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CN118681249A - Device and method for removing ethanol from seabuckthorn fruit oil - Google Patents

Device and method for removing ethanol from seabuckthorn fruit oil Download PDF

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Publication number
CN118681249A
CN118681249A CN202411156283.9A CN202411156283A CN118681249A CN 118681249 A CN118681249 A CN 118681249A CN 202411156283 A CN202411156283 A CN 202411156283A CN 118681249 A CN118681249 A CN 118681249A
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fixedly connected
distillation
tube
stirring
fruit oil
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CN118681249B (en
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赵雄
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Sichuan Qilikang Biotechnology Co ltd
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Sichuan Qilikang Biotechnology Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/02Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B9/00Cleaning hollow articles by methods or apparatus specially adapted thereto
    • B08B9/08Cleaning containers, e.g. tanks
    • B08B9/0804Cleaning containers having tubular shape, e.g. casks, barrels, drums
    • B08B9/0808Cleaning containers having tubular shape, e.g. casks, barrels, drums by methods involving the use of tools, e.g. by brushes, scrapers
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/12Refining fats or fatty oils by distillation

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mechanical Engineering (AREA)
  • Microbiology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

本发明涉及蒸馏装置技术领域,尤其涉及了一种沙棘果油除乙醇的装置及方法,包括蒸馏箱和箱盖,蒸馏箱的内部设置有蒸馏装置,蒸馏装置包括搅拌机构和清除机构,搅拌机构包括电机、搅拌轴、横向搅拌板、竖向搅拌架和混合杆,混合杆的内部设置有空腔,空腔的内部滑动连接有离心块,离心块的内部固定安装有固定磁块,离心块的一端固定连接有弹性绳二,所述混合杆的一端中心连接有活动杆。该沙棘果油除乙醇的装置及方法,离心块推动活动杆伸出,磁性滑动环随着磁性环的靠近会在滑杆外面滑动,从而远离混合杆,磁性滑动环带动清扫刷靠近蒸馏箱的内壁,使清扫刷与蒸馏箱内壁接触,伴随着转动对蒸馏箱内壁进行清扫。

The present invention relates to the technical field of distillation devices, and in particular to a device and method for removing ethanol from seabuckthorn fruit oil, comprising a distillation box and a box cover, wherein a distillation device is arranged inside the distillation box, the distillation device comprises a stirring mechanism and a cleaning mechanism, the stirring mechanism comprises a motor, a stirring shaft, a horizontal stirring plate, a vertical stirring frame and a mixing rod, a cavity is arranged inside the mixing rod, a centrifugal block is slidably connected inside the cavity, a fixed magnetic block is fixedly installed inside the centrifugal block, an elastic rope 2 is fixedly connected to one end of the centrifugal block, and a movable rod is connected to the center of one end of the mixing rod. In the device and method for removing ethanol from seabuckthorn fruit oil, the centrifugal block pushes the movable rod to extend, the magnetic sliding ring slides outside the sliding rod as the magnetic ring approaches, thereby moving away from the mixing rod, the magnetic sliding ring drives a cleaning brush to approach the inner wall of the distillation box, so that the cleaning brush contacts the inner wall of the distillation box, and the inner wall of the distillation box is cleaned along with the rotation.

Description

一种沙棘果油除乙醇的装置及方法Device and method for removing ethanol from seabuckthorn fruit oil

技术领域Technical Field

本发明涉及蒸馏装置技术领域,具体为一种沙棘果油除乙醇的装置及方法。The invention relates to the technical field of distillation devices, in particular to a device and a method for removing ethanol from seabuckthorn fruit oil.

背景技术Background Art

沙棘是植物药中罕见的一种能在恶劣条件下生长,并含有多种活性成份的植物,是我国古代藏蒙医生用来治病的常用中药,具有祛痰利肺、养胃健脾、活血祛病的药理疗效。沙棘果油中类胡萝卜素和维生素E以及多种微量元素。Seabuckthorn is a rare plant that can grow in harsh conditions and contains a variety of active ingredients. It is a common Chinese medicine used by ancient Tibetan and Mongolian doctors to treat diseases. It has the pharmacological effects of removing phlegm and benefiting the lungs, nourishing the stomach and spleen, and promoting blood circulation and curing diseases. Seabuckthorn fruit oil contains carotenoids, vitamin E and a variety of trace elements.

目前从沙棘果浆中提取沙棘果油有超临界流体萃取法、果胶酶法和溶剂萃取等方法。除溶剂萃取法外,其他方法均存在出油效率低的缺点,使用除溶剂萃取法需要用到蒸馏装置回收乙醇,将获得的毛油加热融化直至沸腾,回收乙醇,待回收液酒精份小于1%时,停止蒸馏。At present, there are several methods for extracting seabuckthorn oil from seabuckthorn pulp, such as supercritical fluid extraction, pectinase method and solvent extraction. Except for solvent extraction, other methods have the disadvantage of low oil extraction efficiency. Solvent extraction requires the use of a distillation device to recover ethanol. The crude oil is heated and melted until boiling, and ethanol is recovered. When the alcohol content of the recovered liquid is less than 1%, the distillation is stopped.

现有的蒸馏装置在进行蒸馏过程中蒸馏箱内部会残留一些蒸发液化后的乙醇,造成蒸馏箱内壁有残留,在液化后会进入到沙棘果油中,影响沙棘果油的蒸馏效果,且在蒸馏后乙醇冷却速度较慢。In the existing distillation device, some evaporated and liquefied ethanol will remain inside the distillation box during the distillation process, causing residues on the inner wall of the distillation box. After liquefaction, it will enter the sea buckthorn oil, affecting the distillation effect of the sea buckthorn oil. In addition, the cooling speed of ethanol after distillation is slow.

发明内容Summary of the invention

本发明的目的在于提供一种沙棘果油除乙醇的装置及方法,以解决上述背景技术中提出的问题。The object of the present invention is to provide a device and method for removing ethanol from seabuckthorn fruit oil to solve the problems raised in the above background technology.

为实现上述目的,本发明提供如下技术方案:一种沙棘果油除乙醇的装置,包括蒸馏箱和活动连接于蒸馏箱顶部的箱盖,所述蒸馏箱的内部设置有蒸馏装置,所述蒸馏装置包括搅拌机构和清除机构,所述搅拌机构包括电机、搅拌轴、横向搅拌板、竖向搅拌架和混合杆,所述蒸馏箱的顶部固定安装有安装架,所述电机安装于安装架的顶部中心,所述搅拌轴连接于电机的输出端,所述横向搅拌板固定连接于搅拌轴的外表面,所述竖向搅拌架固定连接于横向搅拌板的底部,所述混合杆固定连接于搅拌轴的外表面,所述搅拌轴的底部固定连接有搅拌棒。To achieve the above-mentioned purpose, the present invention provides the following technical scheme: a device for removing ethanol from seabuckthorn oil, comprising a distillation box and a box cover movably connected to the top of the distillation box, a distillation device is arranged inside the distillation box, the distillation device comprises a stirring mechanism and a cleaning mechanism, the stirring mechanism comprises a motor, a stirring shaft, a horizontal stirring plate, a vertical stirring frame and a mixing rod, a mounting frame is fixedly installed on the top of the distillation box, the motor is installed at the top center of the mounting frame, the stirring shaft is connected to the output end of the motor, the horizontal stirring plate is fixedly connected to the outer surface of the stirring shaft, the vertical stirring frame is fixedly connected to the bottom of the horizontal stirring plate, the mixing rod is fixedly connected to the outer surface of the stirring shaft, and a stirring rod is fixedly connected to the bottom of the stirring shaft.

所述清除机构包括滑槽和清洁环,所述滑槽开设于混合杆的外表面,所述清洁环通过限位滑块滑动连接于滑槽的内部。The cleaning mechanism comprises a slide groove and a cleaning ring. The slide groove is arranged on the outer surface of the mixing rod, and the cleaning ring is slidably connected to the inside of the slide groove through a limiting sliding block.

优选的,所述混合杆的内部设置有空腔,所述空腔的内部滑动连接有离心块,所述离心块的内部固定安装有固定磁块,所述离心块远离搅拌轴的一端固定连接有弹性绳二,所述混合杆的远离搅拌轴的一端中心连接有活动杆。Preferably, a cavity is provided inside the mixing rod, a centrifugal block is slidably connected inside the cavity, a fixed magnetic block is fixedly installed inside the centrifugal block, an end of the centrifugal block away from the stirring shaft is fixedly connected to an elastic rope 2, and a movable rod is connected to the center of the end of the mixing rod away from the stirring shaft.

优选的,所述混合杆的远离搅拌轴的一端两侧固定连接有连接架,所述活动杆远离混合杆的一端固定连接有磁性环,所述连接架远离混合杆的一端固定连接有滑杆,所述滑杆的外表面连接有磁性滑动环,所述滑杆的一端固定连接有限位环,所述磁性滑动环的一侧固定连接有清扫刷。Preferably, the mixing rod has one end away from the stirring shaft and is fixedly connected to a connecting frame on both sides, the movable rod has one end away from the mixing rod and is fixedly connected to a magnetic ring, the connecting frame has one end away from the mixing rod and is fixedly connected to a sliding rod, the outer surface of the sliding rod is connected to a magnetic sliding ring, one end of the sliding rod is fixedly connected to a limiting ring, and one side of the magnetic sliding ring is fixedly connected to a cleaning brush.

优选的,所述滑槽的内壁一侧固定连接有伸缩弹簧,所述伸缩弹簧的一端固定连接有磁性滑块,所述磁性滑块的一侧固定连接有清理板。Preferably, a telescopic spring is fixedly connected to one side of the inner wall of the slide groove, one end of the telescopic spring is fixedly connected to a magnetic slider, and one side of the magnetic slider is fixedly connected to a cleaning plate.

优选的,所述离心块靠近搅拌轴的一侧固定连接有挡板,所述挡板与空腔的内壁滑动连接,挡板与空腔内填充有润滑油。Preferably, a baffle is fixedly connected to one side of the centrifugal block close to the stirring shaft, the baffle is slidably connected to the inner wall of the cavity, and the baffle and the cavity are filled with lubricating oil.

优选的,所述箱盖的顶部连接有蒸馏管,所述蒸馏管的底部通过固定架与箱盖连接,所述蒸馏管的外表面固定连接有保持架,所述蒸馏管远离箱盖的一端固定连接有冷却管,所述冷却管的底部固定连接有收集管,所述保持架的内部连接有取样管,所述取样管的侧面固定连接有检测口。Preferably, the top of the box cover is connected to a distillation tube, the bottom of the distillation tube is connected to the box cover via a fixing frame, the outer surface of the distillation tube is fixedly connected to a retaining frame, the end of the distillation tube away from the box cover is fixedly connected to a cooling tube, the bottom of the cooling tube is fixedly connected to a collecting tube, the inside of the retaining frame is connected to a sampling tube, and the side of the sampling tube is fixedly connected to a detection port.

优选的,所述冷却管的内部安装有冷凝管,所述冷却管的外表面固定连接有金属冷却板,金属冷却板具有良好的导热性,可以及时传递热量。Preferably, a condenser is installed inside the cooling tube, and a metal cooling plate is fixedly connected to the outer surface of the cooling tube. The metal cooling plate has good thermal conductivity and can transfer heat in time.

优选的,所述蒸馏箱的外表面中部和底部分别固定连接有加热管一和加热管二,所述蒸馏箱的侧面底部固定连接有出料管。Preferably, heating tube 1 and heating tube 2 are fixedly connected to the middle and bottom of the outer surface of the distillation box respectively, and a discharge pipe is fixedly connected to the bottom of the side of the distillation box.

一种沙棘果油除乙醇方法,包括以下步骤:A method for removing ethanol from seabuckthorn fruit oil comprises the following steps:

S1:使用除溶剂萃取法从沙棘果浆中提取沙棘果油,打开箱盖将获得的沙棘果油降温后获得的毛油倒入蒸馏箱的内部,打开加热管一和加热管二使蒸馏箱内部升温至沸腾。S1: extracting sea buckthorn fruit oil from sea buckthorn fruit pulp by using solvent removal extraction method, opening the box cover and pouring the crude oil obtained after cooling the sea buckthorn fruit oil into the interior of the distillation box, turning on heating tube 1 and heating tube 2 to heat the interior of the distillation box to boiling.

S2:启动电机带动搅拌轴转动,搅拌轴带动横向搅拌板、竖向搅拌架和混合杆对沙棘果油搅拌,温度达到乙醇的沸点后,乙醇蒸发,产生的乙醇蒸汽进入到蒸馏管的内部。S2: Start the motor to drive the stirring shaft to rotate, and the stirring shaft drives the horizontal stirring plate, the vertical stirring frame and the mixing rod to stir the sea buckthorn oil. When the temperature reaches the boiling point of ethanol, the ethanol evaporates, and the generated ethanol vapor enters the interior of the distillation tube.

S3:乙醇蒸汽进入到蒸馏管内部后流动至冷却管的内部,流经冷凝管后液化,从收集管流出。S3: Ethanol vapor enters the distillation tube and flows to the inside of the cooling tube. It liquefies after passing through the condenser and flows out from the collecting tube.

与现有技术相比,本发明的有益效果是:Compared with the prior art, the present invention has the following beneficial effects:

1.该沙棘果油除乙醇的装置及方法,离心块推动活动杆伸出,此时磁性环与磁性滑动环靠近后,磁性滑动环随着磁性环的靠近会在滑杆外面滑动,从而远离混合杆,磁性滑动环带动清扫刷靠近蒸馏箱的内壁,使清扫刷与蒸馏箱内壁接触,伴随着转动对蒸馏箱内壁进行清扫。1. The device and method for removing ethanol from seabuckthorn oil, the centrifugal block pushes the movable rod to extend, at this time, after the magnetic ring and the magnetic sliding ring are close to each other, the magnetic sliding ring will slide outside the sliding rod as the magnetic rings approach, thereby moving away from the mixing rod, the magnetic sliding ring drives the cleaning brush to approach the inner wall of the distillation box, so that the cleaning brush contacts the inner wall of the distillation box, and cleans the inner wall of the distillation box with the rotation.

2.该沙棘果油除乙醇的装置及方法,在离心块推动活动杆移动时,此时磁性环与磁性滑动环靠近后,磁性滑动环随着磁性环的靠近会在滑杆外面转动,进而带动清扫刷转动对蒸馏箱的内壁进行清扫,进一步提升清扫效果,避免乙醇残留在蒸馏箱内壁。2. The device and method for removing ethanol from seabuckthorn oil, when the centrifugal block pushes the movable rod to move, the magnetic ring and the magnetic sliding ring approach each other, and the magnetic sliding ring rotates outside the sliding rod as the magnetic ring approaches, thereby driving the cleaning brush to rotate and clean the inner wall of the distillation box, further improving the cleaning effect and preventing ethanol from remaining on the inner wall of the distillation box.

3.该沙棘果油除乙醇的装置及方法,通过打开检测口可以对乙醇进行取样检测,若回收液中乙醇份小于1%时,停止蒸馏,通过设置取样管和检测口,可以方便对蒸馏时间进行控制,也可以及时获得蒸馏效果。3. The device and method for removing ethanol from seabuckthorn oil can sample and test ethanol by opening the detection port. If the ethanol content in the recovered liquid is less than 1%, distillation is stopped. By setting the sampling tube and the detection port, the distillation time can be conveniently controlled and the distillation effect can be obtained in time.

4.该沙棘果油除乙醇的装置及方法,在离心块移动的过程中,会带动固定磁块移动,从而吸引磁性滑块移动,磁性滑块在滑槽的内部滑动,进而带动清理板对混合杆的外表面清理,同时伸缩弹簧被挤压,在电机转速降低后,在伸缩弹簧自身回复力作用下,会推动磁性滑块复位,同时使清理板反向滑动一段距离,进一步对混合杆的外表面清理。4. The device and method for removing ethanol from seabuckthorn oil, during the movement of the centrifugal block, will drive the fixed magnetic block to move, thereby attracting the magnetic slider to move, the magnetic slider slides inside the slide groove, and then drives the cleaning plate to clean the outer surface of the mixing rod, and at the same time the telescopic spring is squeezed, after the motor speed is reduced, under the action of the restoring force of the telescopic spring itself, it will push the magnetic slider to reset, and at the same time make the cleaning plate slide in the opposite direction for a distance, so as to further clean the outer surface of the mixing rod.

附图说明BRIEF DESCRIPTION OF THE DRAWINGS

为了更清楚地说明本发明实施例中的技术方案,下面将对实施例描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本发明的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动性的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the drawings required for use in the description of the embodiments will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without creative work.

图1为本发明的整体结构示意图;Fig. 1 is a schematic diagram of the overall structure of the present invention;

图2为本发明的搅拌机构结构示意图;FIG2 is a schematic diagram of the structure of a stirring mechanism of the present invention;

图3为本发明的混合杆整体结构示意图;FIG3 is a schematic diagram of the overall structure of the mixing rod of the present invention;

图4为图3中A处结构放到示意图;FIG4 is a schematic diagram of the structure at A in FIG3;

图5为本发明的混合杆剖视图;FIG5 is a cross-sectional view of a mixing rod according to the present invention;

图6为本发明的蒸馏管整体结构示意图;FIG6 is a schematic diagram of the overall structure of a distillation tube according to the present invention;

图7为本发明的冷却管内部结构示意图;FIG7 is a schematic diagram of the internal structure of a cooling tube according to the present invention;

图8为本发明的实施例四滑杆结构示意图。FIG. 8 is a schematic diagram of the sliding bar structure according to the fourth embodiment of the present invention.

图中:1、蒸馏箱;2、箱盖;3、加热管一;4、加热管二;5、出料管;6、安装架;601、电机;602、搅拌轴;603、横向搅拌板;604、竖向搅拌架;605、混合杆;6051、滑槽;6052、清洁环;6053、伸缩弹簧;6054、磁性滑块;6055、清理板;6056、活动杆;6057、磁性环;6058、滑杆;6059、磁性滑动环;60510、清扫刷;60511、限位环;60512、离心块;60513、固定磁块;60514、弹性绳二;60515、挡板;6010、连接架;606、搅拌棒;7、蒸馏管;701、保持架;702、固定架;703、冷却管;704、收集管;705、取样管;706、检测口;7031、冷凝管;7032、金属冷却板。In the figure: 1, distillation box; 2, box cover; 3, heating tube 1; 4, heating tube 2; 5, discharge pipe; 6, mounting frame; 601, motor; 602, stirring shaft; 603, horizontal stirring plate; 604, vertical stirring frame; 605, mixing rod; 6051, slide; 6052, cleaning ring; 6053, telescopic spring; 6054, magnetic slider; 6055, cleaning plate; 6056, movable rod; 6057, magnetic ring; 6058, sliding rod; 6059 , magnetic sliding ring; 60510, cleaning brush; 60511, limiting ring; 60512, centrifugal block; 60513, fixed magnetic block; 60514, elastic rope 2; 60515, baffle; 6010, connecting frame; 606, stirring rod; 7, distillation tube; 701, retaining frame; 702, fixing frame; 703, cooling tube; 704, collecting tube; 705, sampling tube; 706, detection port; 7031, condenser; 7032, metal cooling plate.

具体实施方式DETAILED DESCRIPTION

下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

在本发明中,除非另有明确的规定和限定,术语“安装”、“相连”、“连接”、“固定”等术语应做广义理解,例如,可以是固定连接,也可以是可拆卸连接,或成一体;可以是机械连接,也可以是电连接;可以是直接相连,也可以通过中间媒介间接相连,可以是两个元件内部的连通或两个元件的相互作用关系。对于本领域的普通技术人员而言,可以根据具体情况理解上述术语在本发明中的具体含义。In the present invention, unless otherwise clearly specified and limited, the terms "installed", "connected", "connected", "fixed" and the like should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium, it can be the internal connection of two elements or the interaction relationship between two elements. For ordinary technicians in this field, the specific meanings of the above terms in the present invention can be understood according to specific circumstances.

请参阅图1-图8,本发明提供一种技术方案:Please refer to Figures 1 to 8, the present invention provides a technical solution:

实施例一:一种沙棘果油除乙醇的装置,包括蒸馏箱1和活动连接于蒸馏箱1顶部的箱盖2,蒸馏箱1的内部设置有蒸馏装置,蒸馏装置包括搅拌机构和清除机构,蒸馏箱1的外表面中部和底部分别固定连接有加热管一3和加热管二4,蒸馏箱1的侧面底部固定连接有出料管5。Embodiment 1: A device for removing ethanol from seabuckthorn oil, comprising a distillation box 1 and a box cover 2 movably connected to the top of the distillation box 1, a distillation device is arranged inside the distillation box 1, the distillation device comprises a stirring mechanism and a cleaning mechanism, a heating tube 1 3 and a heating tube 2 4 are fixedly connected to the middle and bottom of the outer surface of the distillation box 1 respectively, and a discharge pipe 5 is fixedly connected to the bottom of the side of the distillation box 1.

搅拌机构包括电机601、搅拌轴602、横向搅拌板603、竖向搅拌架604和混合杆605,蒸馏箱1的顶部固定安装有安装架6,电机601安装于安装架6的顶部中心,搅拌轴602连接于电机601的输出端,横向搅拌板603固定连接于搅拌轴602的外表面,竖向搅拌架604固定连接于横向搅拌板603的底部,混合杆605固定连接于搅拌轴602的外表面,搅拌轴602的底部固定连接有搅拌棒606;The stirring mechanism includes a motor 601, a stirring shaft 602, a horizontal stirring plate 603, a vertical stirring frame 604 and a mixing rod 605. A mounting frame 6 is fixedly installed on the top of the distillation box 1. The motor 601 is installed at the top center of the mounting frame 6. The stirring shaft 602 is connected to the output end of the motor 601. The horizontal stirring plate 603 is fixedly connected to the outer surface of the stirring shaft 602. The vertical stirring frame 604 is fixedly connected to the bottom of the horizontal stirring plate 603. The mixing rod 605 is fixedly connected to the outer surface of the stirring shaft 602. The bottom of the stirring shaft 602 is fixedly connected with a stirring rod 606.

清除机构包括滑槽6051和清洁环6052,滑槽6051开设于混合杆605的外表面,清洁环6052通过限位滑块滑动连接于滑槽6051的内部,清洁环6052与混合杆605的外表面紧贴,混合杆605的内部设置有空腔,空腔的内部滑动连接有离心块60512,离心块60512的内部固定安装有固定磁块60513,离心块60512远离搅拌轴602的一端固定连接有弹性绳二60514,混合杆605的远离搅拌轴602的一端中心连接有活动杆6056。The cleaning mechanism includes a slide groove 6051 and a cleaning ring 6052. The slide groove 6051 is opened on the outer surface of the mixing rod 605. The cleaning ring 6052 is slidably connected to the inside of the slide groove 6051 through a limiting slider. The cleaning ring 6052 is in close contact with the outer surface of the mixing rod 605. A cavity is provided inside the mixing rod 605. A centrifugal block 60512 is slidably connected inside the cavity. A fixed magnetic block 60513 is fixedly installed inside the centrifugal block 60512. An elastic rope 60514 is fixedly connected to one end of the centrifugal block 60512 away from the stirring shaft 602. A movable rod 6056 is connected to the center of one end of the mixing rod 605 away from the stirring shaft 602.

混合杆605的远离搅拌轴602的一端两侧固定连接有连接架6010,活动杆6056远离混合杆605的一端固定连接有磁性环6057,连接架6010远离混合杆605的一端固定连接有滑杆6058,滑杆6058的外表面连接有磁性滑动环6059,滑杆6058的一端固定连接有限位环60511,磁性滑动环6059的一侧固定连接有清扫刷60510,磁性环6057与磁性滑动环6059靠近的一侧相互排斥。The mixing rod 605 has one end away from the stirring shaft 602 and is fixedly connected to a connecting frame 6010 on both sides. The movable rod 6056 has one end away from the mixing rod 605 and is fixedly connected to a magnetic ring 6057. The connecting frame 6010 has one end away from the mixing rod 605 and is fixedly connected to a sliding rod 6058. The outer surface of the sliding rod 6058 is connected to a magnetic sliding ring 6059. One end of the sliding rod 6058 is fixedly connected to a limiting ring 60511. A cleaning brush 60510 is fixedly connected to one side of the magnetic sliding ring 6059. The magnetic ring 6057 and the side of the magnetic sliding ring 6059 that are close to each other repel each other.

在混合的同时,因为混合杆605的转动会产生离心力,从而使清洁环6052在滑槽6051的内部向远离搅拌轴602的一端滑动,从而带动清洁环6052对混合杆605的表面进行清洁,电机601降速后混合杆605的转动速度降低,清洁环6052会停止滑动,同时离心力会使离心块60512在空腔内向远离搅拌轴602的一端滑动,离心块60512挤压弹性绳二60514,当弹性绳二60514收缩后,离心块60512推动活动杆6056伸出,此时磁性环6057与磁性滑动环6059靠近后,磁性滑动环6059随着磁性环6057的靠近会在滑杆6058外面滑动,从而远离混合杆605,磁性滑动环6059带动清扫刷60510靠近蒸馏箱1的内壁,使清扫刷60510与蒸馏箱1内壁接触,伴随着转动对蒸馏箱1内壁进行清扫。During mixing, the rotation of the mixing rod 605 generates centrifugal force, which causes the cleaning ring 6052 to slide inside the chute 6051 toward the end away from the stirring shaft 602, thereby driving the cleaning ring 6052 to clean the surface of the mixing rod 605. After the motor 601 is decelerated, the rotation speed of the mixing rod 605 is reduced, and the cleaning ring 6052 stops sliding. At the same time, the centrifugal force causes the centrifugal block 60512 to slide inside the cavity toward the end away from the stirring shaft 602, and the centrifugal block 60512 squeezes the elastic rope 60512. 514. When the elastic rope 60514 contracts, the centrifugal block 60512 pushes the movable rod 6056 to extend. At this time, the magnetic ring 6057 and the magnetic sliding ring 6059 are close to each other. As the magnetic ring 6057 approaches, the magnetic sliding ring 6059 slides outside the sliding rod 6058, thereby moving away from the mixing rod 605. The magnetic sliding ring 6059 drives the cleaning brush 60510 to approach the inner wall of the distillation box 1, so that the cleaning brush 60510 contacts the inner wall of the distillation box 1, and cleans the inner wall of the distillation box 1 along with the rotation.

箱盖2的顶部连接有蒸馏管7,蒸馏管7的底部通过固定架702与箱盖2连接,蒸馏管7的外表面固定连接有保持架701,蒸馏管7远离箱盖2的一端固定连接有冷却管703,冷却管703的底部固定连接有收集管704,保持架701的内部连接有取样管705,取样管705的侧面固定连接有检测口706,取样管705内部安装有单向阀,仅允许蒸汽从底部流向顶部,冷却管703的内部安装有冷凝管7031,冷却管703的外表面固定连接有金属冷却板7032,冷却管703与冷凝管7031之间填充有冷却液。A distillation tube 7 is connected to the top of the box cover 2, and the bottom of the distillation tube 7 is connected to the box cover 2 through a fixing frame 702. A retaining frame 701 is fixedly connected to the outer surface of the distillation tube 7. A cooling tube 703 is fixedly connected to the end of the distillation tube 7 away from the box cover 2. A collecting tube 704 is fixedly connected to the bottom of the cooling tube 703. A sampling tube 705 is connected to the inside of the retaining frame 701. A detection port 706 is fixedly connected to the side of the sampling tube 705. A one-way valve is installed inside the sampling tube 705 to only allow steam to flow from the bottom to the top. A condenser 7031 is installed inside the cooling tube 703. A metal cooling plate 7032 is fixedly connected to the outer surface of the cooling tube 703. Coolant is filled between the cooling tube 703 and the condenser 7031.

部分乙醇蒸汽会进入到取样管705内部,然后液化,通过打开检测口706可以对乙醇进行取样检测。Part of the ethanol vapor will enter the sampling tube 705 and then liquefy. By opening the detection port 706, the ethanol can be sampled and tested.

乙醇蒸汽进入到蒸馏管7内部后流动至冷却管703的内部,流经冷凝管7031后液化,从收集管704流出,在经过冷凝管7031内部时,会与冷却液进行热交换,使得乙醇蒸汽快速液化后流下,金属冷却板7032具有良好的导热性,可以传递冷却液中的热量,与空气接触后将热量通过空气传递,可以快速对乙醇液化。After entering the distillation tube 7, the ethanol vapor flows to the inside of the cooling tube 703, flows through the condenser 7031 and is liquefied, and flows out from the collecting tube 704. When passing through the inside of the condenser 7031, it exchanges heat with the coolant, causing the ethanol vapor to quickly liquefy and flow down. The metal cooling plate 7032 has good thermal conductivity and can transfer the heat in the coolant. After contacting with the air, the heat is transferred through the air, which can quickly liquefy the ethanol.

实施例二:滑槽6051的内壁一侧固定连接有伸缩弹簧6053,伸缩弹簧6053的一端固定连接有磁性滑块6054,磁性滑块6054的一侧固定连接有清理板6055,在此实施例中,清理板6055与混合杆605的外表面紧贴,清洁环6052两侧与混合杆605的外表面之前的宽度大于清理板6055的厚度,清洁环6052与混合杆605外表面顶部和底部紧贴,磁性滑块6054与固定磁块60513靠近的一侧相互吸引,在离心块60512移动的过程中,会带动固定磁块60513移动,从而吸引磁性滑块6054移动,磁性滑块6054在滑槽6051的内部滑动,进而带动清理板6055对混合杆605的外表面清理,同时伸缩弹簧6053被挤压,在电机601转速降低后,在伸缩弹簧6053自身回复力作用下,会推动磁性滑块6054复位,同时使清理板6055反向滑动一段距离,进一步对混合杆605的外表面清理。Embodiment 2: A telescopic spring 6053 is fixedly connected to one side of the inner wall of the slide 6051, and a magnetic slider 6054 is fixedly connected to one end of the telescopic spring 6053. A cleaning plate 6055 is fixedly connected to one side of the magnetic slider 6054. In this embodiment, the cleaning plate 6055 is in close contact with the outer surface of the mixing rod 605, and the width between the two sides of the cleaning ring 6052 and the outer surface of the mixing rod 605 is greater than the thickness of the cleaning plate 6055. The cleaning ring 6052 is in close contact with the top and bottom of the outer surface of the mixing rod 605, and the magnetic slider 6054 is close to the fixed magnetic block 60513. The two sides attract each other, and during the movement of the centrifugal block 60512, the fixed magnetic block 60513 is driven to move, thereby attracting the magnetic slider 6054 to move. The magnetic slider 6054 slides inside the slide groove 6051, and then drives the cleaning plate 6055 to clean the outer surface of the mixing rod 605. At the same time, the telescopic spring 6053 is squeezed. After the speed of the motor 601 is reduced, the restoring force of the telescopic spring 6053 itself will push the magnetic slider 6054 to reset, and at the same time, the cleaning plate 6055 will slide in the opposite direction for a distance, so as to further clean the outer surface of the mixing rod 605.

实施例三:离心块60512靠近搅拌轴602的一侧固定连接有挡板60515,挡板60515与空腔的内壁滑动连接,挡板60515的右侧与空腔内部填充有润滑油,在离心块60512移动的过程中,会带动挡板60515移动,挡板60515移动后会改变储存润滑油的空间,使得离心块60512在移动过程中会不断推动润滑油,离心块60512移动的更加顺滑。Embodiment three: A baffle 60515 is fixedly connected to one side of the centrifugal block 60512 close to the stirring shaft 602. The baffle 60515 is slidably connected to the inner wall of the cavity. The right side of the baffle 60515 and the inside of the cavity are filled with lubricating oil. During the movement of the centrifugal block 60512, the baffle 60515 will be driven to move. After the baffle 60515 moves, the space for storing the lubricating oil will be changed, so that the centrifugal block 60512 will continuously push the lubricating oil during the movement, and the centrifugal block 60512 moves more smoothly.

实施例四:滑杆6058的外表面开设有螺纹,磁性滑动环6059与滑杆6058螺纹连接,在离心块60512推动活动杆6056移动时,此时磁性环6057与磁性滑动环6059靠近后,磁性滑动环6059随着磁性环6057的靠近会在滑杆6058外面转动,进而带动清扫刷60510转动对蒸馏箱1的内壁进行清扫,进一步提升清扫效果,避免乙醇残留在蒸馏箱1内壁。Embodiment 4: The outer surface of the slide rod 6058 is provided with a thread, and the magnetic sliding ring 6059 is threadedly connected to the slide rod 6058. When the centrifugal block 60512 pushes the movable rod 6056 to move, the magnetic ring 6057 and the magnetic sliding ring 6059 get close to each other. The magnetic sliding ring 6059 rotates outside the slide rod 6058 as the magnetic ring 6057 approaches, thereby driving the cleaning brush 60510 to rotate and clean the inner wall of the distillation box 1, thereby further improving the cleaning effect and preventing ethanol from remaining on the inner wall of the distillation box 1.

一种沙棘果油除乙醇方法,包括以下步骤:A method for removing ethanol from seabuckthorn fruit oil comprises the following steps:

S1:使用除溶剂萃取法从沙棘果浆中提取沙棘果油,打开箱盖2将获得的沙棘果油降温后获得的毛油倒入蒸馏箱1的内部,打开加热管一3和加热管二4使蒸馏箱1内部升温至沸腾;S1: extracting sea buckthorn fruit oil from sea buckthorn fruit pulp by using a solvent removal extraction method, opening the box cover 2 and pouring the crude oil obtained after cooling the sea buckthorn fruit oil into the interior of the distillation box 1, and turning on the heating tube 1 3 and the heating tube 2 4 to heat the interior of the distillation box 1 to boiling;

S2:启动电机601带动搅拌轴602转动,搅拌轴602带动横向搅拌板603、竖向搅拌架604和混合杆605对沙棘果油搅拌,温度达到乙醇的沸点后,乙醇蒸发,产生的乙醇蒸汽进入到蒸馏管7的内部;S2: starting the motor 601 to drive the stirring shaft 602 to rotate, and the stirring shaft 602 drives the horizontal stirring plate 603, the vertical stirring frame 604 and the mixing rod 605 to stir the sea buckthorn fruit oil. When the temperature reaches the boiling point of ethanol, the ethanol evaporates, and the generated ethanol vapor enters the interior of the distillation tube 7;

S3:乙醇蒸汽进入到蒸馏管7内部后流动至冷却管703的内部,流经冷凝管7031后液化,从收集管704流出。S3: After entering the distillation tube 7 , the ethanol vapor flows to the inside of the cooling tube 703 , flows through the condenser 7031 , and is liquefied, and flows out from the collecting tube 704 .

需要说明的是,在本文中,诸如第一和第二等之类的关系术语仅仅用来将一个实体或者操作与另一个实体或操作区分开来,而不一定要求或者暗示这些实体或操作之间存在任何这种实际的关系或者顺序。而且,术语“包括”、“包含”或者其任何其他变体意在涵盖非排他性的包含,从而使得包括一系列要素的过程、方法、物品或者设备不仅包括那些要素,而且还包括没有明确列出的其他要素,或者是还包括为这种过程、方法、物品或者设备所固有的要素。在没有更多限制的情况下,由语句“包括一个......”限定的要素,并不排除在包括所述要素的过程、方法、物品或者设备中还存在另外的相同要素。It should be noted that, in this article, relational terms such as first and second, etc. are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Moreover, the terms "include", "comprise" or any other variants thereof are intended to cover non-exclusive inclusion, so that a process, method, article or device including a series of elements includes not only those elements, but also other elements not explicitly listed, or also includes elements inherent to such process, method, article or device. In the absence of further restrictions, the elements defined by the statement "including a ..." do not exclude the presence of other identical elements in the process, method, article or device including the elements.

尽管已经示出和描述了本发明的实施例,对于本领域的普通技术人员而言,可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型,本发明的范围由所附权利要求及其等同物限定。Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims (9)

1. The utility model provides a device of sea buckthorn fruit oil ethanol removal, includes stilling box (1) and swing joint in case lid (2) at stilling box (1) top, its characterized in that: the inside of the distillation box (1) is provided with a distillation device, the distillation device comprises a stirring mechanism and a cleaning mechanism, the stirring mechanism comprises a motor (601), a stirring shaft (602), a transverse stirring plate (603), a vertical stirring frame (604) and a mixing rod (605), a mounting frame (6) is fixedly arranged at the top of the distillation box (1), the motor (601) is arranged at the center of the top of the mounting frame (6), the stirring shaft (602) is connected to the output end of the motor (601), the transverse stirring plate (603) is fixedly connected to the outer surface of the stirring shaft (602), the vertical stirring frame (604) is fixedly connected to the bottom of the transverse stirring plate (603), the mixing rod (605) is fixedly connected to the outer surface of the stirring shaft (602), and a stirring rod (606) is fixedly connected to the bottom of the stirring shaft (602).
The cleaning mechanism comprises a sliding groove (6051) and a cleaning ring (6052), the sliding groove (6051) is formed in the outer surface of the mixing rod (605), and the cleaning ring (6052) is connected to the inside of the sliding groove (6051) in a sliding mode through a limiting sliding block.
2. The device for removing ethanol from sea buckthorn fruit oil according to claim 1, wherein: the inside of hybrid pole (605) is provided with the cavity, the inside sliding connection of cavity has centrifugal piece (60512), the inside fixed mounting of centrifugal piece (60512) has fixed magnet (60513), the one end fixedly connected with elasticity rope two (60514) that (602) were kept away from to centrifugal piece (60512), the one end center that keeps away from (602) of hybrid pole (605) is connected with movable rod (6056).
3. The device for removing ethanol from sea buckthorn fruit oil according to claim 2, wherein: one end both sides fixedly connected with link (6010) of keeping away from (602) of hybrid pole (605), one end fixedly connected with magnetic ring (6057) of hybrid pole (605) are kept away from to movable rod (6056), one end fixedly connected with slide bar (6058) of hybrid pole (605) are kept away from to link (6010), the surface connection of slide bar (6058) has magnetic slip ring (6059), one end fixedly connected with spacing ring (60511) of slide bar (6058), one side fixedly connected with brush cleaner (60510) of magnetic slip ring (6059).
4. The device for removing ethanol from sea buckthorn fruit oil according to claim 1, wherein: the inner wall one side fixedly connected with extension spring (6053) of spout (6051), the one end fixedly connected with magnetism slider (6054) of extension spring (6053), one side fixedly connected with clearance board (6055) of magnetism slider (6054).
5. The device for removing ethanol from sea buckthorn fruit oil according to claim 2, wherein: one side of the centrifugal block (60512) close to the stirring shaft (602) is fixedly connected with a baffle plate (60515), and the baffle plate (60515) is in sliding connection with the inner wall of the cavity.
6. The device for removing ethanol from sea buckthorn fruit oil according to claim 1, wherein: the top of case lid (2) is connected with distillation tube (7), the bottom of distillation tube (7) is connected with case lid (2) through mount (702), the surface fixedly connected with holder (701) of distillation tube (7), the one end fixedly connected with cooling tube (703) of case lid (2) is kept away from to distillation tube (7), the bottom fixedly connected with collecting pipe (704) of cooling tube (703), the internal connection of holder (701) has sampling tube (705), the side fixedly connected with of sampling tube (705) detects mouth (706).
7. The device for removing ethanol from sea buckthorn fruit oil according to claim 6, wherein: the cooling tube (703) is internally provided with a condensing tube (7031), and the outer surface of the cooling tube (703) is fixedly connected with a metal cooling plate (7032).
8. The device for removing ethanol from sea buckthorn fruit oil according to claim 1, wherein: the middle part and the bottom of the outer surface of the distillation box (1) are respectively fixedly connected with a heating pipe I (3) and a heating pipe II (4), and the bottom of the side surface of the distillation box (1) is fixedly connected with a discharging pipe (5).
9. A method for removing ethanol from sea buckthorn fruit oil, which is characterized in that the device for removing ethanol from sea buckthorn fruit oil according to any one of claims 1 to 8 comprises the following steps:
S1: extracting sea buckthorn fruit oil from sea buckthorn fruit pulp by using a solvent removal extraction method, opening a box cover (2), pouring crude oil obtained by cooling the obtained sea buckthorn fruit oil into the distillation box (1), and opening a heating pipe I (3) and a heating pipe II (4) to heat the interior of the distillation box (1) to boiling;
S2: starting a motor (601) to drive a stirring shaft (602) to rotate, driving a transverse stirring plate (603), a vertical stirring frame (604) and a mixing rod (605) to stir the sea buckthorn fruit oil by the stirring shaft (602), evaporating the ethanol after the temperature reaches the boiling point of the ethanol, and enabling the generated ethanol steam to enter the distillation tube (7);
S3: the ethanol vapor enters the distillation tube (7) and flows into the cooling tube (703), flows through the condensing tube (7031) and is liquefied, and flows out of the collecting tube (704).
CN202411156283.9A 2024-08-22 2024-08-22 Device and method for removing ethanol from sea buckthorn fruit oil Active CN118681249B (en)

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CN213172262U (en) * 2020-08-12 2021-05-11 江苏鸿祺生物科技有限公司 A kind of desolvation device for preparation of sea buckthorn seed oil
CN115138267A (en) * 2022-07-27 2022-10-04 枣庄市天龙纸业有限公司 Paper pulp mixing device with self-cleaning function
CN116617987A (en) * 2023-07-12 2023-08-22 广东科伟环保科技有限公司 Distillation plant is used in detergent production
CN116808877A (en) * 2023-08-03 2023-09-29 河南华港印务有限公司 Preparation facilities of glazing printing ink of tipping paper for cigarette
CN219783830U (en) * 2023-05-10 2023-10-03 四川正元工贸有限公司 Energy-saving and environment-friendly distillation kettle
CN116889737A (en) * 2023-06-06 2023-10-17 江苏蜂奥生物科技有限公司 Separation equipment and forming process for high-purity ganoderma lucidum spore oil
CN117357950A (en) * 2023-11-22 2024-01-09 枣阳市华威硅氟材料有限公司 Sediment thick liquid filter equipment is used in organosilicon production
CN118293660A (en) * 2024-04-29 2024-07-05 内蒙古宇航人生物工程技术有限公司 Sea buckthorn fiber preparation device and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20180140965A1 (en) * 2016-11-22 2018-05-24 Shale Flora Production system
CN213131964U (en) * 2020-07-28 2021-05-07 菏泽瑞圣化工科技有限公司 Stills is used in o-cresol production
CN213172262U (en) * 2020-08-12 2021-05-11 江苏鸿祺生物科技有限公司 A kind of desolvation device for preparation of sea buckthorn seed oil
CN115138267A (en) * 2022-07-27 2022-10-04 枣庄市天龙纸业有限公司 Paper pulp mixing device with self-cleaning function
CN219783830U (en) * 2023-05-10 2023-10-03 四川正元工贸有限公司 Energy-saving and environment-friendly distillation kettle
CN116889737A (en) * 2023-06-06 2023-10-17 江苏蜂奥生物科技有限公司 Separation equipment and forming process for high-purity ganoderma lucidum spore oil
CN116617987A (en) * 2023-07-12 2023-08-22 广东科伟环保科技有限公司 Distillation plant is used in detergent production
CN116808877A (en) * 2023-08-03 2023-09-29 河南华港印务有限公司 Preparation facilities of glazing printing ink of tipping paper for cigarette
CN117357950A (en) * 2023-11-22 2024-01-09 枣阳市华威硅氟材料有限公司 Sediment thick liquid filter equipment is used in organosilicon production
CN118293660A (en) * 2024-04-29 2024-07-05 内蒙古宇航人生物工程技术有限公司 Sea buckthorn fiber preparation device and preparation method thereof

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