CN1314627C - A kind of wrapping and cooling method of diammonium phosphate product - Google Patents
A kind of wrapping and cooling method of diammonium phosphate product Download PDFInfo
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- CN1314627C CN1314627C CNB2005100033010A CN200510003301A CN1314627C CN 1314627 C CN1314627 C CN 1314627C CN B2005100033010 A CNB2005100033010 A CN B2005100033010A CN 200510003301 A CN200510003301 A CN 200510003301A CN 1314627 C CN1314627 C CN 1314627C
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- wrapping
- diammonium phosphate
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- oil
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- 239000005696 Diammonium phosphate Substances 0.000 title claims abstract description 17
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 229910000388 diammonium phosphate Inorganic materials 0.000 title claims abstract description 17
- 235000019838 diammonium phosphate Nutrition 0.000 title claims abstract description 17
- 238000001816 cooling Methods 0.000 title abstract description 6
- 239000000463 material Substances 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 17
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 6
- 238000004176 ammonification Methods 0.000 claims abstract description 4
- 238000001035 drying Methods 0.000 claims abstract 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- 238000012856 packing Methods 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 239000002245 particle Substances 0.000 abstract description 4
- 239000011248 coating agent Substances 0.000 abstract description 3
- 238000000576 coating method Methods 0.000 abstract description 3
- 239000006185 dispersion Substances 0.000 abstract description 2
- 239000003337 fertilizer Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 239000002686 phosphate fertilizer Substances 0.000 description 2
- 239000002689 soil Substances 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 239000011247 coating layer Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000035558 fertility Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000004533 oil dispersion Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Fertilizers (AREA)
Abstract
本发明公开了一种磷酸二铵产品的包裹及冷却方法,该方法是经磷酸氨化得到的磷酸二铵物料用干燥机干燥后,严格控制磷酸二铵物料的出料温度在70~100℃,接着将热物料直接进入包裹机,进行包裹作业,从包裹机出来的物料着送入流化床冷却机使之冷却到55℃以下。使用本发明的方法,磷酸二铵产品在包裹机内进行包裹时,由于物料温度高,包裹油分散性好,包裹油在颗料表面涂层薄,使包裹油消耗量大幅度降低,可以节约包裹油的消耗量,降低生产成本;包裹后的产品外观颜色一致均匀,使产品具有良好的外观形象。本发明方法适用于利用湿法磷酸生产磷酸二铵的企业。The invention discloses a method for wrapping and cooling a diammonium phosphate product. The method is to strictly control the discharge temperature of the diammonium phosphate material at 70-100°C after drying the diammonium phosphate material obtained through ammonification of phosphoric acid , Then put the hot material directly into the wrapping machine for wrapping operation, and send the material out of the wrapping machine into the fluidized bed cooler to cool it below 55°C. Using the method of the present invention, when the diammonium phosphate product is wrapped in the wrapping machine, due to the high temperature of the material, the dispersion of the wrapping oil is good, and the coating of the wrapping oil on the surface of the particles is thin, so that the consumption of the wrapping oil is greatly reduced, which can save The consumption of wrapping oil reduces the production cost; the appearance and color of the wrapped product are uniform and uniform, so that the product has a good appearance image. The method of the invention is suitable for enterprises that use wet-process phosphoric acid to produce diammonium phosphate.
Description
[技术领域][technical field]
本发明涉及磷肥的生产工艺,具体来说,涉及磷酸二铵产品包裹及冷却方法。The invention relates to a production process of phosphate fertilizer, in particular to a method for wrapping and cooling diammonium phosphate products.
[背景技术][Background technique]
众所周知,化学肥料采用包裹技术,能够使肥料的养分在土壤中逐步释放,较长时间保持土壤肥力,避免肥料养分的流失。人们在肥料包裹技术的研究方面已经取得了许多成果,检索到的有关专利申请就有12件,例如CN00114580.0号“矿物包裹缓释复合肥及其制备方法”、CN02126743.X号“用于包裹型缓释肥料的缓释外包裹层”等。As we all know, chemical fertilizers adopt encapsulation technology, which can gradually release the nutrients of fertilizers in the soil, maintain soil fertility for a long time, and avoid the loss of fertilizer nutrients. People have made many achievements in the research of fertilizer wrapping technology, and there are 12 relevant patent applications retrieved, such as CN00114580.0 "mineral wrapped slow-release compound fertilizer and its preparation method", CN02126743.X "for Slow-release outer coating layer of coated slow-release fertilizer", etc.
传统的磷酸二铵包裹技术,采用先冷却肥料后进行包裹的工艺。这种工艺存在着以下缺点:由于进入包裹机物料温度低,喷入包裹机包裹油在产品粒子外部迅速脂化,导致产品粒子外部不能在包裹机内被包裹油包裹均匀。出包裹机后的产品要么不达到一致的外观颜色,要么会因为包裹油涂层太厚,导致产品包装后出现结块问题。同时由于客户对产品外观要求高,为保证产品外观颜色,只好加大包裹用量。造成包裹油消耗增大。The traditional diammonium phosphate wrapping technology adopts the process of cooling the fertilizer first and then wrapping it. This process has the following disadvantages: due to the low temperature of the material entering the wrapping machine, the wrapping oil sprayed into the wrapping machine is rapidly lipidized outside the product particles, resulting in that the outside of the product particles cannot be evenly wrapped by the wrapping oil in the wrapping machine. The products after leaving the wrapping machine either do not achieve a consistent appearance color, or because the wrapping oil coating is too thick, resulting in agglomeration problems after packaging. At the same time, because customers have high requirements on the appearance of products, in order to ensure the appearance and color of products, they had to increase the amount of packages. Resulting in increased package oil consumption.
[发明内容][Content of the invention]
本发明目的在于提供一种既能够有效降低包裹油消耗,又能够改善产品外观质量的磷酸二铵产品的包裹方法,以克服现有技术的缺点。The purpose of the present invention is to provide a wrapping method for diammonium phosphate products that can effectively reduce wrapping oil consumption and improve product appearance quality, so as to overcome the shortcomings of the prior art.
为达到这一发明目的,发明人在实践中根据生产现状对包裹油的包裹效果进行了充分的实验,得出当产品物料温度在75~85℃之间,包裹油对产品的包裹效果最好。产品温度低于75℃进入包裹机后,产品在包裹期间油分散不好,为保证产品颜色一致,会造成包裹油膜较厚。而当产品温度高于85℃后,过高的产品温度会导致包裹油的分解,不仅对包裹环境造成影响,同时也会增加油的消耗量。In order to achieve the purpose of this invention, the inventor conducted sufficient experiments on the wrapping effect of the wrapping oil in practice according to the current production situation, and concluded that when the temperature of the product material is between 75 and 85°C, the wrapping oil has the best wrapping effect on the product . After the product temperature is lower than 75°C and enters the wrapping machine, the oil dispersion of the product is not good during the wrapping period. In order to ensure the consistent color of the product, the wrapping oil film will be thicker. When the product temperature is higher than 85°C, the high product temperature will lead to the decomposition of the package oil, which will not only affect the package environment, but also increase the consumption of oil.
根据实验结果,发明人提出的包裹方法,是经磷酸氨化得到的磷酸二铵物料通过控制干燥机干燥时,严格控制磷酸二铵物料的出料温度在70~100℃,接着将热物料直接进入包裹机,进行包裹作业,从包裹机出来的物料着送入流化床冷却机使之冷却到55℃以下。According to the experimental results, the wrapping method proposed by the inventor is to strictly control the discharge temperature of the diammonium phosphate material at 70-100°C when the diammonium phosphate material obtained through phosphoric acid ammonification is dried by a controlled dryer, and then the hot material is directly Enter the wrapping machine, carry out the wrapping operation, and send the material from the wrapping machine to the fluidized bed cooler to cool it below 55°C.
发明人指出,进入包裹机的热物料最佳温度为75~85℃。The inventor pointed out that the optimal temperature of the hot material entering the wrapping machine is 75-85°C.
使用本发明所提供的方法,磷酸二铵产品在包裹机内进行包裹时,由于物料温度高,包裹油分散性好,包裹油在颗料表面涂层薄,使包裹油消耗量较原来的先冷却再包裹工艺的消耗小得多,产品包裹油着色剂消耗可由原4.5kg/t降到3.5~4.0kg/t,可以节约包裹油的消耗量,降低生产成本,按每1t包裹油13000元计算,使用本工艺后,产品包裹成本减少6.5~13元;包裹后的产品外观颜色一致均匀,使产品具有良好的外观形象。本发明方法适用于利用湿法磷酸生产磷酸二铵的企业。Using the method provided by the present invention, when the diammonium phosphate product is wrapped in the wrapping machine, because the temperature of the material is high, the dispersion of the wrapping oil is good, and the coating of the wrapping oil on the surface of the particles is thin, so that the consumption of the wrapping oil is higher than the original one. The consumption of the cooling and re-wrapping process is much smaller. The consumption of product wrapping oil colorant can be reduced from 4.5kg/t to 3.5-4.0kg/t, which can save the consumption of wrapping oil and reduce the production cost. It is 13,000 yuan per 1t of wrapping oil It is calculated that after using this process, the cost of product packaging is reduced by 6.5 to 13 yuan; the appearance and color of the packaged product are uniform and uniform, so that the product has a good appearance image. The method of the invention is suitable for enterprises that use wet-process phosphoric acid to produce diammonium phosphate.
[实施例][Example]
某厂磷肥车间的生产中,经磷酸氨化得到的磷酸二铵物料在用干燥机干燥后,控制出料温度为80℃±5℃,将该热物料通过斗提机或输送胶带送到包裹机进行包裹,包裹后的物料温度为75℃左右,再通过斗提机或输送胶带送到流化冷却床冷却机使之冷却到55℃以下,包装入库。In the production of a phosphate fertilizer workshop in a certain factory, after the diammonium phosphate material obtained by ammonification of phosphoric acid is dried with a dryer, the discharge temperature is controlled at 80°C±5°C, and the hot material is sent to the package through a bucket elevator or a conveyor belt The temperature of the packaged material is about 75°C, and then sent to the fluidized cooling bed cooler through the bucket elevator or conveyor belt to cool it to below 55°C, and then packed into the warehouse.
Claims (1)
- The packaging method of 1 one kinds of diammonium phosphate products, it is characterized in that after the diammonium phosphate material that the phosphoric acid ammonification obtains is used the drying machine drying, the drop temperature of strict control diammonium phosphate material is at 75~85 ℃, then thermal material is directly entered packing machine, wrap up operation, the material that comes out from packing machine and is sent into the fluidized-bed cooler and make it to be cooled to below 55 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100033010A CN1314627C (en) | 2005-11-29 | 2005-11-29 | A kind of wrapping and cooling method of diammonium phosphate product |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100033010A CN1314627C (en) | 2005-11-29 | 2005-11-29 | A kind of wrapping and cooling method of diammonium phosphate product |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1793062A CN1793062A (en) | 2006-06-28 |
| CN1314627C true CN1314627C (en) | 2007-05-09 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2005100033010A Expired - Fee Related CN1314627C (en) | 2005-11-29 | 2005-11-29 | A kind of wrapping and cooling method of diammonium phosphate product |
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| CN (1) | CN1314627C (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101747116B (en) * | 2009-12-11 | 2012-10-03 | 湖北富邦科技股份有限公司 | Method for controlling color of diammonium phosphate |
| CN102432387B (en) * | 2011-09-23 | 2013-04-24 | 瓮福(集团)有限责任公司 | Wrapping moisture-proof method for diammonium borophosphate-containing product |
| CN102503674B (en) * | 2011-10-25 | 2014-05-07 | 瓮福(集团)有限责任公司 | Method for coating diammonium phosphate product |
| CN103288525A (en) * | 2012-03-02 | 2013-09-11 | 宁夏鲁西化工化肥有限公司 | Sustained-release diammonium phosphate preparation method and system and sustained-release diammonium phosphate |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RO89058A2 (en) * | 1984-05-09 | 1986-04-30 | Institutul De Invatamint Superior,Ro | PROCESS FOR OBTAINING SLOW SOLUBILIZATION DIAMMONIUM PHOSPHATE-TYPE FERTILIZERS |
| CN1085201A (en) * | 1992-09-30 | 1994-04-13 | 梁宝珩 | Controlled-release laminate granular compound fertilizer and production method |
| CN1145059A (en) * | 1994-12-12 | 1997-03-12 | 宋美莹 | The controlled release matrix-type fertilizer and the process of preparation therefor |
| AU752230B2 (en) * | 1997-12-17 | 2002-09-12 | Schleicher, Dr Franz | Hydrophilic polymer coatings on hydrophobic or hydrophobized surfaces for biotechnological applications |
| CN1454878A (en) * | 2003-04-18 | 2003-11-12 | 重庆双赢化工集团有限公司 | Organic ammonium biphosphate fertilizer and production method thereof |
-
2005
- 2005-11-29 CN CNB2005100033010A patent/CN1314627C/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RO89058A2 (en) * | 1984-05-09 | 1986-04-30 | Institutul De Invatamint Superior,Ro | PROCESS FOR OBTAINING SLOW SOLUBILIZATION DIAMMONIUM PHOSPHATE-TYPE FERTILIZERS |
| CN1085201A (en) * | 1992-09-30 | 1994-04-13 | 梁宝珩 | Controlled-release laminate granular compound fertilizer and production method |
| CN1145059A (en) * | 1994-12-12 | 1997-03-12 | 宋美莹 | The controlled release matrix-type fertilizer and the process of preparation therefor |
| AU752230B2 (en) * | 1997-12-17 | 2002-09-12 | Schleicher, Dr Franz | Hydrophilic polymer coatings on hydrophobic or hydrophobized surfaces for biotechnological applications |
| CN1454878A (en) * | 2003-04-18 | 2003-11-12 | 重庆双赢化工集团有限公司 | Organic ammonium biphosphate fertilizer and production method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 磷铵厂"包裹工程"涉及应注意的问题 程重达,磷肥与复肥,第18卷第1期 2003 * |
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| Publication number | Publication date |
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| CN1793062A (en) | 2006-06-28 |
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Owner name: GUIZHOU KAILIN GROUP CO., LTD. Free format text: FORMER OWNER: GUIYANG ZHONGHUA KAILIN FERTILIZER CO., LTD. Effective date: 20150330 |
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Free format text: CORRECT: ADDRESS; FROM: 551109 GUIYANG, GUIZHOU PROVINCE TO: 550009 GUIYANG, GUIZHOU PROVINCE |
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Effective date of registration: 20150330 Address after: No. 237 Jinyang City Kailin Lake District Road 550009 Guizhou city of Guiyang Province Patentee after: Phosphorylcholine group limited-liability company is opened in Guizhou Address before: 551109 Guizhou County of Xifeng Province Town Village Patentee before: Zhonghuakai Phosphorous Chemical Fertilizer Co., Ltd., Guiyang |
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Granted publication date: 20070509 Termination date: 20181129 |