CN1309366C - Hairdressing agent with Chinese traditional medicine as main material and method for preparing the same - Google Patents

Abstract

A perm agent mainly made of traditional Chinese medicine raw materials and a preparation method thereof. The perm agent is composed of agent No. 1 and agent No. 2. The agent No. 1 uses cystine as a reducing agent and sodium bisulfite as an auxiliary reducing agent. The traditional Chinese medicine clove is used as the penetrating agent; the No. 2 dose uses hydrogen peroxide and Shegan as the combined oxidant, and clove is added as the penetrating agent. The two parts are prepared separately and used together. The invention adopts clove, a traditional Chinese medicine, as a penetrating agent to help cystine enter into the gaps of small hair flakes to enhance curling, and at the same time, sodium bisulfite is added as an auxiliary reducing agent to improve the curling ability of the perm. The perm agent of the present invention does not contain thioglycolic acid, is non-irritating, and has a sensitization rate of 0%. It is safe to use, and the curl degree of the perm is similar to that of chemical perm agents. A perm can last for about three months, and the hydrogen peroxide content is low. Therefore, it can greatly reduce the damage of perm to hair quality.

Description

Perm agent based on traditional Chinese medicine raw materials and preparation method thereof

technical field

The invention relates to a hair perm mainly made of traditional Chinese medicine raw materials and a preparation method thereof, in particular to a hair perm mainly made of cloves as a penetrating agent and a Chinese medicine raw material and a preparation method thereof, belonging to the technical field of the cosmetics industry.

Background technique

With the continuous improvement of people's material level and cultural level, people pay more and more attention to beauty and health as the premise while pursuing beauty. Therefore, the perm agent based on Chinese medicine raw materials will be welcomed by consumers.

However, the vast majority of perm agents used at present use thioglycolic acid chemicals, and people who often contact thioglycolic acid solutions may experience erythrocytes, leukopenia, headache, malaise, gastrointestinal dysfunction, urinary protein, skin allergies, etc.

For health and safety reasons, Japan took the lead in extracting cysteine from natural hair and using cysteine instead of thioglycolic acid to prepare perms, but cysteine perms have two main disadvantages. , Cysteine will oxidize to degrade the product and affect hair dyeing. Direct contact with the user's hands will cause cracks. The second is that due to the oxidation of cysteine to degrade the product, the reduction efficiency is low and the curling ability is poor. In 1981, the homologues and derivatives of cysteine began to be produced by chemical synthesis. Although the stability of the product was improved and the curling ability was improved, it was no longer a perm agent based on natural raw materials in the original sense, but still a chemical Perm agent.

Chinese invention patent "Non-oxidative permanent traditional Chinese medicine black hair dye with clove as penetrating agent" (Patent No.: 02136428.1) uses clove penetrating agent in natural hair dye, which can not damage the hair quality and get a good hair dyeing effect. But do not see at present and adopt clove to be the method report of penetrating agent in the perm agent that takes Chinese medicine as main raw material.

Contents of the invention

The purpose of the present invention is to address the deficiencies in the prior art, to provide a hair perm based on traditional Chinese medicine raw materials and its preparation method, to prepare a perm from natural raw materials, which has a curling effect similar to that of chemical perms, and is safe to use. Toxin, can reduce the damage to hair quality.

In order to realize this object, the perm agent of the present invention is made up of No. 1 agent and No. 2 agent two parts, and No. 1 agent adopts cystine as reducing agent, adds sodium bisulfite as auxiliary reducing agent, and adopts Chinese medicine clove as Penetrant; Agent No. 2 uses hydrogen peroxide and Shegan as the combined oxidant, and adds cloves as the penetrant. The two parts are prepared separately and used together.

Concrete content of the present invention is:

The perm agent based on traditional Chinese medicine raw materials of the present invention includes No. 1 agent and No. 2 agent.

In the No. 1 dose, each component and its mass percentage are:

The reducing agent is cystine, the mass percentage is 3-12%, preferably 3-10%;

The auxiliary reducing agent is sodium bisulfite, and the mass percentage is 3-5%;

Traditional Chinese medicine penetrating agent clove, the mass percentage is 1-10%;

The alkalizing agent is ammonium hydroxide and monoethanolamine, and its consumption keeps the pH value of No. 1 agent at 9-9.8;

The thickener is bletilla striata, the best mass percentage is 3-5%;

The chelating agent is disodium ethylenediamine tetraacetate, the mass percentage is 0.2%; the rest is deionized water.

In the No. 2 dose, each component and its mass percentage are:

Combined oxidizing agent: hydrogen peroxide (calculated by 100%), the mass percentage is 1-2%, shot dry, the mass percentage is 1-15%;

Clove penetrating agent, the mass percentage is 1-10%;

Thickener glyceryl monostearate, the mass percentage is 4-8%;

Stabilizer 8-hydroxyquinoline sulfate, 0.1% by mass;

Chelating agent edetate disodium, the mass percentage is 0.2%;

Acid/buffer phosphoric acid, the dosage is to keep the pH value of No. 2 agent at 2.5-4; the rest is deionized water.

The concrete preparation method of perm agent of the present invention is as follows:

Perm Agent No. 1: Mix deionized water with cloves, bletilla striata, cystine, sodium bisulfite, monoethanolamine, and disodium edetate, heat to 70°C, cool to room temperature, and then hydrogenate ammonium mix. Inspection, filling.

Perm agent No. 2: add 60% deionized water to container No. 1, add glyceryl monostearate, shegan, cloves, and disodium edetate, heat to 70°C, and keep warm for 15 minutes , cooled to 40°C. In No. 2 container, add the remaining 40% deionized water, heat to 40°C, add 8-hydroxyquinoline sulfate, stir until completely dissolved, slowly add to No. 1 container, cool to 30°C, then Add hydrogen peroxide and phosphoric acid. Stirring, testing, filling.

Practical application: Shampoo and blow dry, curl the bar, apply No. 1 agent, put on a shower cap, steam at 50°C for 30 minutes, cool for 5 minutes, rinse, dry, apply No. 2 agent at room temperature for fifteen minutes, remove the bar, Shampoo, blow style.

The present invention aims at the problem that natural cysteine is easily oxidized to cause product degradation. Cystine is selected as the main raw material of perm agent, and cystine is relatively large in molecular weight compared to cysteine, so it is difficult to enter the gap between hair flakes. For the problem that the curling ability is still poor, add the traditional Chinese medicine clove as a penetrating agent to help cystine enter the gap between the small hair flakes and enhance the curling degree. At the same time, add sodium bisulfite as an auxiliary reducing agent to improve the curling ability of the perm. The perm agent of the present invention does not contain thioglycolic acid, is non-irritating, has a sensitization rate of 0%, is safe to use, has a curl degree similar to that of chemical perm agents, and can last about three months for one perm. The hydrogen peroxide content is low, so it can minimize the damage of perm to hair quality.

Detailed ways

The technical solution of the present invention will be further described below through specific examples.

Example 1

The composition and mass percent of No. 1 agent: clove 10%, bletilla striata 5%, cystine 3%, sodium bisulfite 5%, monoethanolamine (99.0%) 4%, ammonium hydroxide (28%) 2%, ethyl alcohol Disodium diamine tetraacetate 0.2%, add deionized water to 100%.

The composition and mass percentage of the No. 2 agent: 15% of Shegan, 10% of clove, 1% of hydrogen peroxide (according to 100%), 8% of glycerol monostearate, 0.5% of phosphoric acid, 0.2% of disodium edetate %, 8-hydroxyquinoline sulfate 0.1%, deionized water added to 100%.

The concrete preparation method of perm agent of the present invention is as follows:

Perm Agent No. 1: Mix deionized water with cloves, bletilla striata, cystine, sodium bisulfite, monoethanolamine, and disodium edetate, heat to 70°C, cool to room temperature, and then hydrogenate ammonium mix. Inspection, filling.

Perm agent No. 2: add 60% deionized water to container No. 1, add glyceryl monostearate, shegan, cloves, and disodium edetate, heat to 70°C, and keep warm for 15 minutes , cooled to 40°C. In No. 2 container, add the remaining 40% deionized water, heat to 40°C, add 8-hydroxyquinoline sulfate, stir until completely dissolved, slowly add to No. 1 container, cool to 30°C, then Add hydrogen peroxide and phosphoric acid. Stirring, testing, filling.

In practical application, shampoo and dry, roll up the bar, apply No. 1 agent, put on a shower cap, steam at 50°C for 30 minutes, cool for 5 minutes, rinse, dry, apply No. 2 agent, keep at room temperature for 15 minutes, remove the bar , wash hair, blow style.

Example 2

The composition and mass percent of No. 1 agent: clove 5%, bletilla striata 4%, cystine 6%, sodium bisulfite 4%, monoethanolamine (99.0%) 3%, NH OH (28%) 2.5%, _ethyl alcohol Disodium diamine tetraacetate 0.2%, add deionized water to 100%.

The composition and mass percentage of No. 2 agent: 1. Shegan 10%, clove 5%, hydrogen peroxide (according to 100%) 1.5%, glyceryl monostearate 6%, phosphoric acid 0.5%, ethylenediaminetetraacetic acid diacetate Sodium 0.2%, 8-hydroxyquinoline sulfate 0.1%, deionized water to 100%.

The preparation method and usage method are the same as in Example 1.

Example 3

The composition and mass percent of No. 1 agent: clove 1%, bletilla striata 3%, cystine 10%, sodium bisulfite 3%, monoethanolamine (99.0%) 2%, NH ₄ OH (28%) 3%, ethyl alcohol Disodium diamine tetraacetate 0.2%, add deionized water to 100%.

The composition and mass percentage of No. 2 agent: Shegan 1%, clove 1%, hydrogen peroxide (according to 100%) 2%, glycerol monostearate 4%, phosphoric acid 0.5%, edetate disodium 0.2 %, 8-hydroxyquinoline sulfate 0.1%, deionized water added to 100%.

The preparation method and usage method are the same as in Example 1.

The curls of the above three embodiments can be kept for about three months after perming. And, since the hydrogen peroxide content is low, it is less damaging to hair. And, because it does not contain thioglycolic acid, it is safe to use. After testing, the perm agent has no irritation, and the sensitization rate is 0%.

Claims (2)

1, a kind of agent for permanent hair waving based on raw material of Chinese medicine, form by No. 1 agent and No. 2 agent, it is characterized in that No. 1 agent made by described mass percent by following component: cystine 3-12%, sodium sulfite 3-5%, Flos Caryophylli 1-10%, Pseudobulbus Bletillae (Rhizoma Bletillae) 3-5%, disodiumedetate 0.2%, ammonium hydroxide and monoethanolamine, addition make the pH value of No. 1 agent keep 9-9.8, and all the other are deionized water; No. 2 agent are made by described mass percent by following component: the hydrogen peroxide 1-2% by 100%, Rhizoma Belamcandae 1-15%, Flos Caryophylli 1-10%, glyceryl monostearate 4-8%, oxine sulfate 0.1%, disodiumedetate 0.2%, phosphoric acid, addition makes the pH value of No. 2 agent keep 2.5-4, and all the other are deionized water.

2, a kind of preparation method of claim 1 based on the agent for permanent hair waving of raw material of Chinese medicine, when it is characterized in that preparing No. 1 agent, deionized water is mixed with Flos Caryophylli, the Pseudobulbus Bletillae (Rhizoma Bletillae), cystine, sodium sulfite, monoethanolamine, disodiumedetate, heat to 70 ℃, be cooled to room temperature, the repeated hydrogenation amine-oxides mixes, and gets No. 1 agent after the check fill; When preparing No. 2 agent, in container, add 60% deionized water, add glyceryl monostearate, Rhizoma Belamcandae, Flos Caryophylli, disodiumedetate again and mix, heat, be incubated 15 minutes, be cooled to 40 ℃ to 70 ℃; In No. two containers, add remaining 40% deionized water, be heated to 40 ℃, oxine sulfate is added, be stirred to fully dissolving, slowly add in container, be cooled to 30 ℃, and then add hydrogen peroxide, phosphoric acid, and stir, get No. 2 agent after the check fill.