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DK3658490T3 - Fremgangsmåde til forbedring af effektiviteten af et ammoniaksyntesegasanlæg - Google Patents

Fremgangsmåde til forbedring af effektiviteten af et ammoniaksyntesegasanlæg Download PDF

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Publication number
DK3658490T3
DK3658490T3 DK18739540.5T DK18739540T DK3658490T3 DK 3658490 T3 DK3658490 T3 DK 3658490T3 DK 18739540 T DK18739540 T DK 18739540T DK 3658490 T3 DK3658490 T3 DK 3658490T3
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Denmark
Prior art keywords
improving
procedure
efficiency
ammonia synthesis
synthesis plant
Prior art date
Application number
DK18739540.5T
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English (en)
Inventor
Pat A Han
Jensen Annette E Krøll
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Topsoe As
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Publication of DK3658490T3 publication Critical patent/DK3658490T3/da

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/025—Preparation or purification of gas mixtures for ammonia synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/382—Multi-step processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/384—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts the catalyst being continuously externally heated
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/48—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents followed by reaction of water vapour with carbon monoxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/04—Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/04—Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • C01C1/0417—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst characterised by the synthesis reactor, e.g. arrangement of catalyst beds and heat exchangers in the reactor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/02—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon from oxides of a carbon
    • C07C1/12—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon from oxides of a carbon from carbon dioxide with hydrogen
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/02—Hydrogen or oxygen
    • C25B1/04—Hydrogen or oxygen by electrolysis of water
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B15/00—Operating or servicing cells
    • C25B15/08—Supplying or removing reactants or electrolytes; Regeneration of electrolytes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0233—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being a steam reforming step
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0283—Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0435—Catalytic purification
    • C01B2203/0445—Selective methanation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0455—Purification by non-catalytic desulfurisation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/0475—Composition of the impurity the impurity being carbon dioxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/06—Integration with other chemical processes
    • C01B2203/068—Ammonia synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0805—Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/0811—Methods of heating the process for making hydrogen or synthesis gas by combustion of fuel
    • C01B2203/0816—Heating by flames
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14—Details of the flowsheet
    • C01B2203/141—At least two reforming, decomposition or partial oxidation steps in parallel
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14—Details of the flowsheet
    • C01B2203/146—At least two purification steps in series
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y02P20/133—Renewable energy sources, e.g. sunlight
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Combustion & Propulsion (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Electrochemistry (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Industrial Gases (AREA)
DK18739540.5T 2017-07-25 2018-07-11 Fremgangsmåde til forbedring af effektiviteten af et ammoniaksyntesegasanlæg DK3658490T3 (da)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DKPA201700425 2017-07-25
DKPA201700522 2017-09-25
PCT/EP2018/068806 WO2019020377A1 (en) 2017-07-25 2018-07-11 METHOD FOR ENHANCING THE EFFICIENCY OF AN AMMONIA SYNTHESIS GAS INSTALLATION

Publications (1)

Publication Number Publication Date
DK3658490T3 true DK3658490T3 (da) 2024-07-22

Family

ID=62873363

Family Applications (1)

Application Number Title Priority Date Filing Date
DK18739540.5T DK3658490T3 (da) 2017-07-25 2018-07-11 Fremgangsmåde til forbedring af effektiviteten af et ammoniaksyntesegasanlæg

Country Status (20)

Country Link
US (2) US20200172406A1 (da)
EP (1) EP3658490B1 (da)
KR (1) KR102599452B1 (da)
CN (1) CN110958988A (da)
AU (1) AU2018305811B2 (da)
CA (1) CA3069871A1 (da)
CL (1) CL2020000152A1 (da)
DK (1) DK3658490T3 (da)
ES (1) ES2982501T3 (da)
FI (1) FI3658490T3 (da)
HR (1) HRP20241029T1 (da)
HU (1) HUE068047T2 (da)
IL (1) IL271943B2 (da)
MY (1) MY203008A (da)
PE (1) PE20200687A1 (da)
PL (1) PL3658490T3 (da)
PT (1) PT3658490T (da)
UA (1) UA126924C2 (da)
WO (1) WO2019020377A1 (da)
ZA (1) ZA201908115B (da)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102019214812A1 (de) 2019-09-27 2020-06-18 Thyssenkrupp Ag Verfahren und Anlage zur Erzeugung von Synthesegas
KR20220148839A (ko) 2020-02-28 2022-11-07 토프쉐 에이/에스 합성 가스의 제조 방법
EP4281410A1 (en) * 2021-01-21 2023-11-29 Casale Sa Method for preparing a synthesis gas
US20240158247A1 (en) * 2021-03-30 2024-05-16 Casale Sa Process for ammonia synthesis using green hydrogen
BE1030241B1 (de) * 2022-02-03 2023-09-04 Thyssenkrupp Ind Solutions Ag Anlage zur Erzeugung von Ammoniak
EP4600203A1 (en) * 2024-02-07 2025-08-13 Yara International ASA System and process for the combined production of ammonia and hydrogen
WO2025219222A1 (de) 2024-04-18 2025-10-23 Thyssenkrupp Uhde Gmbh Anlage und verfahren zur gemeinsamen verdichtung von wasserstoff und erdgas
LU103279B1 (de) * 2024-04-18 2025-10-20 Thyssenkrupp Ag Anlage und Verfahren zur gemeinsamen Verdichtung von Wasserstoff und Erdgas

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4107277A (en) * 1976-07-13 1978-08-15 Da Rosa Aldo Vieira Process for production of ammonia
EP0093502B2 (en) * 1982-04-14 1988-11-17 Imperial Chemical Industries Plc Ammonia production process
WO1999017875A1 (en) * 1997-10-07 1999-04-15 Nkk Corporation Catalyst for producing hydrogen or synthesis gas and method of producing hydrogen or synthesis gas
EP1657409A1 (en) * 2004-11-15 2006-05-17 Elsam A/S A method of and an apparatus for producing electrical power
US7875402B2 (en) * 2005-02-23 2011-01-25 Exxonmobil Research And Engineering Company Proton conducting solid oxide fuel cell systems having temperature swing reforming
CN101880046A (zh) * 2009-05-05 2010-11-10 中村德彦 复合设备
CN101892492A (zh) * 2009-05-19 2010-11-24 无锡尚弗能源科技有限公司 中高压纯水水电解制氢系统
JP5280348B2 (ja) * 2009-12-25 2013-09-04 東京瓦斯株式会社 ハイブリッド水素製造システム
EP2404869A1 (en) * 2010-07-06 2012-01-11 Ammonia Casale S.A. Process for producing ammonia synthesis gas
FR2969998B1 (fr) 2010-12-29 2013-02-08 Areva Procede de synthese d'hydrocarbones avec rejets de co2 minimum
FR2971789B1 (fr) * 2011-02-22 2013-02-22 Areva Methode de production de methanol ou d'hydrocarbures a partir d'une matiere carbonee, avec une etape de reformage dont les conditions de fontionnement sont ajustees selectivement
EP2589574B1 (en) 2011-11-02 2015-10-21 Casale Sa Method for load regulation of an ammonia plant
WO2014056535A1 (en) * 2012-10-11 2014-04-17 Haldor Topsøe A/S Process for the production of synthesis gas
US20150129806A1 (en) * 2013-11-08 2015-05-14 Ammonia Casale Sa Process for Producing Ammonia Synthesis Gas and a Method for Revamping a Front-End of an Ammonia Plant
CA2933420C (en) * 2013-12-12 2021-09-28 Haldor Topsoe A/S Process for reforming synthesis gas from hydrocarbon feedstock
EP3247820A1 (en) * 2015-01-21 2017-11-29 SABIC Global Technologies B.V. Solar powered systems and methods for generating hydrogen gas and oxygen gas from water
WO2016149507A1 (en) * 2015-03-17 2016-09-22 Siluria Technologies, Inc. Oxidative coupling of methane methods and systems
GB2545474A (en) 2015-12-17 2017-06-21 Avocet Infinite Plc Integrated system and method for producing methanol product
CN110944937A (zh) 2017-07-25 2020-03-31 托普索公司 用于制备合成气的方法

Also Published As

Publication number Publication date
FI3658490T3 (fi) 2024-08-09
PE20200687A1 (es) 2020-06-11
US20200172406A1 (en) 2020-06-04
UA126924C2 (uk) 2023-02-22
CN110958988A (zh) 2020-04-03
KR20200031623A (ko) 2020-03-24
BR112020001492A2 (pt) 2020-07-21
AU2018305811B2 (en) 2023-11-23
CA3069871A1 (en) 2019-01-31
PL3658490T3 (pl) 2024-09-09
KR102599452B1 (ko) 2023-11-08
IL271943A (en) 2020-02-27
IL271943B (en) 2022-10-01
CL2020000152A1 (es) 2020-07-31
HRP20241029T1 (hr) 2024-11-08
WO2019020377A1 (en) 2019-01-31
MY203008A (en) 2024-06-03
US20230257275A1 (en) 2023-08-17
EP3658490A1 (en) 2020-06-03
ES2982501T3 (es) 2024-10-16
IL271943B2 (en) 2023-02-01
EP3658490B1 (en) 2024-07-03
AU2018305811A1 (en) 2020-01-23
ZA201908115B (en) 2023-04-26
HUE068047T2 (hu) 2024-12-28
NZ760482A (en) 2023-10-27
PT3658490T (pt) 2024-07-26

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