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CN119164801A - A method for enhancing the contrast of fatigue microcracks in metal materials - Google Patents

A method for enhancing the contrast of fatigue microcracks in metal materials Download PDF

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Publication number
CN119164801A
CN119164801A CN202411220215.4A CN202411220215A CN119164801A CN 119164801 A CN119164801 A CN 119164801A CN 202411220215 A CN202411220215 A CN 202411220215A CN 119164801 A CN119164801 A CN 119164801A
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fatigue
crack
enhancing
contrast
metal materials
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Inventor
叶序彬
郭宁
鲁原
卢紫烨
王盼
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AECC Beijing Institute of Aeronautical Materials
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AECC Beijing Institute of Aeronautical Materials
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Publication of CN119164801A publication Critical patent/CN119164801A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/32Investigating strength properties of solid materials by application of mechanical stress by applying repeated or pulsating forces
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01BMEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
    • G01B11/00Measuring arrangements characterised by the use of optical techniques
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84Systems specially adapted for particular applications
    • G01N21/88Investigating the presence of flaws or contamination
    • G01N21/91Investigating the presence of flaws or contamination using penetration of dyes, e.g. fluorescent ink
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/02Details
    • G01N3/06Special adaptations of indicating or recording means
    • G01N3/068Special adaptations of indicating or recording means with optical indicating or recording means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0001Type of application of the stress
    • G01N2203/0005Repeated or cyclic
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058Kind of property studied
    • G01N2203/0069Fatigue, creep, strain-stress relations or elastic constants
    • G01N2203/0073Fatigue
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/06Indicating or recording means; Sensing means
    • G01N2203/0641Indicating or recording means; Sensing means using optical, X-ray, ultraviolet, infrared or similar detectors
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/06Indicating or recording means; Sensing means
    • G01N2203/067Parameter measured for estimating the property
    • G01N2203/0682Spatial dimension, e.g. length, area, angle

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)
  • Investigating Materials By The Use Of Optical Means Adapted For Particular Applications (AREA)

Abstract

本发明提供一种增强金属材料疲劳微裂纹显示对比度方法,该方法包括如下步骤:步骤1、试样准备;步骤2、表面处理;步骤3、疲劳试验。本发明针对疲劳裂纹扩展速率试验提出一种有效增强金属材料疲劳微裂纹显示对比度方法。在现有疲劳微裂纹的测量方法中,绝大多数采用高清显微镜/摄像机的技术方案,依靠目视观察从材料表面寻找裂纹,由于材料表面一般存在表面加工纹理或者划痕,受到上述影响易导致判断裂纹困难和费时费力的技术缺陷,甚至产生误判。The present invention provides a method for enhancing the contrast of fatigue microcracks in metal materials, and the method comprises the following steps: step 1, sample preparation; step 2, surface treatment; step 3, fatigue test. The present invention proposes a method for effectively enhancing the contrast of fatigue microcracks in metal materials for fatigue crack growth rate test. In the existing fatigue microcrack measurement methods, most of them adopt the technical solution of high-definition microscope/camera, and rely on visual observation to find cracks from the surface of the material. Since the surface of the material generally has surface processing textures or scratches, the above-mentioned influence can easily lead to technical defects such as difficulty in judging cracks and time-consuming and labor-intensive, and even misjudgment.

Description

Method for enhancing fatigue microcrack display contrast of metal material
Technical Field
The invention relates to the technical field of metal material fatigue performance detection, in particular to a method for enhancing the display contrast of fatigue microcracks of a metal material.
Background
The fatigue crack propagation rate test is a test mode for researching the fatigue fracture characteristics of a material by measuring the length of a fatigue crack generated by a sample under the set alternating load in real time. When the fatigue crack growth rate test is performed, in order to ensure the accuracy of the calculation result, it is necessary to precisely measure the crack length during the fatigue crack growth. In the indirect measurement method, the compliance method and the potential method are based on the variation of other physical parameters caused by crack growth, and the average size of crack growth, the range delta K of crack intensity factors and the crack growth rate are obtained through indirect calculation, but the two operation procedures are relatively complex, so that the method is suitable for high-temperature environment tests, and meanwhile, too many variables are introduced during measurement and are sensitive to the crack length and during calculation, so that larger deviation is generated between a calculated value and a true value. In the direct measurement method, a high-definition microscope/camera is adopted to directly read an image scale by visual inspection to obtain the crack propagation size, the operation procedure is simple and convenient, a large number of applications are obtained in room temperature environment test, but the surface of the metal material is generally provided with surface processing textures or scratches, at the moment, the crack morphology is similar to the textures and scratches, the technical defects of difficult crack identification, time and labor waste are often caused, and sometimes even misjudgment is generated. Therefore, there is a need for a method of enhancing fatigue microcrack display contrast to avoid the effects of surface texture or scratches and meet the needs of laboratory accurate measurements.
In the aspect of fatigue crack tracking and monitoring, a part of patents have adopted related technical means to achieve the above-mentioned aim. Patent CN104181225 describes a fatigue crack tracking and monitoring device and monitoring method for steel bridge deck slab, the method sprays contrast enhancer and black water magnetic suspension on the monitored steel bridge deck slab, the magnetic powder flaw detection method is adopted to display the shape and position of the fatigue crack, patent 108760546 describes a fatigue crack propagation rate measuring method based on infrared thermal imaging technology, the method sprays black matt paint on a sample meeting the required geometric dimension and surface roughness, the purpose is to improve the emissivity of the sample surface, the method is suitable for the infrared thermal imaging method to record the temperature field evolution process of the fatigue crack tip area in real time and automatically identify the crack tip position, patent CN110295340 describes a crack monitoring sensor based on plasma spraying, the preparation and monitoring method thereof, the method adopts plasma spraying to integrate an insulating substrate layer, a damage sensor and a packaging protection layer on the surface of a target monitoring structure, the crack length of the detection structure is determined by measuring the potential difference of the two ends of the crack surface of the monitoring structure, and patent CN110926972 describes a micro fatigue surface detecting method and system, the method adopts binary silicon rubber to mutually contact the contact part and the crack contact part is determined by observing the contact part of the film. In summary, the above patent uses related technical means and a matched detection method to improve the crack display contrast, so as to accurately measure the crack size.
Disclosure of Invention
The invention aims to provide a method for enhancing the fatigue microcrack display contrast of a metal material so as to solve the technical problems.
The technical scheme of the invention is as follows:
a method for enhancing fatigue microcrack display contrast of a metal material is provided, which comprises the following steps:
Step 1, sample preparation
Machining the plate-shaped sample to form a crack, and determining that the tip of the crack meets the test requirement
Polishing and burnishing the surface of the plate-shaped sample to ensure that the surface roughness meets the fatigue crack growth rate test requirement;
Step 2, surface treatment
And spraying black light-absorbing paint on the surface of the sample to be tested to form a uniform black light-absorbing coating so as to absorb visible light emitted by the light source and realize a strong light-absorbing effect.
Step 3, fatigue test
Mounting a sample on a fatigue testing machine by adopting a clamp matched with the sample, adjusting a light source to a corresponding position, and adjusting the focal length of a lens of a high-definition camera until the crack tip outline is clearly observed;
and 4, performing fatigue crack growth rate test on the sample.
Further, the light absorbing coating is a strong light absorbing coating.
Further, the machined crack is located in the middle of the plate-like specimen.
Further, the lapping and polishing is oriented in a direction perpendicular to the crack propagation path.
Further, the thickness of the black light absorption coating is 10-20 mu m. When the crack is not expanded, the strong light absorption coating absorbs visible light or ultraviolet rays emitted by a strong light source, and the image shows a black background.
Further, the light absorbing coating is provided with a fluorescent agent, and the light source is ultraviolet light
When the crack propagates, the strong light absorption coating tears along with the crack, and visible light generates diffuse reflection at the crack and is captured by the high-definition camera, so that a bright line which is strongly contrasted with the background and is overlapped with the crack is formed.
Further, the light source is a strong light source.
Further, the light source is a direct or oblique light sample surface.
The method has the advantage that the method is used for effectively enhancing the fatigue microcrack display contrast of the metal material aiming at the fatigue crack propagation rate test. In the existing fatigue microcrack measuring method, most of the technical schemes of a high-definition microscope/camera are adopted, the cracks are found from the surface of the material by means of visual observation, and as the surface of the material is generally provided with surface processing textures or scratches, the technical defects of difficult crack judgment, time and labor waste and even misjudgment are caused due to the influence. The method adopts a method of spraying a thin and uniform black strong light absorption coating or a fluorescent agent coating and the black strong light absorption coating on the surface of a material, when a crack is expanded, the coating tears along with the crack, a bright line which is strongly contrasted with the background and overlapped with the crack position is generated through a strong light source, the crack position and the crack size are judged according to the bright line, and the measurement precision is improved to accurately obtain the crack expansion rate data.
Detailed Description
Indeed, many different examples may be described and should not be construed as limited to the examples set forth herein. Rather, these examples are described so that this disclosure will be thorough and complete, and will fully convey the scope of the disclosure to those skilled in the art.
A method for enhancing fatigue microcrack display contrast of a metal material is provided, which comprises the following steps:
Step 1, sample preparation
Machining the plate-shaped sample to form a crack, and determining that the tip of the crack meets the test requirement
Polishing and burnishing the surface of the plate-shaped sample to ensure that the surface roughness meets the fatigue crack growth rate test requirement;
Step 2, surface treatment
And spraying black light-absorbing paint on the surface of the sample to be tested to form a uniform black light-absorbing coating so as to absorb visible light emitted by the light source and realize a strong light-absorbing effect.
Step 3, fatigue test
Mounting a sample on a fatigue testing machine by adopting a clamp matched with the sample, adjusting a light source to a corresponding position, and adjusting the focal length of a lens of a high-definition camera until the crack tip outline is clearly observed;
and 4, performing fatigue crack growth rate test on the sample.
The light absorbing coating is a strong light absorbing coating.
The machined crack is located in the middle of the plate-like specimen.
The lapping and polishing is oriented in a direction perpendicular to the crack propagation path.
The thickness of the black light absorption coating is 10-20 mu m. When the crack is not expanded, the strong light absorption coating absorbs visible light or ultraviolet rays emitted by a strong light source, and the image shows a black background.
The light absorbing coating is provided with a fluorescent agent, and the light source is ultraviolet light
When the crack propagates, the strong light absorption coating tears along with the crack, and visible light generates diffuse reflection at the crack and is captured by the high-definition camera, so that a bright line which is strongly contrasted with the background and is overlapped with the crack is formed.
The light source is a strong light source.
The light source is directly or obliquely irradiated to the surface of the sample.
The following parameters of embodiment one may also be preferred:
Before the fatigue crack growth rate test was conducted by the method of this example, 7075 aluminum alloy was processed according to ASTM647 into a plate-like specimen having a length of 300.04mm, a width of 100.06mm, and a thickness of 4.76mm, and an artificial crack having a kerf radius of 3.06mm was processed at the center of the specimen.
The surface roughness Ra of the sample is less than 1.6 mu m;
and (3) mounting the test sample on the fatigue testing machine by adopting a proper clamp, adjusting a strong light source to a proper position, and adjusting the focal length of a lens of the high-definition camera until the tip outline of the artificial crack is clearly observed in the acquired image, wherein the rest background except the artificial crack is black.
The fatigue loading adopts stress ratio R=0.1, the pre-cracking process adopts a load-reducing mode, the pre-cracking process is ended when the pre-cracking size is set to be 3mm, when the cyclic loading crack is expanded, the strong light absorption coating can be torn along with the expansion of the crack tip, at the moment, the visible light generated by the strong light source generates diffuse reflection at the crack and is captured by the high-definition camera, a bright line which is strong in contrast with the background and overlapped with the crack is formed, and the crack expansion size is monitored and measured in real time after the image is acquired by the high-definition camera. And after prefabricating the crack, adopting a banner load loading mode, adopting the same method to monitor and measure the crack expansion size, and calculating the crack expansion rate in real time.
The parameters of the second embodiment can also be optimized
Before the fatigue crack growth rate test was conducted by the method of this example, a TC4 titanium alloy was processed according to ASTM647 into a plate-like specimen having a length of 300.14mm, a width of 100.16mm, and a thickness of 4.74mm, and an artificial crack having a kerf radius of 3.02mm was machined in the center of the specimen.
The surface roughness Ra of the sample is less than 1.6 mu m;
and (3) mounting the test sample on the fatigue testing machine by adopting a proper clamp, adjusting a strong light source to a proper position, and adjusting the focal length of a lens of the high-definition camera until the tip outline of the artificial crack is clearly observed in the acquired image, wherein the rest background except the artificial crack is black.
The fatigue loading adopts stress ratio R=0.1, the pre-cracking process is finished when the pre-cracking size is set to be 3mm in a load-reducing mode, when the cyclic loading crack is expanded, the fluorescent agent coating and the strong light absorption coating are torn along with the expansion of the crack tip, ultraviolet rays generated by a strong light source generate fluorescence at the crack to form a bright line which is strongly contrasted with the background and overlapped with the crack, and the crack expansion size is monitored and measured in real time after the image is acquired by a high-definition camera. And after prefabricating the crack, adopting a banner load loading mode, adopting the same method to monitor and measure the crack expansion size, and calculating the crack expansion rate in real time.
The description of the different advantageous arrangements has been presented for purposes of illustration and description, but is not intended to be exhaustive or limited to the examples in the form disclosed. Many modifications and variations will be apparent to those of ordinary skill in the art. Additionally, the different advantageous examples may describe different advantages compared to other advantageous examples. The example or examples selected are chosen and described in order to best explain the principles of the examples, the practical application, and to enable others of ordinary skill in the art to understand the disclosure for various examples with various modifications as are suited to the particular use contemplated.

Claims (8)

1.一种增强金属材料疲劳微裂纹显示对比度方法,其特征在于,包括如下步骤:1. A method for enhancing the contrast of fatigue microcracks in metal materials, comprising the following steps: 步骤1、试样准备Step 1: Sample preparation 对板状试样进行机加工,加工出裂纹,并且确定裂纹尖端符合试验要求Machining of plate specimens to produce cracks and confirming that the crack tip meets the test requirements 对板状试样表面进行打磨和抛光,使得表面粗糙度符合疲劳裂纹扩展速率试验需求;Grind and polish the surface of the plate specimen to make the surface roughness meet the requirements of the fatigue crack growth rate test; 步骤2、表面处理Step 2: Surface treatment 在待测试样表面喷涂黑色吸光涂料,形成均匀的黑色吸光涂层,以吸收光源发射的可见光;实现强吸光效果。Spray black light-absorbing paint on the surface of the sample to be tested to form a uniform black light-absorbing coating to absorb the visible light emitted by the light source; achieving a strong light-absorbing effect. 步骤3、疲劳试验Step 3: Fatigue test 在疲劳试验机上采用与试样适配的夹具安装试样,并将光源调至对应位置,并调整高清摄像机的镜头焦距直至清晰观察到所述裂纹尖端轮廓;The sample is mounted on a fatigue testing machine using a fixture adapted to the sample, the light source is adjusted to a corresponding position, and the lens focal length of the high-definition camera is adjusted until the crack tip profile is clearly observed; 步骤4、对所述试样进行疲劳裂纹扩展速率试验。Step 4: performing a fatigue crack growth rate test on the sample. 2.根据权利要求1所述的一种增强金属材料疲劳微裂纹显示对比度方法,其特征在于:所述吸光涂层为强吸光涂层。2. A method for enhancing the contrast of fatigue microcrack display of metal materials according to claim 1, characterized in that the light-absorbing coating is a strong light-absorbing coating. 3.根据权利要求1所述的一种增强金属材料疲劳微裂纹显示对比度方法,其特征在于:所述机加工的裂纹位于所述板状试样的中部。3. A method for enhancing the contrast of fatigue microcracks in metal materials according to claim 1, characterized in that the machined crack is located in the middle of the plate-shaped specimen. 4.根据权利要求1所述的一种增强金属材料疲劳微裂纹显示对比度方法,其特征在于:所述打磨和抛光的方位为沿垂直于裂纹扩展路径方向进行。4. A method for enhancing the contrast of fatigue microcracks in metal materials according to claim 1, characterized in that the grinding and polishing are carried out in a direction perpendicular to the crack propagation path. 5.根据权利要求1所述的一种增强金属材料疲劳微裂纹显示对比度方法,其特征在于:所述黑色吸光涂层厚度为10~20μm。当裂纹未扩展时,所述强吸光涂料吸收强光源发射的可见光或紫外线,图像显示黑色背景。5. A method for enhancing the contrast of fatigue microcracks in metal materials according to claim 1, characterized in that the thickness of the black light-absorbing coating is 10-20 μm. When the crack does not expand, the strong light-absorbing coating absorbs visible light or ultraviolet light emitted by a strong light source, and the image displays a black background. 6.根据权利要求1所述的一种增强金属材料疲劳微裂纹显示对比度方法,其特征在于:所述吸光涂层中具有荧光剂,所述光源为紫外光。6. A method for enhancing the contrast of fatigue microcrack display of metal materials according to claim 1, characterized in that: the light-absorbing coating contains a fluorescent agent and the light source is ultraviolet light. 7.根据权利要求1所述的一种增强金属材料疲劳微裂纹显示对比度方法,其特征在于:所述光源为强光源。7. A method for enhancing the contrast of fatigue microcrack display of metal materials according to claim 1, characterized in that the light source is a strong light source. 8.根据权利要求1所述的一种增强金属材料疲劳微裂纹显示对比度方法,其特征在于:所述光源为直射或斜射试样表面。8. A method for enhancing the contrast of fatigue microcrack display of metal materials according to claim 1, characterized in that the light source is directly or obliquely irradiated on the sample surface.
CN202411220215.4A 2024-09-02 2024-09-02 A method for enhancing the contrast of fatigue microcracks in metal materials Pending CN119164801A (en)

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