556T2/de not_active Expired - Lifetime
- 1998-12-17 WO PCT/JP1998/005698 patent/WO1999031053A1/ja not_active Ceased
- 1998-12-17 UA UA99095033A patent/UA57064C2/ru unknown
- 1998-12-17 BR BRPI9806081-3A patent/BR9806081B1/pt not_active IP Right Cessation
- 1998-12-17 CN CN98801618A patent/CN1071742C/zh not_active Expired - Fee Related
- 1998-12-17 US US09/269,164 patent/US6093850A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE69829556D1 (de) | 2005-05-04 |
| UA57064C2 (ru) | 2003-06-16 |
| CN1071742C (zh) | 2001-09-26 |
| CN1242763A (zh) | 2000-01-26 |
| EP0976724B1 (en) | 2005-03-30 |
| EP0976724A1 (en) | 2000-02-02 |
| CA2268974A1 (en) | 1999-06-18 |
| WO1999031053A1 (en) | 1999-06-24 |
| BR9806081B1 (pt) | 2010-07-27 |
| ES2238777T3 (es) | 2005-09-01 |
| DE69829556T2 (de) | 2005-08-18 |
| EP0976724A4 (en) | 2001-04-18 |
| JPH11180942A (ja) | 1999-07-06 |
| JP4112056B2 (ja) | 2008-07-02 |
| BR9806081A (pt) | 1999-08-24 |
| US6093850A (en) | 2000-07-25 |
| EA001299B1 (ru) | 2000-12-25 |
| ID23791A (id) | 2000-05-11 |
| CA2268974C (en) | 2003-07-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s) |
Designated state(s): AM AZ KG MD TJ |
|
| MM4A | Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s) |
Designated state(s): BY KZ TM |
|
| MK4A | Patent expired |
Designated state(s): RU |