CN1188035C - Wax emulsion for treating seeds and its preparation and usage - Google Patents
Wax emulsion for treating seeds and its preparation and usage Download PDFInfo
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- CN1188035C CN1188035C CNB991205189A CN99120518A CN1188035C CN 1188035 C CN1188035 C CN 1188035C CN B991205189 A CNB991205189 A CN B991205189A CN 99120518 A CN99120518 A CN 99120518A CN 1188035 C CN1188035 C CN 1188035C
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- seed
- wax emulsion
- wax
- emulsion
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- 239000000839 emulsion Substances 0.000 title claims abstract description 58
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 238000000034 method Methods 0.000 claims abstract description 15
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 14
- 239000003337 fertilizer Substances 0.000 claims abstract description 13
- 239000011347 resin Substances 0.000 claims abstract description 13
- 229920005989 resin Polymers 0.000 claims abstract description 13
- 230000000844 anti-bacterial effect Effects 0.000 claims abstract description 4
- 239000003899 bactericide agent Substances 0.000 claims abstract description 4
- 239000001993 wax Substances 0.000 claims description 54
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 34
- 239000000203 mixture Substances 0.000 claims description 16
- 239000003921 oil Substances 0.000 claims description 15
- 239000000463 material Substances 0.000 claims description 14
- 239000005648 plant growth regulator Substances 0.000 claims description 14
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims description 12
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 claims description 12
- 235000019837 monoammonium phosphate Nutrition 0.000 claims description 12
- 239000003905 agrochemical Substances 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 8
- 239000006185 dispersion Substances 0.000 claims description 8
- 239000012188 paraffin wax Substances 0.000 claims description 8
- QLNJFJADRCOGBJ-UHFFFAOYSA-N propionamide Chemical compound CCC(N)=O QLNJFJADRCOGBJ-UHFFFAOYSA-N 0.000 claims description 8
- 229940080818 propionamide Drugs 0.000 claims description 8
- 229920002367 Polyisobutene Polymers 0.000 claims description 7
- 229920001800 Shellac Polymers 0.000 claims description 7
- JXTHNDFMNIQAHM-UHFFFAOYSA-N dichloroacetic acid Chemical compound OC(=O)C(Cl)Cl JXTHNDFMNIQAHM-UHFFFAOYSA-N 0.000 claims description 7
- 229960005215 dichloroacetic acid Drugs 0.000 claims description 7
- 239000004208 shellac Substances 0.000 claims description 7
- ZLGIYFNHBLSMPS-ATJNOEHPSA-N shellac Chemical compound OCCCCCC(O)C(O)CCCCCCCC(O)=O.C1C23[C@H](C(O)=O)CCC2[C@](C)(CO)[C@@H]1C(C(O)=O)=C[C@@H]3O ZLGIYFNHBLSMPS-ATJNOEHPSA-N 0.000 claims description 7
- 229940113147 shellac Drugs 0.000 claims description 7
- 235000013874 shellac Nutrition 0.000 claims description 7
- NWBJYWHLCVSVIJ-UHFFFAOYSA-N N-benzyladenine Chemical compound N=1C=NC=2NC=NC=2C=1NCC1=CC=CC=C1 NWBJYWHLCVSVIJ-UHFFFAOYSA-N 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- WCOXQTXVACYMLM-UHFFFAOYSA-N 2,3-bis(12-hydroxyoctadecanoyloxy)propyl 12-hydroxyoctadecanoate Chemical compound CCCCCCC(O)CCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCC(O)CCCCCC)COC(=O)CCCCCCCCCCC(O)CCCCCC WCOXQTXVACYMLM-UHFFFAOYSA-N 0.000 claims description 4
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 4
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 4
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims description 4
- GAMFEMAXLMWCRG-UHFFFAOYSA-N bis(dimethylcarbamothioylsulfanyl)arsanyl n,n-dimethylcarbamodithioate Chemical compound CN(C)C(=S)S[As](SC(=S)N(C)C)SC(=S)N(C)C GAMFEMAXLMWCRG-UHFFFAOYSA-N 0.000 claims description 4
- 239000004203 carnauba wax Substances 0.000 claims description 4
- JTEDVYBZBROSJT-UHFFFAOYSA-N indole-3-butyric acid Chemical compound C1=CC=C2C(CCCC(=O)O)=CNC2=C1 JTEDVYBZBROSJT-UHFFFAOYSA-N 0.000 claims description 4
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 4
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 4
- MTBZIGHNGSTDJV-UHFFFAOYSA-N Ditalimfos Chemical compound C1=CC=C2C(=O)N(P(=S)(OCC)OCC)C(=O)C2=C1 MTBZIGHNGSTDJV-UHFFFAOYSA-N 0.000 claims description 3
- 229940096992 potassium oleate Drugs 0.000 claims description 3
- MLICVSDCCDDWMD-KVVVOXFISA-M potassium;(z)-octadec-9-enoate Chemical compound [K+].CCCCCCCC\C=C/CCCCCCCC([O-])=O MLICVSDCCDDWMD-KVVVOXFISA-M 0.000 claims description 3
- 239000004094 surface-active agent Substances 0.000 claims description 3
- GMVHICBNQJYKSP-UHFFFAOYSA-M tributylstannanylium;hydroxide Chemical compound [OH-].CCCC[Sn+](CCCC)CCCC GMVHICBNQJYKSP-UHFFFAOYSA-M 0.000 claims description 3
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 2
- 239000004202 carbamide Substances 0.000 claims description 2
- 239000011248 coating agent Substances 0.000 claims description 2
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 2
- 150000002148 esters Chemical class 0.000 claims description 2
- 229930195729 fatty acid Natural products 0.000 claims description 2
- 239000000194 fatty acid Substances 0.000 claims description 2
- 150000004665 fatty acids Chemical class 0.000 claims description 2
- AZXBHGKSTNMAMK-UHFFFAOYSA-N 3-methyl-2-propan-2-ylphenol Chemical compound CC(C)C1=C(C)C=CC=C1O AZXBHGKSTNMAMK-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- INQZXVMNJLSCGI-UHFFFAOYSA-M azanium;potassium;hydrogen phosphate Chemical compound [NH4+].[K+].OP([O-])([O-])=O INQZXVMNJLSCGI-UHFFFAOYSA-M 0.000 claims 1
- 238000000576 coating method Methods 0.000 claims 1
- 238000003672 processing method Methods 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 230000035784 germination Effects 0.000 abstract description 10
- 239000003795 chemical substances by application Substances 0.000 abstract description 6
- 201000010099 disease Diseases 0.000 abstract description 6
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 6
- 241000607479 Yersinia pestis Species 0.000 abstract description 5
- 238000007598 dipping method Methods 0.000 abstract description 2
- 239000002917 insecticide Substances 0.000 abstract description 2
- 230000008635 plant growth Effects 0.000 abstract description 2
- 238000002791 soaking Methods 0.000 abstract description 2
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 238000003306 harvesting Methods 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 241000209094 Oryza Species 0.000 description 18
- 235000007164 Oryza sativa Nutrition 0.000 description 18
- 235000009566 rice Nutrition 0.000 description 18
- 239000002689 soil Substances 0.000 description 7
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 6
- 235000013339 cereals Nutrition 0.000 description 6
- 229910001220 stainless steel Inorganic materials 0.000 description 6
- 239000010935 stainless steel Substances 0.000 description 6
- 230000012010 growth Effects 0.000 description 5
- 229910000402 monopotassium phosphate Inorganic materials 0.000 description 5
- 235000019796 monopotassium phosphate Nutrition 0.000 description 5
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 description 5
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000005631 2,4-Dichlorophenoxyacetic acid Substances 0.000 description 3
- 240000008042 Zea mays Species 0.000 description 3
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 3
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 3
- 235000005822 corn Nutrition 0.000 description 3
- OVSKIKFHRZPJSS-UHFFFAOYSA-N 2,4-D Chemical compound OC(=O)COC1=CC=C(Cl)C=C1Cl OVSKIKFHRZPJSS-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- -1 Petropols Polymers 0.000 description 2
- 244000044283 Toxicodendron succedaneum Species 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 150000002191 fatty alcohols Chemical class 0.000 description 2
- 239000000025 natural resin Substances 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 239000000057 synthetic resin Substances 0.000 description 2
- 229920003002 synthetic resin Polymers 0.000 description 2
- MGSRCZKZVOBKFT-UHFFFAOYSA-N thymol Chemical compound CC(C)C1=CC=C(C)C=C1O MGSRCZKZVOBKFT-UHFFFAOYSA-N 0.000 description 2
- ZFXMDRXVQKSHRV-UHFFFAOYSA-N 3-methyl-2-propan-2-ylphenol 5-methyl-2-propan-2-ylphenol Chemical compound CC(C)C1=CC=C(C)C=C1O.CC(C)C1=C(C)C=CC=C1O ZFXMDRXVQKSHRV-UHFFFAOYSA-N 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 244000299452 Gouania lupuloides Species 0.000 description 1
- 235000000292 Gouania lupuloides Nutrition 0.000 description 1
- 241001272567 Hominoidea Species 0.000 description 1
- 240000005373 Panax quinquefolius Species 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000005844 Thymol Substances 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 238000003618 dip coating Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000009931 harmful effect Effects 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 229920000191 poly(N-vinyl pyrrolidone) Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000136 polysorbate Polymers 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000007226 seed germination Effects 0.000 description 1
- 229960000790 thymol Drugs 0.000 description 1
- MEYZYGMYMLNUHJ-UHFFFAOYSA-N tunicamycin Natural products CC(C)CCCCCCCCCC=CC(=O)NC1C(O)C(O)C(CC(O)C2OC(C(O)C2O)N3C=CC(=O)NC3=O)OC1OC4OC(CO)C(O)C(O)C4NC(=O)C MEYZYGMYMLNUHJ-UHFFFAOYSA-N 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pretreatment Of Seeds And Plants (AREA)
Abstract
The present invention relates to a wax emulsion for soaking and dipping seeds and a preparation and use method thereof. The wax emulsion is prepared from wax substances, resins, an emulsifying agent, a plant growth regulating agent, insecticide, bactericide and fertilizer. After seeds of grain crops are soaked and dipped in the wax emulsion, the seeds have the capability of resisting drought and preventing underground pest disease, the germination and the root generation of the seeds are promoted, and the germination vigor of the seeds is enhanced; thus, the present invention is beneficial to the sturdiness of seedlings and lays a foundation for plenteous harvests.
Description
The present invention relates to a kind of seed Wax emulsion for treating and preparation and application thereof, dip wax emulsion and the preparation and application thereof of processing especially for the cereal crops seed.
Seed is processed has extremely important meaning for agricultural. Usually seed all is directly to be sown in the soil, by absorbing moisture expansion germination and emergence in the soil. If soil moisture is sufficient, most of seeds can both germination and emergence. But in dry water-deficient area, soil water-containing divides few, seed can not absorb enough moisture, thereby also just can not be by the germination and emergence in season, can cause the phenomenon that few seedling or rice shoot are irregular or rice shoot is thin and delicate, newborn rice shoot is because root system is flourishing not, and it is poor to absorb moisture and nutrient ability, also can cause poor growth. And seed directly is sown into and encroached on by the disease worm. In order to make seed have the ability that drought resisting prevents disease and pest, make the thick shape of seed seedling bud, vitality is strong, and present useful frequency electromagnetic waves is processed seed to prevent and treat the sick and increase output of rice shoot, and also useful various seed pelleting agent, the powder of taking root etc. are processed seeds. Chinese patent C N1076799 also discloses a kind of seed pelleting agent, because this coating agent and like product all contain the high power water-absorbing resin that molecular weight is large, be difficult for degraded, long-term use causes soil compaction easily, and its cost is higher.
The purpose of this invention is to provide a kind of seed that is conducive to and after planting can prevent disease and pest, drought resisting, promote that germination takes root, improve potentiality of seed, make rice shoot strong, and easy to use, simple for production, low-cost seed Wax emulsion for treating, the present invention gives the preparation and application of this wax emulsion in addition.
Seed of the present invention is dipped processing wax emulsion and is contained following component: (by weight percentage meter)
3～16% wax class materials;
3～13% resins;
2～8% emulsifying agents;
0.005～0.01% plant growth regulator;
0～0.5% agricultural chemicals;
0～8% little fertilizer;
56～90% water.
Seed of the present invention is dipped and is processed the described wax class of wax emulsion material to be selected from fusing point be 52～60 ℃ paraffin, and dropping point is 67～75 ℃ ceresine, castor wax, and palm wax etc., also available two or more mixture in them, its preferred content is 3～4%.
Seed of the present invention is dipped and processed the described resin of wax emulsion can be that natural resin also can be synthetic resin, such as rosin, shellac, Petropols, polyvinyl alcohol, polyisobutene, poly-propionamide etc., also available two or more mixture in them, its preferred content is 5～6%.
Seed of the present invention is dipped and processed the described emulsifying agent of wax emulsion is to be selected from non-ionic surface active agent, such as C6-
C
24AEO (peregal), C6-C
24APES (О П series), fatty acid loss water sorbit ester APEO (TWEEN series) etc., its preferred content is 3～4%.
Seed of the present invention is dipped and processed the described plant growth regulator of wax emulsion is to be selected from N-benzyladenine (6BA), indolebutyric acid (1BA), 2,4-dichlorphenoxyacetic acid (2,4-D).
Seed of the present invention is dipped and processed the described agricultural chemicals of wax emulsion is to be selected from organic insecticide or mineral oil pesticide, such as white oil emulsion, Mi Ding, thymol (5-methyl-6-isopropyl phenol), potassium oleate, Dormant oils, be selected from organophosphor, arsenic, tin bactericide, such as Plondrel, asomate, hydroxyl tributyltin etc.
Seed of the present invention is dipped and processed the described little fertilizer of wax emulsion is to be selected from ammonium dihydrogen phosphate (ADP), potassium dihydrogen phosphate, and urea etc., its preferred content are 3～4%.
Seed of the present invention is dipped and is processed wax emulsion preparation method and be: by proportioning take by weighing wax class material, resin (abbreviation oil phase) joins in the reactor, slowly be heated to 120～130 ℃, mix reaction 20～30 minutes, emulsifying agent is added to the water is heated to 80～95 ℃, under the high-speed stirred hot water is joined dispersion and emulsion in the oil phase gradually, hot water adds rear continuation and stirred constant 20～30 minutes, process through homogenizer again, add at last plant growth regulator, agricultural chemicals, water-soluble good little fertilizer namely is that seed of the present invention is dipped processing wax emulsion.
Seed of the present invention is dipped the using method of processing wax emulsion: seed is soaked in water 24～48 hours first, reap in the open-top receptacle after making seed suction moisture, add again seed processing wax emulsion of the present invention and dip coating, after the surface of the seed is all coated, in the time of can pulling airing to mutual adhesion out, just can sow.
Seed of the present invention is dipped and is processed wax emulsion, and selecting the emulsion particle of wax class material, natural or synthetic resin, nonionic surface active agent preparation, tiny evenly adhesion is strong, and stability is good. Seed can form a layer film at the surface of the seed after dipping processing with this agent, and this tunic can play the effect of water conservation moisturizing, and preferably gas permeability is arranged again, can satisfy the required oxygen of seed germination, is of value to the seed expansion and germinates. Contain plant growth regulator in the preparation, can be penetrated into the Root Absorption of Interior Seed or grown rice shoot, to promote seed or the growth differentiation of plant cell and the formation of organ. Preparation forms layer protecting film at the surface of the seed, can effectively prevent disease and pest, if add the disease and pest that suitable agricultural chemicals composition can more effectively prevent seed or plant again. Can add suitable N,P,K fertilizers in the preparation, namely the required element of plant growth is conducive to rice shoot and grows up strong and sturdy, owing to these nutriments concentrate on around the seed, and can be relatively easily by still underdeveloped rice shoot absorption of root system. Resin in the preparation also can absorb a certain amount of moisture, is conducive to rice shoot and improves drought-resistant ability. Seed of the present invention is dipped Wax emulsion for treating can select various suitable components according to the variation of agrotype difference and environment for use, such as the plant growth regulator that can select as the case may be dissimilar and quantity, agricultural chemicals, little fertilizer etc., therefore the wax emulsion scope of application of the present invention is extensive, namely can be applicable to dry crop and also go for wet crop, can also be used for the processing of other seed, such as vegetable seeds, flower seed, trees seed, grass seed etc.
It is extremely convenient to use seed of the present invention to dip processing wax emulsion processing seed, and except the seed that requires specially treated, general seed can both be processed with this agent. Do not need special equipment to process, only need general container to operate during use, and price is extremely cheap, every mu of cereal crops seed is processed and is only cost with 3～4 yuan. The composition of selecting in the preparation is the material of easy degraded, uses for a long time soil without any harmful effect, does not also cause environmental pollution.
The below specifies the present invention with embodiment, and wherein each component by weight percentage.
Embodiment 1
2% paraffin (58 ℃ of fusing points);
1% ceresine (70 ℃ of dropping points);
3% rosin;
4% polyvinyl alcohol;
5% polyisobutene;
0.2% poly-propionamide;
6% SA-20 (laruyl alcohol and ethylene oxide condensate);
0.005% N-benzyladenine (6BA);
0.1% white oil emulsion;
0.1% asomate;
1% ammonium dihydrogen phosphate (ADP);
1% potassium dihydrogen phosphate;
The water of surplus.
Proportioning by embodiment 1 claims the oil phase material adding stainless steel reactors such as wax tree fat, slowly be heated to 120 ℃, mix reaction 20 minutes, then add the mixed dispersion and emulsion of the hot water contain 95 ℃ of emulsifying agents under the high-speed stirred, add behind the hot water constant 30 minutes again, process through homogenizer again, add at last plant growth regulator, agricultural chemicals, water-soluble good little fertilizer namely is that the seed of present embodiment is dipped processing wax emulsion.
Embodiment 2
3% paraffin (54 ℃ of fusing points);
3% ceresine (75 ℃ of dropping points);
1% castor wax;
3% shellac;
2% polyvinyl alcohol;
3% Petropols;
0.4% poly-propionamide;
8% О П-10 (APES);
0.007% the Yin butyric acid (1BA) of tut-tuting;
0.2% meter fourth;
0.1% Plondrel;
2% ammonium dihydrogen phosphate (ADP);
2% potassium dihydrogen phosphate;
The water of surplus.
Proportioning by embodiment 2 claims the oil phase material adding stainless steel reactors such as wax tree fat, slowly be heated to 125 ℃, mix reaction 25 minutes, then add the mixed dispersion and emulsion of the hot water contain 90 ℃ of emulsifying agents under the high-speed stirred, add behind the hot water constant 25 minutes again, process through homogenizer again, add at last plant growth regulator, agricultural chemicals, water-soluble good little fertilizer namely is that the seed of present embodiment is dipped processing wax emulsion.
Embodiment 3
4% paraffin (54 ℃ of fusing points);
3% ceresine (75 ℃ of dropping points);
4% castor wax;
3% shellac;
3% polyisobutene;
0.3% poly-propionamide;
4% O-20 (laruyl alcohol and ethylene oxide condensate);
0.008% 2,4-D (2,4-dichlorphenoxyacetic acid);
0.2% thymol;
0.1% hydroxyl tributyltin;
3% ammonium dihydrogen phosphate (ADP);
3% potassium dihydrogen phosphate;
The water of surplus.
Proportioning by embodiment 3 claims the oil phase materials such as wax, resin to add stainless steel reactor, slowly be heated to 13 0 ℃, mix reaction 30 minutes, then add the mixed dispersion and emulsion of the hot water contain 85 ℃ of emulsifying agents under the high-speed stirred, add behind the hot water constant 20 minutes again, process through homogenizer again, add at last plant growth regulator, agricultural chemicals, water-soluble good little fertilizer namely is that the seed of present embodiment is dipped processing wax emulsion.
Embodiment 4
9% palm wax (three grades);
6% paraffin (52 ℃ of fusing points);
2% shellac;
2% polyisobutene;
2% A-20 (fatty alcohol and ethylene oxide condensate);
0.6% poly-propionamide;
0.01% indolebutyric acid;
0.3 the % potassium oleate;
0.2 asomate;
4% ammonium dihydrogen phosphate (ADP);
4% potassium dihydrogen phosphate;
The water of surplus.
Proportioning by embodiment 4 takes by weighing the oil phase materials adding stainless steel reactors such as wax, resin, slowly be heated to 130 ℃, mix reaction 30 minutes, then add the mixed dispersion and emulsion of the hot water contain 80 ℃ of emulsifying agents under the high-speed stirred, add behind the hot water constant 30 minutes again, process through homogenizer again, add at last plant growth regulator, agricultural chemicals, water-soluble good little fertilizer namely is that the seed of present embodiment is dipped processing wax emulsion.
Embodiment 5
2% ceresine (75 ℃);
3% paraffin (54 ℃ of fusing points);
2% shellac;
2% polyisobutene;
3% Petropols;
1% polyethylene;
7% newborn lark A (fatty alcohol and ethylene oxide condensate);
0.3% poly-propionamide;
0.006% indolebutyric acid;
The water of surplus.
Proportioning by embodiment 5 takes by weighing the oil phase materials adding stainless steel reactors such as wax, resin, slowly be heated to 125 ℃, mix reaction 25 minutes, then add the mixed dispersion and emulsion of the hot water that contains 85 ℃ of emulsifying agents under the high-speed stirred, add behind the hot water constant 25 minutes again, processing through homogenizer, add at last plant growth regulator, namely is that the seed of present embodiment is dipped processing wax emulsion.
Embodiment 6
3% palm wax (three grades);
4% paraffin (52 ℃ of fusing points);
2% ceresine;
1% rosin;
1% shellac;
1% polyisobutene;
4% T-80 (TWEEN-80);
0.2% poly-propionamide;
0.01％2、4-D；
0.3% Dormant oils;
The water of surplus.
Proportioning by embodiment 6 takes by weighing the oil phase materials adding stainless steel reactors such as wax, resin, slowly be heated to 120 ℃, mix reaction 20 minutes, then add the mixed dispersion and emulsion of the hot water that contains 85 ℃ of emulsifying agents under the high-speed stirred, add behind the hot water constant 25 minutes again, process through homogenizer again, add at last plant growth regulator, agricultural chemicals namely is that the seed of present embodiment is dipped processing wax emulsion.
The application situation of following result of the test explanation embodiment:
Test on the corn on dry land crop of Chaoyang area non-irrigated condition northeastward and test.
Table 1: wax emulsion is processed seminal root length, radical investigation
| Date | May 16 | June 2 | ||
| Project | Average root length/cm | Radical/ | Average root length/cm | Radical/ |
| Embodiment 1 | 7.0 | 4 | 10.5 | 15 |
| Embodiment 2 | 8.5 | 4 | 11 | 14 |
| Embodiment 3 | 7.0 | 4 | 11.5 | 15 |
| Embodiment 4 | 7.6 | 4 | 11.7 | 14 |
| Embodiment 5 | 7.8 | 4 | 11.8 | 15 |
| Embodiment 6 | 8.0 | 4 | 11.6 | 14 |
| Do not soak contrast | 6.5 | 3 | 10 | 10 |
Long 2 to 4 centimetres of the long contrast of the seminal root of processing, many 1 to 4 of radical is conducive to moisture and nutrient that rice shoot absorbs soil.
Table 2: corn is processed the seed production contrast
| Project | 100-grain weight/g | Fringe grain weight/g | Seed and cane weight ratio |
| Embodiment 1 | 30.5 | 1145 | 1.4 |
| Embodiment 2 | 30.3 | 1221 | 1.3 |
| Embodiment 3 | 35.4 | 1213 | 1.3 |
| Embodiment 4 | 36.4 | 1211 | 1.2 |
| Embodiment 5 | 32.0 | 1138 | 1.4 |
| Embodiment 6 | 33.0 | 1176 | 1.3 |
| Do not soak contrast | 26.5 | 875 | 1.1 |
Data can find out that processing hundred grain weight, fringe grain heavily are significantly increased from table.
Product of the present invention has carried out field test in gaozhou,guangdong, Leizhou District paddy rice, and the result is as follows.
Table 3: wax emulsion is processed the seedling quality application form
| Project | Stem goes out the number of sheets/sheet | Stem height/cm | False stem height/cm | False stem is thick/cm | The long cm of root | The white root bar | Two tiller seedling rate/% | Single pearl fresh weight/g | Single pearl dry weight/g |
| Embodiment 1 | 5.8 | 39.8 | 14.2 | 0.44 | 4.5 | 14.5 | 5 | 0.56 | 0.14 |
| Embodiment 2 | 5.6 | 38.7 | 14.3 | 0.43 | 4.6 | 15.6 | 4 | 0.66 | 0.15 |
| Embodiment 3 | 6.1 | 42.8 | 14.9 | 0.45 | 4.8 | 14.3 | 5 | 0.79 | 0.15 |
| Embodiment 4 | 5.9 | 39.3 | 14.5 | 0.44 | 4.7 | 18.2 | 5 | 0.75 | 0.15 |
| Embodiment 5 | 5.7 | 39.9 | 14.8 | 0.44 | 4.9 | 16.0 | 4 | 0.68 | 0.15 |
| Embodiment 6 | 6.0 | 40.1 | 14.7 | 0.43 | 4.8 | 15.5 | 5 | 0.71 | 0.15 |
| Contrast | 5.3 | 36.2 | 13.2 | 0.39 | 3.2 | 13.3 | 2 | 0.45 | 0.13 |
Table 4: wax emulsion is processed seed rice leaf-area coefficient and dry matter result of the test
| Growth period | The Sheng of the tillering phase | The figurines fringe phase | Milk stage | |||
| Project | Blade face product (mu) | Total dry weight (gram) | Blade face product (mu) | Total dry weight (gram) | Blade face product (mu) | Total dry weight (gram) |
| Embodiment 1 | 3.56 | 0.38 | 6.43 | 2.31 | 2.30 | 3.25 |
| Embodiment 2 | 3.88 | 0.38 | 6.42 | 2.31 | 2.34 | 3.18 |
| Embodiment 3 | 3.45 | 0.39 | 6.88 | 2.34 | 2.28 | 3.77 |
| Embodiment 4 | 3.65 | 0.38 | 7.11 | 2.33 | 2.26 | 4.0 |
| Embodiment 5 | 3.60 | 0.38 | 6.79 | 2.32 | 2.31 | 3.14 |
| Embodiment 6 | 3.58 | 0.38 | 6.58 | 2.33 | 2.29 | 3.80 |
| Contrast | 3.26 | 0.31 | 6.19 | 2.15 | 1.81 | 2.97 |
Can find out that from table 3, table 4 data the rice seeding growth that this wax emulsion is processed contrasts rapidly, leaf area increases fast, and dry-matter accumulation is many, has the basis of big panicle many grains per panicle.
Table 5: wax emulsion is processed seed rice to the impact of germinating energy germination percentage
| Project | Germinating energy (%) | Germination percentage (%) | Remarks | ||||||
| Process | A | B | C | On average | A | B | C | On average | Process 4 days " Invest, Then Investigate " germinating energies, 6 days " Invest, Then Investigate " germination percentages. |
| Embodiment 1 | 75 | 71 | 76 | 74 | 76 | 76 | 78 | 77 | |
| Embodiment 2 | 76 | 75 | 75 | 75 | 86 | 87 | 84 | 85 | |
| Embodiment 3 | 87 | 83 | 80 | 83 | 83 | 84 | 83 | 83 | |
| Embodiment 4 | 80 | 78 | 79 | 76 | 86 | 84 | 84 | 85 | |
| Embodiment 5 | 76 | 78 | 75 | 76 | 85 | 86 | 83 | 85 | |
| Embodiment 6 | 80 | 78 | 76 | 78 | 86 | 87 | 86 | 86 | |
| Contrast | 5 | 6 | 7 | 6 | 7 | 7 | 8 | 7 | |
Table 5 data can find out that seed rice germinating energy, germination percentage that this agent is processed improve a lot.
Table 6: wax emulsion is processed as a result table of each cell production of seed rice
| Project | Each cell production (kilogram) | Per mu yield/kg | Contrast volume increase/kg | Rate of growth/% | ||||
| A | B | C | D | On average | ||||
| Embodiment 1 | 6.80 | 6.45 | 6.85 | 6.44 | 6.64 | 338.9 | 21.9 | 6.91 |
| Embodiment 2 | 6.98 | 6.55 | 6.98 | 6.55 | 6.77 | 351.0 | 34.0 | 10.73 |
| Embodiment 3 | 6.88 | 6.48 | 6.88 | 6.54 | 6.70 | 346.5 | 29.5 | 9.31 |
| Embodiment 4 | 7.21 | 7.10 | 7.20 | 6.98 | 7.12 | 358.4 | 41.4 | 13.06 |
| Embodiment 5 | 6.92 | 6.96 | 6.99 | 7.01 | 6.97 | 355.3 | 38.3 | 12.08 |
| Embodiment 6 | 6.85 | 6.78 | 6.80 | 6.91 | 6.84 | 352.4 | 35.4 | 11.17 |
| Contrast | 6.65 | 6.15 | 6.55 | 6.01 | 6.34 | 317.0 | ||
Table 6 data show that processing the seed rice ultimate output also is greatly improved.
Dip processing wax emulsion from corn, this seed of rice seed soaking Processing Test presentation of results good effect is arranged.
Claims (10)
1, a kind ofly dip the wax emulsion of processing for seed, comprise following composition, content by weight percentage:
3～16% wax class materials;
3～13% resins;
2～8% emulsifying agents;
0.005～0.01% plant growth regulator;
0～0.5% desinsection, bactericide;
0～8% little fertilizer;
56～90% water.
2, dip by the seed of claim 1 and process wax emulsion, it is characterized in that described wax class material is: paraffin, ceresine, castor wax, palm wax or two or more mixture wherein, content is 3～4% by weight.
3, dip processing wax emulsion by the seed of claim 1, it is characterized in that described resin is: rosin, shellac, Petropols, polyvinyl alcohol, polyisobutene, poly-propionamide or two or more mixture wherein, content is 5～6% by weight.
4, dip processing wax emulsion by the seed of claim 1, it is characterized in that described emulsifying agent is non-ionic surface active agent.
5, dip processing wax emulsion by the seed of claim 1 or 4, it is characterized in that described emulsifying agent is selected from C6-C
24AEO, C6-C
24APES, fatty acid loss water sorbit ester APEO, content are 3～4% by weight.
6, dip by the seed of claim 1 and process wax emulsion, it is characterized in that described plant growth regulator is selected from: N-benzyladenine, indolebutyric acid, 2, the 4-dichlorphenoxyacetic acid.
7, dip processing wax emulsion by the seed of claim 1, it is characterized in that described desinsection, bactericide are selected from: white oil emulsion, Mi Ding, 5-methyl-6-isopropyl phenol, potassium oleate, Dormant oils, Plondrel, asomate, hydroxyl tributyltin or two or more mixture wherein, content is 0.1～0.5% by weight.
8, dip processing wax emulsion by the seed of claim 1, it is characterized in that described little fertilizer is selected from: ammonium dihydrogen phosphate (ADP), potassium dihydrogen phosphate ammonia, urea, content are 3～4% by weight.
9, a kind of seed of claim 1 is dipped the preparation method who processes wax emulsion, it is characterized in that: by proportioning take by weighing wax class material, resin joins in the reactor, slowly be heated to 120～130 ℃, mix reaction 20～30 minutes, emulsifying agent is added to the water is heated to 80～95 ℃, under the high-speed stirred hot water is joined dispersion and emulsion in the oil phase gradually, hot water adds rear continuation and stirred constant 30～40 minutes, process through homogenizer again, add at last plant growth regulator, agricultural chemicals, little fertilizer that water is solvent.
10, a kind of seed is dipped processing method, it is characterized in that seed being soaked in water 24～48 hours first, and then the wax emulsion of right to use requirement 1 is dipped processing, and the surface of the seed is pulled airing out after all coating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB991205189A CN1188035C (en) | 1999-09-17 | 1999-09-17 | Wax emulsion for treating seeds and its preparation and usage |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB991205189A CN1188035C (en) | 1999-09-17 | 1999-09-17 | Wax emulsion for treating seeds and its preparation and usage |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1288661A CN1288661A (en) | 2001-03-28 |
| CN1188035C true CN1188035C (en) | 2005-02-09 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB991205189A Expired - Lifetime CN1188035C (en) | 1999-09-17 | 1999-09-17 | Wax emulsion for treating seeds and its preparation and usage |
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| Country | Link |
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| CN (1) | CN1188035C (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BRPI0507624A (en) * | 2004-02-16 | 2007-07-03 | Basf Ag | formulation for seed treatment, use of a polymer or copolymer, seeds, methods for seed treatment prior to sowing, use of a formulation, method for controlling unwanted vegetation and / or for combating phytopathogenic insects and / or of plant pathogenic backgrounds |
| GB201106747D0 (en) * | 2011-04-20 | 2011-06-01 | Exosect Ltd | Coating compositions for pathogen control in vegetables |
| GB201106758D0 (en) * | 2011-04-20 | 2011-06-01 | Exosect Ltd | Compositions for growth and vigour in vegetables |
| GB201106762D0 (en) * | 2011-04-20 | 2011-06-01 | Exosect Ltd | Compositions for growth and vigour from oilseeds |
| GB201106763D0 (en) * | 2011-04-20 | 2011-06-01 | Exosect Ltd | Compositions for growth and vigour in cotton |
| CN103788874B (en) * | 2012-11-05 | 2016-08-03 | 中国石油化工股份有限公司 | A kind of ginseng seed's inorganic agent and preparation method thereof |
| CN107711867A (en) * | 2017-09-26 | 2018-02-23 | 安徽徽大农业有限公司 | A kind of growth promoter for rice and preparation method thereof |
| GB202000685D0 (en) * | 2020-01-16 | 2020-03-04 | Croda Int Plc | Film & Seed coating composition |
| CN112159268B (en) * | 2020-09-22 | 2022-07-01 | 中国科学院植物研究所 | Pelleting composition and pelleting method for German chamomile seeds |
| CN117158423A (en) * | 2023-08-31 | 2023-12-05 | 福建省农业科学院植物保护研究所 | A kind of piercing-sucking insect repellent insecticide with mouthparts and preparation method and application thereof |
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1999
- 1999-09-17 CN CNB991205189A patent/CN1188035C/en not_active Expired - Lifetime
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