CN1546498A - Method for separation and purification of grape-seed lecithin - Google Patents
Method for separation and purification of grape-seed lecithin Download PDFInfo
- Publication number
- CN1546498A CN1546498A CNA2003101158512A CN200310115851A CN1546498A CN 1546498 A CN1546498 A CN 1546498A CN A2003101158512 A CNA2003101158512 A CN A2003101158512A CN 200310115851 A CN200310115851 A CN 200310115851A CN 1546498 A CN1546498 A CN 1546498A
- Authority
- CN
- China
- Prior art keywords
- acetone
- ether
- vitis viniferae
- semen vitis
- filter
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims abstract description 10
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 title claims abstract description 6
- 239000000787 lecithin Substances 0.000 title claims abstract description 6
- 229940067606 lecithin Drugs 0.000 title claims abstract description 6
- 235000010445 lecithin Nutrition 0.000 title claims abstract description 6
- 229940087559 grape seed Drugs 0.000 title abstract 2
- 238000000746 purification Methods 0.000 title abstract 2
- 238000000926 separation method Methods 0.000 title abstract 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims abstract description 41
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 239000007788 liquid Substances 0.000 claims abstract description 4
- 235000009392 Vitis Nutrition 0.000 claims description 16
- 241000219095 Vitis Species 0.000 claims description 16
- 210000000582 semen Anatomy 0.000 claims description 15
- 239000000284 extract Substances 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 238000004821 distillation Methods 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 239000000047 product Substances 0.000 claims description 5
- 239000000706 filtrate Substances 0.000 claims description 4
- 239000000243 solution Substances 0.000 claims description 4
- 230000008030 elimination Effects 0.000 claims description 3
- 238000003379 elimination reaction Methods 0.000 claims description 3
- 235000012054 meals Nutrition 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 claims description 3
- 238000001556 precipitation Methods 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 2
- 239000012535 impurity Substances 0.000 claims description 2
- 240000006365 Vitis vinifera Species 0.000 abstract description 2
- 235000014787 Vitis vinifera Nutrition 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 238000001914 filtration Methods 0.000 abstract 2
- 238000005292 vacuum distillation Methods 0.000 abstract 2
- 235000009754 Vitis X bourquina Nutrition 0.000 abstract 1
- 235000012333 Vitis X labruscana Nutrition 0.000 abstract 1
- 150000001298 alcohols Chemical class 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 239000012141 concentrate Substances 0.000 abstract 1
- 230000008021 deposition Effects 0.000 abstract 1
- 238000009991 scouring Methods 0.000 abstract 1
- 230000006870 function Effects 0.000 description 3
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 208000024827 Alzheimer disease Diseases 0.000 description 1
- 206010003210 Arteriosclerosis Diseases 0.000 description 1
- 206010012289 Dementia Diseases 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 206010039966 Senile dementia Diseases 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000003035 anti-peroxidant effect Effects 0.000 description 1
- 208000011775 arteriosclerosis disease Diseases 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 210000002969 egg yolk Anatomy 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000003053 immunization Effects 0.000 description 1
- 230000003834 intracellular effect Effects 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 230000003908 liver function Effects 0.000 description 1
- 230000036651 mood Effects 0.000 description 1
- 230000008271 nervous system development Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 230000002792 vascular Effects 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention relates to the process for extracting lecithin, in particular the method for separation and purification of grape-seed lecithin, which comprises the steps of, (1) using grape seeds as raw material, (2) circulation impregnating with propanone, (3) extracting the filter residue with alcohols, (4) proceeding vacuum distillation to the filter liquor, (5) charing ether into the concentrate to settle the insoluble substance, (6) filtering, evolution of deposition, filtering ether, acetone miscible liquid, scouring with acetone, vacuum distillation, reclaiming ether and acetone to obtain the lecithin end product.
Description
[technical field]
The present invention relates to a kind of Yelkin TTS extracting method, promptly is the Semen Vitis viniferae Yelkin TTS separating and purifying method of raw material with the Semen Vitis viniferae.
[background technology]
In prior art, Yelkin TTS is described as and protein, VITAMIN " three big nutrient substances " arranged side by side, and in developed country, Yelkin TTS has become very universal nutritive food.It is reported that the American cooks now and also used Yelkin TTS, the rice grain that cooks is full, glittering and translucent, the fragrance people of overflowing.Modern study shows; Yelkin TTS has liver function protecting, keeps vascular patency, urgees tire, baby's nervous system development, prevents senile dementia, prevents and treats gallbladdergallstonecholetithiasis, regulates mood; relieving psychological pressure, diabetic subject's nutritious prod, decomposer intracellular toxin; cosmetic result is remarkable; as seen the pharmaceutical use of Yelkin TTS, nourishing function will attract great attention; become the important healthcare products of following domestic market, potential market is very big.The extraction of Yelkin TTS is a main raw material with yolk, soybean mainly, is that raw material extraction Yelkin TTS does not appear in the newspapers with the Semen Vitis viniferae.
[summary of the invention]
The objective of the invention is to provide a kind of at above-mentioned deficiency is raw material with the Semen Vitis viniferae, the Semen Vitis viniferae Yelkin TTS separating and purifying method that yield is high.
Technical solution of the present invention is: Semen Vitis viniferae Yelkin TTS separating and purifying method is the refined lecithin that extracts from Semen Vitis viniferae, and extraction yield is more than 15%, and refining rate is more than 9%, and purity is more than 96%.The extraction process step of Semen Vitis viniferae Yelkin TTS: (1) Semen Vitis viniferae is made raw material, gets through cleaning, and the removal of impurity is ground into meal.(2) flooded 36-48 hour with acetone recycle, filter, abandon filtrate (filtrate being used to extracted cholesterol).(3) filter residue adds 95% ethanol after squeezing, and extracts 4-5 time, extracts 30-50 ℃ of temperature, and united extraction liquid, residue are used to obtain through refining the kephalin raw material.(4) with the extracting solution underpressure distillation, reclaim solvent, emit enriched material while hot.(5) add diethyl ether in the enriched material and constantly stir, place, insolubles is precipitated fully.(6) filter, get upper strata ether clear liquor, under stirring rapidly, add in the acetone, separate out precipitation; Elimination ether, acetone mixed solution (being used to extract raisin seed oil) are used washing with acetone 3-4 time, and ether, acetone are reclaimed in underpressure distillation, promptly get the Yelkin TTS finished product.
Use: be used for medicine, health care and food service industry, as: the main raw material of the emulsifying agent of infatmul, foodstuff additive, healthcare products etc.
Function: arteriosclerosis, vessel softening, reducing blood-fat, anti peroxidation of lipid, anti-cell aging, anti-ageing year dementia, functions such as the immunizing power of enhancing body.
Advantage of the present invention is: 1, utilizes the vinify waste-Semen Vitis viniferae of Changbai Mountain affluent resources to be raw material, turns waste into wealth, and the extraction yield height (more than 15%) of Yelkin TTS, purity is more than 96%.2, reasonable, simple, economic, the easy row of technology.
Below in conjunction with embodiment the present invention is described in further detail.
[embodiment]
Semen Vitis viniferae Yelkin TTS separating and purifying method step is as follows:
(1) learns from else's experience to clean and get, deimpurity Semen Vitis viniferae meal 1000 grams;
(2) flooded 45 hours with acetone recycle, filter, go filtrate, get filter residue;
(3) filter residue adds 95% ethanol, extracts 5 times, extracts 45 ℃ of temperature, united extraction liquid;
(4) with the extracting solution underpressure distillation, reclaim solvent, emit enriched material while hot;
(5) add diethyl ether in the enriched material and constantly stir, place, insolubles is precipitated fully;
(6) filter, get upper strata ether clear liquor, add in the acetone under stirring rapidly, separate out precipitation, elimination ether, acetone mixed solution are used washing with acetone 3 times, and ether, acetone are reclaimed in underpressure distillation, promptly get Yelkin TTS finished product 13.5 grams, purity 96%.
Claims (1)
1, a kind of Semen Vitis viniferae Yelkin TTS separating and purifying method is characterized in that it is the refined lecithin that extracts, and specifically may further comprise the steps from Semen Vitis viniferae:
(1) make raw material with Semen Vitis viniferae, get through cleaning, the removal of impurity is ground into meal;
(2) flooded 36-48 hour with acetone recycle, filter, go filtrate, get filter residue;
(3) filter residue adds 95% ethanol, extracts 4-5 time, extracts 30-50 ℃ of temperature, united extraction liquid;
(4) with the extracting solution underpressure distillation, reclaim solvent, emit enriched material while hot;
(5) add diethyl ether in the enriched material and constantly stir, place, insolubles is precipitated fully;
(6) filter, get upper strata ether clear liquor, add in the acetone under stirring rapidly, separate out precipitation, elimination ether, acetone mixed solution are used washing with acetone 3-4 time, and ether, acetone are reclaimed in underpressure distillation, promptly get the Yelkin TTS finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2003101158512A CN1546498A (en) | 2003-11-28 | 2003-11-28 | Method for separation and purification of grape-seed lecithin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2003101158512A CN1546498A (en) | 2003-11-28 | 2003-11-28 | Method for separation and purification of grape-seed lecithin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1546498A true CN1546498A (en) | 2004-11-17 |
Family
ID=34337409
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNA2003101158512A Pending CN1546498A (en) | 2003-11-28 | 2003-11-28 | Method for separation and purification of grape-seed lecithin |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1546498A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101239988B (en) * | 2008-01-22 | 2010-12-08 | 浙江工业大学 | A kind of powdered rape phospholipid and its production method |
| WO2014099726A1 (en) * | 2012-12-20 | 2014-06-26 | Cargill, Incorporated | Method for the purification of lecithin |
| CN110078758A (en) * | 2019-06-10 | 2019-08-02 | 中国科学院新疆理化技术研究所 | A kind of method and application for extracting phosphatide from walnut flower |
-
2003
- 2003-11-28 CN CNA2003101158512A patent/CN1546498A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101239988B (en) * | 2008-01-22 | 2010-12-08 | 浙江工业大学 | A kind of powdered rape phospholipid and its production method |
| WO2014099726A1 (en) * | 2012-12-20 | 2014-06-26 | Cargill, Incorporated | Method for the purification of lecithin |
| US9328314B2 (en) | 2012-12-20 | 2016-05-03 | Cargill, Incorporated | Method for the purification of lecithin |
| US9605009B2 (en) | 2012-12-20 | 2017-03-28 | Cargill, Incorporated | Method for the purification of lecithin |
| CN110078758A (en) * | 2019-06-10 | 2019-08-02 | 中国科学院新疆理化技术研究所 | A kind of method and application for extracting phosphatide from walnut flower |
| CN110078758B (en) * | 2019-06-10 | 2021-10-22 | 中国科学院新疆理化技术研究所 | A kind of method and application of extracting phospholipid from walnut flower |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |