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DE200980C - - Google Patents

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Publication number
DE200980C
DE200980C DE1907200980D DE200980DD DE200980C DE 200980 C DE200980 C DE 200980C DE 1907200980 D DE1907200980 D DE 1907200980D DE 200980D D DE200980D D DE 200980DD DE 200980 C DE200980 C DE 200980C
Authority
DE
Germany
Prior art keywords
vapors
spirit
floors
upwards
rising
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE1907200980D
Other languages
German (de)
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Application granted granted Critical
Publication of DE200980C publication Critical patent/DE200980C/de
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/26Fractionating columns in which vapour and liquid flow past each other, or in which the fluid is sprayed into the vapour, or in which a two-phase mixture is passed in one direction

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Description

KAISERLICHESIMPERIAL

PATENTAMT.PATENT OFFICE.

Gegenstand der Erfindung ist ein Spiritusrektifizierapparat mit horizontal angeordneten Böden, durch welche der aufsteigende Spiritusdampf gezwungen wird, den Apparat im Zickzackwege zu durchziehen. Das kennzeichnende Merkmal der Erfindung besteht darin, daß von den Böden je zwei derart angeordnet sind und miteinander in Verbindung stehen, daß beide nach oben gewölbt sind,The invention relates to a spirit rectifier with horizontally arranged Soils through which the rising spirit vapor is forced to keep the apparatus in the To pull through zigzag paths. The characteristic feature of the invention is that two of the floors are arranged in this way and are connected to each other so that both are arched upwards,

to der obere dicht an den Mantel der Säule heranreicht und die Dämpfe in der Mitte nach oben durchläßt, der untere dagegen voll ausgebildet ist, aber einen ringförmigen Durchgang für die Dämpfe freiläßt. Infolge dieser Anordnung sammelt sich der Lutter auf beiden Böden nur an ihrem Rande an und bietet daher dem aufsteigenden Spiritusdampf nur wenig Oberfläche, so daß die Gefahr, daß der Lutter durch den über ihn hinwegziehenden Spiritusdampf nochmals zur Verdampfung gebracht wird, wesentlich herabgemindert ist. Die Zeichnung zeigt die Erfindung in
Fig. ι in einem Längsschnitt, während
Fig. 2 in größerem Maßstabe die Anordnung der Böden erkennen läßt.
to the upper one comes close to the jacket of the column and lets the vapors through in the middle upwards, while the lower one is fully formed, but leaves an annular passage for the vapors. As a result of this arrangement, the Lutter only collects at the edge of both floors and therefore offers little surface to the rising spirit vapor, so that the risk of the Lutter being caused to evaporate again by the spirit vapor flowing over it is considerably reduced. The drawing shows the invention in
Fig. Ι in a longitudinal section, while
Fig. 2 shows the arrangement of the floors on a larger scale.

Der Apparat α ist vorteilhaft über einer mit Wasser gefüllten Blase b angeordnet, welcher der Rohspiritus in Dampfform durch das Rohr c zugeführt wird. Die Böden d, e zwingen den Spiritus, den Apparat α im Zickzackwege zu durchwandern.The apparatus α is advantageously arranged above a water-filled bladder b to which the raw alcohol is fed in vapor form through the pipe c . The floors d, e force the spirit to wander through the apparatus α in a zigzag path.

Wie aus der Zeichnung zu erkennen ist, sind sowohl die Böden d als auch die Boden e nach oben gewölbt, und zwar reichen die Böden d bis an den Mantel der Säule a. heran und besitzen in ihrer Mitte eine Durchtrittsöffnung/ für den aufsteigenden Spiritusdampf, während die Böden e voll ausgebildet und derart angeordnet sind, daß sie einen ringförmigen Durchgang g für die aufsteigenden Spiritusdämpfe freilassen. Jeder Boden ist mit dem darunterliegenden durch ein Überlaufrohr h verbunden, so daß der sich am Rande der Böden sammelnde Lutter immer wieder auf den darunterliegenden Boden geleitet wird, bis er schließlich vom untersten Boden d durch das Rohr i abgezogen werden kann.As can be seen from the drawing, both the bottoms d and the bottoms e are arched upwards, namely the bottoms d extend to the jacket of the column a. approach and have in their middle a passage opening / for the rising spirit vapor, while the floors e are fully formed and are arranged in such a way that they leave an annular passage g free for the rising spirit vapors. Each tray is connected to the one below by an overflow pipe h , so that the Lutter that collects at the edge of the floors is repeatedly directed onto the tray below until it can finally be drawn off from the lowest tray d through the pipe i .

Claims (1)

Patent-Anspruch:Patent claim: Rektifizierapparat mit horizontal angeordneten Böden, dadurch gekennzeichnet, daß von den Böden je zwei (d, e) derart angeordnet sind und miteinander in Verbindung stehen, daß beide nach oben gewölbt sind, der obere (d) dicht an den Mantel der Säule (a) heranreicht und die Dämpfe in der Mitte nach oben durchläßt, der untere (e) dagegen voll ausgebildet ist, aber einen ringförmigen Durchgang für die Dämpfe freiläßt.Rectifying apparatus with horizontally arranged trays, characterized in that two of the trays (d, e) are arranged and connected to one another in such a way that both are arched upwards, the upper one (d) close to the jacket of the column (a) reaches and lets the vapors through in the middle upwards, the lower (e), however, is fully formed, but leaves an annular passage for the vapors. Hierzu ι Blatt Zeichnungen.For this purpose ι sheet of drawings.
DE1907200980D 1907-11-05 1907-11-05 Expired DE200980C (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE200980T 1907-11-05

Publications (1)

Publication Number Publication Date
DE200980C true DE200980C (en) 1908-08-05

Family

ID=34484445

Family Applications (1)

Application Number Title Priority Date Filing Date
DE1907200980D Expired DE200980C (en) 1907-11-05 1907-11-05

Country Status (1)

Country Link
DE (1) DE200980C (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2671053A (en) * 1947-06-20 1954-03-02 Shell Dev Method and apparatus for high vacuum distillation

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2671053A (en) * 1947-06-20 1954-03-02 Shell Dev Method and apparatus for high vacuum distillation

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