CN2649227Y - Metal uniform particle generator - Google Patents
Metal uniform particle generator Download PDFInfo
- Publication number
- CN2649227Y CN2649227Y CN 03258305 CN03258305U CN2649227Y CN 2649227 Y CN2649227 Y CN 2649227Y CN 03258305 CN03258305 CN 03258305 CN 03258305 U CN03258305 U CN 03258305U CN 2649227 Y CN2649227 Y CN 2649227Y
- Authority
- CN
- China
- Prior art keywords
- crucible
- generator
- nozzle
- battery lead
- lead plate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000002184 metal Substances 0.000 title claims abstract description 30
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 30
- 239000002245 particle Substances 0.000 title abstract description 10
- 239000010453 quartz Substances 0.000 claims abstract description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 230000001681 protective effect Effects 0.000 claims description 12
- 230000005284 excitation Effects 0.000 claims description 10
- 239000000110 cooling liquid Substances 0.000 claims description 5
- 239000012809 cooling fluid Substances 0.000 claims description 3
- 230000009286 beneficial effect Effects 0.000 claims description 2
- 229910001338 liquidmetal Inorganic materials 0.000 claims description 2
- 229910045601 alloy Inorganic materials 0.000 abstract description 12
- 239000000956 alloy Substances 0.000 abstract description 12
- 239000000126 substance Substances 0.000 abstract description 4
- 238000003466 welding Methods 0.000 abstract description 4
- 239000012798 spherical particle Substances 0.000 abstract description 2
- 239000002826 coolant Substances 0.000 abstract 2
- 230000002964 excitative effect Effects 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 10
- 239000007788 liquid Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 229910052757 nitrogen Inorganic materials 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 239000011261 inert gas Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000009826 distribution Methods 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 238000012387 aerosolization Methods 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 229910000679 solder Inorganic materials 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000009692 water atomization Methods 0.000 description 1
Images
Landscapes
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Abstract
A metal uniform particle generator consists of a quartz container, a crucible, a piezoelectric excitative generator, a thermocouple, a heating device, a gas-protected supplying pipe, a vibration generator, an electrode plate and a vessel with coolant. The piezoelectric excitative generator is arranged on top of the crucible; the vibration generator is arranged inside the lower part of the crucible; the thermocouple and the gas-protected supplying pipe are inserted respectively in the crucible; a nozzle is provided at the bottom of the crucible; the electrode plate is provided outside the lower part of the nozzle, wherein an opening is arranged, opposite to the electrode plate; potential difference is produced between the crucible and the electrode plate; the vessel with coolant is arranged right under the opening of the electrode plate; the devices above-mentioned are arranged in the vacuum quartz container. The advantages are that the utility model can produce uniform spherical particles of metal or alloy of a single size; the physical and chemical properties between particles are highly consistent and can be applied to the welding of integrated circuit and also improves the consistency of the electronic system therefore has a wide prospect of application.
Description
(1) field under:
The utility model belongs to a kind of device of producing the metal or alloy powder, particularly a kind of metal single-size generator.
(2) background technology:
At present, the method of the production metal or alloy powder (particle) of comparative maturity and extensive use on China's powder metallurgy industry is aerosolization, water atomization method, but metal or alloy powder (particle) size distribution that this method is prepared is inhomogeneous, each intergranular microstructure and physical and chemical performance have certain difference, use morely in traditional field such as surperficial anticorrosion with painting, but can not satisfy the application of high-tech sector.
(3) summary of the invention:
The purpose of this utility model is to design a kind of metal single-size generator, and it makes the problems referred to above be solved, and produces the metal or alloy powder of even particle size distribution, satisfies the needs that high-tech sector is used.
The technical solution of the utility model: a kind of metal single-size generator is characterized in that this device is made up of the container of quartz container, crucible, piezoelectric excitation generator, thermocouple, heater, protective gas feeding pipe, clapp oscillator, battery lead plate and interior dress cooling fluid; Said piezoelectric excitation generating apparatus is in crucible top oral area, the clapp oscillator that is connected with the piezoelectric excitation generator places bottom in the crucible, thermocouple and protective gas feeding pipe insert from top, crucible both sides respectively, heater places the crucible wall periphery, there is a micropore crucible bottom, nozzle is equipped with at the micropore place, battery lead plate places the outside below of crucible bottom nozzle, there is opening at battery lead plate and nozzle place relative crucible bottom parallel with crucible bottom, between crucible and battery lead plate potential difference is arranged, the container that cooling liquid is housed place the battery lead plate opening under; Said said apparatus places in the quartz container that vacuumizes.
The diameter of above-mentioned said crucible bottom nozzle is between 20-100 μ m.
Clapp oscillator can be that disk and rocking beam constitute in the above-mentioned said crucible, also can be other shapes that are beneficial to the liquid metals vibration.
The protective gas that the above-mentioned said protective gas feeding pipe that is inserted in the crucible provides can be nitrogen or other inert gas.
A certain amount of anti-oxidation high pure nitrogen or other inert gas also should be arranged in the above-mentioned said quartz container, and with crucible in gas have pressure difference.
The course of work of the present utility model and operation principle are: quartz container is vacuumized, charge into then to avoid high pure nitrogen or other inert gas of metal (alloy) oxidation, to be heated to the uniform temperature fusion in metal or the platform gold crucible and keep several minutes, input surpasses an atmospheric nitrogen or other inert gas in crucible then.The pressure difference of crucible and quartz container makes molten metal or alloy liquid spray from nozzle, forms cylindrical metal liquid stream, applies the higher-order of oscillation in this metal liquid, makes metal liquid be fractured into fine drop when ejection.The metal or alloy drop is when nozzle sprays, and charging electrode fills on drop and adds electric charge, because the skin effect of drop electric charge, makes between each drop mutually exclusively, avoids the polymerization in dropping process.When tiny molten drop falls, remove to collect the metal or alloy drop of these whereabouts with the container that cooling liquid is housed, then can obtain the metal or alloy single-size of single size.
Superiority of the present utility model is: the metal or alloy particle that 1, adopts metal single-size generator to produce, visible granular is the even spherical particle of single size under the light microscope, physics between the particle is consistent with the chemical property height, and is in full accord as each particle resistance value; 2, with this device fabrication welding material particle, can be applied in the welding of integrated circuit, because each soldered ball of gained all has identical physical and chemical performance, can guarantee the welding quality of thousands of solder joints on the integrated circuit mainboard, greatly improve the uniformity of electronic system, reduce the defective occurrence probability of entire product greatly; 3, with this device fabrication metal dust, also can be applied on the static pressure powder mould-forming process, greatly improve the performance and the life-span of mould; 4, with this equipment depositing metal films (or coating) on substrate, can obtain the bonding jumper (or band) of property, have broad application prospects.
(4) description of drawings:
Accompanying drawing is the overall structure schematic diagram of the related a kind of metal single-size generator of the utility model.
Wherein: 1 is the piezoelectric excitation generator, and 2 is thermocouple, and 3 is that protective gas is given pipeline altogether, and 4 is crucible; 5 is clapp oscillator, and 6 is heater, and 7 is melt metal or alloy liquid, and 8 is nozzle; 9 is the positively charged battery lead plate, and 10 is even molten drop, and 11 have the container of cooling liquid in being.
(5) specific embodiment:
Embodiment: a kind of metal single-size generator (seeing accompanying drawing) is characterized in that this device is made up of the container 11 of quartz container, crucible 4, piezoelectric excitation generator 1, thermocouple 2, heater 6, protective gas feeding pipe 3, clapp oscillator 5, battery lead plate 9 and interior dress cooling fluid; Said piezoelectric excitation generator 1 is installed on crucible 4 top oral areas, the clapp oscillator 5 that is connected with piezoelectric excitation generator 1 places bottom in the crucible 4, thermocouple 2 and protective gas feeding pipe 3 insert from top, crucible 4 both sides respectively, heater 6 places crucible 4 side wall perimeter, there is a micropore crucible 4 bottoms, nozzle 8 is equipped with at the micropore place, battery lead plate 9 places the outside below of crucible 4 bottom nozzles 8, there is opening at battery lead plate 9 and nozzle place relative crucible bottom parallel with crucible 4 bottoms, 9 of crucible 4 and battery lead plates have potential difference, the container 11 that cooling liquid is housed place battery lead plate 9 openings under; Said said apparatus places in the quartz container that vacuumizes.
The diameter of above-mentioned said crucible 4 bottom nozzles 8 is got 60 μ m.
The protective gas that the above-mentioned said protective gas feeding pipe 3 that is inserted in the crucible 4 provides is a nitrogen.
The atmospheric pressure that the above-mentioned said protective gas feeding pipe 3 that is inserted in the crucible 4 provides should surpass an atmospheric pressure.
Claims (3)
1, a kind of metal single-size generator is characterized in that this device is made up of the container of quartz container, crucible, piezoelectric excitation generator, thermocouple, heater, protective gas feeding pipe, clapp oscillator, battery lead plate and interior dress cooling fluid; Said piezoelectric excitation generating apparatus is in crucible top oral area, the clapp oscillator that is connected with the piezoelectric excitation generator places bottom in the crucible, thermocouple and protective gas feeding pipe insert from top, crucible both sides respectively, heater places the crucible wall periphery, there is a micropore crucible bottom, nozzle is equipped with at the micropore place, battery lead plate places the outside below of crucible bottom nozzle, there is opening at battery lead plate and nozzle place relative crucible bottom parallel with crucible bottom, between crucible and battery lead plate potential difference is arranged, the container that cooling liquid is housed place the battery lead plate opening under; Said said apparatus places in the quartz container that vacuumizes.
2, according to the said a kind of metal single-size generator of claim 1, the diameter that it is characterized in that said crucible bottom nozzle is between 20-100 μ m.
3, according to the said a kind of metal single-size generator of claim 1, it is characterized in that clapp oscillator can be that disk and rocking beam constitute in the said crucible, also can be other shapes that are beneficial to the liquid metals vibration.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 03258305 CN2649227Y (en) | 2003-08-21 | 2003-08-21 | Metal uniform particle generator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 03258305 CN2649227Y (en) | 2003-08-21 | 2003-08-21 | Metal uniform particle generator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2649227Y true CN2649227Y (en) | 2004-10-20 |
Family
ID=34328868
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 03258305 Expired - Fee Related CN2649227Y (en) | 2003-08-21 | 2003-08-21 | Metal uniform particle generator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2649227Y (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100402201C (en) * | 2006-05-08 | 2008-07-16 | 西安交通大学 | A short-flow process for preparing metal particles |
| CN100431746C (en) * | 2005-07-21 | 2008-11-12 | 北京有色金属研究总院 | Method and device for preparing precision welding ball |
| CN101279373B (en) * | 2007-12-28 | 2010-05-19 | 天津大学 | A device for preparing nanoparticles by secondary Coulomb splitting |
| CN101244460B (en) * | 2008-03-13 | 2010-06-02 | 大连理工大学 | A kind of method for preparing micro-conductive fiber |
| CN106714955A (en) * | 2014-09-29 | 2017-05-24 | 卡萨尔公司 | Apparatus and method for prilling a liquid, preferably urea melt |
| US20170312849A1 (en) * | 2016-05-02 | 2017-11-02 | Electronics And Telecommunications Research Institute | Extruder for metal material and 3d printer using the same |
| WO2020063625A1 (en) * | 2018-09-25 | 2020-04-02 | 大连理工大学 | Device and method for preparing ultrafine spherical metal powder using drop-by-drop centrifugal atomization method |
| CN114850484A (en) * | 2022-04-29 | 2022-08-05 | 中国科学院赣江创新研究院 | Preparation device and preparation method of rare earth metal microspheres |
-
2003
- 2003-08-21 CN CN 03258305 patent/CN2649227Y/en not_active Expired - Fee Related
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100431746C (en) * | 2005-07-21 | 2008-11-12 | 北京有色金属研究总院 | Method and device for preparing precision welding ball |
| CN100402201C (en) * | 2006-05-08 | 2008-07-16 | 西安交通大学 | A short-flow process for preparing metal particles |
| CN101279373B (en) * | 2007-12-28 | 2010-05-19 | 天津大学 | A device for preparing nanoparticles by secondary Coulomb splitting |
| CN101244460B (en) * | 2008-03-13 | 2010-06-02 | 大连理工大学 | A kind of method for preparing micro-conductive fiber |
| CN106714955A (en) * | 2014-09-29 | 2017-05-24 | 卡萨尔公司 | Apparatus and method for prilling a liquid, preferably urea melt |
| CN106714955B (en) * | 2014-09-29 | 2019-12-31 | 卡萨尔公司 | Apparatus and method for granulating a liquid, preferably a urea melt |
| US20170312849A1 (en) * | 2016-05-02 | 2017-11-02 | Electronics And Telecommunications Research Institute | Extruder for metal material and 3d printer using the same |
| US11110540B2 (en) * | 2016-05-02 | 2021-09-07 | Electronics And Telecommunications Research Institute | Extruder for metal material and 3D printer using the same |
| WO2020063625A1 (en) * | 2018-09-25 | 2020-04-02 | 大连理工大学 | Device and method for preparing ultrafine spherical metal powder using drop-by-drop centrifugal atomization method |
| CN114850484A (en) * | 2022-04-29 | 2022-08-05 | 中国科学院赣江创新研究院 | Preparation device and preparation method of rare earth metal microspheres |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1422718A (en) | Method and apparatus for making globular metallic powder by ultrasonic atomising | |
| CN106435270B (en) | Laser 3D printing TC21 titanium alloy powders and preparation and application | |
| EP3456857A1 (en) | Method for preparing target material and target material | |
| CN2649227Y (en) | Metal uniform particle generator | |
| CN106636748A (en) | TC4 titanium alloy powder for 3D (Three Dimensional) printing and preparation method thereof | |
| CN110961646B (en) | Metal powder and method for producing the same | |
| CN111872388A (en) | A method for preparing high-entropy alloys based on laser selective melting technology | |
| CN106623959A (en) | Preparation method of Waspalloy spherical powder for additive manufacturing | |
| CN101992301A (en) | Method for producing spherical stainless steel powder material by using high pressure water atomization method | |
| CN114054775B (en) | Aging strengthening type nickel-based high-temperature alloy 3D printing process and manufactured 3D printing piece | |
| CN102925824A (en) | Preparation method for zirconium-based amorphous alloy as well as powder and large-sized block of zirconium-based amorphous alloy | |
| CN109014203A (en) | Metal powder SLM forming process dynamic recycling repair system | |
| JPWO2003037553A1 (en) | Method and apparatus for producing metal powder | |
| CN107716934A (en) | A kind of preparation method of Inconel718 alloy powders for 3D printing technique | |
| US20220001448A1 (en) | Device and method for high-efficiency preparation of spherical metal powder for 3d printing employing separation into fibers | |
| CN107498059B (en) | Method for preparing titanium-based spherical powder with refined particle size by gas atomization | |
| JP2019531400A (en) | Alloy powder and manufacturing method thereof | |
| Goudar et al. | Effect of atomization parameters on size and morphology of Al-17Si alloy powder produced by free fall atomizer | |
| CN104096845A (en) | Method and device for manufacturing metallic glass particles | |
| CN1254355C (en) | Fast forming micro manufacturing method for non homogeneous functional device | |
| CN115889791A (en) | Rare earth reinforced titanium-based composite material and preparation method thereof | |
| CN2510207Y (en) | Spherical metallic powder supersonic-atomising preparation apparatus | |
| CN104416161A (en) | Method for quickly producing uniform core-shell type alloy solder balls | |
| CN108421984A (en) | Stainless steel powder for additive manufacturing and preparation method thereof | |
| EP3693104A1 (en) | Methods for additive manufacturing with masticated particles |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |