CO2018005804A2 - Proceso para producción de ácido 2,5-furandicarboxílico (fdca) - Google Patents
Proceso para producción de ácido 2,5-furandicarboxílico (fdca)Info
- Publication number
- CO2018005804A2 CO2018005804A2 CONC2018/0005804A CO2018005804A CO2018005804A2 CO 2018005804 A2 CO2018005804 A2 CO 2018005804A2 CO 2018005804 A CO2018005804 A CO 2018005804A CO 2018005804 A2 CO2018005804 A2 CO 2018005804A2
- Authority
- CO
- Colombia
- Prior art keywords
- fdca
- hmf
- acid
- production
- oxidation
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/33—Heterocyclic compounds
- A61K31/335—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin
- A61K31/34—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having five-membered rings with one oxygen as the only ring hetero atom, e.g. isosorbide
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/04—Antibacterial agents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oncology (AREA)
- Communicable Diseases (AREA)
- General Chemical & Material Sciences (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Epidemiology (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Furan Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
RESUMEN La presente invención se relaciona con un proceso para la producción de ácido 2,5-furandicarboxílico (FDCA) mediante la oxidación de 5-hidroximetil-2-furfural (HMF), estando presente el HMF en una solución en un solvente polar de alto punto de ebullición y agua. El proceso se caracteriza por la combinación de: - una primera etapa de oxidación en la que el HMF se oxida por lo menos parcialmente en la solución para producir una primera mezcla de reacción que comprende por lo menos un monoácido seleccionado del grupo que consiste de ácido 5-hidroximetilfuran-2-carboxílico (HMFA), ácido 5-formilfuran-2-carboxílico (FFCA) y, opcionalmente, FDCA, - una etapa de extracción después de la primera etapa de oxidación en donde el solvente polar de alto punto de ebullición se extrae de la primera mezcla de reacción por medio de un solvente de extracción, en donde por lo menos un monoácido permanece en una fase acuosa, - una segunda etapa de oxidación en la que por lo menos un monoácido se oxida a FDCA.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP15199377 | 2015-12-10 | ||
| PCT/EP2016/080107 WO2017097843A1 (en) | 2015-12-10 | 2016-12-07 | Process for the production of 2,5-furandicarboxylic acid (fdca) |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CO2018005804A2 true CO2018005804A2 (es) | 2018-09-20 |
Family
ID=55024755
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CONC2018/0005804A CO2018005804A2 (es) | 2015-12-10 | 2016-12-07 | Proceso para producción de ácido 2,5-furandicarboxílico (fdca) |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US10316011B2 (es) |
| EP (1) | EP3386958B1 (es) |
| JP (1) | JP6943855B2 (es) |
| KR (1) | KR20180090840A (es) |
| CN (1) | CN108368076B (es) |
| AU (1) | AU2016368620B2 (es) |
| BR (1) | BR112018011492B1 (es) |
| CA (1) | CA3007305A1 (es) |
| CO (1) | CO2018005804A2 (es) |
| HU (1) | HUE052833T2 (es) |
| MX (1) | MX384284B (es) |
| RU (1) | RU2745266C2 (es) |
| UA (1) | UA127338C2 (es) |
| WO (1) | WO2017097843A1 (es) |
| ZA (1) | ZA201803510B (es) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BR112018014278B1 (pt) | 2016-01-13 | 2022-07-12 | Stora Enso Oyj | Processos para a preparação de ácido 2,5-furandicarboxílico e intermediários e derivados dos mesmos |
| SG11201913469PA (en) | 2017-07-12 | 2020-01-30 | Stora Enso Oyj | Purified 2,5-furandicarboxylic acid pathway products |
| CN109912549A (zh) * | 2017-12-12 | 2019-06-21 | 南京林业大学 | 一种5－羟甲基糠醛选择氧化制备5－羟甲基糠酸的新方法 |
| CN109666011A (zh) * | 2018-12-27 | 2019-04-23 | 厦门大学 | 一种制备2,5-呋喃二甲酸的方法 |
| CN109824636A (zh) * | 2019-03-11 | 2019-05-31 | 重庆化工职业学院 | 2,5-呋喃二甲酸的制备方法 |
| WO2020190080A1 (en) | 2019-03-20 | 2020-09-24 | Samyang Corporation | Method for the synthesis of 2,5-furandicarboxylic acid |
| KR102347177B1 (ko) | 2020-02-13 | 2022-01-04 | 한국화학연구원 | 5-알콕시메틸퍼퓨랄 제조방법 |
| DE102022201794A1 (de) | 2022-02-21 | 2023-08-24 | Südzucker AG | Verfahren zur Oxidation von Hydroxymethylfurfural |
| CN118894822A (zh) * | 2024-06-17 | 2024-11-05 | 清华大学 | 5-羟甲基糠醛氧化制备2,5-呋喃二甲酸的方法及应用 |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3826073A1 (de) * | 1988-07-30 | 1990-02-01 | Hoechst Ag | Verfahren zur oxidation von 5-hydroxymethylfurfural |
| WO2008054804A2 (en) * | 2006-10-31 | 2008-05-08 | Battelle Memorial Institute | Hydroxymethyl furfural oxidation methods |
| JP2009013079A (ja) | 2007-07-02 | 2009-01-22 | Canon Inc | フラン−２，５−ジカルボン酸の製造方法 |
| US8865921B2 (en) * | 2009-10-07 | 2014-10-21 | Furanix Technologies B.V. | Method for the preparation of 2,5-furandicarboxylic acid and for the preparation of the dialkyl ester of 2,5-furandicarboxylic acid |
| KR101769503B1 (ko) * | 2009-10-07 | 2017-08-18 | 퓨라닉스 테크놀러지스 비.브이. | 2,5-퓨란다이카르복시산 및 이들의 에스테르의 제조방법 |
| US8796477B2 (en) * | 2011-05-24 | 2014-08-05 | Eastman Chemical Company | Oxidation process to produce a crude and/or purified carboxylic acid product |
| FR3001970B1 (fr) * | 2013-02-11 | 2015-02-27 | Centre Nat Rech Scient | Procede de preparation d'acide 2,5-furane dicarboxylique |
| MX354925B (es) * | 2013-03-14 | 2018-03-23 | Archer Daniels Midland Co | Proceso para obtener un acido 2,5-furandicarboxilico. |
| NO3157910T3 (es) * | 2014-06-17 | 2018-08-11 |
-
2016
- 2016-12-07 CN CN201680072169.5A patent/CN108368076B/zh not_active Expired - Fee Related
- 2016-12-07 BR BR112018011492-8A patent/BR112018011492B1/pt not_active IP Right Cessation
- 2016-12-07 JP JP2018530145A patent/JP6943855B2/ja not_active Expired - Fee Related
- 2016-12-07 AU AU2016368620A patent/AU2016368620B2/en not_active Ceased
- 2016-12-07 HU HUE16810305A patent/HUE052833T2/hu unknown
- 2016-12-07 KR KR1020187018309A patent/KR20180090840A/ko not_active Ceased
- 2016-12-07 US US16/060,382 patent/US10316011B2/en active Active
- 2016-12-07 UA UAA201807628A patent/UA127338C2/uk unknown
- 2016-12-07 CO CONC2018/0005804A patent/CO2018005804A2/es unknown
- 2016-12-07 RU RU2018124987A patent/RU2745266C2/ru active
- 2016-12-07 MX MX2018006741A patent/MX384284B/es unknown
- 2016-12-07 EP EP16810305.9A patent/EP3386958B1/en not_active Not-in-force
- 2016-12-07 WO PCT/EP2016/080107 patent/WO2017097843A1/en not_active Ceased
- 2016-12-07 CA CA3007305A patent/CA3007305A1/en active Pending
-
2018
- 2018-05-28 ZA ZA2018/03510A patent/ZA201803510B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| JP2019504001A (ja) | 2019-02-14 |
| BR112018011492B1 (pt) | 2022-02-22 |
| ZA201803510B (en) | 2021-03-31 |
| RU2745266C2 (ru) | 2021-03-22 |
| CN108368076A (zh) | 2018-08-03 |
| EP3386958A1 (en) | 2018-10-17 |
| US10316011B2 (en) | 2019-06-11 |
| EP3386958B1 (en) | 2020-09-09 |
| CN108368076B (zh) | 2021-08-06 |
| AU2016368620B2 (en) | 2020-09-03 |
| BR112018011492A2 (pt) | 2018-12-04 |
| MX384284B (es) | 2025-03-14 |
| RU2018124987A (ru) | 2020-01-10 |
| KR20180090840A (ko) | 2018-08-13 |
| JP6943855B2 (ja) | 2021-10-06 |
| RU2018124987A3 (es) | 2020-04-10 |
| WO2017097843A1 (en) | 2017-06-15 |
| UA127338C2 (uk) | 2023-07-26 |
| MX2018006741A (es) | 2018-08-01 |
| AU2016368620A1 (en) | 2018-06-14 |
| US20180362486A1 (en) | 2018-12-20 |
| CA3007305A1 (en) | 2017-06-15 |
| HUE052833T2 (hu) | 2021-05-28 |
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