CN1351985A - Process for producing veratryl alcohol and its use in food, drink and grape wind - Google Patents
Process for producing veratryl alcohol and its use in food, drink and grape wind Download PDFInfo
- Publication number
- CN1351985A CN1351985A CN 00113971 CN00113971A CN1351985A CN 1351985 A CN1351985 A CN 1351985A CN 00113971 CN00113971 CN 00113971 CN 00113971 A CN00113971 A CN 00113971A CN 1351985 A CN1351985 A CN 1351985A
- Authority
- CN
- China
- Prior art keywords
- resveratrol
- trans
- food
- grape
- drink
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000009754 Vitis X bourquina Nutrition 0.000 title claims abstract description 21
- 235000012333 Vitis X labruscana Nutrition 0.000 title claims abstract description 21
- 235000014787 Vitis vinifera Nutrition 0.000 title claims abstract description 21
- 235000013305 food Nutrition 0.000 title claims abstract description 8
- 238000000034 method Methods 0.000 title claims description 7
- OEGPRYNGFWGMMV-UHFFFAOYSA-N (3,4-dimethoxyphenyl)methanol Chemical compound COC1=CC=C(CO)C=C1OC OEGPRYNGFWGMMV-UHFFFAOYSA-N 0.000 title description 4
- 240000006365 Vitis vinifera Species 0.000 title 1
- LUKBXSAWLPMMSZ-OWOJBTEDSA-N Trans-resveratrol Chemical compound C1=CC(O)=CC=C1\C=C\C1=CC(O)=CC(O)=C1 LUKBXSAWLPMMSZ-OWOJBTEDSA-N 0.000 claims abstract description 56
- 241000219095 Vitis Species 0.000 claims abstract description 32
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 235000014101 wine Nutrition 0.000 claims abstract description 13
- 229940016667 resveratrol Drugs 0.000 claims abstract description 12
- QNVSXXGDAPORNA-UHFFFAOYSA-N Resveratrol Natural products OC1=CC=CC(C=CC=2C=C(O)C(O)=CC=2)=C1 QNVSXXGDAPORNA-UHFFFAOYSA-N 0.000 claims abstract description 11
- 235000021283 resveratrol Nutrition 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 7
- 238000004519 manufacturing process Methods 0.000 claims abstract description 7
- 239000002775 capsule Substances 0.000 claims abstract description 4
- 235000018991 trans-resveratrol Nutrition 0.000 claims description 45
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 15
- 235000009392 Vitis Nutrition 0.000 claims description 12
- 235000019441 ethanol Nutrition 0.000 claims description 9
- 235000015203 fruit juice Nutrition 0.000 claims description 7
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 6
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 6
- 235000013376 functional food Nutrition 0.000 claims description 4
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 3
- 239000012141 concentrate Substances 0.000 claims description 3
- 230000008030 elimination Effects 0.000 claims description 3
- 238000003379 elimination reaction Methods 0.000 claims description 3
- 239000000469 ethanolic extract Substances 0.000 claims description 3
- 239000012259 ether extract Substances 0.000 claims description 3
- 238000013467 fragmentation Methods 0.000 claims description 3
- 238000006062 fragmentation reaction Methods 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- 238000001953 recrystallisation Methods 0.000 claims description 3
- 238000010898 silica gel chromatography Methods 0.000 claims description 3
- 229940095064 tartrate Drugs 0.000 claims description 3
- 235000020510 functional beverage Nutrition 0.000 claims description 2
- 206010028980 Neoplasm Diseases 0.000 abstract description 7
- 201000011510 cancer Diseases 0.000 abstract description 7
- 239000002994 raw material Substances 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 2
- 230000000747 cardiac effect Effects 0.000 abstract 1
- 201000010099 disease Diseases 0.000 abstract 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract 1
- 201000005577 familial hyperlipidemia Diseases 0.000 abstract 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 abstract 1
- 208000019553 vascular disease Diseases 0.000 abstract 1
- 239000012467 final product Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 3
- 208000024172 Cardiovascular disease Diseases 0.000 description 2
- 235000013361 beverage Nutrition 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000000069 prophylactic effect Effects 0.000 description 2
- 235000020095 red wine Nutrition 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- GHOKWGTUZJEAQD-UHFFFAOYSA-N Chick antidermatitis factor Natural products OCC(C)(C)C(O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-UHFFFAOYSA-N 0.000 description 1
- 208000031226 Hyperlipidaemia Diseases 0.000 description 1
- 244000153955 Reynoutria sachalinensis Species 0.000 description 1
- 235000003202 Reynoutria sachalinensis Nutrition 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 208000007536 Thrombosis Diseases 0.000 description 1
- 241000489520 Veratrum album Species 0.000 description 1
- 229930003571 Vitamin B5 Natural products 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- FAPWYRCQGJNNSJ-UBKPKTQASA-L calcium D-pantothenic acid Chemical compound [Ca+2].OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O.OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O FAPWYRCQGJNNSJ-UBKPKTQASA-L 0.000 description 1
- NEEHYRZPVYRGPP-IYEMJOQQSA-L calcium gluconate Chemical compound [Ca+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O NEEHYRZPVYRGPP-IYEMJOQQSA-L 0.000 description 1
- 229960002079 calcium pantothenate Drugs 0.000 description 1
- 208000015606 cardiovascular system disease Diseases 0.000 description 1
- 208000026106 cerebrovascular disease Diseases 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000002113 chemopreventative effect Effects 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 238000005304 joining Methods 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000009492 vitamin B5 Nutrition 0.000 description 1
- 239000011675 vitamin B5 Substances 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 229940104757 vitamin E 50 mg Drugs 0.000 description 1
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
The present invention relates to a production process of resverated and its application to food, drink and grape wine. Resveratrol is a kind of cancer preventer and has obvious effect of preventing cancer, cardiac vascular disease, hyperlipemia and other diseases. The present invention produces resveratrol by using grape peel with high-resveratrol content as raw material and through depuration, rinsing, crushing, and 95 % ethanol extractino to produce grape peel resveratrol. Resveratrol may be used in producing resveratrol juice, resveratrol capsule, oral resveratrol liquid and resveratrol wine.
Description
The present invention relates to a kind of production technique of trans-resveratrol and the utilization in food, drink and grape wind thereof.
Modern medicine study proves, trans-resveratrol is a kind of cancer chemoprevention agent, to cancer initial, promote, the development three phases all plays prophylactic effect, can suppress simultaneously interior triglyceride of human body and total cholesterol in the accumulation of liver and the formation of inhibition thrombus, cancer, cardiovascular system diseases are had special prophylactic effect.(No. 40, No. 1 the-the 16 volume of the Chinese invention patent and the utility model patent communique first roll) finds two pieces of documents by retrieval; it is all different with the present invention with " a kind of technology of extracting trans-resveratrol from the Chinese medicine giant knotweed; application number 99115156, notification number 1251361 " its product, technology and scope of patent protection promptly " to utilize Pericarpium Vitis viniferae to make the method for vinegar; application number 89104214; notification number 1039841 ".
The object of the present invention is to provide a kind of is that raw material (it is the highest to contain trans-resveratrol, is 50-100mg/g) is produced the technology of trans-resveratrol and used trans-resveratrol to produce trans-resveratrol functional food beverage, method vinous with the Pericarpium Vitis viniferae.
The technology that among the present invention with the Pericarpium Vitis viniferae is the raw material production trans-resveratrol is: utilize Pericarpium Vitis viniferae, through sorting and impurity elimination, rinsing, fragmentation, 95% extraction using alcohol, ethanol extract, tartrate dissolving, extracted with diethyl ether acid solution, ether extraction liquid concentrating under reduced pressure, ether extract, silica gel column chromatography, collection acetone: chloroform elutriant (1: 1), elutriant concentrate, ethyl alcohol recrystallization, produce the Pericarpium Vitis viniferae trans-resveratrol.
Among the present invention the utilization trans-resveratrol produce functional food, beverage, raw material weight vinous when production technique be:
One, trans-resveratrol fruit juice.Trans-resveratrol: fruit juice=5-100mg: 1000ml is with white hellebore
Alcohol is dissolved in the fruit juice and gets final product.
Two, trans-resveratrol capsule.Trans-resveratrol: auxiliary material=5-50mg: 495-450mg is through joining
Expect, mix, granulate, dry, pulverize, incapsulate and get final product.
Three, oral resveratrol liquid.Trans-resveratrol: red wine=50-1000mg: 1000ml,
Take by weighing trans-resveratrol by prescription and be dissolved in a small amount of edible ethanol, again with the grape wine allotment,
After embedding, sterilization, pack again.
Four, trans-resveratrol grape wine.Trans-resveratrol: grape wine=5-100mg: 1000ml will be white
Veratryl alcohol is dissolved in the grape wine and gets final product.
The present invention utilizes the trans-resveratrol high-content of Pericarpium Vitis viniferae to extract trans-resveratrol, utilize the anti-cancer and kill cancer action of trans-resveratrol simultaneously, produce trans-resveratrol functional food, beverage and grape wine, have effects such as preventing cancer, hyperlipidemia and cardiovascular and cerebrovascular diseases, can produce very high social benefit and economic benefit, be beneficial to popularization.
With embodiment the present invention is described in further detail below:
Embodiment one:
The technology that among the present invention with the Pericarpium Vitis viniferae is the raw material production trans-resveratrol is: utilize Pericarpium Vitis viniferae, through sorting and impurity elimination, rinsing, fragmentation, 95% extraction using alcohol, ethanol extract, tartrate dissolving, extracted with diethyl ether acid solution, ether extraction liquid concentrating under reduced pressure, ether extract, silica gel column chromatography, collection acetone: chloroform elutriant (1: 1), elutriant concentrate, ethyl alcohol recrystallization, produce the Pericarpium Vitis viniferae trans-resveratrol.
Embodiment two:
Trans-resveratrol fruit juice.Trans-resveratrol: fruit juice=100mg: 1000ml is dissolved in trans-resveratrol in the fruit juice and gets final product.
Embodiment three:
The trans-resveratrol capsule.Trans-resveratrol: auxiliary material=10mg: 480mg, wherein auxiliary material is vitamins C 50mg, vitamin B5 0mg, vitamin-E 50mg, calglucon 50mg, active selenium 10mg and Pericarpium Vitis viniferae ground-slag 270mg, gets final product through preparing burden, mix, granulate, dry, pulverize, incapsulating.
Embodiment four:
Oral resveratrol liquid.Trans-resveratrol: red wine=600mg: 1000ml takes by weighing trans-resveratrol by prescription and is dissolved in a small amount of edible ethanol, with the grape wine allotment, after embedding, sterilization, packs again again.
Embodiment five:
Trans-resveratrol grape wine.Trans-resveratrol: grape wine=100mg: 1000ml is dissolved in trans-resveratrol in the grape wine and gets final product.
Claims (3)
1. the production technique of a trans-resveratrol, it is characterized in that it be with Pericarpium Vitis viniferae through sorting and impurity elimination, rinsing, fragmentation, 95% extraction using alcohol, ethanol extract, tartrate dissolving, extracted with diethyl ether acid solution, ether extraction liquid concentrating under reduced pressure, ether extract, silica gel column chromatography, collection acetone: chloroform elutriant (1: 1), elutriant concentrate, ethyl alcohol recrystallization, produce the Pericarpium Vitis viniferae trans-resveratrol.
2. the utilization of trans-resveratrol in food, drink and grape wind is characterized in that it is that trans-resveratrol is used in the food, drink and grape wind, can produce functional food, beverage and trans-resveratrol grape wine.
3. the utilization of a kind of trans-resveratrol as claimed in claim 2 in food, drink and grape wind, its feature is trans-resveratrol fruit juice, trans-resveratrol capsule, oral resveratrol liquid and trans-resveratrol grape wine at described trans-resveratrol food, drink and grape wind.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 00113971 CN1351985A (en) | 2000-11-13 | 2000-11-13 | Process for producing veratryl alcohol and its use in food, drink and grape wind |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 00113971 CN1351985A (en) | 2000-11-13 | 2000-11-13 | Process for producing veratryl alcohol and its use in food, drink and grape wind |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1351985A true CN1351985A (en) | 2002-06-05 |
Family
ID=4583703
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 00113971 Pending CN1351985A (en) | 2000-11-13 | 2000-11-13 | Process for producing veratryl alcohol and its use in food, drink and grape wind |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1351985A (en) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100441555C (en) * | 2004-04-09 | 2008-12-10 | 汪云 | Composition containing resveratrol and soybean isoflavone and its preparation and use |
| WO2009055840A1 (en) * | 2007-10-31 | 2009-05-07 | Phillip Anthony Norrie | Resveratrol enhanced wine |
| EP1792974A4 (en) * | 2004-07-23 | 2011-06-15 | Suntory Holdings Ltd | PHOTOELECTODE, SOLAR CELL, FLEXIBLE COLOR USING SAME, AND CELL MODULE |
| EP2172118A3 (en) * | 2006-06-13 | 2011-09-07 | IdeaMed LLC | Fluid compositions comprising polyphenols and methods for making and packaging the same |
| CN102994323A (en) * | 2011-09-09 | 2013-03-27 | 冯武文 | Method for improving content of resveratrol in wine base |
| US8993024B2 (en) | 2006-01-23 | 2015-03-31 | Suntory Holdings Limited | Food or drink and method of production thereof |
| CN104893921A (en) * | 2015-05-20 | 2015-09-09 | 张国庆 | Health-care wine and manufacturing method thereof |
| CN105473456A (en) * | 2013-06-26 | 2016-04-06 | 巴洛克斯私人有限公司 | Beverage container coated with a resveratrol layer |
| CN105796536A (en) * | 2016-04-27 | 2016-07-27 | 刘萍 | Natural health care composition for improving red wine health care function and application thereof to red wine |
| CN107868740A (en) * | 2017-11-11 | 2018-04-03 | 威龙葡萄酒股份有限公司 | A kind of brewing method for improving resveratrol in wines content |
| CN109294858A (en) * | 2018-10-29 | 2019-02-01 | 姚舜 | A kind of vinegar of the ingredient containing peanut sprout and preparation method thereof |
| CZ309060B6 (en) * | 2010-11-23 | 2022-01-05 | Výzkumný ústav potravinářský Praha, v.v.i. | Method of producinging non - alcoholic grape juice enriched with resveratrol |
-
2000
- 2000-11-13 CN CN 00113971 patent/CN1351985A/en active Pending
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100441555C (en) * | 2004-04-09 | 2008-12-10 | 汪云 | Composition containing resveratrol and soybean isoflavone and its preparation and use |
| EP1792974A4 (en) * | 2004-07-23 | 2011-06-15 | Suntory Holdings Ltd | PHOTOELECTODE, SOLAR CELL, FLEXIBLE COLOR USING SAME, AND CELL MODULE |
| US8163319B2 (en) | 2004-07-23 | 2012-04-24 | Suntory Holdings Limited | Method of production of an alcohol-dipped food or drink |
| US8993024B2 (en) | 2006-01-23 | 2015-03-31 | Suntory Holdings Limited | Food or drink and method of production thereof |
| EP2172118A3 (en) * | 2006-06-13 | 2011-09-07 | IdeaMed LLC | Fluid compositions comprising polyphenols and methods for making and packaging the same |
| WO2009055840A1 (en) * | 2007-10-31 | 2009-05-07 | Phillip Anthony Norrie | Resveratrol enhanced wine |
| AU2008318262B2 (en) * | 2007-10-31 | 2012-04-05 | Norrie, Philip Anthony Dr | Resveratrol enhanced wine |
| CZ309060B6 (en) * | 2010-11-23 | 2022-01-05 | Výzkumný ústav potravinářský Praha, v.v.i. | Method of producinging non - alcoholic grape juice enriched with resveratrol |
| CN102994323A (en) * | 2011-09-09 | 2013-03-27 | 冯武文 | Method for improving content of resveratrol in wine base |
| CN105473456A (en) * | 2013-06-26 | 2016-04-06 | 巴洛克斯私人有限公司 | Beverage container coated with a resveratrol layer |
| US9962734B2 (en) | 2013-06-26 | 2018-05-08 | Barokes Pty Ltd | Process for making a container with a resveratrol layer |
| CN104893921A (en) * | 2015-05-20 | 2015-09-09 | 张国庆 | Health-care wine and manufacturing method thereof |
| CN105796536A (en) * | 2016-04-27 | 2016-07-27 | 刘萍 | Natural health care composition for improving red wine health care function and application thereof to red wine |
| CN107868740A (en) * | 2017-11-11 | 2018-04-03 | 威龙葡萄酒股份有限公司 | A kind of brewing method for improving resveratrol in wines content |
| CN109294858A (en) * | 2018-10-29 | 2019-02-01 | 姚舜 | A kind of vinegar of the ingredient containing peanut sprout and preparation method thereof |
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| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |