CN205324701U - Device and have its system of infiltrating infiltrates - Google Patents
Device and have its system of infiltrating infiltrates Download PDFInfo
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Abstract
本实用新型公开了一种浸渗装备及具有其的浸渗系统,所述浸渗装备包括:密闭的第一容器,所述第一容器限定出第一腔室;第二容器,所述第二容器置于所述第一腔室内且限定出用于盛装浸渗液的第二腔室;成型模具,所述成型模具设有第三腔室,所述成型模具上设置有用于连通所述第二腔室和所述第三腔室的连通结构,所述连通结构构造成使得所述第二容器内的浸渗液能够依靠重力至少部分地通过所述连通结构进入到所述第三腔室内;温场控制装置,所述温场控制装置设置成用于对所述浸渗液的温度进行控制。根据本实用新型的浸渗装备控制简单、生产安全,且产品成品率高,无缩孔/收缩不良等缺陷。
The utility model discloses an impregnation equipment and an impregnation system with the same. The impregnation equipment comprises: a first airtight container, the first container defines a first chamber; a second container, the first Two containers are placed in the first chamber and define a second chamber for containing the infiltration liquid; a forming mold, the forming mold is provided with a third chamber, and the forming mold is provided with a device for communicating with the A communication structure between the second chamber and the third chamber, the communication structure is configured such that the impregnating liquid in the second container can at least partially enter the third chamber through the communication structure by gravity Indoor: a temperature field control device, the temperature field control device is configured to control the temperature of the immersion liquid. According to the impregnation equipment of the utility model, the control is simple, the production is safe, and the product yield is high, without defects such as shrinkage cavity/shrinkage defect.
Description
技术领域 technical field
本实用新型涉及一种陶瓷和金属复合材料生产的技术领域,特别涉及一种浸渗装置及具有其的浸渗系统。 The utility model relates to the technical field of ceramic and metal composite material production, in particular to an impregnation device and an impregnation system with the same.
背景技术 Background technique
相关技术中的金属和陶瓷复合材料基板的生产效率低下、良品率低,且生产设备结构复杂,制作难度大、生产时具有安全隐患。 The metal and ceramic composite substrates in the related art have low production efficiency and low yield rate, and the production equipment has a complex structure, which is difficult to manufacture and has potential safety hazards during production.
实用新型内容 Utility model content
本实用新型旨在至少在一定程度上解决相关技术中的技术问题之一。为此,本实用新型的一个目的在于提出一种浸渗装备,该浸渗装备控制简单、生产安全,且产品成品率高,无缩孔/收缩不良等缺陷。 The utility model aims to solve one of the technical problems in the related art at least to a certain extent. Therefore, an object of the present utility model is to provide an impregnation equipment, which is simple to control, safe to produce, has a high yield of products, and has no defects such as shrinkage cavities or poor shrinkage.
本实用新型的另外一个目的在于提出一种具有上述浸渗装备的浸渗系统。 Another purpose of the present utility model is to provide an infiltration system with the above infiltration equipment.
根据本实用新型的浸渗装备,包括:第一容器,所述第一容器限定出第一腔室;第二容器,所述第二容器置于所述第一腔室内且限定出用于盛装浸渗液的第二腔室;成型模具,所述成型模具设有第三腔室,所述成型模具上设置有用于连通所述第二腔室和所述第三腔室的连通结构,所述连通结构构造成使得所述第二容器内的浸渗液能够依靠重力至少部分地通过所述连通结构进入到所述第三腔室内;温场控制装置,所述温场控制装置设置成用于对所述浸渗液的温度进行控制,所述温场控制装置包括加热单元,所述加热单元为设置在所述第二容器周壁外侧的感应加热线圈;所述第二容器的上端设有用于对所述第二容器上部的浸渗液进行保温的保温隔热装置。 The impregnation equipment according to the present invention includes: a first container, the first container defines a first chamber; a second container, the second container is placed in the first chamber and defines a container for containing The second chamber of the infiltrating liquid; a forming mold, the forming mold is provided with a third chamber, and the forming mold is provided with a communication structure for communicating the second chamber and the third chamber, so The communication structure is configured so that the impregnating liquid in the second container can enter the third chamber at least partially through the communication structure by gravity; the temperature field control device is configured to use In order to control the temperature of the impregnating liquid, the temperature field control device includes a heating unit, the heating unit is an induction heating coil arranged outside the peripheral wall of the second container; the upper end of the second container is provided with a The thermal insulation device is used to keep the impregnating liquid in the upper part of the second container warm.
根据本实用新型的浸渗装备,第二容器内的浸渗液可以在重力的作用下进入到第三容器内,由此控制简单、安全且易于实现。 According to the impregnation equipment of the present invention, the impregnating liquid in the second container can enter into the third container under the action of gravity, so the control is simple, safe and easy to realize.
此外,第二容器内部的浸渗液的温度可以控制,进而可以控制浸渗液的凝固速度,保证了成品质量,无缩孔/收缩不良等缺陷。 In addition, the temperature of the impregnating liquid inside the second container can be controlled, and thus the solidification speed of the impregnating liquid can be controlled, thereby ensuring the quality of the finished product without defects such as shrinkage cavity/shrinkage defects.
另外,根据本实用新型的浸渗装备还可以具有如下附加的技术特征; In addition, the impregnation equipment according to the utility model can also have the following additional technical features;
根据本实用新型的一个实施例,所述温场控制装置设置在所述第一容器内且邻近所述第二容器布置。 According to an embodiment of the present invention, the temperature field control device is arranged in the first container and arranged adjacent to the second container.
根据本实用新型的一个实施例,所述温场控制装置包括:冷却单元,所述冷却单元设在所述第二容器的底壁下方。 According to an embodiment of the present utility model, the temperature field control device includes: a cooling unit arranged below the bottom wall of the second container.
根据本实用新型的一个实施例,所述加热单元为多组,且多组所述加热单元在从下到上的方向上依次分布在所述第二容器的周壁外侧。 According to an embodiment of the present invention, there are multiple groups of the heating units, and the multiple groups of the heating units are sequentially distributed outside the peripheral wall of the second container from bottom to top.
根据本实用新型的一个实施例,所述多组加热单元基于所需的工艺温度在上下方向上进行布置以对浸渗复合过程进行温度梯度控制。 According to an embodiment of the present invention, the multiple groups of heating units are arranged in the vertical direction based on the required process temperature to control the temperature gradient of the impregnation compound process.
实用新型根据本实用新型的一个实施例,所述成型模具包括:相对设置的第一模板和第二模板,所述第一模板与所述第二模板之间设有隔板以将所述第三腔室分隔为两个成型腔。 According to an embodiment of the utility model, the forming mold includes: a first template and a second template that are oppositely arranged, and a partition is provided between the first template and the second template to separate the first template and the second template. The three-chamber is divided into two molding cavities.
根据本实用新型的一个实施例,所述成型模具为多个,且多个成型模具置于所述第二腔室内。 According to an embodiment of the present utility model, there are multiple forming molds, and the multiple forming molds are placed in the second cavity.
根据本实用新型的一个实施例,所述连通结构构造为连通孔,所述连通孔位于所述第三腔室的上方。 According to an embodiment of the present invention, the communication structure is configured as a communication hole, and the communication hole is located above the third chamber.
根据本实用新型的一个实施例,所述第二容器为上端敞口的筒状结构,在所述浸渗复合过程中,所述浸渗液的液面位于所述连通孔之上。 According to an embodiment of the present invention, the second container is a cylindrical structure with an open upper end, and during the impregnation and compounding process, the liquid level of the impregnation liquid is above the communication hole.
根据本实用新型的一个实施例,所述第一容器为密闭容器,在浸渗复合前,对所述第一腔室抽真空。 According to an embodiment of the present invention, the first container is an airtight container, and the first chamber is evacuated before impregnation and compounding.
根据本实用新型的一个实施例,所述第一容器包括:本体部和顶盖部,所述顶盖部可开合地设在所述本体部上以用于打开或关闭所述第一腔室。 According to an embodiment of the present invention, the first container includes: a body part and a top cover part, and the top cover part is openably and closably arranged on the body part for opening or closing the first cavity room.
根据本实用新型的一个实施例,所述顶盖上设有用于测量所述浸渗液温度的测温孔。 According to an embodiment of the present utility model, the top cover is provided with a temperature measuring hole for measuring the temperature of the soaking liquid.
实用新型根据本实用新型的一个实施例,所述第一容器上设置有真空阀和压力阀。 Utility model According to an embodiment of the utility model, the first container is provided with a vacuum valve and a pressure valve.
根据本实用新型的一个实施例,所述第二容器为上端敞口的筒状结构,所述第二腔室的纵截面为倒置的圆台形。 According to an embodiment of the present invention, the second container is a cylindrical structure with an open upper end, and the longitudinal section of the second chamber is an inverted truncated cone.
根据本实用新型的一个实施例,所述浸渗装备用于制作铝碳化硅复合材料板。 According to an embodiment of the present utility model, the infiltration equipment is used for making aluminum silicon carbide composite material plates.
根据本实用新型的浸渗系统,包括:上述的浸渗装备;浸渗液供给装备,所述浸渗液供给装备用于向所述浸渗装备内供给浸渗液;抽真空装备,所述抽真空装备与所述浸渗装备相连用于对所述浸渗装备内部抽真空;高压加载装备,所述高压加载装备与所述浸渗装备相连用于对所述浸渗装备加压/泄压。 The impregnation system according to the present invention includes: the above impregnation equipment; the impregnation liquid supply equipment, the impregnation liquid supply equipment is used to supply the impregnation liquid into the impregnation equipment; the vacuum equipment, the Vacuum equipment is connected to the impregnation equipment for vacuuming the interior of the impregnation equipment; high-pressure loading equipment, the high-pressure loading equipment is connected to the impregnation equipment for pressurizing/releasing the impregnation equipment pressure.
根据本实用新型的浸渗系统,可以保证产品的成品质量且降低了产品的生产成本。 According to the impregnation system of the utility model, the finished product quality of the product can be guaranteed and the production cost of the product can be reduced.
本实用新型的附加方面和优点将在下面的描述中部分给出,部分将从下面的描述中变得明显,或通过本实用新型的实践了解到。 Additional aspects and advantages of the invention will be set forth in the description which follows, and in part will be obvious from the description, or may be learned by practice of the invention.
附图说明 Description of drawings
本实用新型的上述和/或附加的方面和优点从结合下面附图对实施例的描述中将变得明显和容易理解,其中: The above and/or additional aspects and advantages of the present utility model will become apparent and easy to understand from the description of the embodiments in conjunction with the following drawings, wherein:
图1是根据本实用新型实施例的浸渗装备的示意图; Fig. 1 is the schematic diagram of the impregnation equipment according to the utility model embodiment;
图2是根据本实用新型实施例的成型模具放置在第二容器内的示意图。 Fig. 2 is a schematic diagram of a forming mold placed in a second container according to an embodiment of the present invention.
附图标记: Reference signs:
浸渗装备100, Infiltration equipment 100,
第一容器110,本体部111,顶盖部112,第一腔室101,真空阀113,压力阀114,增压阀114a,泄压阀114b, The first container 110, the body part 111, the top cover part 112, the first chamber 101, the vacuum valve 113, the pressure valve 114, the boost valve 114a, the pressure relief valve 114b,
第二容器120,第二腔室102, The second container 120, the second chamber 102,
成型模具130,第一模板131,第二模板132,第三腔室103,连通孔104,型腔105, Forming mold 130, first template 131, second template 132, third cavity 103, communication hole 104, cavity 105,
温场控制装置140,冷却单元141,加热单元142, Temperature field control device 140, cooling unit 141, heating unit 142,
隔板150。 Partition 150.
具体实施方式 detailed description
下面详细描述本实用新型的实施例,所述实施例的示例在附图中示出。下面通过参考附图描述的实施例是示例性的,旨在用于解释本实用新型,而不能理解为对本实用新型的限制。 Embodiments of the invention are described in detail below, examples of which are illustrated in the accompanying drawings. The embodiments described below by referring to the figures are exemplary and are intended to explain the present invention, but should not be construed as limiting the present invention.
在本实用新型的描述中,需要理解的是,术语“中心”、“纵向”、“横向”、“长度”、“宽度”、“厚度”、“上”、“下”、“前”、“后”、“左”、“右”、“竖直”、“水平”、“顶”、“底”“内”、“外”、“顺时针”、“逆时针”、“轴向”、“径向”、“周向”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本实用新型和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本实用新型的限制。 In describing the present invention, it should be understood that the terms "center", "longitudinal", "transverse", "length", "width", "thickness", "upper", "lower", "front", "Back", "Left", "Right", "Vertical", "Horizontal", "Top", "Bottom", "Inner", "Outer", "Clockwise", "Counterclockwise", "Axial" The orientation or positional relationship indicated by , "radial", "circumferential", etc. is based on the orientation or positional relationship shown in the drawings, and is only for the convenience of describing the utility model and simplifying the description, rather than indicating or implying the referred device Or elements must have a specific orientation, be constructed and operate in a specific orientation, and thus should not be construed as limiting the invention.
此外,术语“第一”、“第二”仅用于描述目的,而不能理解为指示或暗示相对重要性或者隐含指明所指示的技术特征的数量。由此,限定有“第一”、“第二”的特征可以明示或者隐含地包括至少一个该特征。在本实用新型的描述中,“多个”的含义是至少两个,例如两个,三个等,除非另有明确具体的限定。 In addition, the terms "first" and "second" are used for descriptive purposes only, and cannot be interpreted as indicating or implying relative importance or implicitly specifying the quantity of indicated technical features. Thus, the features defined as "first" and "second" may explicitly or implicitly include at least one of these features. In the description of the present utility model, "plurality" means at least two, such as two, three, etc., unless otherwise specifically defined.
在本实用新型中,除非另有明确的规定和限定,术语“安装”、“相连”、“连接”、“固定”等术语应做广义理解,例如,可以是固定连接,也可以是可拆卸连接,或成一体;可以是机械连接,也可以是电连接或彼此可通讯;可以是直接相连,也可以通过中间媒介间接相连,可以是两个元件内部的连通或两个元件的相互作用关系,除非另有明确的限定。对于本领域的普通技术人员而言,可以根据具体情况理解上述术语在本实用新型中的具体含义。 In this utility model, unless otherwise specified and limited, terms such as "installation", "connection", "connection" and "fixation" should be understood in a broad sense, for example, it can be a fixed connection or a detachable connection. Connected, or integrated; it can be mechanically connected, or electrically connected, or can communicate with each other; it can be directly connected, or indirectly connected through an intermediary, and it can be the internal communication of two components or the interaction relationship between two components , unless expressly defined otherwise. Those of ordinary skill in the art can understand the specific meanings of the above terms in the present utility model according to specific situations.
下面结合图1至图2对本实用新型实施例的浸渗装备100进行详细描述,本实用新型实施例的浸渗装备100可以用于制备金属和陶瓷复合材料,例如铝碳化硅复合材料,但不限于此。 The impregnation equipment 100 of the embodiment of the utility model is described in detail below in conjunction with FIGS. limited to this.
根据本实用新型实施例的浸渗装备100可以包括第一容器110、第二容器120、成型模具130以及温场控制装置140。 The infiltration equipment 100 according to the embodiment of the present utility model may include a first container 110 , a second container 120 , a forming mold 130 and a temperature field control device 140 .
其中,第一容器110是密闭的且限定出第一腔室101,第一容器110为密闭的容器可以方便后续对第一腔室101做抽真空处理。 Wherein, the first container 110 is airtight and defines the first chamber 101 , and the first container 110 is an airtight container to facilitate subsequent vacuuming of the first chamber 101 .
第二容器120置于第一腔室101内且限定出用于盛装浸渗液的第二腔室102,浸渗液可以为熔融的金属液,例如可以为铝液或铜液等。由于第二容器120需要盛装金属液等高温的熔融液体,因此第二容器120需要耐高温,例如,第二容器120可以为坩埚。 The second container 120 is placed in the first chamber 101 and defines the second chamber 102 for containing the infiltration liquid. The infiltration liquid can be molten metal, such as aluminum liquid or copper liquid. Since the second container 120 needs to contain high-temperature molten liquid such as molten metal, the second container 120 needs to be resistant to high temperature. For example, the second container 120 can be a crucible.
成型模具130设有用于放置待成型产品(例如,碳化硅骨架)的第三腔室103,成型模具130上设置有用于连通第二腔室102和第三腔室103的连通结构,连通结构构造成使得第二腔室102内的浸渗液能够依靠重力至少部分地通过连通结构进入到第三腔室103内。 The forming mold 130 is provided with a third chamber 103 for placing the product to be formed (for example, a silicon carbide skeleton), and the forming mold 130 is provided with a communication structure for communicating with the second chamber 102 and the third chamber 103, and the communication structure is configured Such that the immersion liquid in the second chamber 102 can enter the third chamber 103 at least partially through the communication structure by gravity.
也就是说,本实用新型实施例中的浸渗液可以在重力的作用下流入第三腔室103,操作简单、安全,而不必进行反重力操作,例如依靠压力使得浸渗液从下向上流动到模具内部。 That is to say, the impregnating liquid in the embodiment of the present invention can flow into the third chamber 103 under the action of gravity, which is simple and safe to operate, without the need of anti-gravity operation, for example relying on pressure to make the impregnating liquid flow from bottom to top into the mold.
可选地,连通结构可以为连通孔104,连通孔104可以设置在第三腔室103的上方,由此浸渗液可以通过连通孔104进入到第三腔室103内,并在压力的作用下与待成型产品生成复合材料板。 Optionally, the communication structure may be a communication hole 104, and the communication hole 104 may be arranged above the third chamber 103, so that the infiltrating liquid can enter the third chamber 103 through the communication hole 104, and under the action of pressure Next, generate a composite material plate with the product to be formed.
温场控制装置140设置成用于对浸渗液的温度进行控制。例如,可以使得第二容器120内的温度保持一定的温度,或者从下到上逐步降低第三腔室103内浸渗液的温度,以实现复合材料板的逐步成型。 The temperature field control device 140 is configured to control the temperature of the immersion liquid. For example, the temperature in the second container 120 can be maintained at a certain temperature, or the temperature of the impregnating liquid in the third chamber 103 can be gradually lowered from bottom to top, so as to realize the step-by-step molding of the composite material board.
下面简单描述本实用新型实施例的浸渗装备100的工作过程。 The working process of the impregnation equipment 100 in the embodiment of the present utility model is briefly described below.
将成型模具130放置在第二容器120内,对第二容器120加热,当第二容器120的温度达到设定值时,将浸渗液导入第二容器120直至浸渗液没过成型模具130上的连通结构,浸渗液在重力的作用下通过连通结构进入到第三腔室103; Place the forming mold 130 in the second container 120, heat the second container 120, and when the temperature of the second container 120 reaches the set value, introduce the impregnating liquid into the second container 120 until the impregnating liquid is submerged in the forming mold 130 The connecting structure above, the impregnating liquid enters the third chamber 103 through the connecting structure under the action of gravity;
对第一腔室101进行抽真空处理,避免成品内部细微气孔的产生,将惰性气体充入到第一腔室101内以对第一容器110进行加压处理,并保压一段时间; Vacuumize the first chamber 101 to avoid the generation of fine pores inside the finished product, fill the first chamber 101 with inert gas to pressurize the first container 110, and keep the pressure for a period of time;
温场控制装置140控制浸渗液的温度,使得浸渗液的温度在从下到上的方向上逐步降低,即浸渗液下部的温度首先降低,浸渗液上部的温度后降低,由此,上部的浸渗液可以对下部逐渐凝固的浸渗液进行凝固补缩; The temperature field control device 140 controls the temperature of the impregnating liquid, so that the temperature of the impregnating liquid gradually decreases from bottom to top, that is, the temperature of the lower part of the impregnating liquid decreases first, and then the temperature of the upper part of the impregnating liquid decreases, thus , the upper impregnating liquid can solidify and feed the gradually solidifying impregnating liquid in the lower part;
凝固完成后,对第一腔室101进行泄压处理,取出第二容器120并将其内部凝固的金属块顶出,然后对金属块切割以取出成型模具130,用脱模工具把成型模具130中的成型件顶出。 After the solidification is completed, the first chamber 101 is depressurized, the second container 120 is taken out and the solidified metal block inside is ejected, then the metal block is cut to take out the forming mold 130, and the forming mold 130 is removed with a demoulding tool. The molded parts in the ejection.
根据本实用新型实施例的浸渗装备100,第二容器120内的浸渗液可以在重力的作用下进入到第三容器内,由此控制简单、安全且易于实现。 According to the impregnation equipment 100 of the embodiment of the present invention, the impregnation liquid in the second container 120 can enter into the third container under the action of gravity, so the control is simple, safe and easy to implement.
此外,第二容器120内部的浸渗液的温度可以控制,进而可以控制浸渗液的凝固速度,保证了成品质量,无缩孔/收缩不良等缺陷。 In addition, the temperature of the impregnating liquid inside the second container 120 can be controlled, thereby controlling the solidification speed of the impregnating liquid, ensuring the quality of the finished product without defects such as shrinkage cavities/shrinkage defects.
在本实用新型的一些实施例中,如图1所示,温场控制装置140设置在第一容器110内且邻近第二容器120布置。 In some embodiments of the present invention, as shown in FIG. 1 , the temperature field control device 140 is disposed in the first container 110 and adjacent to the second container 120 .
具体地,温场控制装置140包括冷却单元141和加热单元142,冷却单元141设在第二容器120的底壁下方,加热单元142可以设置在第二容器120的周壁外侧。 Specifically, the temperature field control device 140 includes a cooling unit 141 and a heating unit 142 , the cooling unit 141 is disposed below the bottom wall of the second container 120 , and the heating unit 142 may be disposed outside the peripheral wall of the second container 120 .
由此,浸渗液的冷却可以从底部开始,保证顶部的熔融状态的浸渗液可以对下方的逐渐凝固的浸渗液进行补缩,避免成型后的产品出现缩孔或收缩不良等缺陷。 Thus, the cooling of the impregnating liquid can start from the bottom, ensuring that the molten impregnating liquid at the top can feed the gradually solidified impregnating liquid below, avoiding defects such as shrinkage cavities or poor shrinkage of the formed product.
有利地,如图1所示,加热单元142为多组,每组加热单元142环绕在第二容器120的周壁外侧,且多组加热单元142在从下到上的方向上依次分布在第二容器120的周壁外侧。由此,可以通过打开或闭合每组加热单元142来逐步控制浸渗液的冷却,确保产品的良品率。 Advantageously, as shown in FIG. 1 , there are multiple groups of heating units 142 , each group of heating units 142 surrounds the outside of the peripheral wall of the second container 120 , and multiple groups of heating units 142 are sequentially distributed in the second container 120 in the direction from bottom to top. outside the peripheral wall of the container 120 . Thus, the cooling of the impregnating liquid can be gradually controlled by opening or closing each group of heating units 142 to ensure the yield rate of the product.
优选地,加热单元142可以为感应加热线圈。由此,通过磁场来实现对浸渗液的加热,安全可靠且占用的空间少。 Preferably, the heating unit 142 may be an induction heating coil. Therefore, the heating of the impregnating liquid is realized through the magnetic field, which is safe and reliable and occupies less space.
多组加热单元142基于待成型产品所需的工艺温度在上下方向上布置以对浸渗复合过程进行温度梯度控制。换言之,通过在上下方向上设置多组加热单元142,并从下到上依次关闭加多组热单元142,可以实现浸渗液的逐步凝固,进而使得浸渗液的上部分可以对下部分进行凝固补缩。 Multiple groups of heating units 142 are arranged in an up-and-down direction based on the process temperature required by the product to be formed to perform temperature gradient control on the impregnation and compounding process. In other words, by arranging multiple sets of heating units 142 in the up and down direction, and closing and adding multiple sets of heating units 142 sequentially from bottom to top, the gradual solidification of the impregnating liquid can be realized, so that the upper part of the impregnating liquid can be heated to the lower part. Freezing and feeding.
例如,加热单元142可以为三个或四个,在浸渗复合过程中,可以首先使底部的冷却单元141对浸渗液进行冷却,然后逐步从下到上关闭多组加热单元142,进而实现在浸渗复合过程中的对浸渗液的温度梯度控制。 For example, the number of heating units 142 can be three or four. During the impregnation and compounding process, the cooling unit 141 at the bottom can be used to cool the impregnating liquid, and then gradually close multiple groups of heating units 142 from bottom to top, thereby realizing The temperature gradient control of the impregnation solution during the impregnation compounding process.
有利地,第二容器120内的浸渗液的高度大于模具的高度,由此第二容器120内的浸渗液可以随时对第三腔室103内的浸渗液进行凝固补缩。此外,还可以将缩孔等缺陷留在模具上方的金属块中,而不会对成型件造成影响。 Advantageously, the height of the impregnating liquid in the second container 120 is greater than that of the mould, so that the impregnating liquid in the second container 120 can solidify and feed the impregnating liquid in the third chamber 103 at any time. In addition, defects such as shrinkage cavities can be left in the metal block above the mold without affecting the formed part.
在本实用新型的一些实施例中,如图2所示,成型模具130包括相对设置的第一模板131和第二模板132,第一模板131与第二模板132之间设有隔板150以将第三腔室103分隔成两个型腔105。 In some embodiments of the present utility model, as shown in FIG. 2 , the molding die 130 includes a first template 131 and a second template 132 arranged oppositely, and a partition 150 is provided between the first template 131 and the second template 132 to The third chamber 103 is divided into two cavities 105 .
每个型腔105可以放置一个待成型产品(例如,碳化硅骨架),在待成型产品置于型腔105内时,其上的至少两个侧面(例如,投影面积最大的两个面)应当与型腔105的内侧壁和隔板150间隔开,以方便浸渗液流入以与待成型产品结合。 Each cavity 105 can place a product to be formed (for example, a silicon carbide skeleton), and when the product to be formed is placed in the cavity 105, at least two sides on it (for example, the two surfaces with the largest projected area) should It is spaced apart from the inner wall of the cavity 105 and the partition 150 to facilitate the inflow of the impregnating liquid to combine with the product to be formed.
可选地,成型模具130可以为多个,且多个成型模具130置于第二腔室102内。由此,可以提高产品的成型效率,进而至少在一定程度上降低产品的生产成本。 Optionally, there may be multiple molding molds 130 , and multiple molding molds 130 are placed in the second cavity 102 . Thus, the molding efficiency of the product can be improved, and the production cost of the product can be reduced at least to a certain extent.
在本实用新型的一些实施例中,如图1和图2所示,第二容器120为上部敞口的筒状结构,在浸渗复合过程中,浸渗液的液面位于连通孔104之上。由此,可以保证模具上方的浸渗液可以对第三腔室103内的浸渗液进行补缩。 In some embodiments of the present utility model, as shown in Figures 1 and 2, the second container 120 is a cylindrical structure with an open upper part, and during the process of impregnation and compounding, the liquid level of the impregnating liquid is located between the communication holes 104 superior. Thus, it can be ensured that the impregnating liquid above the mold can feed the impregnating liquid in the third chamber 103 .
优选地,在浸渗复合之前,可以对第一腔室101进行抽真空。由此,可以避免成品内部细微气孔的产生。 Preferably, the first chamber 101 may be evacuated before infiltration and compounding. Thus, the generation of fine pores inside the finished product can be avoided.
在本实用新型的一些实施例中,如图1所示,第一容器110包括本体部111和顶盖部112,顶盖部112可开合的设在本体部111上以用于打开或关闭第一腔室101。当顶盖部112关闭第一腔室101时,第一容器110为密闭容器。 In some embodiments of the present invention, as shown in FIG. 1 , the first container 110 includes a body portion 111 and a top cover portion 112, and the top cover portion 112 is openably and closably arranged on the body portion 111 for opening or closing. The first chamber 101 . When the top cover portion 112 closes the first chamber 101 , the first container 110 is an airtight container.
也就是说,第一容器110可以重复利用,且结构简单,至少在一定程度上提高了产品的生产效率,降低了产品的成本。 That is to say, the first container 110 can be reused and has a simple structure, which improves the production efficiency of the product and reduces the cost of the product at least to a certain extent.
有利地,如图1所示,顶盖部112上设置有用于测量浸渗液温度的测温孔112a。当顶盖部112上的测温孔检测到第二容器120内部的浸渗液的温度达到设定值后,可以停止对第一腔室101抽真空,然后对第一腔室101进行加压,最高压力可以到9Mpa。 Advantageously, as shown in FIG. 1 , the top cover part 112 is provided with a temperature measuring hole 112a for measuring the temperature of the immersion liquid. When the temperature measuring hole on the top cover 112 detects that the temperature of the impregnating liquid inside the second container 120 reaches the set value, the vacuuming of the first chamber 101 can be stopped, and then the first chamber 101 can be pressurized , the maximum pressure can reach 9Mpa.
在本实用新型的一些实施例中,第二容器120的上端还设置有用于对第二容器120上部的浸渗液进行保温的保温隔热装置。由此,避免第二容器120内的热量过度散失,使得第二容器120上部的浸渗液在浸渗复合过程中一直保持熔融状态并可以对第三腔室103内的浸渗液进行补缩。 In some embodiments of the present invention, the upper end of the second container 120 is further provided with a thermal insulation device for keeping the soaking liquid in the upper part of the second container 120 warm. In this way, excessive loss of heat in the second container 120 is avoided, so that the impregnating liquid in the upper part of the second container 120 is kept in a molten state during the impregnation and compounding process, and the impregnating liquid in the third chamber 103 can be fed. .
在本实用新型的一些实施例中,如图1所示,第一腔室101上设置有真空阀113和压力阀114。真空阀113与抽真空装置相连以实现对第一腔室101进行抽真空,压力阀114与高压加载装置相连实现对第一腔室101加压/泄压。具体地,压力阀114可以包括增压阀114a和泄压阀114b。 In some embodiments of the present utility model, as shown in FIG. 1 , the first chamber 101 is provided with a vacuum valve 113 and a pressure valve 114 . The vacuum valve 113 is connected with a vacuum device to vacuumize the first chamber 101 , and the pressure valve 114 is connected with a high-pressure loading device to pressurize/release the first chamber 101 . Specifically, the pressure valve 114 may include a boost valve 114a and a pressure relief valve 114b.
在本实用新型的一些实施例中,如图1和图2所示,第二容器120为上端敞口的筒状结构,第二腔室102的纵截面为倒置的圆台形。也就是说,第二腔室102的横截面的面积在从下到上的方向上逐渐增大。由此,可以使得第二容器120中的浸渗液更容易没过成型模具130,降低了每次使用的浸渗液的用量。 In some embodiments of the present invention, as shown in FIG. 1 and FIG. 2 , the second container 120 is a cylindrical structure with an open upper end, and the longitudinal section of the second chamber 102 is an inverted frustum of a cone. That is to say, the area of the cross section of the second chamber 102 gradually increases from bottom to top. As a result, the impregnating liquid in the second container 120 can more easily pass through the forming mold 130 , reducing the amount of impregnating liquid used each time.
下面简单描述本实用新型实施例的浸渗系统。 The impregnation system of the embodiment of the utility model is briefly described below.
根据本实用新型实施例的浸渗系统包括上述实施例的浸渗装备100、浸渗液供给装备、抽真空装备以及高压加载装备。 The infiltration system according to the embodiment of the present utility model includes the infiltration equipment 100 of the above-mentioned embodiment, the infiltration liquid supply equipment, the vacuum equipment and the high-pressure loading equipment.
其中,浸渗液供给装备与浸渗装备100相连用于向浸渗装备100内供给浸渗液;抽真空装备与浸渗装备100相连用于对浸渗装备100内部抽真空;高压装载装备,高压装载装备与浸渗装备100相连用于对浸渗装备100加压/泄压。 Wherein, the impregnating liquid supply equipment is connected with the impregnating equipment 100 for supplying the impregnating liquid into the impregnating equipment 100; the vacuuming equipment is connected with the impregnating equipment 100 for vacuuming the interior of the impregnating equipment 100; the high pressure loading equipment, The high pressure loading equipment is connected to the impregnation equipment 100 for pressurizing/depressurizing the impregnation equipment 100 .
根据本实用新型实施例的浸渗系统,可以保证产品的成品质量且降低了产品的生产成本。 According to the impregnation system of the embodiment of the utility model, the quality of the finished product can be guaranteed and the production cost of the product can be reduced.
下面详细描述本实用新型浸渗系统的一个具体实施例以及工作过程。 A specific embodiment and working process of the impregnation system of the present invention will be described in detail below.
本实用新型实施例的浸渗装备100,可以用来实现铝碳化硅复合材料IGBT(InsulatedGateBipolarTransistor)基板的精密成型。 The impregnation equipment 100 of the embodiment of the utility model can be used to realize precise molding of an aluminum silicon carbide composite material IGBT (Insulated Gate Bipolar Transistor) substrate.
第一容器110的顶盖部112可以自动打开和关闭,顶盖部112设置有测温孔112a,第一容器110的内壁由不锈钢制作并抛光处理,内部可以耐高压且使用温度最高可达1250度;第一容器110的筒壁设置有真空阀113、压力阀114(可以包括:增压阀114a和泄压阀114b);测温孔112a用来检测第二容器120内部的浸渗液的温度。 The top cover 112 of the first container 110 can be opened and closed automatically. The top cover 112 is provided with a temperature measuring hole 112a. The inner wall of the first container 110 is made of stainless steel and polished. The inside can withstand high pressure and the maximum service temperature can reach 1250 degree; the cylinder wall of the first container 110 is provided with a vacuum valve 113 and a pressure valve 114 (may include: a booster valve 114a and a pressure relief valve 114b); temperature.
第二容器120的底壁下方设置了冷却单元141,冷却单元141内部导入冷却介质;冷却介质的流动速度和输入温度可以根据工艺要求进行调节,从而通过调节冷却单元141的冷却速率,最终调节第二容器120内部的浸渗液的凝固速度。 A cooling unit 141 is arranged below the bottom wall of the second container 120, and a cooling medium is introduced inside the cooling unit 141; the flow rate and input temperature of the cooling medium can be adjusted according to the process requirements, thereby adjusting the cooling rate of the cooling unit 141 to finally adjust the first Second, the solidification speed of the soaking liquid inside the container 120.
第一容器110内部设置有第二容器120,第二容器120可以放置在冷却单元141的顶面;第二容器120外围设置加热单元142,分为可以单独控制的上加热单元和下加热单元;上加热单元和下加热单元可以对第二容器120以及第二容器120内部的物质(即,浸渗液)进行加热,加热温度最高达到1250度;第二容器120的端口还可以设置保温隔热装置(未示出);第二容器120内部放置了成型模具130,成型模具130内部设有隔板150以将第三腔室103分隔成两个成型腔105,成型腔105内放置碳化硅骨架,成型模具130顶部设置有连通孔104用于铝液流入成型模具130内的第三腔室103中;第二容器120、成型模具130和隔板150均由耐800度以上高温且热膨胀系数较低的材料(如石墨、钨钼材料等)加工而成,且可以反复利用。 A second container 120 is arranged inside the first container 110, and the second container 120 can be placed on the top surface of the cooling unit 141; a heating unit 142 is arranged on the periphery of the second container 120, which is divided into an upper heating unit and a lower heating unit that can be controlled separately; The upper heating unit and the lower heating unit can heat the second container 120 and the substance inside the second container 120 (that is, the impregnation liquid), and the heating temperature can reach up to 1250 degrees; the port of the second container 120 can also be provided with thermal insulation device (not shown); a forming mold 130 is placed inside the second container 120, and a partition 150 is provided inside the forming mold 130 to separate the third chamber 103 into two forming cavities 105, and a silicon carbide skeleton is placed in the forming cavity 105 The top of the forming mold 130 is provided with a communication hole 104 for the aluminum liquid to flow into the third chamber 103 in the forming mold 130; the second container 120, the forming mold 130 and the separator 150 are all resistant to high temperatures above 800 degrees and have a relatively high thermal expansion coefficient. It is made of low-cost materials (such as graphite, tungsten and molybdenum materials, etc.), and can be used repeatedly.
铝液自动给料系统可以把已经熔融的铝合金液体从熔炼炉(图中未画出)中加载到第二容器120内部,每次加载的铝液重量可以根据工艺要求进行调节。抽真空系统可以对第一容器110进行真空处理,极限真空值为0.1pa,保证浸渗复合前把碳化硅骨架内部的气体全部抽出。高压加载系统可以对第一容器110进行加压处理,加压介质为惰性气体(如氮气/氩气),最大压力可以达到9Mpa。 The aluminum liquid automatic feeding system can load the molten aluminum alloy liquid from the melting furnace (not shown in the figure) into the second container 120, and the weight of the aluminum liquid loaded each time can be adjusted according to the process requirements. The vacuum system can perform vacuum treatment on the first container 110, and the ultimate vacuum value is 0.1 Pa, so as to ensure that all the gas inside the silicon carbide skeleton is exhausted before impregnation and compounding. The high-pressure loading system can pressurize the first container 110, and the pressurizing medium is an inert gas (such as nitrogen/argon), and the maximum pressure can reach 9Mpa.
铝碳化硅复合材料是一种新型的复合材料,具有密度低、热导率高、热膨胀系数低等优点,广泛应用于电子散热封装和航天航空领域。在能源紧缺和大气严重污染的环境下,很多企业都在推出新能源动力方案的交通工具,铝硅碳复合材料是新能源动力控制装置中的关键部件,用来对IGBT模块中的芯片进行承载和散热,应用前景长远。在实际的制备工艺和成品使用中,需要控制碳化硅骨架表面的覆铝厚度在0.15mm以内,平面度控制在0.2mm以内,内部质地紧密,无气孔、缩孔,表面光滑,无划伤、缩痕。由于碳化硅骨架为孔隙结构且与铝合金液体不浸润,一般采用高温高压浸渗工艺进行复合。 Aluminum silicon carbide composite material is a new type of composite material, which has the advantages of low density, high thermal conductivity, and low thermal expansion coefficient. It is widely used in electronic heat dissipation packaging and aerospace fields. In the environment of energy shortage and severe air pollution, many companies are launching vehicles with new energy power solutions. Aluminum silicon carbon composite materials are key components in new energy power control devices, and are used to carry chips in IGBT modules. And heat dissipation, the application prospect is long-term. In the actual preparation process and the use of finished products, it is necessary to control the thickness of the aluminum coating on the surface of the silicon carbide skeleton within 0.15mm, the flatness within 0.2mm, the internal texture is tight, no pores, shrinkage cavities, smooth surface, no scratches, sink marks. Since the silicon carbide skeleton has a pore structure and does not infiltrate with the aluminum alloy liquid, it is generally compounded by high temperature and high pressure infiltration process.
具体实施方案:采用近净成型原则,根据碳化硅骨架的外形尺寸设计和加工成型模具130的模芯,保证碳化硅骨架在模具内部与模芯的间隙单边≤0.15mm,从而控制复合材料表面的覆铝厚度,保证产品质量。相对设置的第一模板131和第二模板132的中间放置一个隔板150,可以根据复合材料和第二容器120的大小放置相应数量的成型模具130和隔板150。 Specific implementation plan: adopt the principle of near-net shape, design and process the mold core of the mold 130 according to the external dimensions of the silicon carbide skeleton, and ensure that the gap between the silicon carbide skeleton and the mold core in the mold is ≤0.15mm on one side, so as to control the surface of the composite material The thickness of aluminum cladding ensures product quality. A partition 150 is placed in the middle of the first template 131 and the second template 132 which are arranged oppositely, and a corresponding number of forming molds 130 and partitions 150 can be placed according to the size of the composite material and the second container 120 .
把装有碳化硅骨架的成型模具130和隔板150放置在第二容器120内部,第一容器110的顶盖自动打开,然后把第二容器120放置在冷却单元141上。加热单元142对第二容器120进行加热,当成型模具130温度达到设定值后,铝液自动给料系统把设定重量的铝液加载到第二容器120内部,铝液把模具完全浸没。第一容器110的顶盖自动关闭,真空阀113打开,抽真空系统工作,对第一容器110进行抽真空,极限真空值可以到0.1pa。当顶盖测温孔112a检测到第二容器120内部温度达到设定值后,真空阀113关闭,增压阀114a打开,高压加载系统对第一容器110进行加压(惰性气体),最高压力可以到9Mpa。当第一容器110内部压力达到设定值后,增压阀114a关闭,进行保压处理,在压力的作用下,熔融的铝液可以与型腔105内的碳化硅陶瓷骨架更好的复合。 The forming mold 130 and the separator 150 equipped with the silicon carbide skeleton are placed inside the second container 120 , the top cover of the first container 110 is automatically opened, and then the second container 120 is placed on the cooling unit 141 . The heating unit 142 heats the second container 120. When the temperature of the forming mold 130 reaches the set value, the aluminum liquid automatic feeding system loads the set weight of aluminum liquid into the second container 120, and the aluminum liquid completely submerges the mold. The top cover of the first container 110 is automatically closed, the vacuum valve 113 is opened, the vacuum system works, and the first container 110 is vacuumed, and the ultimate vacuum value can reach 0.1 Pa. When the temperature measuring hole 112a of the top cover detects that the internal temperature of the second container 120 reaches the set value, the vacuum valve 113 is closed, the booster valve 114a is opened, and the high-pressure loading system pressurizes the first container 110 (inert gas), the maximum pressure It can reach 9Mpa. When the internal pressure of the first container 110 reaches the set value, the booster valve 114a is closed and the pressure maintaining process is performed. Under the action of the pressure, the molten aluminum can be better compounded with the silicon carbide ceramic skeleton in the cavity 105 .
保压结束后,冷却单元141的冷却介质按照一定速度导入,下加热单元停止工作,上加热单元保持工作,实现第二容器120内部的浸渗液从底部向上开始顺序凝固;凝固一段时间后,上加热单元也停止工作,同时加大梯度控制冷却托盘冷却介质的流速,完成第二容器120内部预制件上部的顺序凝固。在第二容器120内部浸渗液的整个顺序冷却过程中,开始阶段时上加热单元处于工作状态,保证成型模具130上部的铝液处于较高温度,可以对下部进行凝固补缩。 After the pressure holding is completed, the cooling medium of the cooling unit 141 is introduced at a certain speed, the lower heating unit stops working, and the upper heating unit keeps working, so that the impregnating liquid in the second container 120 is sequentially solidified from the bottom to the top; after solidification for a period of time, The upper heating unit also stops working, and at the same time increases the gradient to control the flow rate of the cooling medium in the cooling tray to complete the sequential solidification of the upper part of the preform inside the second container 120 . During the entire sequential cooling process of the impregnating liquid inside the second container 120, the upper heating unit is in working state at the beginning to ensure that the aluminum liquid in the upper part of the forming mold 130 is at a higher temperature, and the lower part can be solidified and fed.
凝固过程结束后,打开泄压阀114b,对第一容器110的内部压力进行泄压,打开顶盖部112并取出第二容器120。冷却后,通过工装把第二容器120内部的预制件取出,对预制件进行切割,取出成型模具130。用脱模工装把成型模具130中的铝碳化硅复合材料顶出,得到近净成型的成品。从实际生产的情况来看,采用本实用新型的冷却梯度控制工艺,良品率极高。对近净成型的成品进行后加工处理和表面处理后,得到合格的成品。第一容器110、第二容器120、成型模具130和隔板150都可以重复利用,切割下来的铝锭也可以重新熔炼使用。 After the solidification process is completed, the pressure release valve 114b is opened to release the internal pressure of the first container 110 , the top cover 112 is opened and the second container 120 is taken out. After cooling, the preform inside the second container 120 is taken out by tooling, the preform is cut, and the forming mold 130 is taken out. The aluminum-silicon carbide composite material in the forming mold 130 is ejected with a demoulding tool to obtain a near-net-shaped finished product. From the actual production situation, adopting the cooling gradient control process of the utility model, the good product rate is extremely high. After post-processing and surface treatment of the near-net-shaped finished product, a qualified finished product can be obtained. The first container 110 , the second container 120 , the molding die 130 and the separator 150 can all be reused, and the cut aluminum ingots can also be remelted for use.
有益效果: Beneficial effect:
1、采用成型模具130近净成型,满足复合材料外表面覆铝厚度≤0.15mm和平面度≤0.2mm的要求,第二容器120和成型模具130可以重复利用,大大节省了耗材成本; 1. The molding die 130 is used for near-net molding, which meets the requirements that the thickness of the outer surface of the composite material is not more than 0.15mm and the flatness is not more than 0.2mm. The second container 120 and the molding die 130 can be reused, which greatly saves the cost of consumables;
2、利用浸渗液的自身重力进行补缩,区别于反重力方向浸渗液补缩,控制简单,易于实现; 2. Using the gravity of the impregnating liquid for feeding, which is different from the feeding of the impregnating liquid in the direction of anti-gravity, the control is simple and easy to realize;
3、第二容器120内部的浸渗液的冷却凝固速率可控,完全保证了成品质量,无缩孔/收缩不良; 3. The cooling and solidification rate of the impregnating liquid inside the second container 120 is controllable, which fully guarantees the quality of the finished product without shrinkage cavity/shrinkage defect;
4、浸渗液在外部熔炼,提高了安全系数,减少了装备体积; 4. The impregnation liquid is smelted outside, which improves the safety factor and reduces the volume of equipment;
5、浸渗复合前,采取了抽真空处理,避免了成品内部细微气孔的产生; 5. Before impregnation and compounding, vacuum treatment is adopted to avoid the generation of fine pores inside the finished product;
6、第二容器120置于第一容器110的内部,安全系数高,有利于保证生产安全。 6. The second container 120 is placed inside the first container 110, which has a high safety factor and is conducive to ensuring production safety.
在本实用新型中,除非另有明确的规定和限定,第一特征在第二特征“上”或“下”可以是第一和第二特征直接接触,或第一和第二特征通过中间媒介间接接触。而且,第一特征在第二特征“之上”、“上方”和“上面”可是第一特征在第二特征正上方或斜上方,或仅仅表示第一特征水平高度高于第二特征。第一特征在第二特征“之下”、“下方”和“下面”可以是第一特征在第二特征正下方或斜下方,或仅仅表示第一特征水平高度小于第二特征。 In the present invention, unless otherwise clearly specified and limited, the first feature may be in direct contact with the first feature or the first feature and the second feature through an intermediary indirect contact. Moreover, "above", "above" and "above" the first feature on the second feature may mean that the first feature is directly above or obliquely above the second feature, or simply means that the first feature is higher in level than the second feature. "Below", "beneath" and "beneath" the first feature may mean that the first feature is directly below or obliquely below the second feature, or simply means that the first feature is less horizontally than the second feature.
在本说明书的描述中,参考术语“一个实施例”、“一些实施例”、“示例”、“具体示例”、或“一些示例”等的描述意指结合该实施例或示例描述的具体特征、结构、材料或者特点包含于本实用新型的至少一个实施例或示例中。在本说明书中,对上述术语的示意性表述不必须针对的是相同的实施例或示例。而且,描述的具体特征、结构、材料或者特点可以在任一个或多个实施例或示例中以合适的方式结合。此外,在不相互矛盾的情况下,本领域的技术人员可以将本说明书中描述的不同实施例或示例以及不同实施例或示例的特征进行结合和组合。 In the description of this specification, descriptions referring to the terms "one embodiment", "some embodiments", "example", "specific examples", or "some examples" mean that specific features described in connection with the embodiment or example , structures, materials or features are included in at least one embodiment or example of the present invention. In this specification, the schematic representations of the above terms are not necessarily directed to the same embodiment or example. Furthermore, the described specific features, structures, materials or characteristics may be combined in any suitable manner in any one or more embodiments or examples. In addition, those skilled in the art can combine and combine different embodiments or examples and features of different embodiments or examples described in this specification without conflicting with each other.
尽管上面已经示出和描述了本实用新型的实施例,可以理解的是,上述实施例是示例性的,不能理解为对本实用新型的限制,本领域的普通技术人员在本实用新型的范围内可以对上述实施例进行变化、修改、替换和变型。 Although the embodiments of the present invention have been shown and described above, it can be understood that the above-mentioned embodiments are exemplary and should not be construed as limitations of the present invention, and those skilled in the art are within the scope of the present invention. Variations, modifications, substitutions and variations can be made to the above-described embodiments.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106424667A (en) * | 2016-12-19 | 2017-02-22 | 湖南顶立科技有限公司 | Impregnating equipment and method |
| CN106694859A (en) * | 2016-12-19 | 2017-05-24 | 湖南顶立科技有限公司 | Impregnating equipment |
| CN106733421A (en) * | 2016-12-19 | 2017-05-31 | 湖南顶立科技有限公司 | A kind of immersion system and dipping method |
| CN110227797A (en) * | 2019-07-12 | 2019-09-13 | 维捷(苏州)三维打印有限公司 | The preparation process and equipment of 3 D-printing ceramic shell for Ti alloy casting |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106424667A (en) * | 2016-12-19 | 2017-02-22 | 湖南顶立科技有限公司 | Impregnating equipment and method |
| CN106694859A (en) * | 2016-12-19 | 2017-05-24 | 湖南顶立科技有限公司 | Impregnating equipment |
| CN106733421A (en) * | 2016-12-19 | 2017-05-31 | 湖南顶立科技有限公司 | A kind of immersion system and dipping method |
| CN106424667B (en) * | 2016-12-19 | 2018-08-03 | 湖南顶立科技有限公司 | A kind of impregnating equipment and dipping method |
| CN106694859B (en) * | 2016-12-19 | 2019-02-26 | 湖南顶立科技有限公司 | A kind of impregnating equipment |
| CN106733421B (en) * | 2016-12-19 | 2019-12-17 | 湖南顶立科技有限公司 | Impregnation device and impregnation method |
| CN110227797A (en) * | 2019-07-12 | 2019-09-13 | 维捷(苏州)三维打印有限公司 | The preparation process and equipment of 3 D-printing ceramic shell for Ti alloy casting |
| CN110227797B (en) * | 2019-07-12 | 2021-05-28 | 维捷(苏州)三维打印有限公司 | Preparation process of three-dimensional printing ceramic shell for titanium alloy casting |
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