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CN113100323A - Chewing gum capable of changing color and protecting teeth and preparation method thereof - Google Patents

Chewing gum capable of changing color and protecting teeth and preparation method thereof Download PDF

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Publication number
CN113100323A
CN113100323A CN202110370124.9A CN202110370124A CN113100323A CN 113100323 A CN113100323 A CN 113100323A CN 202110370124 A CN202110370124 A CN 202110370124A CN 113100323 A CN113100323 A CN 113100323A
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Prior art keywords
chewing gum
gum
pigment
mass
preparation
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CN202110370124.9A
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Chinese (zh)
Inventor
冯明昊
邓阿敏
陈贤帅
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Foshan Angels Biotechnology Co ltd
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Foshan Angels Biotechnology Co ltd
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Priority to CN202110370124.9A priority Critical patent/CN113100323A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G4/00Chewing gum
    • A23G4/06Chewing gum characterised by the composition containing organic or inorganic compounds
    • A23G4/10Chewing gum characterised by the composition containing organic or inorganic compounds characterised by the carbohydrates used, e.g. polysaccharides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G4/00Chewing gum
    • A23G4/06Chewing gum characterised by the composition containing organic or inorganic compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G4/00Chewing gum
    • A23G4/06Chewing gum characterised by the composition containing organic or inorganic compounds
    • A23G4/064Chewing gum characterised by the composition containing organic or inorganic compounds containing inorganic compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G4/00Chewing gum
    • A23G4/06Chewing gum characterised by the composition containing organic or inorganic compounds
    • A23G4/068Chewing gum characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G4/00Chewing gum
    • A23G4/06Chewing gum characterised by the composition containing organic or inorganic compounds
    • A23G4/12Chewing gum characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Microbiology (AREA)
  • Molecular Biology (AREA)
  • Botany (AREA)
  • Confectionery (AREA)
  • Medicinal Preparation (AREA)

Abstract

The invention relates to the technical field of chewing gum, and discloses a chewing gum with variable color and tooth protection and a preparation method thereof, wherein the chewing gum comprises the following raw materials: gum base, acidulant, mouthguard and pigment; the tooth protecting agent comprises phosphate and sugar alcohol; the color of the pigment changes with the change of the pH value. After being chewed, the chewing gum of the invention can present different colors according to different pH values of the oral cavity environment, thereby not only having great interest, but also reflecting the pH value of the oral cavity of a human body to a certain extent, and simultaneously having the effect of preventing decayed teeth.

Description

Chewing gum capable of changing color and protecting teeth and preparation method thereof
Technical Field
The invention relates to the technical field of chewing gum, in particular to chewing gum with color changing and tooth protecting functions and a preparation method thereof.
Background
Dental caries is a common disease and frequently encountered disease, and has high incidence rate, wide distribution and great harm to human bodies. With the diligent efforts of scientists, bacteria are now generally regarded as the main cause of dental caries, and streptococcus mutans is the main pathogenic bacteria, and the plaque formed by streptococcus mutans is adhered to the tooth surface, grows on the tooth surface, produces acid, corrodes the tooth and finally forms dental caries.
The anticariogenic products used on the market are roughly classified into the following categories: one is a fluorine-containing preparation, and the anticarious principle of the preparation is to promote tooth calcification and reduce acid corrosion, which is an indirect effect and has limited curative effect; secondly, the application of antibacterial drugs, such as mouthwash containing chlorhexidine, metronidazole and the like, is limited due to obvious side effects; and thirdly, the caries prevention product prepared from the plant extract, such as gargle, chewing gum tablet and the like prepared from the traditional Chinese medicine extract, has certain effect on preventing and treating the caries, but is a medicament, needs to be used under the guidance of doctors, has poor taste and is not suitable for long-term use.
At present, the frequent chewing of chewing gum is a good choice for preventing dental caries in addition to conventional gargling. The mechanical stimulation caused by chewing the chewing gum can accelerate the secretion of saliva in the oral cavity, increase the flow rate of the saliva, wash the surface of the oral cavity and play a certain role in cleaning the oral cavity. However, the conventional chewing gum has a single function and has a poor caries prevention effect.
Disclosure of Invention
The invention aims to provide a chewing gum with variable colors and tooth protection, which solves one or more technical problems in the prior art and at least provides a beneficial selection or creation condition.
The technical scheme adopted for solving the technical problems is as follows:
a chewing gum with color changing and tooth protecting functions comprises the following raw materials: gum base, acidulant, mouthguard and pigment; the tooth protecting agent comprises phosphate and sugar alcohol; the color of the pigment changes with the change of the pH value. The gum base is prepared from conventional edible gum base for preparing chewing gum.
Preferably, the sour agent accounts for 0.2-1.2% of the mass of the chewing gum; the sour agent comprises at least one of citric acid, tartaric acid and malic acid.
Preferably, the pigment accounts for 0.05-0.5% of the mass of the chewing gum; the pigment comprises at least one of acid red, anthocyanin and curcumin. The pigment is edible pigment, and has no influence on human body.
The chewing gum contains a small amount of pigment, such as acid red, which has pH sensitive property, i.e. colorless under acidic condition, and gradually develops red as pH increases to neutral or alkaline. Therefore, by adding a flavoring agent such as citric acid to the chewing gum, the chewing gum is slightly acidic before chewing, at which point the chewing gum appears milky white, and then by chewing in the mouth, the citric acid penetrates into the saliva, the ambient pH increases and the chewing gum gradually appears rose-red.
Preferably, the phosphate accounts for 0.2-1% of the mass of the chewing gum; the phosphate comprises at least one of calcium hydrogen phosphate and calcium glycerophosphate. Calcium hydrogen phosphate and calcium glycerophosphate can improve the content of calcium and phosphorus in the enamel, inhibit demineralization of the enamel and improve remineralization of the enamel; can change the acid-base property of enamel surface and enhance the acid-resistant ability.
Preferably, the sugar alcohol accounts for 10-20% of the mass of the chewing gum; the sugar alcohol comprises at least one of xylitol, sorbitol and erythritol.
The sugar alcohol can replace sucrose, and reduce dental caries incidence rate caused by sucrose residue in oral cavity. The sugar alcohol is not utilized by oral bacteria of human body, so that the problems of harm to teeth caused by acidic substances and dental caries caused by acidic substances are avoided, and the growth of oral bacteria is inhibited, thereby playing a role in protecting teeth. For example: xylitol can not be fermented and utilized by bacteria which can generate dental caries in the oral cavity, and the growth of streptococcus and the generation of acid are inhibited; and secondly, when the xylitol is chewed, the secretion of saliva can be promoted, more saliva can wash bacteria in oral cavities and teeth, the concentration of basic amino acid and ammonia at saliva and decayed tooth spots can be increased, the reduction of the pH value in the oral cavity is slowed down, acidic substances which harm the teeth are neutralized and diluted, and the adsorption of the bacteria on the surfaces of the teeth is inhibited, so that the acid erosion of the teeth is reduced, the decayed teeth are prevented, the generation of dental plaque is reduced, and the teeth are consolidated.
Preferably, the gum base accounts for 70-85% of the mass of the chewing gum.
Preferably, the pH of the chewing gum is less than 7.
A second object of the present invention is to provide a process for the preparation of the above chewing gum, comprising the steps of:
heating the gum base to be softened, sequentially adding the phosphate, the sugar alcohol, the pigment and the sour agent, and forming to obtain the chewing gum.
Preferably, the specific process of heating is as follows: and (3) heating the gum base in a water bath at the temperature of 60-75 ℃.
Preferably, before the pigment is added, a proper amount of raw powder is also added to prevent adhesion.
Compared with the prior art, the invention has the following beneficial effects:
the chewing gum contains sour agent, tooth protecting agent and pigment with color capable of changing with pH value; the sour agent can adjust the pH value of the chewing gum and improve the taste of the chewing gum; the tooth protecting agent has the function of preventing decayed teeth; after being chewed, the chewing gum can present different colors according to different pH values of the oral cavity environment, thereby not only having great interest, but also reflecting the pH value of the oral cavity of a human body to a certain extent.
Drawings
The invention is further described below with reference to the accompanying drawings and examples.
FIG. 1 is a graph showing the color development effect of chewing gum of example 1 of the present invention soaked in simulated oral fluid having pH values of 4, 6, 7 and 9, respectively;
FIG. 2 is a graph showing the color development effect of the chewing gum of example 4 of the present invention soaked in simulated oral fluid having pH of 4-9.
Detailed Description
The concept and technical effects of the present invention will be clearly and completely described below in conjunction with the embodiments to fully understand the objects, features and effects of the present invention. It is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments, and those skilled in the art can obtain other embodiments without inventive effort based on the embodiments of the present invention, and all embodiments are within the protection scope of the present invention.
Example 1
A chewing gum capable of changing color and protecting teeth comprises the following raw materials in percentage by mass: gum base 85%, citric acid 1%, calcium hydrogen phosphate 0.5%, xylitol 13%, anthocyanin 0.25% and curcumin 0.25%.
The preparation method of the chewing gum with color changing and tooth protecting functions comprises the following steps:
placing the gum base in a water bath heating environment at 60 ℃, heating to soften, sequentially adding calcium hydrogen phosphate and xylitol, adding a proper amount of raw powder while adding to prevent adhesion, finally adding anthocyanin, curcumin and citric acid, kneading for 5-10 minutes, and forming to obtain the chewing gum with variable colors and tooth protection. By soaking the gum in simulated oral fluid at pH 4, 6, 7, 9, respectively, the gum will appear different colors, as shown in fig. 1, with increasing alkalinity, the gum color will gradually change from purplish red to yellowish green.
Example 2
A chewing gum capable of changing color and protecting teeth comprises the following raw materials in percentage by mass: gum base 78%, tartaric acid 1%, calcium glycerophosphate 0.6%, xylitol 10%, sorbitol 10%, anthocyanidin 0.2% and curcumin 0.2%.
The preparation method of the chewing gum with color changing and tooth protecting functions comprises the following steps:
placing the gum base in a water bath heating environment at 70 ℃, heating to soften, sequentially adding calcium glycerophosphate, xylitol and sorbitol, adding a proper amount of raw powder while adding to prevent adhesion, finally adding anthocyanin, curcumin and tartaric acid, kneading for 5-10 minutes, and molding to obtain the chewing gum with variable colors and tooth protection. By soaking the gum in simulated oral fluid at pH 4, 6, 7, 9, respectively, the gum will appear different colors.
Example 3
A chewing gum capable of changing color and protecting teeth comprises the following raw materials in percentage by mass: gum base 78%, citric acid 0.5%, tartaric acid 0.5%, calcium hydrogen phosphate 0.4%, calcium glycerophosphate 0.4%, xylitol 10%, erythritol 10%, anthocyanin 0.1%, and curcumin 0.1%.
The preparation method of the chewing gum with color changing and tooth protecting functions comprises the following steps:
placing the gum base in a water bath heating environment at 75 ℃, heating to soften, sequentially adding calcium hydrogen phosphate, calcium glycerophosphate, xylitol and erythritol, adding a proper amount of raw powder while adding to prevent adhesion, finally adding anthocyanin, curcumin, citric acid and tartaric acid, kneading for 5-10 minutes, and forming to obtain the chewing gum with variable color and tooth protection. By soaking the gum in simulated oral fluid at pH 4, 6, 7, 9, respectively, the gum will appear different colors.
Example 4
A chewing gum capable of changing color and protecting teeth comprises the following raw materials in percentage by mass: gum base 85%, citric acid 1%, calcium hydrogen phosphate 0.5%, xylitol 13%, acid red 0.5%.
The preparation method of the chewing gum with color changing and tooth protecting functions comprises the following steps:
placing the gum base in a water bath heating environment at 65 ℃, heating to soften, sequentially adding calcium hydrogen phosphate and xylitol, adding a proper amount of raw powder while adding to prevent adhesion, finally adding acid red and citric acid, kneading for 5-10 minutes, and molding to obtain the chewing gum with variable colors and tooth protection. By separately soaking the gum in simulated oral fluid having a pH of 4-9, the gum will exhibit different colors, as shown in figure 2, and gradually change from colorless to rose-red with increasing alkalinity.
Example 5
A chewing gum capable of changing color and protecting teeth comprises the following raw materials in percentage by mass: 78% of gum base, 0.5% of citric acid, 0.5% of tartaric acid, 0.4% of calcium hydrophosphate, 0.4% of calcium glycerophosphate, 10% of xylitol, 10% of sorbitol and 0.2% of acid red.
The preparation method of the chewing gum with color changing and tooth protecting functions comprises the following steps:
placing the gum base in a water bath heating environment at 65 ℃, heating to soften, sequentially adding calcium hydrogen phosphate, calcium glycerophosphate, xylitol and sorbitol, adding a proper amount of raw powder while adding to prevent adhesion, finally adding acid red, citric acid and tartaric acid, kneading for 5-10 minutes, and forming to obtain the chewing gum with variable color and tooth protection. By separately immersing the chewing gum in simulated oral fluid having a pH of 4-9, the chewing gum will exhibit different colors.
Test of bacteriostatic Effect
The chewing gums (experimental groups 1-5) prepared in examples 1-5 and the negative control group were tested for the inhibition of two common pathogenic bacteria in the oral cavity, according to the antibacterial test method in section 2.1.8 of the Disinfection technical Specification.
Preparation of experimental group samples: slabs of gum (5 mm diameter, no more than 4mm thickness) were made into groups of 4 slabs in a clean sterile plate. Preparation of negative control group sample: sterile dry filter paper is taken and added with sterile distilled water for standby.
Two common pathogenic bacteria in the oral cavity are: streptococcus mutans and Porphyromonas gingivalis.
And (3) bacteriostatic test evaluation standard: if the diameter of the bacteriostatic ring is less than or equal to 7mm, judging that no bacteriostatic effect exists. If the diameter of the bacteriostatic ring is larger than 7mm, the bacteriostatic effect is judged to be achieved. The test results are shown in table 1.
TABLE 1
Figure BDA0003008934390000071
Figure BDA0003008934390000081
As can be seen from Table 1, the average diameter of the inhibition rings of the experimental groups 1-5 on Streptococcus mutans is more than 13.5mm, and the average diameter of the inhibition rings on Porphyromonas gingivalis is more than 12.5mm, so that the chewing gum has obvious inhibition effect on Streptococcus mutans and Porphyromonas gingivalis, and can effectively prevent dental caries.
While the preferred embodiments of the present invention have been illustrated and described, it will be understood by those skilled in the art that the present invention is not limited to the details of the embodiments shown and described, but is capable of numerous equivalents and substitutions without departing from the spirit of the invention as set forth in the claims appended hereto.

Claims (10)

1. The chewing gum is characterized by comprising the following raw materials: gum base, acidulant, mouthguard and pigment; the tooth protecting agent comprises phosphate and sugar alcohol; the color of the pigment changes with the change of the pH value.
2. A chewing gum according to claim 1, wherein the sour agent comprises 0.2-1.2% by mass of the chewing gum; the sour agent comprises at least one of citric acid, tartaric acid and malic acid.
3. The chewing gum of claim 1, wherein the pigment comprises 0.05-0.5% by mass of the chewing gum; the pigment comprises at least one of acid red, anthocyanin and curcumin.
4. The chewing gum of claim 1, wherein the phosphate comprises 0.2-1% by mass of the chewing gum; the phosphate comprises at least one of calcium hydrogen phosphate and calcium glycerophosphate.
5. The chewing gum of claim 1, wherein the sugar alcohol comprises 10-20% by mass of the chewing gum; the sugar alcohol comprises at least one of xylitol, sorbitol and erythritol.
6. A chewing gum according to claim 1, wherein the gum base comprises 70-85% by mass of the chewing gum.
7. A chewing gum according to claim 1, wherein the pH of the chewing gum is less than 7.
8. A process for the preparation of a chewing gum according to any of claims 1-7, comprising the steps of:
heating the gum base to be softened, sequentially adding the phosphate, the sugar alcohol, the pigment and the sour agent, and forming to obtain the chewing gum.
9. The preparation method according to claim 8, wherein the heating is carried out by the following specific process: and (3) heating the gum base in a water bath at the temperature of 60-75 ℃.
10. The method of claim 8, wherein a suitable amount of starch is added before the pigment is added.
CN202110370124.9A 2021-04-07 2021-04-07 Chewing gum capable of changing color and protecting teeth and preparation method thereof Pending CN113100323A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116711875A (en) * 2023-06-15 2023-09-08 东莞市吉纯生物技术有限公司 A gum-based chew for preventing and treating dental caries and its preparation method

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2151780A6 (en) * 1971-11-10 1973-04-20 Concentrados Nacionals Chewing gum - or bubble gum giving colour changes during mastication controlled by acid/dye addition
WO1996029047A1 (en) * 1995-03-21 1996-09-26 Warner-Lambert Company Color-changing systems for oral hygiene products
CN1233964A (en) * 1996-08-20 1999-11-03 美国牙科协会健康基金 Anti-carious chewing gums, candies, gels, toothpaste and dentifrices
WO2002087352A1 (en) * 2001-04-25 2002-11-07 Wm. Wrigley Jr. Company Gum having multiple colors
CN1582705A (en) * 2004-05-26 2005-02-23 施建勇 Radix zanthoxyli and xylitol chewing gum and its preparation
CN107509851A (en) * 2017-09-29 2017-12-26 杭州高烯科技有限公司 A kind of graphene chewing gum and preparation method thereof
US20180360068A1 (en) * 2015-12-11 2018-12-20 Wm. Wrigley Jr. Company Color indicating formulations
CN111568940A (en) * 2020-06-19 2020-08-25 河南华药药业有限公司 Formula for preventing dental caries and preparation method thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2151780A6 (en) * 1971-11-10 1973-04-20 Concentrados Nacionals Chewing gum - or bubble gum giving colour changes during mastication controlled by acid/dye addition
WO1996029047A1 (en) * 1995-03-21 1996-09-26 Warner-Lambert Company Color-changing systems for oral hygiene products
CN1233964A (en) * 1996-08-20 1999-11-03 美国牙科协会健康基金 Anti-carious chewing gums, candies, gels, toothpaste and dentifrices
WO2002087352A1 (en) * 2001-04-25 2002-11-07 Wm. Wrigley Jr. Company Gum having multiple colors
CN1582705A (en) * 2004-05-26 2005-02-23 施建勇 Radix zanthoxyli and xylitol chewing gum and its preparation
US20180360068A1 (en) * 2015-12-11 2018-12-20 Wm. Wrigley Jr. Company Color indicating formulations
CN107509851A (en) * 2017-09-29 2017-12-26 杭州高烯科技有限公司 A kind of graphene chewing gum and preparation method thereof
CN111568940A (en) * 2020-06-19 2020-08-25 河南华药药业有限公司 Formula for preventing dental caries and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116711875A (en) * 2023-06-15 2023-09-08 东莞市吉纯生物技术有限公司 A gum-based chew for preventing and treating dental caries and its preparation method

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Application publication date: 20210713