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CN111284097A - Far infrared geothermal packaging composite film and processing method thereof - Google Patents

Far infrared geothermal packaging composite film and processing method thereof Download PDF

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Publication number
CN111284097A
CN111284097A CN201910940509.7A CN201910940509A CN111284097A CN 111284097 A CN111284097 A CN 111284097A CN 201910940509 A CN201910940509 A CN 201910940509A CN 111284097 A CN111284097 A CN 111284097A
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CN
China
Prior art keywords
resin
eva
geothermal
film
composite film
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Pending
Application number
CN201910940509.7A
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Chinese (zh)
Inventor
卞姣
王军林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
YIXING WANGZHE LAMINATING FILM CO Ltd
Original Assignee
YIXING WANGZHE LAMINATING FILM CO Ltd
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Priority to CN201910940509.7A priority Critical patent/CN111284097A/en
Publication of CN111284097A publication Critical patent/CN111284097A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00Layered products comprising a layer of synthetic resin
    • B32B27/06Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material
    • B32B27/08Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C69/00Combinations of shaping techniques not provided for in a single one of main groups B29C39/00 - B29C67/00, e.g. associations of moulding and joining techniques; Apparatus therefore
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00Layered products comprising a layer of synthetic resin
    • B32B27/18Layered products comprising a layer of synthetic resin characterised by the use of special additives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00Layered products comprising a layer of synthetic resin
    • B32B27/30Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers
    • B32B27/306Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers comprising vinyl acetate or vinyl alcohol (co)polymers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00Layered products comprising a layer of synthetic resin
    • B32B27/36Layered products comprising a layer of synthetic resin comprising polyesters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29LINDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
    • B29L2007/00Flat articles, e.g. films or sheets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29LINDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
    • B29L2009/00Layered products
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2255/00Coating on the layer surface
    • B32B2255/10Coating on the layer surface on synthetic resin layer or on natural or synthetic rubber layer
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2255/00Coating on the layer surface
    • B32B2255/26Polymeric coating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00Properties of the layers or laminate
    • B32B2307/20Properties of the layers or laminate having particular electrical or magnetic properties, e.g. piezoelectric
    • B32B2307/206Insulating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00Properties of the layers or laminate
    • B32B2307/70Other properties
    • B32B2307/714Inert, i.e. inert to chemical degradation, corrosion

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Laminated Bodies (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention provides a far infrared geothermal packaging composite film and a processing method thereof, wherein the composite film is formed by laminating and compounding an EVA hot melting layer and a PET substrate film which is treated by corona, and a tackifying coating is coated on the surface of the EVA hot melting layer; the EVA hot-melt layer consists of EVA, polyolefin resin and an anti-aging agent, wherein the mass ratio of the EVA resin to the polyolefin resin is 1-4: 1, and the mass fraction of the anti-aging agent is 0.1-2% of the total mass of the resin; the tackifying coating is a solution of graft modified hydrogenated tackifying resin. The invention improves the peeling strength of the original geothermal film, improves the anti-aging performance, selects the polyolefin material as the modified material, has excellent comprehensive properties of high strength, high toughness, high electrical insulation, high chemical corrosion resistance and the like, improves the melting point of the geothermal film packaging film, and is not easy to generate the conditions of bubbles, delamination and the like in later use.

Description

Far infrared geothermal packaging composite film and processing method thereof
Technical Field
The invention relates to the technical field of composite films, in particular to a far infrared geothermal packaging composite film and a processing method thereof.
Background
The geothermal film heating is one of the advanced heating modes in the world at present, and the geothermal film heating is a high-tech product which takes electric power as energy and conducts heat by infrared radiation, thereby saving energy, protecting environment, and reducing carbon and emission. Is the most comfortable and healthy heating method in various heating products in the development of human society so far. The geothermal film heating system has the advantages of environmental protection, energy saving, material saving, money saving, safety and the like.
At present, most of geothermal film packaging films are formed by compounding polyester films and common hot melt adhesives, and the problems of low peeling strength, easy delamination, low melting point, easy aging, bubbles in the use process and the like exist. The service life of the geothermal film is greatly reduced due to the above conditions, so that the use cost is increased, and certain potential safety hazards exist. On the basis, a novel geothermal film packaging film which is high in peel strength, high in melting point and not prone to aging and delamination needs to be developed.
Disclosure of Invention
The invention aims to solve the problems of the prior art and provides a far infrared geothermal packaging composite film and a processing method thereof, which improve the peeling strength of the original geothermal film and improve the ageing resistance, select polyolefin materials as modified materials, have excellent comprehensive properties such as high strength, high toughness, high electric insulation, high chemical corrosion resistance and the like, improve the melting point of the geothermal film packaging film, and are not easy to generate bubbles, delamination and the like in later use.
The invention provides a far infrared geothermal packaging composite film, which is formed by laminating and compounding an EVA hot melting layer and a PET substrate film subjected to corona treatment, wherein the surface of the EVA hot melting layer is coated with a tackifying coating; the EVA hot-melt layer consists of EVA, polyolefin resin and an anti-aging agent, wherein the mass ratio of the EVA resin to the polyolefin resin is 1-4: 1, and the mass fraction of the anti-aging agent is 0.1-2% of the total mass of the resin; the tackifying coating is a solution of graft modified hydrogenated tackifying resin.
Further improved, the thickness of the PET base material film is 50-150 μm; the thickness of the EVA hot melting layer is 50-150 μm.
In a further improvement, the polyolefin resin is one or more of polyvinyl chloride, polyethylene, polypropylene and polystyrene.
The further improvement is that the anti-aging agent is an inorganic anti-aging agent, and comprises talcum powder, calcium carbonate, titanium dioxide and carbon black.
Further improved, the anti-aging agent is an organic anti-aging agent, and comprises salicylic acid esters, benzophenones, benzotriazoles and substituted acrylonitrile.
The invention also provides a processing method of the far infrared geothermal packaging composite film, which is characterized by mainly comprising the following steps:
1) preparing EVA resin and polyolefin resin in a mass ratio of 1-4: 1, and uniformly mixing the EVA resin and the polyolefin resin with an anti-aging agent accounting for 0.1-2% of the total weight of the resin by a high-speed mixer to obtain a mixed resin solution;
2) the PET substrate film is subjected to low-temperature plasma corona surface treatment to improve the surface tension of the PET substrate film;
3) melting and extruding the mixed resin solution obtained in the step 1) through an extruder to obtain an EVA hot melt layer, and laminating and compounding the EVA hot melt layer with the PET substrate film subjected to corona surface treatment in the step 2);
4) coating a tackifying coating on the EVA hot melt layer by gluing and roller coating, and drying to obtain the composite film with a three-layer structure.
The invention has the beneficial effects that:
1. the peeling strength of the original geothermal film is improved, the ageing resistance is improved, the polyolefin material is selected as the modified material, the modified geothermal film has excellent comprehensive properties such as high strength, high toughness, high electric insulation and high chemical corrosion resistance, the melting point of the geothermal film packaging film is improved, and the conditions such as bubbles and delamination are not easy to occur in later use.
2. And the adhesion strength of the film and heating materials such as graphene is enhanced by adding the tackifying coating.
Detailed Description
The present invention will be further described with reference to the following embodiments.
The invention provides a specific implementation mode of a far infrared geothermal packaging composite film, which comprises the following steps: the composite film is formed by laminating and compounding an EVA hot melting layer and a PET substrate film which is subjected to corona treatment, wherein the surface of the EVA hot melting layer is coated with a tackifying coating; the EVA hot-melt layer consists of EVA, polyolefin resin and an anti-aging agent, wherein the mass ratio of the EVA resin to the polyolefin resin is 2:1, and the mass fraction of the anti-aging agent is 0.2% of the total mass of the resin; the tackifying coating is a solution of graft modified hydrogenated tackifying resin. The thickness of the PET base material film is 75 μm; the thickness of the EVA hot melt layer is 75 μm. The polyolefin resin is LDPE.
The processing method of the novel composite membrane comprises the following steps:
(1) preparing anti-aging EVA/polyolefin resin: the anti-aging agent is benzophenone anti-aging agent, and the polyolefin resin is LDPE. The mass ratio of the EVA resin to the LDPE resin is 2:1, and the anti-aging agent is 0.2% (mass fraction of the total weight of the resin), and the EVA resin and the LDPE resin are uniformly mixed by a high-speed mixer.
(2) Surface treatment of the PET base material film: the PET substrate film needs to be processed by low-temperature plasma corona treatment to improve the surface tension. The thickness of the PET substrate film was 75 μm.
(3) And (3) performing melt extrusion on the anti-aging EVA/polyolefin resin through an extruder to obtain an anti-aging EVA/polyolefin film with the thickness of 75 microns, and laminating and compounding the anti-aging EVA/polyolefin film with the modified PET substrate film. And obtaining the anti-aging (EVA & polyolefin)/PET two-layer structure composite film.
(4) The hot-melt resin surface of the composite film is coated with a tackifying coating through a gluing roller and is dried through an oven.
(5) And finally, trimming and winding.
The following table shows the performance test data of the novel far infrared heat-seal packaging film:
Figure BDA0002222729200000031
from the test data it can be seen that:
1. the initial peel strength and the heat seal peel strength of the novel composite film are respectively 8N/3cm and 50N/3cm, which are far higher than the standards (3N/3cm and 25N/3cm) of the common composite film.
2. The yellowing index of the novel composite film in an ultraviolet radiation test is 1.8, which is far lower than the standard of the old and foreign index of 5. As further explained above, the novel composite film improves the initial peel strength of the original geothermal film, enhances the adhesive strength of the film and heating materials such as graphene, improves the anti-aging performance, and is more suitable for long-term use.
While the invention has been described in terms of its preferred embodiments, it will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention.

Claims (6)

1. A far infrared geothermal packaging composite film is characterized in that: the PET film is formed by laminating and compounding an EVA hot melting layer and a PET substrate film which is subjected to corona treatment, and a tackifying coating is coated on the surface of the EVA hot melting layer; the EVA hot-melt layer consists of EVA, polyolefin resin and an anti-aging agent, wherein the mass ratio of the EVA resin to the polyolefin resin is 1-4: 1, and the mass fraction of the anti-aging agent is 0.1-2% of the total mass of the resin; the tackifying coating is a solution of graft modified hydrogenated tackifying resin.
2. The far infrared geothermal packaging composite film according to claim 1, wherein: the thickness of the PET base material film is 50-150 μm; the thickness of the EVA hot melting layer is 50-150 mu m.
3. The far infrared geothermal packaging composite film according to claim 1, wherein: the polyolefin resin is one or more of polyvinyl chloride, polyethylene, polypropylene and polystyrene.
4. The far infrared geothermal packaging composite film according to claim 1, wherein: the anti-aging agent is an inorganic anti-aging agent and comprises talcum powder, calcium carbonate, titanium dioxide and carbon black.
5. The far infrared geothermal packaging composite film according to claim 1, wherein: the anti-aging agent is an organic anti-aging agent, and comprises salicylic acid esters, benzophenones, benzotriazoles and substituted acrylonitrile.
6. A processing method of a far infrared geothermal packaging composite film is characterized by mainly comprising the following steps:
1) preparing EVA resin and polyolefin resin in a mass ratio of 1-4: 1, and uniformly mixing the EVA resin and the polyolefin resin with an anti-aging agent accounting for 0.1-2% of the total weight of the resin by a high-speed mixer to obtain a mixed resin solution;
2) the PET substrate film is subjected to low-temperature plasma corona surface treatment to improve the surface tension of the PET substrate film;
3) melting and extruding the mixed resin solution obtained in the step 1) through an extruder to obtain an EVA hot melt layer, and laminating and compounding the EVA hot melt layer with the PET substrate film subjected to corona surface treatment in the step 2);
4) coating a tackifying coating on the EVA hot melt layer by gluing and roller coating, and drying to obtain the composite film with a three-layer structure.
CN201910940509.7A 2019-09-30 2019-09-30 Far infrared geothermal packaging composite film and processing method thereof Pending CN111284097A (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1555396A (en) * 2001-09-19 2004-12-15 埃克森美孚化学专利公司 Adhesive components and methods of manufacture
CN1761729A (en) * 2003-03-20 2006-04-19 埃克森美孚化学专利公司 Adhesive compositions and method for selection thereof
CN105563981A (en) * 2016-01-25 2016-05-11 宜兴市王者塑封有限公司 Composite film for geothermal film packaging and preparation method thereof
CN106947099A (en) * 2016-11-30 2017-07-14 宜兴市王者塑封有限公司 A kind of ink print product composite membrane of high compound fastness and preparation method thereof
CN107254023A (en) * 2017-06-26 2017-10-17 四会市邦得利化工有限公司 Preparation method and application of graft modified tackifying resin
CN208327900U (en) * 2018-04-16 2019-01-04 东莞市华一新材料科技有限公司 A kind of PET pre-coating film
CN110172306A (en) * 2019-06-11 2019-08-27 北京康得新功能材料有限公司 A kind of carve characters pre-coating film and preparation process for in-mould injection

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1555396A (en) * 2001-09-19 2004-12-15 埃克森美孚化学专利公司 Adhesive components and methods of manufacture
CN1761729A (en) * 2003-03-20 2006-04-19 埃克森美孚化学专利公司 Adhesive compositions and method for selection thereof
CN105563981A (en) * 2016-01-25 2016-05-11 宜兴市王者塑封有限公司 Composite film for geothermal film packaging and preparation method thereof
CN106947099A (en) * 2016-11-30 2017-07-14 宜兴市王者塑封有限公司 A kind of ink print product composite membrane of high compound fastness and preparation method thereof
CN107254023A (en) * 2017-06-26 2017-10-17 四会市邦得利化工有限公司 Preparation method and application of graft modified tackifying resin
CN208327900U (en) * 2018-04-16 2019-01-04 东莞市华一新材料科技有限公司 A kind of PET pre-coating film
CN110172306A (en) * 2019-06-11 2019-08-27 北京康得新功能材料有限公司 A kind of carve characters pre-coating film and preparation process for in-mould injection

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Application publication date: 20200616