CN111759756A - Anti-hair loss shampoo and production method thereof - Google Patents
Anti-hair loss shampoo and production method thereof Download PDFInfo
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- CN111759756A CN111759756A CN202010798897.2A CN202010798897A CN111759756A CN 111759756 A CN111759756 A CN 111759756A CN 202010798897 A CN202010798897 A CN 202010798897A CN 111759756 A CN111759756 A CN 111759756A
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- hair loss
- hair
- essential oil
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- 230000003656 anti-hair-loss Effects 0.000 title claims abstract description 77
- 239000002453 shampoo Substances 0.000 title claims abstract description 74
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 15
- 239000000203 mixture Substances 0.000 claims abstract description 59
- 239000000341 volatile oil Substances 0.000 claims abstract description 50
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 238000000034 method Methods 0.000 claims abstract description 14
- 239000007788 liquid Substances 0.000 claims description 46
- 238000002156 mixing Methods 0.000 claims description 36
- 239000011259 mixed solution Substances 0.000 claims description 27
- 238000003756 stirring Methods 0.000 claims description 27
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 21
- 239000006185 dispersion Substances 0.000 claims description 19
- 239000012046 mixed solvent Substances 0.000 claims description 19
- 238000001816 cooling Methods 0.000 claims description 18
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 claims description 18
- 150000001875 compounds Chemical class 0.000 claims description 17
- 235000006468 Thea sinensis Nutrition 0.000 claims description 13
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 11
- 238000013329 compounding Methods 0.000 claims description 11
- 239000000377 silicon dioxide Substances 0.000 claims description 11
- VFKZECOCJCGZQK-UHFFFAOYSA-M 3-hydroxypropyl(trimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCO VFKZECOCJCGZQK-UHFFFAOYSA-M 0.000 claims description 10
- 239000004386 Erythritol Substances 0.000 claims description 10
- UNXHWFMMPAWVPI-UHFFFAOYSA-N Erythritol Natural products OCC(O)C(O)CO UNXHWFMMPAWVPI-UHFFFAOYSA-N 0.000 claims description 10
- FPVVYTCTZKCSOJ-UHFFFAOYSA-N Ethylene glycol distearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCOC(=O)CCCCCCCCCCCCCCCCC FPVVYTCTZKCSOJ-UHFFFAOYSA-N 0.000 claims description 10
- 229920002907 Guar gum Polymers 0.000 claims description 10
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 10
- 125000000217 alkyl group Chemical group 0.000 claims description 10
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 10
- UNXHWFMMPAWVPI-ZXZARUISSA-N erythritol Chemical compound OC[C@H](O)[C@H](O)CO UNXHWFMMPAWVPI-ZXZARUISSA-N 0.000 claims description 10
- 229940009714 erythritol Drugs 0.000 claims description 10
- 235000019414 erythritol Nutrition 0.000 claims description 10
- 239000000665 guar gum Substances 0.000 claims description 10
- 229960002154 guar gum Drugs 0.000 claims description 10
- 235000010417 guar gum Nutrition 0.000 claims description 10
- 239000000843 powder Substances 0.000 claims description 10
- 238000002360 preparation method Methods 0.000 claims description 10
- 229910052708 sodium Inorganic materials 0.000 claims description 10
- 239000011734 sodium Substances 0.000 claims description 10
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- 241000168525 Haematococcus Species 0.000 claims description 9
- 244000179970 Monarda didyma Species 0.000 claims description 9
- 235000010672 Monarda didyma Nutrition 0.000 claims description 9
- 238000007605 air drying Methods 0.000 claims description 9
- 238000001914 filtration Methods 0.000 claims description 9
- 230000005484 gravity Effects 0.000 claims description 9
- 238000000227 grinding Methods 0.000 claims description 9
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- 239000003921 oil Substances 0.000 claims description 9
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 claims description 9
- 229960004889 salicylic acid Drugs 0.000 claims description 9
- 238000010298 pulverizing process Methods 0.000 claims description 8
- 238000001132 ultrasonic dispersion Methods 0.000 claims description 2
- 240000000662 Anethum graveolens Species 0.000 claims 1
- 244000269722 Thea sinensis Species 0.000 claims 1
- 210000004209 hair Anatomy 0.000 abstract description 15
- 230000000694 effects Effects 0.000 abstract description 11
- 239000003814 drug Substances 0.000 abstract description 9
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- 239000000126 substance Substances 0.000 abstract description 8
- 230000008569 process Effects 0.000 abstract description 4
- 230000003670 easy-to-clean Effects 0.000 abstract description 2
- 239000002085 irritant Substances 0.000 abstract description 2
- 231100000021 irritant Toxicity 0.000 abstract description 2
- 230000007794 irritation Effects 0.000 abstract description 2
- 230000000149 penetrating effect Effects 0.000 abstract description 2
- 201000004384 Alopecia Diseases 0.000 description 12
- 244000052707 Camellia sinensis Species 0.000 description 12
- 241000125205 Anethum Species 0.000 description 8
- 231100000360 alopecia Toxicity 0.000 description 8
- 125000001181 organosilyl group Chemical group [SiH3]* 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 6
- 239000000686 essence Substances 0.000 description 5
- 241000168517 Haematococcus lacustris Species 0.000 description 4
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- 230000003676 hair loss Effects 0.000 description 4
- 208000024963 hair loss Diseases 0.000 description 4
- 229940057950 sodium laureth sulfate Drugs 0.000 description 4
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 description 4
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- 239000011159 matrix material Substances 0.000 description 2
- 230000003658 preventing hair loss Effects 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
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- 239000000243 solution Substances 0.000 description 2
- XMAYWYJOQHXEEK-OZXSUGGESA-N (2R,4S)-ketoconazole Chemical compound C1CN(C(=O)C)CCN1C(C=C1)=CC=C1OC[C@@H]1O[C@@](CN2C=NC=C2)(C=2C(=CC(Cl)=CC=2)Cl)OC1 XMAYWYJOQHXEEK-OZXSUGGESA-N 0.000 description 1
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 1
- OYINQIKIQCNQOX-UHFFFAOYSA-M 2-hydroxybutyl(trimethyl)azanium;chloride Chemical compound [Cl-].CCC(O)C[N+](C)(C)C OYINQIKIQCNQOX-UHFFFAOYSA-M 0.000 description 1
- 244000303965 Cyamopsis psoralioides Species 0.000 description 1
- 208000001840 Dandruff Diseases 0.000 description 1
- 101710088194 Dehydrogenase Proteins 0.000 description 1
- 241001289529 Fallopia multiflora Species 0.000 description 1
- 239000009429 Ginkgo biloba extract Substances 0.000 description 1
- 240000002045 Guettarda speciosa Species 0.000 description 1
- 235000001287 Guettarda speciosa Nutrition 0.000 description 1
- 206010019233 Headaches Diseases 0.000 description 1
- 241000555676 Malassezia Species 0.000 description 1
- 108010052285 Membrane Proteins Proteins 0.000 description 1
- 235000017784 Mespilus germanica Nutrition 0.000 description 1
- 244000182216 Mimusops elengi Species 0.000 description 1
- 235000000560 Mimusops elengi Nutrition 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 206010039793 Seborrhoeic dermatitis Diseases 0.000 description 1
- 235000007837 Vangueria infausta Nutrition 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229920006317 cationic polymer Polymers 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000001524 citrus aurantium oil Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- WSDISUOETYTPRL-UHFFFAOYSA-N dmdm hydantoin Chemical compound CC1(C)N(CO)C(=O)N(CO)C1=O WSDISUOETYTPRL-UHFFFAOYSA-N 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 229940124274 edetate disodium Drugs 0.000 description 1
- 230000003721 exogen phase Effects 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 210000003780 hair follicle Anatomy 0.000 description 1
- 239000003676 hair preparation Substances 0.000 description 1
- 231100000869 headache Toxicity 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- 229960004125 ketoconazole Drugs 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 230000003340 mental effect Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 229940105902 mint extract Drugs 0.000 description 1
- 230000036651 mood Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 230000002040 relaxant effect Effects 0.000 description 1
- 208000008742 seborrheic dermatitis Diseases 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 210000003491 skin Anatomy 0.000 description 1
- 150000003431 steroids Chemical class 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 229940043810 zinc pyrithione Drugs 0.000 description 1
- PICXIOQBANWBIZ-UHFFFAOYSA-N zinc;1-oxidopyridine-2-thione Chemical compound [Zn+2].[O-]N1C=CC=CC1=S.[O-]N1C=CC=CC1=S PICXIOQBANWBIZ-UHFFFAOYSA-N 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9722—Chlorophycota or Chlorophyta [green algae], e.g. Chlorella
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61P17/08—Antiseborrheics
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- A—HUMAN NECESSITIES
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- A61P17/00—Drugs for dermatological disorders
- A61P17/14—Drugs for dermatological disorders for baldness or alopecia
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- A—HUMAN NECESSITIES
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- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to the technical field of daily chemical products, and particularly relates to an anti-hair loss shampoo and a production method thereof, which solve the problems that a large amount of chemical substances are added into the anti-hair loss shampoo in the prior art, the irritation is large, the anti-hair loss composition is added with more traditional Chinese medicine components, the effect is single, the process is complex, and the like, and the anti-hair loss shampoo comprises the following raw materials in parts by weight: 30-40 parts of anti-dropping composition, 3-8 parts of auxiliary agent, 5-10 parts of essential oil and 30-50 parts of water. The anti-hair-loss shampoo disclosed by the invention is scientific in formula and strict in proportion, mild and non-irritant in the prepared anti-hair-loss shampoo, fragrant in smell and easy to clean, can effectively remove dirt on hair and scalp, enables the hair to be smooth and easy to manage, has super-strong penetrating power and stability, can enhance the activity of cells, and can effectively keep the elasticity, tension and smooth feeling of the hair.
Description
Technical Field
The invention relates to the technical field of daily chemical products, and particularly relates to anti-hair loss shampoo and a production method thereof.
Background
Shampoo, also known as shampoo, hair lotion, hair essence or hair cream, is one of the most widely used hair washing products and hair cosmetics. The shampoo is used for cleaning human body secreted oil and fat, sweat scale, cells detached from scalp, foreign dust, microorganism, residues of styling product and unpleasant odor, etc. attached to scalp and hair, and keeping scalp and hair clean and beautiful. The shampoo is indispensable for modern people to wash hair, and the shampoo on the market at present has various varieties and different functions, thereby providing various hair care and health care choices for people. However, most of the prior shampoos contain more or less chemical substances, such as ketoconazole for removing dandruff and relieving itching, zinc pyrithione, 0ctopirox, 17-hydroxypivalic steroid dehydrogenase, silicone oil for caring and cationic polymer, essence, bactericide, preservative and the like. Although these chemicals have a positive effect, there are still some side effects. In recent years, cosmetics gradually develop towards the trend of returning to nature, and shampoo containing traditional Chinese medicine additives is researched, but the problems of more traditional Chinese medicine components, single effect, complex process and the like exist.
With the development of society, the pressure of life and work of people is getting greater, and the phenomena of alopecia, hair loss and white hair generation become more serious. According to incomplete statistics, nearly 70% of people in asia are suffering from alopecia, and the causes of alopecia are mainly the following: firstly, alopecia caused by excessive mental stress; ② alopecia caused by abnormal secretion of hormones in vivo, such as postpartum and climacteric alopecia; ③ alopecia caused by insufficient nutrient of hair follicle; and fourthly, hair loss and the like caused by excessive use of the hairdressing product. Chinese patent application ZL201410664830.4 'Hair loss prevention traditional Chinese medicine composition, shampoo and preparation method thereof' discloses hair loss prevention shampoo which comprises the following components in parts by weight: 85 parts of shampoo matrix and 10 parts of anti-hair loss traditional Chinese medicine composition, wherein the shampoo matrix comprises the following components in percentage by weight: 65% of sodium laureth sulfate, 2.5% of silica dimethyl silylate, 0.5% of guar hydroxypropyltrimonium chloride, 2.5% of cocamide monoethanolamine, 0.1% of dimethyloldimethylhydantoin, 0.2% of essence and 29.2% of water; the anti-hair loss traditional Chinese medicine composition is prepared from the following components in parts by weight: the ratio of the polygonum multiflorum extract, the medlar extract, the angelica extract, the ginkgo leaf extract and the mint extract is 15:15:15:10: 10. The shampoo prepared by the patent contains a large amount of chemical substances, the total weight of raw materials is only 95 parts, wherein, the sodium laureth sulfate accounts for 55.25 parts, the sodium laureth sulfate can disintegrate (die) cell membranes, combine with hydrophobic parts of membrane proteins and separate the hydrophobic parts from the membranes, and the high concentration of the sodium laureth sulfate can also destroy non-covalent bonds such as ionic bonds, hydrogen bonds and the like in proteins and even change the conformations of the proteins. Moreover, the anti-hair loss composition in the patent is prepared by combining five traditional Chinese medicine extract solutions, and has the problems of multiple obviously added traditional Chinese medicine components, single effect, complex process and the like. Based on the statement, the invention provides anti-hair loss shampoo and a production method thereof.
Disclosure of Invention
The invention aims to solve the problems that a large amount of chemical substances added into anti-hair loss shampoo in the prior art are high in irritation, the anti-hair loss composition is added with a large amount of traditional Chinese medicine components, single in effect, complex in process and the like, and provides the anti-hair loss shampoo and a production method thereof.
The anti-hair loss shampoo comprises the following raw materials in parts by weight: 30-40 parts of anti-dropping composition, 3-8 parts of auxiliary agent, 5-10 parts of essential oil and 30-50 parts of water;
the anti-dropping composition is prepared by the following method: 1) air-drying Haematococcus and Camellia sinensis, adding into a wall breaking machine at a mass ratio of 1-3:5-8, breaking wall at 0-18 deg.C, and pulverizing to obtain mixed micropowder; 2) adding the obtained mixed micro powder into a mixed solvent according to the mass ratio of 1:10-14, and performing ultrasonic dispersion for 10-20min at the temperature of 55-75 ℃ to obtain dispersion liquid; 3) adding disodium edetate and erythritol into the dispersion liquid together according to the mass ratio of 1:12-20:110-150, stirring and mixing uniformly at the rotating speed of 800-1000r/min, heating to 70-90 ℃, keeping the temperature and standing for 3-5h, and filtering to obtain the anti-dropping composition.
Preferably, the anti-hair loss shampoo comprises the following raw materials in parts by weight: 32-38 parts of anti-dropping composition, 4-7 parts of auxiliary agent, 6-9 parts of essential oil and 35-45 parts of water.
Preferably, the anti-hair loss shampoo comprises the following raw materials in parts by weight: 35 parts of anti-dropping composition, 5.5 parts of auxiliary agent, 7.5 parts of essential oil and 40 parts of water.
Preferably, the auxiliary agent is prepared by compounding dimethyl silylated silica, guar gum hydroxypropyl trimethyl ammonium chloride, secondary alkyl sodium sulfonate and ethylene glycol distearate in a mass ratio of 2-5:2-5:1-3: 1-3.
Preferably, the essential oil is a compound composition of orange flower oil, dill essential oil and bergamot essential oil in a mass ratio of 1-3:1-3: 1-3.
Preferably, the mixed solvent is a compound liquid of salicylic acid and absolute ethyl alcohol in a mass ratio of 1: 1-3.
The invention also provides a production method of the anti-hair loss shampoo, which comprises the following steps:
s1, adding the auxiliary agent and the essential oil into a liquid grinder according to the specific gravity, and grinding and mixing for 10-20min to obtain a mixed solution I;
s2, adding the mixed solution I obtained in the step S1 and water into a preparation pot together, stirring and mixing for 10-20min at the temperature of 70-90 ℃, and then cooling to 48-60 ℃ to obtain a mixed solution II;
s3, adding the anti-hair loss composition into the mixed liquid II obtained in the step (A), continuously stirring and mixing for 20-40min, cooling, and subpackaging to obtain the anti-hair loss shampoo.
The anti-hair loss shampoo provided by the invention has the following beneficial effects:
1. the anti-hair loss composition is prepared by selecting haematococcus pluvialis and camellia sinensis as main anti-hair loss raw materials, breaking the walls of the haematococcus pluvialis and camellia sinensis, dispersing the crushed haematococcus pluvialis and camellia sinensis into a mixed solvent, and finally modifying the haematococcus pluvialis and camellia sinensis by using edetate disodium and erythritol to prepare the anti-hair loss composition; according to the invention, the disodium edetate and the erythritol composite dispersion liquid are used for modifying, so that the dispersibility and compatibility of the anti-hair loss composition can be obviously improved, the anti-hair loss composition can be uniformly distributed in shampoo, agglomeration is avoided, and the viscosity stability of the shampoo is improved.
2. The anti-hair loss shampoo additive is prepared by compounding dimethyl silyl silica, guar gum hydroxypropyl trimethyl ammonium chloride, secondary alkyl sodium sulfonate and ethylene glycol distearate, and the additive is low in dosage, but has strong foaming and cleaning capabilities, and does not stimulate scalp.
3. The essential oil is prepared by compounding the neroli oil, the dill essential oil and the bergamot essential oil, replaces essence to be used for the anti-hair loss shampoo, can play the effects of relaxing mood and relieving pressure and headache while endowing the shampoo with pleasant fragrance, and in addition, the essential oil used by the shampoo can improve greasy and unclean skin and has a curative effect on seborrheic dermatitis of scalp.
4. The anti-hair-loss shampoo disclosed by the invention is scientific in formula and strict in proportion, mild and non-irritant in the prepared anti-hair-loss shampoo, fragrant in smell and easy to clean, can effectively remove dirt on hair and scalp, enables the hair to be smooth and easy to manage, has super-strong penetrating power and stability, can enhance the activity of cells, and can effectively keep the elasticity, tension and smooth feeling of the hair.
Detailed Description
The present invention will be further illustrated with reference to the following specific examples.
Example one
The invention provides anti-hair loss shampoo which comprises the following raw materials in parts by weight: 30 parts of anti-dropping composition, 3 parts of auxiliary agent, 5 parts of essential oil and 30 parts of water;
the anti-dropping composition is prepared by the following method: 1) air-drying Haematococcus and Camellia sinensis, adding into a wall breaking machine at a mass ratio of 1:5, breaking wall at 0 deg.C, and pulverizing to obtain mixed micropowder; 2) adding the obtained mixed micro powder into a mixed solvent according to the mass ratio of 1:10, and ultrasonically dispersing for 10min at the temperature of 55 ℃ to obtain a dispersion liquid, wherein the mixed solvent is a compound liquid of salicylic acid and absolute ethyl alcohol according to the mass ratio of 1: 1; 3) adding disodium edetate and erythritol together into the dispersion liquid according to the mass ratio of 1:12:110, stirring and mixing uniformly at the rotating speed of 800r/min, heating to 70 ℃, keeping the temperature and standing for 3 hours, and filtering to obtain the anti-dropping composition;
the auxiliary agent is prepared by compounding dimethyl silyl silica, guar gum hydroxypropyl trimethyl ammonium chloride, secondary alkyl sodium sulfonate and ethylene glycol distearate in a mass ratio of 2:2:1: 1;
the essential oil is a compound composition of orange flower oil, dill essential oil and bergamot essential oil in a mass ratio of 1:3: 1.
The invention also provides a production method of the anti-hair loss shampoo, which comprises the following steps:
s1, adding the auxiliary agent and the essential oil into a liquid grinder according to the specific gravity, and grinding and mixing for 10min to obtain a mixed solution I;
s2, adding the mixed solution I obtained in the step S1 and water into a preparation pot together, stirring and mixing for 10min at the temperature of 70 ℃, and then cooling to 48 ℃ to obtain a mixed solution II;
s3, adding the anti-hair loss composition into the mixed liquid II obtained in the step (A), continuously stirring and mixing for 20min, cooling, and subpackaging to obtain the anti-hair loss shampoo.
Example two
The invention provides anti-hair loss shampoo which comprises the following raw materials in parts by weight: 35 parts of anti-dropping composition, 5.5 parts of auxiliary agent, 7.5 parts of essential oil and 40 parts of water;
the anti-dropping composition is prepared by the following method: 1) air-drying Haematococcus and Camellia sinensis, adding into a wall breaking machine at a mass ratio of 2:6.5, breaking wall at 9 deg.C, and pulverizing to obtain mixed micropowder; 2) adding the obtained mixed micro powder into a mixed solvent according to the mass ratio of 1:12, and ultrasonically dispersing for 15min at the temperature of 65 ℃ to obtain a dispersion liquid, wherein the mixed solvent is a compound liquid of salicylic acid and absolute ethyl alcohol according to the mass ratio of 1: 2; 3) adding disodium edetate and erythritol together into the dispersion liquid according to the mass ratio of 1:16:130, stirring and mixing uniformly at the rotating speed of 900r/min, heating to 80 ℃, keeping the temperature and standing for 4 hours, and filtering to obtain the anti-dropping composition;
the auxiliary agent is prepared by compounding dimethyl silylated silica, guar gum hydroxypropyl trimethyl ammonium chloride, secondary alkyl sodium sulfonate and ethylene glycol distearate in a mass ratio of 3.5:3.5:2: 2;
the essential oil is a compound composition of orange flower oil, dill essential oil and bergamot essential oil in a mass ratio of 3:1: 3.
The invention also provides a production method of the anti-hair loss shampoo, which comprises the following steps:
s1, adding the auxiliary agent and the essential oil into a liquid grinder according to the specific gravity, and grinding and mixing for 15min to obtain a mixed solution I;
s2, adding the mixed solution I obtained in the step S1 and water into a preparation pot together, stirring and mixing for 15min at the temperature of 80 ℃, and then cooling to 54 ℃ to obtain a mixed solution II;
s3, adding the anti-hair loss composition into the mixed liquid II obtained in the step (A), continuously stirring and mixing for 30min, cooling, and subpackaging to obtain the anti-hair loss shampoo.
EXAMPLE III
The invention provides anti-hair loss shampoo which comprises the following raw materials in parts by weight: 40 parts of anti-dropping composition, 8 parts of auxiliary agent, 10 parts of essential oil and 50 parts of water;
the anti-dropping composition is prepared by the following method: 1) air-drying Haematococcus and Camellia sinensis, adding into a wall breaking machine according to the mass ratio of 3:8, breaking the wall at 18 ℃, and crushing to obtain mixed micro powder; 2) adding the obtained mixed micro powder into a mixed solvent according to the mass ratio of 1:14, and ultrasonically dispersing for 20min at the temperature of 75 ℃ to obtain a dispersion liquid, wherein the mixed solvent is a compound liquid of salicylic acid and absolute ethyl alcohol according to the mass ratio of 1: 3; 3) adding disodium edetate and erythritol together into the dispersion liquid according to the mass ratio of 1:20:150, stirring and mixing uniformly at the rotating speed of 1000r/min, heating to 90 ℃, keeping the temperature and standing for 5 hours, and filtering to obtain the anti-dropping composition;
the auxiliary agent is prepared by compounding dimethyl silyl silica, guar gum hydroxypropyl trimethyl ammonium chloride, secondary alkyl sodium sulfonate and ethylene glycol distearate in a mass ratio of 5:5:3: 3;
the essential oil is a compound composition of orange flower oil, dill essential oil and bergamot essential oil in a mass ratio of 1:2: 3.
The invention also provides a production method of the anti-hair loss shampoo, which comprises the following steps:
s1, adding the auxiliary agent and the essential oil into a liquid grinder according to the specific gravity, and grinding and mixing for 20min to obtain a mixed solution I;
s2, adding the mixed solution I obtained in the step S1 and water into a preparation pot together, stirring and mixing for 20min at the temperature of 90 ℃, and then cooling to 60 ℃ to obtain a mixed solution II;
s3, adding the anti-hair loss composition into the mixed liquid II obtained in the step (A), continuously stirring and mixing for 40min, cooling, and subpackaging to obtain the anti-hair loss shampoo.
Comparative example 1
The invention provides anti-hair loss shampoo which comprises the following raw materials in parts by weight: 30 parts of anti-dropping composition, 3 parts of auxiliary agent, 5 parts of essential oil and 30 parts of water;
the anti-dropping composition is prepared by the following method: 1) air-drying Haematococcus and Camellia sinensis, adding into a wall breaking machine at a mass ratio of 1:5, breaking wall at 0 deg.C, and pulverizing to obtain mixed micropowder; 2) adding the obtained mixed micro powder into a mixed solvent according to the mass ratio of 1:10, and ultrasonically dispersing for 10min at the temperature of 55 ℃ to obtain a dispersion liquid, wherein the mixed solvent is a compound liquid of salicylic acid and absolute ethyl alcohol according to the mass ratio of 1: 1; 3) uniformly stirring and mixing the dispersion liquid at the rotating speed of 800r/min, heating to 70 ℃, keeping the temperature, standing for 3 hours, and filtering to obtain the anti-falling composition;
the auxiliary agent is prepared by compounding dimethyl silyl silica, guar gum hydroxypropyl trimethyl ammonium chloride, secondary alkyl sodium sulfonate and ethylene glycol distearate in a mass ratio of 2:2:1: 1;
the essential oil is a compound composition of orange flower oil, dill essential oil and bergamot essential oil in a mass ratio of 1:3: 1.
The invention also provides a production method of the anti-hair loss shampoo, which comprises the following steps:
s1, adding the auxiliary agent and the essential oil into a liquid grinder according to the specific gravity, and grinding and mixing for 10min to obtain a mixed solution I;
s2, adding the mixed solution I obtained in the step S1 and water into a preparation pot together, stirring and mixing for 10min at the temperature of 70 ℃, and then cooling to 48 ℃ to obtain a mixed solution II;
s3, adding the anti-hair loss composition into the mixed liquid II obtained in the step (A), continuously stirring and mixing for 20min, cooling, and subpackaging to obtain the anti-hair loss shampoo.
Comparative example No. two
The invention provides anti-hair loss shampoo which comprises the following raw materials in parts by weight: 30 parts of anti-dropping composition, 3 parts of auxiliary agent, 5 parts of essential oil and 30 parts of water;
the anti-dropping composition is prepared by the following method: 1) air-drying Haematococcus and Camellia sinensis, adding into a wall breaking machine at a mass ratio of 1:5, breaking wall at 0 deg.C, and pulverizing to obtain mixed micropowder; 2) adding the obtained mixed micro powder into a mixed solvent according to the mass ratio of 1:10, and ultrasonically dispersing for 10min at the temperature of 55 ℃ to obtain a dispersion liquid, wherein the mixed solvent is a compound liquid of salicylic acid and absolute ethyl alcohol according to the mass ratio of 1: 1; 3) adding disodium edetate into the dispersion liquid according to the mass ratio of 1:110, stirring and mixing uniformly at the rotating speed of 800r/min, heating to 70 ℃, keeping the temperature and standing for 3 hours, and filtering to obtain the anti-dropping composition;
the auxiliary agent is prepared by compounding dimethyl silyl silica, guar gum hydroxypropyl trimethyl ammonium chloride, secondary alkyl sodium sulfonate and ethylene glycol distearate in a mass ratio of 2:2:1: 1;
the essential oil is a compound composition of orange flower oil, dill essential oil and bergamot essential oil in a mass ratio of 1:3: 1.
The invention also provides a production method of the anti-hair loss shampoo, which comprises the following steps:
s1, adding the auxiliary agent and the essential oil into a liquid grinder according to the specific gravity, and grinding and mixing for 10min to obtain a mixed solution I;
s2, adding the mixed solution I obtained in the step S1 and water into a preparation pot together, stirring and mixing for 10min at the temperature of 70 ℃, and then cooling to 48 ℃ to obtain a mixed solution II;
s3, adding the anti-hair loss composition into the mixed liquid II obtained in the step (A), continuously stirring and mixing for 20min, cooling, and subpackaging to obtain the anti-hair loss shampoo.
Comparative example No. three
The invention provides anti-hair loss shampoo which comprises the following raw materials in parts by weight: 30 parts of anti-dropping composition, 3 parts of auxiliary agent, 5 parts of essential oil and 30 parts of water;
the anti-dropping composition is prepared by the following method: 1) air-drying Haematococcus and Camellia sinensis, adding into a wall breaking machine at a mass ratio of 1:5, breaking wall at 0 deg.C, and pulverizing to obtain mixed micropowder; 2) adding the obtained mixed micro powder into a mixed solvent according to the mass ratio of 1:10, and ultrasonically dispersing for 10min at the temperature of 55 ℃ to obtain a dispersion liquid, wherein the mixed solvent is a compound liquid of salicylic acid and absolute ethyl alcohol according to the mass ratio of 1: 1; 3) adding disodium edetate and erythritol together into the dispersion liquid according to the mass ratio of 12:110, stirring and mixing uniformly at the rotating speed of 800r/min, heating to 70 ℃, preserving heat, standing for 3 hours, and filtering to obtain the anti-dropping composition;
the auxiliary agent is prepared by compounding dimethyl silyl silica, guar gum hydroxypropyl trimethyl ammonium chloride, secondary alkyl sodium sulfonate and ethylene glycol distearate in a mass ratio of 2:2:1: 1;
the essential oil is a compound composition of orange flower oil, dill essential oil and bergamot essential oil in a mass ratio of 1:3: 1.
The invention also provides a production method of the anti-hair loss shampoo, which comprises the following steps:
s1, adding the auxiliary agent and the essential oil into a liquid grinder according to the specific gravity, and grinding and mixing for 10min to obtain a mixed solution I;
s2, adding the mixed solution I obtained in the step S1 and water into a preparation pot together, stirring and mixing for 10min at the temperature of 70 ℃, and then cooling to 48 ℃ to obtain a mixed solution II;
s3, adding the anti-hair loss composition into the mixed liquid II obtained in the step (A), continuously stirring and mixing for 20min, cooling, and subpackaging to obtain the anti-hair loss shampoo.
Comparative example No. four
The invention provides anti-hair loss shampoo which comprises the following raw materials in parts by weight: 30 parts of anti-dropping composition, 3 parts of auxiliary agent, 5 parts of essence and 30 parts of water;
the anti-dropping composition is prepared by the following method: 1) air-drying Haematococcus and Camellia sinensis, adding into a wall breaking machine at a mass ratio of 1:5, breaking wall at 0 deg.C, and pulverizing to obtain mixed micropowder; 2) adding the obtained mixed micro powder into a mixed solvent according to the mass ratio of 1:10, and ultrasonically dispersing for 10min at the temperature of 55 ℃ to obtain a dispersion liquid, wherein the mixed solvent is a compound liquid of salicylic acid and absolute ethyl alcohol according to the mass ratio of 1: 1; 3) adding disodium edetate and erythritol together into the dispersion liquid according to the mass ratio of 1:12:110, stirring and mixing uniformly at the rotating speed of 800r/min, heating to 70 ℃, keeping the temperature and standing for 3 hours, and filtering to obtain the anti-dropping composition;
the auxiliary agent is prepared by compounding dimethyl silyl silica, guar gum hydroxypropyl trimethyl ammonium chloride, secondary alkyl sodium sulfonate and ethylene glycol distearate in a mass ratio of 2:2:1: 1;
the invention also provides a production method of the anti-hair loss shampoo, which comprises the following steps:
s1, adding the auxiliary agent and the essential oil into a liquid grinder according to the specific gravity, and grinding and mixing for 10min to obtain a mixed solution I;
s2, adding the mixed solution I obtained in the step S1 and water into a preparation pot together, stirring and mixing for 10min at the temperature of 70 ℃, and then cooling to 48 ℃ to obtain a mixed solution II;
s3, adding the anti-hair loss composition into the mixed liquid II obtained in the step (A), continuously stirring and mixing for 20min, cooling, and subpackaging to obtain the anti-hair loss shampoo.
The physical and chemical indexes of the anti-hair loss shampoo prepared in the first to third examples and the first to fourth comparative examples are respectively tested, and the following results are obtained:
table 1:
as can be seen from Table 1: the anti-hair loss shampoo prepared in the first to third embodiments of the invention has high viscosity, good viscosity stability, weak acidity, no stimulation to scalp, and the antibacterial rate (malassezia) is as high as 97.3%.
According to the first embodiment and the first to third comparative examples, the disodium edetate and the erythritol are compounded and added, so that the viscosity and the viscosity stability of the anti-hair loss shampoo can be effectively improved.
The inventor randomly selects 400 alopecia people between 18 and 60 years old, and randomly divides 400 test objects into 4 groups which are respectively marked as a test group 1, a test group 2, a test group 3 and a test group 4; the anti-hair loss shampoo prepared in the first to third embodiments of the present invention is used in test groups 1 to 3, the commercially available anti-hair loss shampoo (bawang shampoo) is used in test group 4, the test cycle of the test group 4 is 3 months, the use frequency is twice a week, and the test results are as follows:
table 2:
note: the significant effect means that the number of the hair shedding roots is reduced by more than 60 percent in a combing test compared with that before use;
effective means that the number of hair loss in the combing test is reduced by 30 to 60 percent compared with that before use;
the ineffectiveness means that the number of hair loss in the combing test is reduced by less than 30% compared with that before use.
As can be seen from Table 2: the anti-hair loss shampoo prepared in the first to third embodiments of the invention has an anti-hair loss effect far superior to that of the anti-hair loss shampoo sold in the market.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (7)
1. The anti-hair loss shampoo is characterized by comprising the following raw materials in parts by weight: 30-40 parts of anti-dropping composition, 3-8 parts of auxiliary agent, 5-10 parts of essential oil and 30-50 parts of water;
the anti-dropping composition is prepared by the following method: 1) air-drying Haematococcus and Camellia sinensis, adding into a wall breaking machine at a mass ratio of 1-3:5-8, breaking wall at 0-18 deg.C, and pulverizing to obtain mixed micropowder; 2) adding the obtained mixed micro powder into a mixed solvent according to the mass ratio of 1:10-14, and performing ultrasonic dispersion for 10-20min at the temperature of 55-75 ℃ to obtain dispersion liquid; 3) adding disodium edetate and erythritol into the dispersion liquid together according to the mass ratio of 1:12-20:110-150, stirring and mixing uniformly at the rotating speed of 800-1000r/min, heating to 70-90 ℃, keeping the temperature and standing for 3-5h, and filtering to obtain the anti-dropping composition.
2. The anti-hair loss shampoo as claimed in claim 1, characterized by comprising the following raw materials in parts by weight: 32-38 parts of anti-dropping composition, 4-7 parts of auxiliary agent, 6-9 parts of essential oil and 35-45 parts of water.
3. The anti-hair loss shampoo as claimed in claim 1, characterized by comprising the following raw materials in parts by weight: 35 parts of anti-dropping composition, 5.5 parts of auxiliary agent, 7.5 parts of essential oil and 40 parts of water.
4. The anti-hair loss shampoo as claimed in claim 1, wherein the auxiliary agent is prepared by compounding dimethyl silylated silica, guar gum hydroxypropyl trimethyl ammonium chloride, secondary alkyl sodium sulfonate and ethylene glycol distearate in a mass ratio of 2-5:2-5:1-3: 1-3.
5. The anti-hair loss shampoo as claimed in claim 1, wherein the essential oil is a compound composition of orange flower oil, dill essential oil and bergamot essential oil in a mass ratio of 1-3:1-3: 1-3.
6. The anti-hair loss shampoo as claimed in claim 1, wherein the mixed solvent is a compound liquid of salicylic acid and absolute ethyl alcohol in a mass ratio of 1: 1-3.
7. The production method of the anti-hair loss shampoo as claimed in any one of claims 1 to 6, wherein the method comprises the following steps:
s1, adding the auxiliary agent and the essential oil into a liquid grinder according to the specific gravity, and grinding and mixing for 10-20min to obtain a mixed solution I;
s2, adding the mixed solution I obtained in the step S1 and water into a preparation pot together, stirring and mixing for 10-20min at the temperature of 70-90 ℃, and then cooling to 48-60 ℃ to obtain a mixed solution II;
s3, adding the anti-hair loss composition into the mixed liquid II obtained in the step (A), continuously stirring and mixing for 20-40min, cooling, and subpackaging to obtain the anti-hair loss shampoo.
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