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CN118304199A - A high-oil cream cleanser - Google Patents

A high-oil cream cleanser Download PDF

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Publication number
CN118304199A
CN118304199A CN202410423226.6A CN202410423226A CN118304199A CN 118304199 A CN118304199 A CN 118304199A CN 202410423226 A CN202410423226 A CN 202410423226A CN 118304199 A CN118304199 A CN 118304199A
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oil
sodium
skin
composition according
cocoyl
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CN118304199B (en
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池水兴
张艳萍
吕雪莲
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Qianyan Cosmetics Technology Shanghai Co ltd
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Qianyan Cosmetics Technology Shanghai Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/46Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
    • A61K8/466Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0295Liquid crystals
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/447Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof containing sulfur
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/14Preparations for removing make-up
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/596Mixtures of surface active compounds

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention relates to the field of human body surface cleaners, in particular to a high-oil cream facial cleanser. The components of the invention comprise grease, sodium cocoyl isethionate and sodium C14-16 olefin sulfonate. The invention is an amino acid facial cleanser with high grease content, has three-in-one effects of skin care, makeup removal/sun protection and facial cleansing, has the characteristics of cream texture and deep cleaning, plays the effect of immediately moistening skin, and does not need to care skin again. The cream has high vegetable oil content, is easy to spread, foams quickly, can deeply remove dirt in pores, protects the water locking layer of skin from being damaged while cleaning the skin, and keeps clean and clear for a long time.

Description

一种高油乳霜洁面乳A high-oil cream cleanser

技术领域Technical Field

本发明涉及人体表面清洁剂领域,具体涉及一种高油乳霜洁面乳。The invention relates to the field of human body surface cleansers, in particular to a high-oil cream facial cleanser.

背景技术Background technique

洁面乳为清洁类化妆品;用作清除面部皮肤表面的污垢,使皮肤保持清爽舒适,有助于保持皮肤正常生理功能。Facial cleanser is a cleansing cosmetic; it is used to remove dirt from the surface of facial skin, keeping the skin refreshed and comfortable, and helping to maintain the normal physiological functions of the skin.

洁面乳清洗皮肤时,清洗是人体皮肤上的皮脂和角质层碎片及其氧化分解物,或者是美容化妆品残留物。这些残留代谢产物不稳定,在暴露于阳光时或皮肤上有细菌存在,会发生各种物理化学和生物化学反应,形成一些可能伤害皮肤的物质。因而皮肤清洁也是皮肤护理所必需的过程。When cleansing the skin, it removes sebum and stratum corneum fragments and their oxidative decomposition products, or cosmetic residues. These residual metabolites are unstable. When exposed to sunlight or bacteria on the skin, various physical, chemical and biochemical reactions will occur, forming some substances that may harm the skin. Therefore, skin cleansing is also a necessary process for skin care.

洁面乳的功能依靠表面活性剂来实现,目前常用的表面活性剂主要有四大类,分别为:皂基、SLS/SLES、氨基酸、APG四大类;由于清洁力和温和性在一定程度上存在冲突,所以通常清洁力强的洁面乳洗完脸后会水分流失快,出现干涩、脱皮现象;而较为温和的油类洁面乳,肤感过于油腻,且清洁力不足。The function of facial cleanser is achieved by surfactants. There are four main types of commonly used surfactants, namely: soap base, SLS/SLES, amino acid, and APG. Since there is a certain degree of conflict between cleansing power and mildness, cleansers with strong cleansing power usually cause moisture loss quickly after washing the face, resulting in dryness and peeling. Milder oil-based cleansers feel too greasy on the skin and lack cleansing power.

发明内容Summary of the invention

针对传统洁面乳的问题本发明提供了一种高油乳霜洁面乳,本发明采用以下技术方案来实现:In view of the problems of traditional facial cleansers, the present invention provides a high-oil cream facial cleanser, which is achieved by the following technical solutions:

一种组合物,以质量份计算含有以下组分:A composition comprising the following components in parts by mass:

油脂 5-40Grease 5-40

椰油酰羟乙磺酸酯钠 2-10Sodium Cocoyl Isethionate 2-10

C14-16烯烃磺酸钠 5-15。Sodium C14-16 Olefin Sulfonate 5-15.

优选的,所述组合物还包括保湿剂;所述保湿剂的质量份为5-25;所述保湿剂包括但不限于透明质酸钠、甘油、山梨糖醇、1,2-己二醇。Preferably, the composition further comprises a moisturizer; the mass parts of the moisturizer are 5-25; the moisturizer includes but is not limited to sodium hyaluronate, glycerin, sorbitol, and 1,2-hexanediol.

优选的,所述油脂为动物源、植物源油脂、矿物油脂、合成油脂中的至少一种。Preferably, the oil is at least one of animal-derived oil, plant-derived oil, mineral oil, and synthetic oil.

进一步优选的,油脂为向日葵籽油、橄榄油、霍霍巴油、白池花籽油等。More preferably, the oil is sunflower seed oil, olive oil, jojoba oil, meadowfoam seed oil, etc.

优选的,所述组合物还包括组分:Preferably, the composition further comprises:

阴离子表面活性剂 2-15Anionic surfactant 2-15

两性表面活性剂 3-8。Amphoteric surfactants 3-8.

所述阴离子表面活性剂包括但不限于:月桂醇聚醚硫酸酯钠、甲基椰油酰基牛磺酸钠、椰油酰氨基丙酸钠、椰油酰甘氨酸钾、椰油酰谷氨酸钠。The anionic surfactants include, but are not limited to, sodium laureth sulfate, sodium methyl cocoyl taurate, sodium cocoyl aminopropionate, potassium cocoyl glycinate, and sodium cocoyl glutamate.

所述两性表面活性剂包括但不限于:月桂酰胺丙基甜菜碱、月桂酰两性基乙酸、椰油酰胺丙基甜菜碱。The amphoteric surfactants include, but are not limited to, lauroyl amphoacetic acid, and cocamidopropyl betaine.

前述组合物的制备方法,将各组分和适量的水混合,然后加热、搅拌、均质至完全溶解。The preparation method of the above composition comprises mixing each component with an appropriate amount of water, and then heating, stirring and homogenizing until the components are completely dissolved.

一种高油乳霜洁面乳,包含前述任意一种组合物。A high-oil cream cleanser comprises any one of the above compositions.

前述任意一种组合物在制备人体清洁产品中的应用,所述人体清洁产品为淋洗类产品。Use of any of the above-mentioned compositions in the preparation of a human body cleaning product, wherein the human body cleaning product is a rinse-off product.

本发明为高油脂含量氨基酸洁面产品,具有护肤、卸妆/防晒和清洁的三合一功效,乳霜质地,深层清洁的同时起到即时滋润肌肤的效果,无需再次护肤。乳霜质地高含量植物油脂,易铺展、快速起泡能深层去除毛孔污垢,在清洁皮肤的同时,保护肌肤锁水层免受伤害,持久保持洁净清透。The present invention is a high-oil amino acid facial cleanser with three-in-one effects of skin care, makeup removal/sunscreen and cleansing. It has a cream texture and can instantly moisturize the skin while deep cleansing, without the need for re-skin care. The cream texture has a high content of plant oil, is easy to spread, and foams quickly to deeply remove dirt from the pores. While cleaning the skin, it protects the skin's water-locking layer from damage, keeping it clean and clear for a long time.

本发明的有益技术效果体现在以下方面:The beneficial technical effects of the present invention are embodied in the following aspects:

(1)本发明使用特定的表活搭配体系(椰油酰羟乙磺酸酯钠、C14-16烯烃磺酸钠等)可以使高含量(5-40%)的各种油脂被包裹在表活形成的特定胶束结构中,形成稳定的体系。(1) The present invention uses a specific surfactant system (sodium cocoyl isethionate, sodium C14-16 olefin sulfonate, etc.) to allow high content (5-40%) of various oils to be encapsulated in a specific micelle structure formed by the surfactant to form a stable system.

(2)本发明优选了温和的表活和天然植物油脂起到即时滋润肌肤的效果,深层清洁的同时令肌肤如丝般柔软顺滑。(2) The present invention selects mild surfactants and natural plant oils to instantly moisturize the skin, deeply cleansing it while leaving the skin soft and smooth as silk.

(3)本发明使用特殊的皮肤调理剂组合,使得在清洁后具有良好的保湿润肤效果,且天然来源易降解、无污染。(3) The present invention uses a special combination of skin conditioning agents, which has a good moisturizing and emollient effect after cleansing, and is of natural origin, easily degradable and pollution-free.

(4)本发明在不添加乳化剂的情况下,表面活性剂和大量天然油脂形成了稳定的液晶结构,遇水泡沫丰富且微乳化,清洁且滋润肌肤。(4) In the present invention, without adding an emulsifier, the surfactant and a large amount of natural oil form a stable liquid crystal structure, which produces rich and micro-emulsified foam when in contact with water, cleansing and moisturizing the skin.

(5)本发明配方中,可以添加大量的水溶性的活性成分,也可以添加大量油溶性的活性成分,拓展了产品的功效及配方的灵活性。(5) A large amount of water-soluble active ingredients or oil-soluble active ingredients can be added to the formula of the present invention, thereby expanding the efficacy of the product and the flexibility of the formula.

附图说明BRIEF DESCRIPTION OF THE DRAWINGS

图1为本发明成品在显微镜下的液晶图片。FIG. 1 is a liquid crystal picture of the finished product of the present invention under a microscope.

图2为本发明发泡后的实验图片。FIG. 2 is an experimental picture of the present invention after foaming.

具体实施方式Detailed ways

为了更好地理解本发明,下面结合具体实施例对本发明作进一步的描述,其中实施例中使用的术语是为了描述特定的具体实施方案,不构成对本发明保护范围的限制。In order to better understand the present invention, the present invention is further described below in conjunction with specific examples, wherein the terms used in the examples are for describing specific embodiments and do not constitute limitations on the scope of protection of the present invention.

本发明中部分成分的来源如下表1:The sources of some ingredients in the present invention are shown in Table 1 below:

表1Table 1

制备方法:Preparation:

开启加热,在搅拌状态下加入水、保湿剂、PH调节剂、润肤剂、表面活性剂搅拌至完全溶解,加入油脂保持高速搅拌至体系均一。Turn on the heating, add water, moisturizer, pH regulator, emollient, and surfactant while stirring until completely dissolved, add oil and keep stirring at high speed until the system is uniform.

具体成分配比如下表2所示。The specific composition ratio is shown in Table 2 below.

表2高油乳霜洁面乳配比Table 2 High oil cream cleanser ratio

原料/序号Raw material/serial number 实施例1Example 1 实施例2Example 2 实施例3Example 3 实施例4Example 4 实施例5Example 5 白池花籽油Lignum Meadowfoam Seed Oil -- -- 4040 -- -- 霍霍巴油Jojoba Oil -- -- -- 1010 -- 橄榄油olive oil -- -- -- 1010 -- 分馏椰子油Fractionated Coconut Oil -- -- -- 1010 -- 甜杏仁油Sweet almond oil -- -- -- -- 1010 凡士林Vaseline -- -- -- -- 2020 高油酸葵花籽油High Oleic Sunflower Oil 55 4040 -- -- -- 椰油酰羟乙磺酸酯钠Sodium Cocoyl Isethionate 22 1010 88 22 22 C14-16烯烃磺酸钠Sodium C14-16 Olefin Sulfonate 55 1515 1010 55 55 甘油glycerin -- -- 55 -- -- 硬脂醇Stearyl Alcohol -- -- -- 2525 -- 山梨糖醇Sorbitol -- -- -- -- 2020 椰油酰氨基丙酸钠Sodium Cocoamidopropionate -- -- 55 -- -- LHSB-50LHSB-50 -- -- 55 -- -- 椰油酰甘氨酸钾Potassium Cocoyl Glycinate -- -- 55 -- -- 柠檬酸Citric Acid -- -- 0.10.1 0.10.1 0.10.1 月桂醇聚醚硫酸酯钠Sodium Laureth Sulfate -- -- -- 11 -- 甲基椰油酰基牛磺酸钠Sodium Methyl Cocoyl Taurate -- -- -- -- 55 月桂酰两性基乙酸Lauroamphoacetic acid -- -- -- 22 88 椰油酰胺丙基甜菜碱Cocamidopropyl Betaine -- -- -- 11 11 椰油酰谷氨酸钠Sodium Cocoyl Glutamate -- -- -- -- 22

表2(续)高油乳霜洁面乳配比Table 2 (Continued) High Oil Cream Cleanser Ratio

原料/序号Raw material/serial number 对比例6Comparative Example 6 对比例7Comparative Example 7 对比例8Comparative Example 8 对比例9Comparative Example 9 对比例10Comparative Example 10 高油酸葵花籽油High Oleic Sunflower Oil 4040 4040 4040 4040 5050 椰油酰羟乙磺酸酯钠Sodium Cocoyl Isethionate -- 1818 1818 1313 88 C14-16烯烃磺酸钠Sodium C14-16 Olefin Sulfonate 1818 -- 1010 1010 1010 甘油glycerin 55 55 55 55 55 椰油酰氨基丙酸钠Sodium Cocoamidopropionate 55 55 -- 55 55 LHSB-50LHSB-50 55 55 -- 55 55 椰油酰甘氨酸钾Potassium Cocoyl Glycinate 55 55 55 -- 55 柠檬酸Citric Acid 0.10.1 0.10.1 0.10.1 0.10.1 0.10.1

表2中“-”表示没有添加;单位为质量份。In Table 2, “-” means no addition; the unit is part by mass.

对比例6与实施例3的区别在于:没有椰油酰羟乙磺酸酯钠。The difference between Comparative Example 6 and Example 3 is that there is no sodium cocoyl isethionate.

对比例7与实施例3的区别在于:没有使用C14-16烯烃磺酸钠。The difference between Comparative Example 7 and Example 3 is that no sodium C14-16 olefin sulfonate was used.

对比例8与实施例3的区别在于:没有使用椰油酰氨基丙酸钠和月桂酰胺丙基羟磺基甜菜碱。The difference between Comparative Example 8 and Example 3 is that sodium cocoamidopropionate and lauramidopropyl hydroxysulfobetaine are not used.

对比例9与实施例3的区别在于:没有使用椰油酰甘氨酸钾。The difference between Comparative Example 9 and Example 3 is that potassium cocoyl glycinate is not used.

对比例10与实施例3的区别在于:使用了过量油脂。The difference between Comparative Example 10 and Example 3 is that excessive grease was used.

性能测试:Performance Testing:

(1)斑贴测试(1) Patch test

以2015年《化妆品安全技术规范》为参照标准,对实施例1-5的组合物进行化妆品刺激性评价,测试方法为皮肤贴斑试验,对年龄16-65岁随机分布的60人进行试验。With reference to the 2015 Technical Specifications for Safety of Cosmetics, the compositions of Examples 1-5 were evaluated for cosmetic irritation. The test method was a skin patch test, and 60 randomly distributed people aged 16-65 were tested.

测试方法:将受试物放入斑试器中,用量为0.02-0.025ml,将加有受试物的斑试器用无刺激布基胶带覆于受试者背部或前臂曲侧,用手掌轻压使之均匀贴附在皮肤表面,持续24小时,去除受试斑试器后30分钟,待压痕消失后观察皮肤反应。若结果为阴性,于斑贴试验后24小时和48小时分别再次进行观察。Test method: Put the test substance into the patch tester, the dosage is 0.02-0.025ml, cover the patch tester with the test substance on the back or forearm of the subject with non-irritating cloth-based tape, and gently press it with the palm to make it evenly adhere to the skin surface for 24 hours. After removing the test patch tester, observe the skin reaction 30 minutes after the indentation disappears. If the result is negative, observe again 24 hours and 48 hours after the patch test.

评价标准:evaluation standard:

0级:阴性反应;Grade 0: negative reaction;

1级:可疑反应,仅有微弱红斑;Grade 1: Suspicious reaction, only slight erythema;

2级:弱阳性反应,红斑、浸润、水肿、可有丘疹;Grade 2: weak positive reaction, erythema, infiltration, edema, and papules may be present;

3级:强阳性反应,红斑、浸润、水肿、可有丘疹、反应可超出受试区;Grade 3: Strong positive reaction, erythema, infiltration, edema, papules, and the reaction may extend beyond the test area;

4级:极强阳性反应,明显红斑、严重浸润、水肿、融合性疱疹、反应超出受试区。Grade 4: Very strong positive reaction, obvious erythema, severe infiltration, edema, confluent herpes, and reaction beyond the test area.

测试结果:所有受试者的皮肤反应均为阴性。Test results: Skin reactions were negative in all subjects.

上述测试结果表明,实施例1-5的组合物对皮肤温和无刺激,使用安全。The above test results show that the compositions of Examples 1-5 are mild and non-irritating to the skin and safe to use.

(2)起泡测试(2) Foaming test

利用罗氏泡沫仪测试实施例和对比例得到产品的增泡和稳泡性能,测试方法参照GB/T 7462-1994,分别记录30s、15min的泡沫高度,结果见表3所示。The foam increasing and stabilizing properties of the products of the examples and comparative examples were tested using a Roche foam meter. The testing method was based on GB/T 7462-1994. The foam heights at 30 seconds and 15 minutes were recorded, respectively. The results are shown in Table 3.

表3泡沫高度测试Table 3 Foam height test

组别Group 30S(mm)30S(mm) 15min(mm)15min(mm) 实施例1Example 1 164164 147147 实施例2Example 2 175175 164164 实施例3Example 3 194194 180180 实施例4Example 4 190190 175175 实施例5Example 5 192192 173173 对比例6Comparative Example 6 172172 153153 对比例7Comparative Example 7 168168 152152 对比例8Comparative Example 8 169169 156156 对比例9Comparative Example 9 174174 153153 对比例10Comparative Example 10 164164 128128

根据实施例3和对比例6、7、8、9的对比可知,当本发明的表面活性剂组合缺少了任意一种成分时,起泡量以及泡沫持久度都会相应的减少。According to the comparison between Example 3 and Comparative Examples 6, 7, 8 and 9, when the surfactant combination of the present invention lacks any one component, the foaming amount and the foam durability will be reduced accordingly.

根据实施例3和对比例10的对比可知,本发明能承载大量的油脂,但是有较高的上限。According to the comparison between Example 3 and Comparative Example 10, it can be seen that the present invention can carry a large amount of grease, but has a higher upper limit.

本发明图1为实施例3起泡实验前的显微图片,可看到明显的液晶结构;图2为实施例3在正式起泡实验前的初试图片。FIG1 of the present invention is a microscopic picture of Example 3 before the bubbling experiment, in which an obvious liquid crystal structure can be seen; FIG2 is an initial attempt film of Example 3 before the formal bubbling experiment.

(3)保湿能力测试(3) Moisturizing ability test

以实施例和对比例制备的洁面乳作为比较对象,采用Corneometer CM825测量使用前后皮肤角质层的电容量,衡量角质层含水量的变化。The facial cleansers prepared in the examples and comparative examples were used as comparison objects, and Corneometer CM825 was used to measure the capacitance of the stratum corneum before and after use to measure the change in the water content of the stratum corneum.

受试者共30名,其中女性15名,男性15名,年龄为20-40岁,平均年龄为28岁。受试者洗净双手前臂,在设定的湿度环境下静坐30min,在受试者的左右前臂各选取3×3cm2的正方形实验区域,以左臂作为实施例和对比例的洁面乳的测试区域,右臂的对称区域作为空白对照,用Corneometer CM825检测每个实验部位的水分含量,重复5次,得出平均值进行记录。There were 30 subjects in total, including 15 females and 15 males, aged 20-40 years old, with an average age of 28 years old. The subjects washed their forearms and sat quietly for 30 minutes in a set humidity environment. A 3×3 cm 2 square experimental area was selected from each of the left and right forearms of the subjects, and the left arm was used as the test area for the facial cleansing milk of the embodiment and the comparative example, and the symmetrical area of the right arm was used as a blank control. The moisture content of each experimental part was detected by Corneometer CM825, and the test was repeated 5 times to obtain the average value for recording.

皮肤水合率的计算公式为:The formula for calculating skin hydration rate is:

水合率(%)=[(测试值-空白值)/空白值]*100%Hydration rate (%) = [(test value - blank value) / blank value] * 100%

结果如表4所示。The results are shown in Table 4.

表4保湿能力测试Table 4 Moisturizing ability test

组别Group 0h0h 1h1h 4h4h 实施例1Example 1 68.24%68.24% 47.77%47.77% 39.58%39.58% 实施例2Example 2 74.81%74.81% 53.12%53.12% 44.89%44.89% 实施例3Example 3 79.11%79.11% 56.96%56.96% 49.05%49.05% 实施例4Example 4 80.15%80.15% 57.71%57.71% 49.69%49.69% 实施例5Example 5 78.32%78.32% 56.39%56.39% 48.56%48.56% 对比例6Comparative Example 6 72.1%72.1% 49.03%49.03% 39.66%39.66% 对比例7Comparative Example 7 75.4%75.4% 50.52%50.52% 42.22%42.22% 对比例8Comparative Example 8 74.3%74.3% 50.48%50.48% 39.38%39.38% 对比例9Comparative Example 9 76.8%76.8% 49.92%49.92% 41.47%41.47% 对比例10Comparative Example 10 83.12%83.12% 57.21%57.21% 48.68%48.68%

根据实施例3和对比例6、7、8、9的对比可知,当本发明的表面活性剂组合缺少了任意一种成分时,其保湿能力都有一定的下降。According to the comparison between Example 3 and Comparative Examples 6, 7, 8 and 9, it can be seen that when the surfactant combination of the present invention lacks any one component, its moisturizing ability is reduced to a certain extent.

虽然对比例10的保湿性能最好,但这是由大量的油脂所带来的,受试者反馈对比例10的样品较为粘滞,肤感不适。Although Comparative Example 10 has the best moisturizing performance, this is caused by a large amount of oil. The test subjects reported that the sample of Comparative Example 10 was relatively sticky and uncomfortable to the skin.

上述详细说明是针对本发明其中之一可行实施例的具体说明,该实施例并非用以限制本发明的专利范围,凡未脱离本发明所为的等效实施或变更,均应包含于本发明技术方案的范围内。The above detailed description is a specific description of one feasible embodiment of the present invention. The embodiment is not intended to limit the patent scope of the present invention. Any equivalent implementation or modification that does not deviate from the present invention should be included in the scope of the technical solution of the present invention.

Claims (9)

1.一种组合物,其特征在于,以质量份计算含有以下组分:1. A composition, characterized in that it contains the following components calculated by mass: 油脂5-40Grease 5-40 椰油酰羟乙磺酸酯钠2-10Sodium Cocoyl Isethionate 2-10 C14-16烯烃磺酸钠5-15。Sodium C14-16 olefin sulfonate 5-15. 2.根据权利要求1所述的组合物,其特征在于,还包括保湿剂,所述保湿剂的质量份为5-25。2. The composition according to claim 1, further comprising a humectant, wherein the mass parts of the humectant is 5-25. 3.根据权利要求1所述的组合物,其特征在于,所述油脂为动物源、植物源油脂、矿物油脂、合成油脂中的至少一种。3. The composition according to claim 1, characterized in that the oil is at least one of animal-derived oil, plant-derived oil, mineral oil, and synthetic oil. 4.根据权利要求1所述的组合物,其特征在于,还包括组分:4. The composition according to claim 1, further comprising: 阴离子表面活性剂2-15Anionic surfactant 2-15 两性表面活性剂3-8。Amphoteric surfactants 3-8. 5.根据权利要求4所述的组合物,其特征在于,所述阴离子表面活性剂包括以下中的至少一种:月桂醇聚醚硫酸酯钠、甲基椰油酰基牛磺酸钠、椰油酰氨基丙酸钠、椰油酰甘氨酸钾、椰油酰谷氨酸钠。5. The composition according to claim 4, characterized in that the anionic surfactant comprises at least one of the following: sodium laureth sulfate, sodium methyl cocoyl taurate, sodium cocoyl aminopropionate, potassium cocoyl glycinate, sodium cocoyl glutamate. 6.根据权利要求4所述的组合物,其特征在于,所述两性表面活性剂包括以下中的至少一种:月桂酰胺丙基甜菜碱、月桂酰两性基乙酸、椰油酰胺丙基甜菜碱。6. The composition according to claim 4, characterized in that the amphoteric surfactant comprises at least one of the following: lauroyl amphoacetic acid, cocoyl amphopropyl betaine. 7.权利要求1-6任一所述的组合物的制备方法,其特征在于,将各组分和适量的水混合,然后加热搅拌、均质至完全溶解。7. A method for preparing the composition according to any one of claims 1 to 6, characterized in that each component is mixed with an appropriate amount of water, and then heated, stirred and homogenized until completely dissolved. 8.一种高油乳霜洁面乳,其特征在于包含权利要求1-7任一所述的组合物。8. A high-oil cream cleanser, characterized by comprising the composition according to any one of claims 1 to 7. 9.权利要求1-6任一所述的组合物在制备人体清洁产品中的应用,其特征在于,所述人体清洁产品为淋洗类产品。9. Use of the composition according to any one of claims 1 to 6 in the preparation of a human body cleaning product, characterized in that the human body cleaning product is a rinse-off product.
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