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DE3235561A1 - WORKING MATERIAL PAIR FOR USE IN SORPTION REFRIGERATORS, CONTAINING TRIFLUORETHANOL - Google Patents

WORKING MATERIAL PAIR FOR USE IN SORPTION REFRIGERATORS, CONTAINING TRIFLUORETHANOL

Info

Publication number
DE3235561A1
DE3235561A1 DE19823235561 DE3235561A DE3235561A1 DE 3235561 A1 DE3235561 A1 DE 3235561A1 DE 19823235561 DE19823235561 DE 19823235561 DE 3235561 A DE3235561 A DE 3235561A DE 3235561 A1 DE3235561 A1 DE 3235561A1
Authority
DE
Germany
Prior art keywords
diethyl
dibutyl
dipropyl
refrigerant
sorption
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE19823235561
Other languages
German (de)
Inventor
Armin 2000 Hamburg Hildebrandt
Dieter Dipl.-Chem.Dipl.-Ing.Dr. 2080 Pinneberg Veltwisch
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Deutsche BP AG
Original Assignee
Deutsche BP AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Deutsche BP AG filed Critical Deutsche BP AG
Priority to DE19823235561 priority Critical patent/DE3235561A1/en
Priority to EP19830903002 priority patent/EP0120048A1/en
Priority to JP58503057A priority patent/JPS59501632A/en
Priority to PCT/GB1983/000231 priority patent/WO1984001165A1/en
Publication of DE3235561A1 publication Critical patent/DE3235561A1/en
Priority to DK2594/84A priority patent/DK259484D0/en
Withdrawn legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K5/00Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
    • C09K5/02Materials undergoing a change of physical state when used
    • C09K5/04Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa
    • C09K5/047Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa for absorption-type refrigeration systems

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Combustion & Propulsion (AREA)
  • Thermal Sciences (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Sorption Type Refrigeration Machines (AREA)

Abstract

Mixtures of trifluoroethanol and at least one of sulfolane, 3-methylsulfolane, ethylene-, diethylene-, triethylene- or tetratethylene glycol, tri- or tetraethylene glycol dimethylether, di- or tripropylene glycol, di- or tripropylene glycol dimethyl ether.

Description

Beschreibung description

Die Erfindung betrifft Arbeitsstoffpaare zur Verwendung in Sorptionskältemaschinen, enthaltend 2,2, 2-Trifluorethanol als Kältemittel.The invention relates to pairs of working substances for use in sorption refrigeration machines, containing 2,2,2-trifluoroethanol as a refrigerant.

Bei Sorptionskühlmaschinen bzw. -warmepumpen wird in einem geschlossenen System ein Arbeitsstoffpaar, bestehend aus einem Kältemittel und einem Absorptionsmittel, verwendet, wobei das Absorptionsmittel häufig aus einer hochsiedenden Flüssigkeit besteht. Die Kühlung wird durch Verdampfung des Kältemittels in einer Verdampfereinrichtung oder dergleichen erreicht, wobei an der Verdampfereinrichtung ein Strömungsmittel abgekühlt wird, das an das Kältemittel Verdampfungswärme liefert. Das verdampfte Kältemittel wird in einem Absorberteil in dem an Kältemittel armen Absorptionsmittel absorbiert. Die bei der Absorption gebildete Wärme wird an ein externes Kühlmittel abgegeben. Die an Kältemittel reiche Lösung wird zu einem Austreiberteil (Kocherteil) geführt, wo man die Lösung zum Austreiben des Kältemittels erwärmt.Sorption cooling machines or heat pumps are used in a closed System a pair of working materials, consisting of a refrigerant and an absorbent, used, the absorbent often consisting of a high-boiling liquid consists. The cooling is achieved by evaporation of the refrigerant in an evaporator device or the like, with a fluid at the evaporator device is cooled, which supplies heat of vaporization to the refrigerant. That evaporated Refrigerant is in an absorber part in the absorbent poor in refrigerant absorbed. The heat generated during absorption is transferred to an external coolant submitted. The refrigerant-rich solution becomes an expeller part (cooker part) led, where the solution is heated to drive off the refrigerant.

Die erhaltene, an Kältemittel arme Lösung, die noch wenig Kältemittel enthält, wird zum Absorberteil zurückgeführt.The solution obtained, low in refrigerant, which is still low in refrigerant contains, is returned to the absorber part.

Das ausgetriebene dampfförmige Kältemittel wird durch Wärmeaustausch mit einem externen Kühlmittel verflüssigt und dann erneut dem Verdampferteil zugeführt.The expelled vaporous refrigerant is through heat exchange liquefied with an external coolant and then fed back to the evaporator section.

Arbeitsstoffpaare für die Verwendung in Sorptionskältemaschinen sollen insbesondere die folgenden Anforderungen erfüllen: a) Eine möglichst große Differenz der Siedetemperaturen zwischen dem Kältemittel und der Mischung aus Kälte-und Sorptionsmittel, b) ein flüssiger Aggregatzustand der Mischung aus Kälte-und Sorptionsmittel im Arbeitsbereich, c) thermische Stabilität der Mischung aus Kälte- und Sorptionsmittel, d) ein geringer Rektfikationsaufwand für das Gemisch aus Kälte- und Sorptionsmittel, e) eine geringe Viskosität des Gemisches aus Kälte- und Sorptionsmittel im Arbeitsbereich. sowie f) eine hohe Austreibertemperatur der Mischung aus Kälte-und Sorptionsmittel, wenn ein hohes Nutztemperaturniveau gewünscht wird.Working substance pairs for use in sorption chillers are intended in particular meet the following requirements: a) One if possible large difference in boiling temperatures between the refrigerant and the mixture of refrigerants and sorbents, b) a liquid state of aggregation of the mixture Refrigerants and sorbents in the work area, c) thermal stability of the mixture from refrigerants and sorbents, d) a low rectification effort for the mixture of refrigerants and sorbents, e) a low viscosity of the mixture of refrigerants and sorbents in the work area. and f) a high expeller temperature Mixture of refrigerant and sorbent, if a high useful temperature level is required will.

Aufgabe der Erfindung ist die Zurverfügungstellung von Arbeitsstoffpaaren der eingangs genannten Art, die die oben genannten Anforderungen erfüllen.The object of the invention is to provide pairs of working materials of the type mentioned above, which meet the above requirements.

Die Arbeitsstoffpaare der Erfindung enthalten als Sorptionsmittel Benzylalkohol, Ethylen-, Diethylen-, Triethylen-und/oder Tetraethylenglykol, Triethylen- und/oder Tetraethylenglykoldimethylether, Diethylenglykoldibutylether, 1, 3-Propandiol, 1 , 4-Butandiol, 1 5-Pentandiol, Mono-, Di- und/oder Tripropylenglykol, Di- und/oder Tripropylenglykoldimethylether, Diethyl-, Dipropyl- undZoder Dibutylphthalat, Benzoesäurebutyl- und/oder-benzylester, Diethyl-, Dipropyl- und/oder Dibutylsuccinat, Sebacinsäurediethylester, Propylencarbonat, Dimethyl-, Diethyl-, Dipropyl- und/oder Dibutylsulfoxid, Sulfolan undfoder 3-Methyl-sulfolan, Phosphorsäuretriethyl- , -tripropyl- und/oder-tributylester, Di- -und/oder Triethanolamin und/oder N-Methylddethanolamin sowie gegebenenfalls übliche Additive wie Korrosionsinhibitoren, Stabilisatoren und/oder Tenside, Bevorzugt sind Arbeitsstoffpaare, die das Sorptionsmittel in einer Menge von 50 - 95 Gew-%, bezogen auf das Gesamtgewicht des Arbeitsstoffpaares, enthalten.The working substance pairs of the invention contain as sorbents Benzyl alcohol, ethylene, diethylene, triethylene and / or tetraethylene glycol, triethylene and / or tetraethylene glycol dimethyl ether, diethylene glycol dibutyl ether, 1,3-propanediol, 1, 4-butanediol, 15-pentanediol, mono-, di- and / or tripropylene glycol, di- and / or Tripropylene glycol dimethyl ether, Diethyl, dipropyl and Z or dibutyl phthalate, Butyl and / or benzyl benzoate, diethyl, dipropyl and / or dibutyl succinate, Diethyl sebacate, propylene carbonate, dimethyl, diethyl, dipropyl and / or Dibutyl sulfoxide, sulfolane andfor 3-methyl-sulfolane, phosphoric acid triethyl-, -tripropyl- and / or tributyl ester, di- and / or triethanolamine and / or N-methylddethanolamine and, if appropriate, customary additives such as corrosion inhibitors, stabilizers and / or surfactants, preferred are pairs of working substances that contain the sorbent in one Contains an amount of 50 - 95% by weight, based on the total weight of the working substance pair.

Claims (2)

Arbeitsstoffpaar zur Verwendung in Sorptionskältemaschinen, enthaltend Trifluorethanol.A pair of working materials for use in sorption refrigeration machines, containing Trifluoroethanol. Patentansprüche Arbeitsstoffpaar zur Verwendung in Sorptionskältemaschinen, enthaltend 2,2,2-Trifluorethanol als Kältemittel, dadurch gekennzeichnet, daß es als Sorptionsmittel Benzylalkohol, Ethylen-, Diethylen-, Triethylen- und/oder Tetraethylenglykol, Triethylen- und/oder Tetraethylenglykoldimethylether, Diethylenglykoldibutylether, 1,3-Propandiol, 1, 4-Butandiol, 1, 5-Pentandiol, Mono-, Di- und/oder Tripropylenglykol, Di- und/oder Tripropylenglykoldimethylether, Diethyl-, Dipropyl- und/oder Dibutylphthalat, Benzoesäurebutyl- und/oder -benzylester, Diethyl-, Dipropyl- und/oder Dibutylsuccinat, Sebacinsäurediethylester, Propylencarbonat, Dimethyl-, Diethyl-, Dipropyl- und/oder Dibutylsulfoxid, Sulfolan und/oder 3-Methyl-sulfolan, Phosphorsäuretriethyl-, -tripropyl- und/oder-tributylester, Di- und/oder Triethanolamin und/oder N-Methyldiethanolamin sowie gegebenenfalls übliche Additive wie Korrosionsinhibitoren, Stabilisatoren und/oder Tenside enthält. Patent claims working substance pair for use in sorption chillers, containing 2,2,2-trifluoroethanol as refrigerant, characterized in that it as a sorbent benzyl alcohol, ethylene, diethylene, triethylene and / or tetraethylene glycol, Triethylene and / or tetraethylene glycol dimethyl ether, diethylene glycol dibutyl ether, 1,3-propanediol, 1,4-butanediol, 1,5-pentanediol, mono-, di- and / or tripropylene glycol, Di- and / or tripropylene glycol dimethyl ether, diethyl, dipropyl and / or dibutyl phthalate, Butyl and / or benzyl benzoate, diethyl, dipropyl and / or dibutyl succinate, Diethyl sebacate, propylene carbonate, dimethyl, diethyl, dipropyl and / or Dibutyl sulfoxide, sulfolane and / or 3-methyl-sulfolane, phosphoric acid triethyl, tripropyl and / or tributyl ester, di- and / or triethanolamine and / or N-methyldiethanolamine and, if appropriate, customary additives such as corrosion inhibitors, stabilizers and / or contains surfactants. 2. Arbeitsstoffpaar nach Anspruch 1, dadurch gekennzeichnet, daß es das Sorptionsmittel in einer Menge von 50 bis 95 Gew.-%, bezogen auf das Gesamtgewicht des Arbeitsstoffpaares, enthält.2. Working substance pair according to claim 1, characterized in that it the sorbent in an amount of 50 to 95% by weight, based on the total weight of the working substance pair.
DE19823235561 1982-09-25 1982-09-25 WORKING MATERIAL PAIR FOR USE IN SORPTION REFRIGERATORS, CONTAINING TRIFLUORETHANOL Withdrawn DE3235561A1 (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
DE19823235561 DE3235561A1 (en) 1982-09-25 1982-09-25 WORKING MATERIAL PAIR FOR USE IN SORPTION REFRIGERATORS, CONTAINING TRIFLUORETHANOL
EP19830903002 EP0120048A1 (en) 1982-09-25 1983-09-21 Fluids for use in sorption refrigerators and heat pumps
JP58503057A JPS59501632A (en) 1982-09-25 1983-09-21 Fluids used in absorption refrigerators and heat pumps
PCT/GB1983/000231 WO1984001165A1 (en) 1982-09-25 1983-09-21 Fluids for use in sorption refrigerators and heat pumps
DK2594/84A DK259484D0 (en) 1982-09-25 1984-05-25 LIQUIDS FOR USE IN SORPTION COOLERS AND HEAT PUMPS

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19823235561 DE3235561A1 (en) 1982-09-25 1982-09-25 WORKING MATERIAL PAIR FOR USE IN SORPTION REFRIGERATORS, CONTAINING TRIFLUORETHANOL

Publications (1)

Publication Number Publication Date
DE3235561A1 true DE3235561A1 (en) 1984-03-29

Family

ID=6174155

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19823235561 Withdrawn DE3235561A1 (en) 1982-09-25 1982-09-25 WORKING MATERIAL PAIR FOR USE IN SORPTION REFRIGERATORS, CONTAINING TRIFLUORETHANOL

Country Status (5)

Country Link
EP (1) EP0120048A1 (en)
JP (1) JPS59501632A (en)
DE (1) DE3235561A1 (en)
DK (1) DK259484D0 (en)
WO (1) WO1984001165A1 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3418705A1 (en) * 1984-05-19 1985-12-12 GEA Luftkühlergesellschaft Happel GmbH & Co, 4630 Bochum Systems of materials for sorption processes
DE3514108A1 (en) * 1985-04-19 1986-10-23 Dieter Dipl.-Ing. 7024 Filderstadt Seher Multi-component mixtures for sorption heat pumps, sorption refrigerators and sorption heat transformers
WO1990005172A1 (en) * 1988-11-11 1990-05-17 Asahi Glass Company Ltd. Tetrafluoroethane composition for a regrigerator

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4948525A (en) * 1988-04-06 1990-08-14 Nippon Oil Co., Ltd. Lubricating oil compositions for refrigerators
US5543068A (en) * 1988-04-08 1996-08-06 Japan Energy Corporation Lubricating oils for flon compressors, compositions adapted for flon compressors and composed of mixtures of said lubricating oils and flon, and process for lubricating flon compressor by using said lubricating oils
US6962665B2 (en) * 2000-12-08 2005-11-08 E. I. Du Pont De Nemours And Company Refrigerant compositions containing a compatibilizer
US6991744B2 (en) 2000-12-08 2006-01-31 E. I. Du Pont De Nemours And Company Refrigerant compositions containing a compatibilizer

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2615443A1 (en) * 1975-04-10 1976-10-21 Allied Chem PROCEDURE FOR ABSORPTION HEATING AND ABSORPTION PAIR FOR CARRYING OUT THE PROCEDURE
DE2832237A1 (en) * 1977-07-22 1979-02-08 Allied Chem ABSORPTION PAIR FOR ABSORPTION HEATING PROCESS

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3722211A (en) * 1970-09-28 1973-03-27 Halocarbon Prod Corp Prime mover system utilizing trifluoroethanol as working fluid
JPS5679175A (en) * 1979-11-30 1981-06-29 Daikin Ind Ltd Absorption refrigerant carrier composition
DE3003471C2 (en) * 1980-01-31 1983-02-17 M.A.N. Maschinenfabrik Augsburg-Nürnberg AG, 8000 München Working substance pair for sorption heat pumps
JPS592477B2 (en) * 1980-02-12 1984-01-18 三洋電機株式会社 Absorption liquid for absorption refrigerators

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2615443A1 (en) * 1975-04-10 1976-10-21 Allied Chem PROCEDURE FOR ABSORPTION HEATING AND ABSORPTION PAIR FOR CARRYING OUT THE PROCEDURE
DE2832237A1 (en) * 1977-07-22 1979-02-08 Allied Chem ABSORPTION PAIR FOR ABSORPTION HEATING PROCESS

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
DE-Z: Klima-Kälte-Heizung, 1/1980, S.865-876 *
US-Z: Refrigerating Engineering, 8/1944, S.97-100 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3418705A1 (en) * 1984-05-19 1985-12-12 GEA Luftkühlergesellschaft Happel GmbH & Co, 4630 Bochum Systems of materials for sorption processes
DE3514108A1 (en) * 1985-04-19 1986-10-23 Dieter Dipl.-Ing. 7024 Filderstadt Seher Multi-component mixtures for sorption heat pumps, sorption refrigerators and sorption heat transformers
WO1990005172A1 (en) * 1988-11-11 1990-05-17 Asahi Glass Company Ltd. Tetrafluoroethane composition for a regrigerator

Also Published As

Publication number Publication date
DK259484A (en) 1984-05-25
DK259484D0 (en) 1984-05-25
EP0120048A1 (en) 1984-10-03
JPS59501632A (en) 1984-09-13
WO1984001165A1 (en) 1984-03-29

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