CN111657286A - 一种环保抗菌去味清新剂及其制备方法 - Google Patents
一种环保抗菌去味清新剂及其制备方法 Download PDFInfo
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/12—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
- A01N47/42—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides containing —N=CX2 groups, e.g. isothiourea
- A01N47/44—Guanidine; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
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- Animal Behavior & Ethology (AREA)
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
本发明公开了一种环保抗菌去味清新剂，包括(按质量分数计)：聚六亚甲基双胍0.03％‑0.1％、双癸基二甲基氯化铵、0.08％‑0.12％、柠檬酸0.01％‑0.12％、乙二胺四乙酸二钠0.001％‑0.003％、柠檬香精(食用级)0.8％‑1.2％、其余为纯化水、及与该配方相应的制备方法。与现有技术相比，本发明的有益效果是：本发明将柠檬酸、聚六亚甲基双胍、双癸基二甲基氯化铵以及食用级香精结合，既能杀菌抑菌，又能去味改味，同时配置方法简单易行且无毒无害，性能稳定长效抑菌又能清新改味、不燃、不爆、使用安全；而且价格适中制备方法简单，使用方便。
Description
技术领域
本发明涉及清新剂技术领域，具体为一种环保抗菌去味清新剂及其制备方法。
背景技术
据全国老龄办最新统计2020年，全国60岁以上老年人口将增加到2.55亿人左右，占总人口比重提升到17.8％左右；高龄老年人口(85岁以上)将增加到2900万人左右，独居和空巢老年人将增加到1.18亿人左右，老年扶养比例将提高到28％左右。
新兴养护院或护理院以老年人为目标。截至2019年6月底，中国共有各类养老机构2.99万个，社区养老服务机构和设施14.34万个，养老服务床位合计735.3万张。
老年人体味重，目前市场的84(次氯酸钠溶液)、来苏水、酒精等因刺激性气味易引起老年人不适，而空气清新剂无杀菌效果且只能掩盖异味，市场急需一种新的环保抑菌去味清新剂。
柠檬酸(CitricAcid，简称CA)是一种重要的有机酸，分子式C6H8O7，无色晶体，常含一分子结晶水，无臭，有很强的酸味，易溶于水，密度1.542g/cm3，熔点153℃(失水)，175℃以上分解释放出水及二氧化碳。柠檬酸易溶于水和乙醇，20℃时溶解度(w/w)为59％，其2％水溶液的pH为2.1。柠檬酸为食用酸类，可增强体内正常代谢，适当的剂量对人体无害。制备柠檬酸的原料都是来源于粮食，这是安全的食品级微生物。柠檬酸的使用对环境不会造成影响，在微生物以及热等作用下比较容易降解，其自身的螯合能力也比较强。
柠檬酸与80℃温度联合作用具有良好杀灭细菌芽孢的作用，有机酸可以进入细菌的细胞壁，使细菌内部和外部出现pH梯度变化，抑制细菌生长。常见的几种病原菌生长的适宜pH均是中性偏碱，如大肠杆菌适宜的pH为6.0-8.0，链球菌为6.0-7.5，而乳酸菌等益生菌宜于酸性环境繁殖。柠檬酸使胃肠道内pH下降，肠道内乳酸菌等益生菌得到良好的生长条件，从而维持消化道中微生物菌群的正常平衡。柠檬酸是一种天然防腐剂。由于柠檬酸可降低pH，有害微生物的增殖及毒素的产生受到抑制，有明显的防霉作用。
发明内容
针对上述技术中存在的不足之处，本发明提供环保抗菌去味清新剂，通过简单的制备方法，便能获取杀菌效果好、又能去味改味，而且无毒无害。
为了实现根据本发明的这些目的和其它优点，本发明通过以下技术方案实现：
一种环保抗菌去味清新剂，包括(按质量分数计)：
优选的是，所述的环保抗菌去味清新剂，包括(按质量分数计)：
优选的是，所述的环保抗菌去味清新剂，其特征在于，包括(按质量分数计)：
本发明还提出一种环保抗菌去味清新剂的制备方法，包括如下步骤：
将聚六亚甲基双胍、双癸基二甲基氯化铵、柠檬酸、乙二胺四乙酸二钠、柠檬香精(食用级)和纯化水加入反应釜中，搅拌均匀后，得到无色透明溶液，即为新型环保抑菌去味清新剂。
与现有技术相比，本发明的有益效果是：本发明将柠檬酸、聚六亚甲基双胍、双癸基二甲基氯化铵以及食用级香精结合，既能杀菌抑菌，又能去味改味，同时配置方法简单易行且无毒无害，性能稳定长效抑菌又能清新改味、不燃、不爆、使用安全；而且价格适中制备方法简单，使用方便。
具体实施方式
下面对本发明做进一步的详细说明，以令本领域技术人员参照说明书文字能够据以实施。
应当理解，本文所使用的诸如“具有”、“包含”以及“包括”术语并不排除一个或多个其它元件或其组合的存在或添加。
实施例1
一种环保抗菌去味清新剂，包括(按质量分数计)：
实施例2
一种环保抗菌去味清新剂，包括(按质量分数计)：
实施例3
一种环保抗菌去味清新剂，包括(按质量分数计)：
实施例4
一种环保抗菌去味清新剂，包括(按质量分数计)：
实施例1、2、3、4均通过以下步骤制备：
将聚六亚甲基双胍、双癸基二甲基氯化铵、柠檬酸、乙二胺四乙酸二钠、柠檬香精(食用级)和纯化水加入反应釜中，搅拌均匀后，得到无色透明溶液，即为新型环保抑菌去味清新剂。
本发明提出环保抗菌去味清新剂杀菌效果实验
实验准备：
大肠菌群、大肠杆菌培养液、环保抑菌去味清新剂溶液、大肠菌群快速检验纸片等。
实验过程：
1.大肠杆菌培养液接种大肠菌群，恒温培养。
2.将15组大肠菌群快速检验纸片通过大肠杆菌培养液接种大肠菌群，恒温培养24小时，检测大肠菌群数。
3.向其中12组大肠菌群快速检验纸片滴入环保抑菌去味清新剂溶液，恒温培养30min，检测15组大肠菌群快速检验纸片的大肠菌群数。
实验结果：
实验结论：环保抑菌去味清新剂作用30min的大肠菌群杀灭率大于99.9％。
本发明提出聚六亚甲基双胍性能比较
| 聚六亚甲基双胍 | 醛类 | 酚类 | 季铵盐类 | 含氯消毒剂 | 碘类 | 醇类 | |
| 杀菌效果 | 优 | 优 | 中 | 良 | 优 | 良 | 一般 |
| 黏膜刺激性 | 无 | 中 | 中 | 中 | 强 | 中 | 弱 |
| 腐蚀性 | 无 | 中 | 中 | 弱 | 强 | 中 | 无 |
| 毒性 | 无 | 中 | 中 | 中低 | 极强 | 中 | 弱 |
| 长效性 | 长 | 中 | 中 | 中 | 极短 | 中 | 短 |
| 气味 | 无 | 刺激 | 刺激 | 弱 | 极刺激 | 中 | 中 |
| 着色性 | 无 | 无 | 发黄 | 无 | 漂白 | 发黄 | 无 |
| 环境污染 | 无 | 中 | 中 | 中 | 强 | 中 | 微 |
聚六亚甲基双胍是一种环保型高分子聚合物杀菌抑菌剂，结构式：C3H6—NH—C(＝NH)—NH—C3H6。具有杀菌广谱；有效浓度低；作用速度快；性质稳定；易溶于水的优良性能；可在常温下使用；长期抑菌、无副作用；无腐蚀性；无色、无嗅；无毒；不燃、不爆、使用安全；价格适中；运输方便，可以说是最佳的杀菌剂。
作用方式、机理：
本品为多胍类高分子聚合物，在水溶液中能产生电离，它的亲水基部分含有强烈的正电性，吸附通常呈负电性的各类细菌、病毒，进入细胞膜，抑制膜内脂质体合成，造成菌体凋亡，达到最佳的杀菌效果。
性能优越性：
1、易溶于水；
2、水溶液无毒、无色、无嗅；
3、不燃、不爆；
4、有极强的杀灭细菌的能力，而且广谱、高效、并具有长期抑菌作用；
5、对各种材料无浸蚀作用；
6、无腐蚀性；
7、不含醛、碘、活性氯等有害物质。
毒性
1、1％聚六亚甲基双胍大于5000mg/kgBW属实际无毒级；
2、0.5％聚六亚甲基双胍眼刺激试验积分为3.0分属无刺激性；
3、0.5％聚六亚甲基双胍急性皮肤刺激试验积分为0分，属无刺激性；
4、0.5％聚六亚甲基双胍小鼠骨髓嗜多染红细胞微核试验为阴性，无致突变性；
5、0.5％聚六亚甲基双胍精子畸形试验结果为阴性；
6、0.5％聚六亚甲基双胍蓄积毒性试验为弱蓄积毒性；蓄积系数K>5。
聚六亚甲基双胍稳定性
1、0.5％聚六亚甲基双胍放置于37℃，相对湿度为75％～80％的环境中90天，其下降率为4.91％。
金属腐蚀性：0.5％聚六亚甲基双胍对不锈钢、铜无腐蚀，对碳钢、铝基本无腐蚀。
尽管已经示出和描述了本发明的实施例，对于本领域的普通技术人员而言，可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型，本发明的范围由所附权利要求及其等同物限定。
Claims (4)
1.一种环保抗菌去味清新剂，其特征在于，包括(按质量分数计)：
2.根据权利要求1所述的环保抗菌去味清新剂，其特征在于，包括(按质量分数计)：
3.根据权利要求1所述的环保抗菌去味清新剂，其特征在于，包括(按质量分数计)：
4.根据权利要求1至3任一项所述的环保抗菌去味清新剂的制备方法，其特征在于，包括如下步骤：
将聚六亚甲基双胍、双癸基二甲基氯化铵、柠檬酸、乙二胺四乙酸二钠、柠檬香精和纯化水加入反应釜中，搅拌均匀后，得到无色透明溶液，即为新型环保抑菌去味清新剂。
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