CN111759002A - Composite aroma-carrying core line for cigarettes - Google Patents
Composite aroma-carrying core line for cigarettes Download PDFInfo
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- CN111759002A CN111759002A CN202010665556.8A CN202010665556A CN111759002A CN 111759002 A CN111759002 A CN 111759002A CN 202010665556 A CN202010665556 A CN 202010665556A CN 111759002 A CN111759002 A CN 111759002A
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- core wire
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- weight
- release agent
- slow
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 35
- 239000002131 composite material Substances 0.000 title claims abstract description 27
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 38
- 239000011248 coating agent Substances 0.000 claims abstract description 25
- 238000000576 coating method Methods 0.000 claims abstract description 25
- 238000002156 mixing Methods 0.000 claims abstract description 22
- 239000000686 essence Substances 0.000 claims abstract description 19
- 241000208125 Nicotiana Species 0.000 claims abstract description 13
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 13
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000002270 dispersing agent Substances 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims abstract description 7
- 235000021314 Palmitic acid Nutrition 0.000 claims abstract description 6
- 229920002472 Starch Polymers 0.000 claims abstract description 6
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229920001610 polycaprolactone Polymers 0.000 claims abstract description 6
- 239000004632 polycaprolactone Substances 0.000 claims abstract description 6
- 239000008107 starch Substances 0.000 claims abstract description 6
- 235000019698 starch Nutrition 0.000 claims abstract description 6
- 239000003906 humectant Substances 0.000 claims abstract description 5
- 239000002562 thickening agent Substances 0.000 claims abstract description 5
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 27
- 239000000203 mixture Substances 0.000 claims description 27
- 239000000463 material Substances 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 13
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 9
- 229920000742 Cotton Polymers 0.000 claims description 6
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 6
- 229920002125 Sokalan® Polymers 0.000 claims description 6
- 239000012153 distilled water Substances 0.000 claims description 6
- 239000004584 polyacrylic acid Substances 0.000 claims description 6
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 6
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims description 6
- 229940048086 sodium pyrophosphate Drugs 0.000 claims description 6
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 6
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims description 6
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 238000005303 weighing Methods 0.000 claims description 6
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 5
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims description 5
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims description 5
- 229920002126 Acrylic acid copolymer Polymers 0.000 claims description 4
- 239000000853 adhesive Substances 0.000 claims description 4
- 230000001070 adhesive effect Effects 0.000 claims description 4
- 239000005018 casein Substances 0.000 claims description 4
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims description 4
- 235000021240 caseins Nutrition 0.000 claims description 4
- 229920001661 Chitosan Polymers 0.000 claims description 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 3
- 229920002907 Guar gum Polymers 0.000 claims description 3
- 108010073771 Soybean Proteins Proteins 0.000 claims description 3
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 3
- 239000000835 fiber Substances 0.000 claims description 3
- 239000000665 guar gum Substances 0.000 claims description 3
- 235000010417 guar gum Nutrition 0.000 claims description 3
- 229960002154 guar gum Drugs 0.000 claims description 3
- 229920000609 methyl cellulose Polymers 0.000 claims description 3
- 239000001923 methylcellulose Substances 0.000 claims description 3
- 235000010981 methylcellulose Nutrition 0.000 claims description 3
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims description 3
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims description 3
- 239000000600 sorbitol Substances 0.000 claims description 3
- 235000019710 soybean protein Nutrition 0.000 claims description 3
- 229920001817 Agar Polymers 0.000 claims description 2
- 241001474374 Blennius Species 0.000 claims description 2
- 244000025254 Cannabis sativa Species 0.000 claims description 2
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 claims description 2
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 claims description 2
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 2
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 2
- 229920001353 Dextrin Polymers 0.000 claims description 2
- 239000004375 Dextrin Substances 0.000 claims description 2
- 108010010803 Gelatin Proteins 0.000 claims description 2
- 229920000881 Modified starch Polymers 0.000 claims description 2
- 239000004698 Polyethylene Substances 0.000 claims description 2
- 239000008272 agar Substances 0.000 claims description 2
- 235000010419 agar Nutrition 0.000 claims description 2
- 235000009120 camo Nutrition 0.000 claims description 2
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 2
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 2
- 235000010418 carrageenan Nutrition 0.000 claims description 2
- 239000000679 carrageenan Substances 0.000 claims description 2
- 229920001525 carrageenan Polymers 0.000 claims description 2
- 229940113118 carrageenan Drugs 0.000 claims description 2
- 235000005607 chanvre indien Nutrition 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 235000019425 dextrin Nutrition 0.000 claims description 2
- 239000003925 fat Substances 0.000 claims description 2
- 235000019197 fats Nutrition 0.000 claims description 2
- 239000008273 gelatin Substances 0.000 claims description 2
- 229920000159 gelatin Polymers 0.000 claims description 2
- 235000019322 gelatine Nutrition 0.000 claims description 2
- 235000011852 gelatine desserts Nutrition 0.000 claims description 2
- 239000011521 glass Substances 0.000 claims description 2
- 239000011487 hemp Substances 0.000 claims description 2
- 235000019426 modified starch Nutrition 0.000 claims description 2
- 239000004745 nonwoven fabric Substances 0.000 claims description 2
- 239000001814 pectin Substances 0.000 claims description 2
- 235000010987 pectin Nutrition 0.000 claims description 2
- 229920001277 pectin Polymers 0.000 claims description 2
- 229920002401 polyacrylamide Polymers 0.000 claims description 2
- -1 polyethylene Polymers 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 2
- 239000003205 fragrance Substances 0.000 abstract description 13
- 239000000126 substance Substances 0.000 abstract description 13
- 230000000391 smoking effect Effects 0.000 abstract description 6
- 229920001030 Polyethylene Glycol 4000 Polymers 0.000 abstract description 4
- 239000007788 liquid Substances 0.000 abstract description 4
- 229940057838 polyethylene glycol 4000 Drugs 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- 235000019568 aromas Nutrition 0.000 abstract description 2
- 239000004094 surface-active agent Substances 0.000 abstract description 2
- 239000000084 colloidal system Substances 0.000 abstract 2
- 239000006185 dispersion Substances 0.000 abstract 2
- 239000011162 core material Substances 0.000 description 64
- 239000000796 flavoring agent Substances 0.000 description 16
- 235000019634 flavors Nutrition 0.000 description 14
- 238000011156 evaluation Methods 0.000 description 9
- 230000001953 sensory effect Effects 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 4
- 235000013599 spices Nutrition 0.000 description 4
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 3
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 3
- 239000011324 bead Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 3
- 229940041616 menthol Drugs 0.000 description 3
- 239000007968 orange flavor Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000007901 soft capsule Substances 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000001246 colloidal dispersion Methods 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000004014 plasticizer Substances 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 238000013268 sustained release Methods 0.000 description 2
- 239000012730 sustained-release form Substances 0.000 description 2
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 229920006221 acetate fiber Polymers 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000001087 glyceryl triacetate Substances 0.000 description 1
- 235000013773 glyceryl triacetate Nutrition 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000008368 mint flavor Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 229960002622 triacetin Drugs 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a composite aroma-carrying core wire for cigarettes. Is prepared by flavoring the core wire of the conventional cigarette filter stick and coating the core wire with a slow release agent. The slow release agent is prepared by uniformly mixing polyethylene glycol-4000, palmitic acid, polycaprolactone, starch, a thickening agent, a humectant and a dispersing agent according to a specific proportion. The essence for tobacco generates stable colloid dispersion liquid under the action of the surfactant, and the stable colloid dispersion liquid is coated on the surface of the core wire, so that the stability of the essence is good. The slow release agent can effectively embed core wire fragrance, organically combines fragrance protection and release, and effectively solves the problems of easy volatilization of fragrance substances, uneven fragrance volatilization and the like of the traditional perfuming core wire. Different tobacco essences are further added into the slow release agent, so that one filter rod can simultaneously load two kinds of aromas, and the smoking taste of the cigarette is enriched. The method is simple and convenient, has low cost and obvious effect, and has good application prospect.
Description
Technical Field
The invention belongs to the technical field of cigarette flavoring, and particularly relates to a composite flavor-carrying core wire for flavoring a cigarette filter stick.
Background
In order to improve the smoking quality of cigarettes, make up for the deficiency of the original fragrance of tobacco and achieve the aims of increasing fragrance and keeping moisture, the cigarettes are usually required to be flavored. At present, cigarette flavoring mainly adopts two modes: tobacco shred perfuming and filter stick perfuming. The tobacco shred flavoring is to add a flavoring substance into a tobacco leaf rolling formula to directly participate in cigarette combustion, which easily causes the waste of expensive essence substances; meanwhile, the added aroma substances can generate uncontrollable products due to high temperature during smoking of the cigarettes, so that the sensory quality of the cigarettes is influenced. And in the mode of flavoring the filter stick, because the flavor substances added in the filter tip do not directly participate in the cigarette combustion, the cigarette filter stick is safe, controllable, convenient to qualitatively and quantitatively add the flavor substances, more beneficial to adding the flavor substances in a targeted manner, increasing the richness of the flavor, and harmonizing the cigarette flavor and the smoke. In recent years, the addition of materials with adsorption and flavor-blending effects in filter sticks has become an important subject of research in the tobacco industry.
At present, the perfuming of the cigarette filter stick mainly comprises the following modes: 1. when the filter stick is formed, the essence and the spice with good solubility are added into the plasticizer (glyceryl triacetate), the method is simple and convenient, but the problem is that the essence and the spice have good miscibility with the plasticizer, so that the application of most of water-soluble essence and spice is limited. In addition, the essence and the spice are easy to volatilize and lose in the process of storing the filter stick. 2. The particles are added into the cigarette filter stick, and when main stream smoke of the cigarette passes through, the fragrant substances are released, so that the purpose of flavoring is achieved. The perfuming of the particles has the advantages of simple equipment and process, low requirement on the character of the fragrant substance and the like, but has the defects of less attachment of the fragrant substance, low transmission efficiency and the like. 3. The flavoring of the puffed bead is to wrap the essence in the soft capsule, place the soft capsule in the cigarette filter, and pinch the soft capsule with the help of external force to release the essence therein during smoking. However, the problems that the exploded beads are not easy to store at high humidity temperature, are easy to absorb moisture and deteriorate, and the oil-soluble essence is easy to pollute the filter stick forming paper after the exploded beads are extruded are solved.
In the prior art, a filter stick perfuming mode, namely perfuming a fragrant line, is adopted, one or more core wires which are soaked in plant perfume are added into the filter stick, so that the purposes of perfuming and fragrance supplementing are achieved, and the core wires are mainly made of cotton threads or cellulose. However, the problem is that the fragrance is not uniformly released in the front and rear sections when the cigarette is smoked, and the fragrance substances adsorbed on the core line are volatile along with the prolonging of the storage time of the filter stick.
Disclosure of Invention
The invention aims to provide a composite aroma-carrying core wire for cigarettes aiming at the defects of the prior art and solving the problems of volatile aroma substances and uneven aroma release of the existing core wire for cigarettes.
The purpose of the invention is realized by the following technical scheme.
All percentages used herein are by weight unless otherwise indicated.
A composite flavor-carrying core wire for cigarettes is prepared by the following method:
(1) perfuming a core wire:
weighing 20-30 parts by weight of distilled water, 10-20 parts by weight of adhesive, 20-30 parts by weight of propylene glycol, 1-5 parts by weight of polyvinyl alcohol and 1-2 parts by weight of dispersant, uniformly mixing, and completely dissolving to obtain a mixture A; uniformly mixing the tobacco essence and the mixture A according to the weight ratio of 20-60: 10-30 to obtain a mixture B; uniformly coating the mixture B on a core wire by using a multifunctional precise coating instrument to obtain a flavored core wire; the adhesive is one of sodium carboxymethylcellulose, casein acrylic acid copolymer, soybean protein or carboxymethyl cellulose; the dispersing agent is one of polyacrylic acid, sodium polyacrylate, sodium pyrophosphate or sodium tripolyphosphate;
(2) preparing a slow release agent:
weighing polyethylene glycol-400030-40 parts by weight, palmitic acid 25-35 parts by weight, polycaprolactone 18-32 parts by weight and starch 15-25 parts by weight, uniformly mixing, and stirring at a constant temperature of 50-60 ℃ for 200-400 r/min until completely dissolving to obtain a slow-release base material; weighing 30-70 parts of slow-release base material, 1-10 parts of thickening agent, 10-30 parts of humectant and 1-2 parts of dispersing agent, and uniformly mixing to prepare a slow-release agent; the thickening agent is one of pectin, agar, gelatin, seaweed fat, carrageenan, dextrin, methylcellulose, starch derivatives, polyacrylamide, guar gum or chitosan; the humectant is one of glycerol, propylene glycol or sorbitol; the dispersing agent is one of polyacrylic acid, sodium polyacrylate, sodium pyrophosphate or sodium tripolyphosphate;
(3) preparing a composite fragrance-carrying core wire:
and (3) uniformly coating the prepared slow release agent on the perfuming core wire obtained in the step (1) by adopting a multifunctional precise coating instrument, and quickly cooling and solidifying the prepared slow release agent to attach the slow release agent to the surface of the perfuming core wire to obtain the required composite perfuming core wire for the cigarettes.
The core wire is made of one of corrugated paper, glass paper, non-woven fabric, cotton paper, cotton thread, fiber thread, hemp thread or silk thread.
Further, 1-20 parts of tobacco essence is added into the prepared slow release agent, so that secondary perfuming of the core wire is realized.
Compared with the prior art, the invention has the following beneficial effects:
(1) according to the invention, the surfactant is added to pretreat the essence to generate the stable colloidal dispersion liquid, and the stable colloidal dispersion liquid is coated on the surface of the core material, so that the stability of the essence is good.
(2) The slow release agent is coated on the surface of the perfuming core wire, so that fragrance carried by the core wire can be effectively embedded, the organic combination of fragrance protection and release is realized, and the problems of easy volatilization of fragrance substances, uneven fragrance volatilization and the like of the traditional perfuming core wire are effectively solved.
(3) The compound aroma-carrying core wire can also realize that one filter stick simultaneously carries two aromas, thereby enriching the smoking taste of cigarettes.
Detailed Description
The present invention is further described in detail by the following examples, which are not intended to limit the technical scope of the present invention, and all changes and equivalents made based on the teaching of the present invention shall fall within the scope of the present invention.
Example 1: preparing a mint-flavored composite flavor-carrying core wire:
(1) perfuming of core materials
Mixing and stirring 30 parts by weight of distilled water, 10 parts by weight of sodium carboxymethylcellulose, 20 parts by weight of propylene glycol, 1 part by weight of polyvinyl alcohol and 1 part by weight of polyacrylic acid uniformly, completely dissolving the materials to obtain a mixture A, and mixing and stirring menthol and the mixture A uniformly according to 60 parts by weight to 10 parts by weight to obtain a mixture B. And uniformly coating the mixture B on the cotton thread core material by using a multifunctional precise coating instrument.
(2) Preparing the slow-release agent
Mixing 30 parts by weight of polyethylene glycol-4000, 25 parts by weight of palmitic acid, 24 parts by weight of polycaprolactone and 17 parts by weight of starch, and stirring at a constant temperature of 50-60 ℃ at a stirring speed of 200-400 r/min until the mixture is completely dissolved to obtain the slow-release base material. And then uniformly mixing 55 parts by weight of slow-release base material, 15 parts by weight of propylene glycol, 1 part by weight of sodium polyacrylate and 4 parts by weight of guar gum to obtain the slow-release agent.
(3) Preparing composite incense-carrying core wire
And (3) uniformly coating the slow release agent obtained in the step (2) on the core material obtained in the step (1) by adopting a multifunctional precise coating instrument, and after the slow release agent is rapidly cooled and solidified, attaching the slow release agent to the surface of the perfuming core material to obtain the mint-flavor composite fragrance-carrying core wire.
Example 2: preparing orange-flavor composite fragrance-carrying core wire
(1) Perfuming of core materials
20 parts by weight of distilled water, 15 parts by weight of soybean protein, 25 parts by weight of propylene glycol, 3 parts by weight of polyvinyl alcohol and 2 parts by weight of sodium pyrophosphate are mixed and stirred uniformly, the materials are completely dissolved to obtain a mixture A, and the orange essence and the mixture A are mixed and stirred uniformly according to the weight ratio of 40 parts to 20 parts to obtain a mixture B. And uniformly coating the mixture B on the core material of the fiber wire by using a multifunctional precise coating instrument.
(2) Preparing the slow-release agent
Mixing 35 parts by weight of polyethylene glycol-4000, 30 parts by weight of palmitic acid, 20 parts by weight of polycaprolactone and 20 parts by weight of starch, and stirring at a constant temperature of 50-60 ℃ at a stirring speed of 200-400 r/min until the mixture is completely dissolved to obtain the slow-release base material. And then uniformly mixing 60 parts by weight of sustained-release base material, 15 parts by weight of glycerol, 1 part by weight of sodium pyrophosphate and 4 parts by weight of methylcellulose to obtain the sustained-release agent.
(3) Preparing composite incense-carrying core material
And (3) uniformly coating the slow-release agent obtained in the step (2) on the core material obtained in the step (1) by adopting a multifunctional precise coating instrument, and after the slow-release agent is rapidly cooled and solidified, attaching the slow-release agent to the surface of the perfuming core material to obtain the orange-flavor composite fragrance-carrying core wire.
Example 3: preparing double-flavor composite fragrance-carrying core wire
(1) Perfuming of core materials
Mixing and stirring uniformly 25 parts by weight of distilled water, 20 parts by weight of casein acrylic acid copolymer, 25 parts by weight of propylene glycol, 2 parts by weight of polyvinyl alcohol and 1 part by weight of sodium tripolyphosphate, completely dissolving the materials to obtain a mixture A, and mixing and stirring uniformly menthol and the mixture A according to the parts by weight of 20: 30 to obtain a mixture B. And uniformly coating the mixture B on a corrugated paper core material by using a multifunctional precise coating instrument.
(2) Preparing the slow-release agent
Mixing 35 parts by weight of polyethylene glycol-4000, 35 parts by weight of palmitic acid, 25 parts by weight of polycaprolactone and 20 parts by weight of starch, and stirring at a constant temperature of 50-60 ℃ at a stirring speed of 200-400 r/min until the mixture is completely dissolved to obtain the slow-release base material. And then uniformly mixing 60 parts by weight of slow-release base material, 15 parts by weight of sorbitol, 1 part by weight of polyacrylic acid, 4 parts by weight of chitosan and 15 parts by weight of orange essence to obtain the secondary perfuming slow-release agent.
(3) Preparing composite incense-carrying core material
And (3) uniformly coating the slow release agent obtained in the step (2) on the core material obtained in the step (1) by adopting a multifunctional precise coating instrument, and after the slow release agent is rapidly cooled and solidified, attaching the slow release agent to the surface of the aromatized core material to obtain the mint-flavored and orange-flavored double-flavor compound aroma-carrying core wire.
Comparative example 1
The preparation process is the same as the step (1) of the example 1, and the core material is perfumed without coating the slow release agent, so that the single fragrance-carrying core wire is prepared.
Comparative example 2
The preparation process is the same as the step (1) of the example 2, and the core material is perfumed without coating the slow release agent, so that the single fragrance-carrying core wire is prepared.
Comparative example 3
The preparation steps are as follows: mixing and stirring uniformly 25 parts by weight of distilled water, 20 parts by weight of casein acrylic acid copolymer, 25 parts by weight of propylene glycol, 2 parts by weight of polyvinyl alcohol and 1 part by weight of sodium tripolyphosphate, completely dissolving the materials to obtain a mixture A, and uniformly mixing 5 parts by weight of menthol, 15 parts by weight of orange flavor and 30 parts by weight of the mixture A to obtain a mixture B. The mixture B was uniformly coated on the core material by a multifunctional precision coater. And (4) after perfuming, obtaining a finished product, and preparing the single fragrance-carrying core wire without coating the slow release agent.
The prepared samples are respectively subjected to filter stick aroma retention time testing and related sensory evaluation, and the specific contents are as follows:
firstly, preparing a composite filter stick carrying a fragrant core line and a single filter stick carrying a fragrant core line:
when the core wire filter stick is formed, the composite/single aroma-carrying core wire is guided into the opened acetate fiber tow in the core wire positioning device, tightened through the bell mouth and wrapped by the forming paper, and the filter stick containing the composite/single aroma-carrying core wire is obtained. And replacing the cloud cigarette (soft) filter stick with a composite/single aroma-carrying core wire filter stick to obtain a composite/single aroma-carrying core wire cigarette sample.
The physical indexes of the filter rods are shown in table 1.
TABLE 1 physical index of composite/single flavor-carrying core filter stick
| Item | Unit of | Index requirement |
| Circumference of circle | mm | 24.0±0.15 |
| Pressure drop | Pa | 3600±270 |
| Length of | mm | 120±0.4 |
| Roundness degree | mm | ≤0.35 |
| Hardness of | ％ | ≥84.0 |
Second, sensory evaluation
The prepared cigarette samples are placed in a constant temperature and humidity adjusting box, namely the temperature is 22 ℃ and the humidity is 60%, and the cigarette samples are stored for 30 days, and a group of cigarettes are taken every 5 days for smoking evaluation. The evaluation was carried out by a group of 7 evaluation experts according to the standard GB5606.4-2005 "cigarette sensory technical requirements", and the evaluation results are shown in Table 1.
TABLE 1 sensory evaluation results of cigarettes
From the evaluation results of the embodiments 1 to 3, compared with a single flavor-carrying core wire, the compound flavor-carrying core wire filter stick has the advantages that the flavor is uniformly released, enough strength can be ensured, and better flavor can be obtained, compared with the comparative examples 1 to 3, the slow-release effect is poor due to serious flavor volatilization because the coating step of the slow-release agent is lacked, the flavor loss is fast, and the influence on the flavor and the flavor is large, the evaluation results show that whether the slow-release agent is coated on the core material in the process of preparing the flavor-carrying core wire or not can greatly influence on the final flavor and the flavor, the slow-release agent is coated on the flavor-carrying core wire under the condition of equal adding amount of the flavor, the sensory comfort degree of the compound flavor-carrying core wire is improved, and the flavor-holding time period is obviously prolonged.
Claims (3)
1. The composite flavor-carrying core wire for the cigarettes is characterized by being prepared by the following method:
(1) perfuming a core wire: weighing 20-30 parts by weight of distilled water, 10-20 parts by weight of adhesive, 20-30 parts by weight of propylene glycol, 1-5 parts by weight of polyvinyl alcohol and 1-2 parts by weight of dispersant, uniformly mixing, and completely dissolving to obtain a mixture A; uniformly mixing the tobacco essence and the mixture A according to the weight ratio of 20-60: 10-30 to obtain a mixture B; uniformly coating the mixture B on a core wire by using a multifunctional precise coating instrument to obtain a flavored core wire; the adhesive is one of sodium carboxymethylcellulose, casein acrylic acid copolymer, soybean protein or carboxymethyl cellulose; the dispersing agent is one of polyacrylic acid, sodium polyacrylate, sodium pyrophosphate or sodium tripolyphosphate;
(2) preparing a slow release agent: weighing polyethylene glycol-400030-40 parts by weight, palmitic acid 25-35 parts by weight, polycaprolactone 18-32 parts by weight and starch 15-25 parts by weight, uniformly mixing, and stirring at a constant temperature of 50-60 ℃ for 200-400 r/min until completely dissolving to obtain a slow-release base material; weighing 30-70 parts of slow-release base material, 1-10 parts of thickening agent, 10-30 parts of humectant and 1-2 parts of dispersing agent, and uniformly mixing to prepare a slow-release agent; the thickening agent is one of pectin, agar, gelatin, seaweed fat, carrageenan, dextrin, methylcellulose, starch derivatives, polyacrylamide, guar gum or chitosan; the humectant is one of glycerol, propylene glycol or sorbitol; the dispersing agent is one of polyacrylic acid, sodium polyacrylate, sodium pyrophosphate or sodium tripolyphosphate;
(3) preparing a composite fragrance-carrying core wire: and (3) uniformly coating the prepared slow release agent on the perfuming core wire obtained in the step (1) by adopting a multifunctional precise coating instrument, and quickly cooling and solidifying the prepared slow release agent to attach the slow release agent to the surface of the perfuming core wire to obtain the required composite perfuming core wire for the cigarettes.
2. The composite flavor-carrying core wire for tobacco as claimed in claim 1, wherein: the core wire is made of one of corrugated paper, glass paper, non-woven fabric, cotton paper, cotton thread, fiber thread, hemp thread or silk thread.
3. The composite flavor-carrying core wire for tobacco as claimed in claim 1, wherein: further, 1-20 parts of tobacco essence is added into the prepared slow release agent.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113817547A (en) * | 2021-11-03 | 2021-12-21 | 江苏大亚滤嘴材料有限公司 | A kind of hawthorn essence for cigarette and its application in filter rod |
| CN116289308A (en) * | 2023-01-09 | 2023-06-23 | 四川三联新材料有限公司 | A kind of scented film paper, its preparation method and its application in cigarette mouthpiece |
| CN116969188A (en) * | 2022-06-07 | 2023-10-31 | 云南云烁科技有限公司 | A method for adding fragrance to natural plant fiber core threads |
Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20000058785A (en) * | 2000-06-28 | 2000-10-05 | 이재덕 | Perfume / Deodorant Emission Sustained-release Aroma Gel Composition for Indoor Air Cleaners |
| US20070051383A1 (en) * | 2002-12-11 | 2007-03-08 | Woods Debra D | Smoking articles |
| CN101390657A (en) * | 2007-09-21 | 2009-03-25 | 武汉烟草(集团)有限公司 | Slow-release menthol cigarette filter rod and its production process |
| CN106387994A (en) * | 2016-08-31 | 2017-02-15 | 刘迎春 | Cigarette filter stick containing controlled-release spice core wire |
| CN107173848A (en) * | 2017-06-30 | 2017-09-19 | 云南恩典科技产业发展有限公司 | A kind of temperature becomes sustained release gel complex material and its application in cigarette filter rod |
| CN108095188A (en) * | 2018-01-25 | 2018-06-01 | 中国烟草总公司郑州烟草研究院 | A kind of core-skin type flavoring filter stick and preparation method thereof |
| CN108142993A (en) * | 2017-12-29 | 2018-06-12 | 玉溪笃行创新科技有限公司 | A kind of phase transformation filter stick additive and its preparation method and application |
| CN207836752U (en) * | 2018-01-05 | 2018-09-11 | 牡丹江卷烟材料厂有限责任公司 | A kind of fragrant core wire sustained-release gel filter stick of coaxial core load |
| CN207948889U (en) * | 2018-01-25 | 2018-10-12 | 中国烟草总公司郑州烟草研究院 | A kind of core-skin type flavoring filter stick |
| CN109007971A (en) * | 2018-09-26 | 2018-12-18 | 云南中烟新材料科技有限公司 | A kind of slow-release fragrance gel combination and preparation method thereof |
| CN110003980A (en) * | 2019-02-22 | 2019-07-12 | 深圳烟草工业有限责任公司 | A kind of cigarette minty note sustained release congealed fat and minty note cigarette filter rod |
-
2020
- 2020-07-11 CN CN202010665556.8A patent/CN111759002A/en active Pending
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20000058785A (en) * | 2000-06-28 | 2000-10-05 | 이재덕 | Perfume / Deodorant Emission Sustained-release Aroma Gel Composition for Indoor Air Cleaners |
| US20070051383A1 (en) * | 2002-12-11 | 2007-03-08 | Woods Debra D | Smoking articles |
| CN101390657A (en) * | 2007-09-21 | 2009-03-25 | 武汉烟草(集团)有限公司 | Slow-release menthol cigarette filter rod and its production process |
| CN106387994A (en) * | 2016-08-31 | 2017-02-15 | 刘迎春 | Cigarette filter stick containing controlled-release spice core wire |
| CN107173848A (en) * | 2017-06-30 | 2017-09-19 | 云南恩典科技产业发展有限公司 | A kind of temperature becomes sustained release gel complex material and its application in cigarette filter rod |
| CN108142993A (en) * | 2017-12-29 | 2018-06-12 | 玉溪笃行创新科技有限公司 | A kind of phase transformation filter stick additive and its preparation method and application |
| CN207836752U (en) * | 2018-01-05 | 2018-09-11 | 牡丹江卷烟材料厂有限责任公司 | A kind of fragrant core wire sustained-release gel filter stick of coaxial core load |
| CN108095188A (en) * | 2018-01-25 | 2018-06-01 | 中国烟草总公司郑州烟草研究院 | A kind of core-skin type flavoring filter stick and preparation method thereof |
| CN207948889U (en) * | 2018-01-25 | 2018-10-12 | 中国烟草总公司郑州烟草研究院 | A kind of core-skin type flavoring filter stick |
| CN109007971A (en) * | 2018-09-26 | 2018-12-18 | 云南中烟新材料科技有限公司 | A kind of slow-release fragrance gel combination and preparation method thereof |
| CN110003980A (en) * | 2019-02-22 | 2019-07-12 | 深圳烟草工业有限责任公司 | A kind of cigarette minty note sustained release congealed fat and minty note cigarette filter rod |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113817547A (en) * | 2021-11-03 | 2021-12-21 | 江苏大亚滤嘴材料有限公司 | A kind of hawthorn essence for cigarette and its application in filter rod |
| CN116969188A (en) * | 2022-06-07 | 2023-10-31 | 云南云烁科技有限公司 | A method for adding fragrance to natural plant fiber core threads |
| CN116289308A (en) * | 2023-01-09 | 2023-06-23 | 四川三联新材料有限公司 | A kind of scented film paper, its preparation method and its application in cigarette mouthpiece |
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