CN1303661A - Hibiscus syriacus - Google Patents
Hibiscus syriacus Download PDFInfo
- Publication number
- CN1303661A CN1303661A CN 00113205 CN00113205A CN1303661A CN 1303661 A CN1303661 A CN 1303661A CN 00113205 CN00113205 CN 00113205 CN 00113205 A CN00113205 A CN 00113205A CN 1303661 A CN1303661 A CN 1303661A
- Authority
- CN
- China
- Prior art keywords
- folium hibisci
- hibiscus syriacus
- powder
- protein hydrolyzate
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 244000130592 Hibiscus syriacus Species 0.000 title claims abstract description 19
- 235000018081 Hibiscus syriacus Nutrition 0.000 title claims abstract description 17
- 239000003531 protein hydrolysate Substances 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 10
- 230000007062 hydrolysis Effects 0.000 claims abstract description 9
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims abstract description 9
- 239000007788 liquid Substances 0.000 claims abstract description 6
- FPVVYTCTZKCSOJ-UHFFFAOYSA-N Ethylene glycol distearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCOC(=O)CCCCCCCCCCCCCCCCC FPVVYTCTZKCSOJ-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000004166 Lanolin Substances 0.000 claims abstract description 5
- BTBJBAZGXNKLQC-UHFFFAOYSA-N ammonium lauryl sulfate Chemical compound [NH4+].CCCCCCCCCCCCOS([O-])(=O)=O BTBJBAZGXNKLQC-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229940063953 ammonium lauryl sulfate Drugs 0.000 claims abstract description 5
- 229940039717 lanolin Drugs 0.000 claims abstract description 5
- 235000019388 lanolin Nutrition 0.000 claims abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 3
- 238000002360 preparation method Methods 0.000 claims abstract description 3
- 238000010298 pulverizing process Methods 0.000 claims abstract description 3
- 238000005516 engineering process Methods 0.000 claims description 5
- 108091005658 Basic proteases Proteins 0.000 claims description 4
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 4
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 4
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 4
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 claims description 4
- 229960001617 ethyl hydroxybenzoate Drugs 0.000 claims description 4
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 claims description 4
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 claims description 4
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 230000008569 process Effects 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 238000007796 conventional method Methods 0.000 claims description 2
- 108090000765 processed proteins & peptides Proteins 0.000 abstract description 7
- 239000002453 shampoo Substances 0.000 abstract description 7
- 235000015097 nutrients Nutrition 0.000 abstract description 3
- 108010016626 Dipeptides Proteins 0.000 abstract description 2
- 230000003301 hydrolyzing effect Effects 0.000 abstract description 2
- 229920001184 polypeptide Polymers 0.000 abstract description 2
- 102000004196 processed proteins & peptides Human genes 0.000 abstract description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 abstract 1
- 101710138460 Leaf protein Proteins 0.000 abstract 1
- KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 abstract 1
- 108010009736 Protein Hydrolysates Proteins 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 108010051873 alkaline protease Proteins 0.000 abstract 1
- 229960003237 betaine Drugs 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 230000000249 desinfective effect Effects 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 229940100608 glycol distearate Drugs 0.000 abstract 1
- 229920001296 polysiloxane Polymers 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 235000016709 nutrition Nutrition 0.000 description 9
- 230000035764 nutrition Effects 0.000 description 9
- 239000004480 active ingredient Substances 0.000 description 4
- 239000002537 cosmetic Substances 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 230000002421 anti-septic effect Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 108010082495 Dietary Plant Proteins Proteins 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 108091005804 Peptidases Proteins 0.000 description 2
- 239000004365 Protease Substances 0.000 description 2
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 2
- 108090000787 Subtilisin Proteins 0.000 description 2
- 235000001014 amino acid Nutrition 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 238000005202 decontamination Methods 0.000 description 2
- 230000003588 decontaminative effect Effects 0.000 description 2
- 230000008676 import Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- QRYRORQUOLYVBU-VBKZILBWSA-N Carnosic acid Natural products CC([C@@H]1CC2)(C)CCC[C@]1(C(O)=O)C1=C2C=C(C(C)C)C(O)=C1O QRYRORQUOLYVBU-VBKZILBWSA-N 0.000 description 1
- 108010087806 Carnosine Proteins 0.000 description 1
- 208000001840 Dandruff Diseases 0.000 description 1
- 108090000371 Esterases Proteins 0.000 description 1
- 241000533849 Gleditsia Species 0.000 description 1
- 241000218033 Hibiscus Species 0.000 description 1
- 235000005206 Hibiscus Nutrition 0.000 description 1
- 235000007185 Hibiscus lunariifolius Nutrition 0.000 description 1
- GDBQQVLCIARPGH-UHFFFAOYSA-N Leupeptin Natural products CC(C)CC(NC(C)=O)C(=O)NC(CC(C)C)C(=O)NC(C=O)CCCN=C(N)N GDBQQVLCIARPGH-UHFFFAOYSA-N 0.000 description 1
- 241000243684 Lumbricus Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- CQOVPNPJLQNMDC-UHFFFAOYSA-N N-beta-alanyl-L-histidine Natural products NCCC(=O)NC(C(O)=O)CC1=CN=CN1 CQOVPNPJLQNMDC-UHFFFAOYSA-N 0.000 description 1
- 241001597008 Nomeidae Species 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 102220470372 Thymosin beta-10_K12A_mutation Human genes 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 230000006229 amino acid addition Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- CQOVPNPJLQNMDC-ZETCQYMHSA-N carnosine Chemical compound [NH3+]CCC(=O)N[C@H](C([O-])=O)CC1=CNC=N1 CQOVPNPJLQNMDC-ZETCQYMHSA-N 0.000 description 1
- 229940044199 carnosine Drugs 0.000 description 1
- 230000002354 daily effect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- RWSXRVCMGQZWBV-WDSKDSINSA-N glutathione Chemical compound OC(=O)[C@@H](N)CCC(=O)N[C@@H](CS)C(=O)NCC(O)=O RWSXRVCMGQZWBV-WDSKDSINSA-N 0.000 description 1
- 229960003180 glutathione Drugs 0.000 description 1
- 235000003969 glutathione Nutrition 0.000 description 1
- UYTPUPDQBNUYGX-UHFFFAOYSA-N guanine Chemical compound O=C1NC(N)=NC2=C1N=CN2 UYTPUPDQBNUYGX-UHFFFAOYSA-N 0.000 description 1
- 230000003779 hair growth Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 230000000622 irritating effect Effects 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- GDBQQVLCIARPGH-ULQDDVLXSA-N leupeptin Chemical compound CC(C)C[C@H](NC(C)=O)C(=O)N[C@@H](CC(C)C)C(=O)N[C@H](C=O)CCCN=C(N)N GDBQQVLCIARPGH-ULQDDVLXSA-N 0.000 description 1
- 108010052968 leupeptin Proteins 0.000 description 1
- 230000000474 nursing effect Effects 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 210000000582 semen Anatomy 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
A preparation method of shrubalthea leaf liquid shampoo includes the following steps: disinfecting shrubalthea leaf, drying and pulverizing to 100 meshes: placing 80%-90% of water, 8%-18% of shrubalthea leaf powder and 0.5%-2% of alkaline proteinase in a hydrolysis tank to make hydrolysis, controlled temp. is 45-50 deg.C, pH valus is 6-10, hydrolyzing time is 22-26 hr, press-filtering and separating to obtain shrubalthea leaf protein hydrolysate; using 8%-10% of the said hydrolysate, 12%-15% of ammonium alcohol ether sulfate, 8%-10% of ammonium lauryl sulfate, 0.8%-1% of aectylated lanolin, 4%-5% of dedecyl betaine, 15%-12% methyl-silicone, 0.6-1% of glycol distearate, and proservative and essence each 0.1%-0.2% to compound them into invented finished product containing rich nutrient components of dipeptide and polypeptide which are easy to be absorbed by the skin of human body.
Description
The present invention relates to the Folium Hibisci protein hydrolyzate is the shampoo of main active ingredient.
Prior art is extracted protein, aminoacid and derivant thereof and is added in the cosmetics or Application in Food from animal, plant, early reported in literature is arranged both at home and abroad, and commercial large in the variety.For example the Lumbricus lixiviating solution is used for superior cosmetics, extracts aminoacid addition to the cosmetics or the like from Semen sojae atricolor.In recent years, the ONI Fructus Gleditsia shampoo that finds a good market has appearred again in the daily use chemicals industry, and it also is the case history that the plant nutrient active ingredient is used for cosmetics of everyday use.
Plant Hibiscus syriacus L. aboundresources, widely distributed, especially see in south more.Hibiscus syriacus L. is studied, develops, and the active ingredient that makes full use of it is a useful thing for human service.
The objective of the invention is, develop a kind of hibiscus syriacus, it is main active ingredient with the Folium Hibisci protein hydrolyzate that is rich in needed by human body multiple nutrients composition that obtains with special process, and use and to specialize in the suitable prescription that draws, for people provide nutritious and are easy to by skin absorbs, the effective natural nutrition type shampoo of hair-washing hair-care.Exploitation of the present invention, application also provide the outlet of a deep processing and utilization for resourceful Folium Hibisci.
Technical scheme of the present invention is that raw material components of described hibiscus syriacus (percentage by weight) and reparation technology are:
(1) with the bright leaf remove impurity of Hibiscus syriacus L., sterilize and be dried to water content less than 3% (weight ratio), obtaining granularity through pulverizing is 100 purpose Folium Hibisci powder;
Produce the Folium Hibisci protein hydrolyzate by following proportioning and process conditions by the Folium Hibisci powder:
Water 80%-90%,
Folium Hibisci powder 8%-18%,
Alkaline protease 0.5%-2%,
The control hydrolysis temperature is 45-50 ℃, liquid pH value scope 6-10, hydrolysis time 22-26 hour;
Through conventional filter pressing separating technology slagging-off, obtain the Folium Hibisci protein hydrolyzate again;
(2) following component is obtained hibiscus syriacus with the conventional method preparation:
Folium Hibisci protein hydrolyzate 8%-10%,
Alcohol ether ammonium sulfate 12%-15%,
Ammonium lauryl sulfate 8%-10%,
Acetylated lanolin 0.8%-1%,
Empgen BB 4%-5%,
Polymethyl siloxane 1.5%-2%,
Ethylene Glycol Distearate 0.6%-1%,
Ethylparaben 0.1%-0.2%,
Essence 0.1%-0.2%,
Water 60%-65%.
The present invention is a raw material just to plant Hibiscus syriacus L. (Hibiscus syriaus L.), and hydrolysis can be adopted subtilisin, the products such as Carlsberg, esterase of homemade 2709 protease or import with alkaline protease.Check and analysis show, use the Folium Hibisci protein hydrolyzate that technology of the present invention is produced, and the washing decontamination is not only arranged, and also are rich in needed by human body and easily by the peptide class nutrition of skin absorbs, comprise polypeptide compositions such as dipeptides and carnosine, glutathion, leupeptin.According to needed by human body several amino acids content in the Folium Hibisci dry powder is 13.4% measuring and calculating, and described peptide class content is more than 10%.
There are some researches show, vegetable protein is difficult to be absorbed by human body skin because of molecular weight is excessive, can play a role though it adds in various shampoos, the skincare product, and practical efficiency is very low, not only cause the wasting of resources, its nutrition hair care skin protection, health-care effect also have much room for improvement.The present invention has effectively realized vegetable protein in the Folium Hibisci being hydrolyzed and obtaining molecular weight described multiple peptide class nutrition less, that easily absorbed by human body skin, its molecular weight generally can be controlled in below 4000, skin there is moist moisture-keeping function, hair there are relieving itching and removing dandruff and nutrition nursing role, can promote natural on-off cycles of hair growth and melanic formation, can fully be absorbed by skin, this be prior art so far not opinion determine, also be one of outstanding feature of the present invention.
The present invention optimizes and has chosen described other related component and proportioning also through further investigation and repetition test, and these components do not influence the activity of peptide class nutrition in the liquid, also hair washing, hair care is played due effect; As used pure ether ammonium sulfate (AESA) and ammonium lauryl sulfate (K12A) can foam decontamination and action temperature and, minimum to skin irritation, acetylated lanolin and empgen BB (BS-12) play skin care respectively and reduce skin irritant effect, and polymethyl siloxane (estersil) and Ethylene Glycol Distearate (pearl essence) then play softness and interception respectively; Water is solvent, and ethylparaben (nipalgin) is an antiseptic (also can adopt other corresponding antiseptic); The suitable essence of essence can be selected for use commercially available " Japanese Pantene essence " or " U.S.'s Pantene essence " or other prior art, it makes product give out pleasant fragrance.
As known from the above, the present invention is a kind of hibiscus syriacus, the Folium Hibisci protein hydrolyzate that it makes with special process is rich in needed by human body and easily by the nutritions such as multiple peptide of skin absorbs, resulting shampoo hair washing, hair care and Nutrition are remarkable, be a kind of natural nutrition type shampoo, simultaneously for developing, utilizing the Hibiscus syriacus L. resource to open up approach.
Embodiment: select for use the bright leaf of Hibiscus syriacus L. after the remove impurity under ultra violet lamp, to sterilize and be dried to water content less than 3% (weight ratio), with Universalpulverizer described leaf is crushed to 100 orders then with red line vibrosieve far away;
With weight ratio is that 14% Folium Hibisci powder is thrown to the water that 85% weight ratio is arranged (container is a hydrolytic tank), and the interpolation weight ratio is 1% alkaline protease (homemade 2709 protease or import subtilisin), the control hydrolysis temperature is 45 ℃, the liquid pH value is 8, hydrolysis time 24 hours, become liquid to separate (removing slag) to obtain the Folium Hibisci protein hydrolyzate through filter pressing; Getting Folium Hibisci protein hydrolyzate 10%, pure ether ammonium sulfate 12%, ammonium lauryl sulfate 9%, acetylated lanolin 1%, empgen BB 5% is dissolved in the 50-70 ℃ of deionized water; add polymethyl siloxane 1.8%, Ethylene Glycol Distearate 1% and agitation as appropriate then, be cooled to about 35 ℃; add antiseptic ethylparaben 0.1% and essence (Japanese Pantene spice) 1% and be cooled to room temperature, become finished product through fill after the assay was approved.
Claims (1)
1, a kind of hibiscus syriacus, its raw material components (percentage by weight) and reparation technology are:
(1) with the bright leaf remove impurity of Hibiscus syriacus L., sterilize and be dried to water content less than 3% (weight ratio), obtaining granularity through pulverizing is 100 purpose Folium Hibisci powder;
Produce the Folium Hibisci protein hydrolyzate by following proportioning and process conditions by the Folium Hibisci powder:
Water 80%-90%,
Folium Hibisci powder 8%-18%,
Alkaline protease 0.5%-2%,
The control hydrolysis temperature is 45-50 ℃, liquid pH value scope 6-10, hydrolysis time 22-26 hour;
Through conventional filter pressing separating technology slagging-off, obtain the Folium Hibisci protein hydrolyzate again;
(2) following component is obtained hibiscus syriacus with the conventional method preparation:
Folium Hibisci protein hydrolyzate 8%-10%,
Alcohol ether ammonium sulfate 12%-15%,
Ammonium lauryl sulfate 8%-10%,
Acetylated lanolin 0.8%-1%,
Empgen BB 4%-5%,
Polymethyl siloxane 1.5%-2%,
Ethylene Glycol Distearate 0.6%-1%,
Ethylparaben 0.1%-0.2%,
Essence 0.1%-0.2%,
Water 60%-65%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 00113205 CN1303661A (en) | 2000-01-07 | 2000-01-07 | Hibiscus syriacus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 00113205 CN1303661A (en) | 2000-01-07 | 2000-01-07 | Hibiscus syriacus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1303661A true CN1303661A (en) | 2001-07-18 |
Family
ID=4583013
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 00113205 Pending CN1303661A (en) | 2000-01-07 | 2000-01-07 | Hibiscus syriacus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1303661A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2246036A1 (en) * | 2009-04-27 | 2010-11-03 | KPSS-Kao Professional Salon Services GmbH | Aqueous cleansing composition |
| WO2018021848A1 (en) * | 2016-07-29 | 2018-02-01 | 주식회사 티젠 농업회사법인 | Composition for preventing hair loss or stimulating hair growth, containing hibiscus extract |
| CN108434072A (en) * | 2018-04-24 | 2018-08-24 | 湖南叶姿国际植物化妆品有限公司 | A kind of pure natural rose of Sharon shampoo of anti-dandruff and itching-relieving and preparation method thereof |
-
2000
- 2000-01-07 CN CN 00113205 patent/CN1303661A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2246036A1 (en) * | 2009-04-27 | 2010-11-03 | KPSS-Kao Professional Salon Services GmbH | Aqueous cleansing composition |
| WO2010124818A3 (en) * | 2009-04-27 | 2012-03-15 | Kpss-Kao Professional Salon Services Gmbh | Aqueous cleansing composition |
| WO2018021848A1 (en) * | 2016-07-29 | 2018-02-01 | 주식회사 티젠 농업회사법인 | Composition for preventing hair loss or stimulating hair growth, containing hibiscus extract |
| CN108434072A (en) * | 2018-04-24 | 2018-08-24 | 湖南叶姿国际植物化妆品有限公司 | A kind of pure natural rose of Sharon shampoo of anti-dandruff and itching-relieving and preparation method thereof |
| CN108434072B (en) * | 2018-04-24 | 2020-12-01 | 湖南叶姿国际植物化妆品有限公司 | Pure natural hibiscus shampoo capable of removing dandruff and relieving itching and preparation method thereof |
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| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |