CN118162603A - A device and method for controlling the grain growth direction of a directional or single crystal casting - Google Patents
A device and method for controlling the grain growth direction of a directional or single crystal casting Download PDFInfo
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- CN118162603A CN118162603A CN202410592362.8A CN202410592362A CN118162603A CN 118162603 A CN118162603 A CN 118162603A CN 202410592362 A CN202410592362 A CN 202410592362A CN 118162603 A CN118162603 A CN 118162603A
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- 238000005266 casting Methods 0.000 title claims abstract description 83
- 239000013078 crystal Substances 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title claims abstract description 33
- 238000010438 heat treatment Methods 0.000 claims abstract description 83
- 239000007788 liquid Substances 0.000 claims abstract description 27
- 238000001816 cooling Methods 0.000 claims description 34
- 238000003723 Smelting Methods 0.000 claims description 19
- 239000000498 cooling water Substances 0.000 claims description 15
- 239000000956 alloy Substances 0.000 claims description 13
- 229910045601 alloy Inorganic materials 0.000 claims description 13
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 229910002804 graphite Inorganic materials 0.000 claims description 3
- 239000010439 graphite Substances 0.000 claims description 3
- 238000001363 water suppression through gradient tailored excitation Methods 0.000 claims description 3
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- 230000007547 defect Effects 0.000 abstract description 6
- 238000007711 solidification Methods 0.000 abstract description 4
- 230000008023 solidification Effects 0.000 abstract description 4
- 238000005516 engineering process Methods 0.000 abstract description 3
- 238000005058 metal casting Methods 0.000 abstract description 2
- 238000002474 experimental method Methods 0.000 description 12
- 238000009413 insulation Methods 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 238000010586 diagram Methods 0.000 description 4
- 239000007787 solid Substances 0.000 description 3
- 239000002826 coolant Substances 0.000 description 2
- 238000009415 formwork Methods 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
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- 101100012902 Saccharomyces cerevisiae (strain ATCC 204508 / S288c) FIG2 gene Proteins 0.000 description 1
- 241001062472 Stokellia anisodon Species 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D27/00—Treating the metal in the mould while it is molten or ductile ; Pressure or vacuum casting
- B22D27/04—Influencing the temperature of the metal, e.g. by heating or cooling the mould
- B22D27/045—Directionally solidified castings
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B11/00—Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method
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- Crystallography & Structural Chemistry (AREA)
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- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
本发明公开了一种定向或单晶铸件晶粒生长方向控制设备及其控制方法,属于金属铸造技术领域,包括设备外罩、设备底座和水冷托盘,水冷底盘包括由外至内依次套设的水冷外环、水冷中环和水冷内圆,水冷外环固定在设备底座的顶部,控制腔室内设有升降机构,设备底座的顶部设有进出口,水冷中环的顶面可拆卸的安装有环形模壳,水冷内圆的顶面安装有位于环形模壳中心的加热棒,设备外罩固定在水冷外环上并罩设在环形模壳外,设备外罩的内壁上设有加热体,设备外罩的顶部安装有浇口杯。加热棒和加热体可提高铸件凝固过程中的温度梯度,使铸件晶粒取向好,不易产生断头晶和杂晶,在水冷托盘尤其是水冷内圆作用下,能够改善固液界面形貌,降低缺陷的产生。
The invention discloses a directional or single crystal casting grain growth direction control device and a control method thereof, belonging to the field of metal casting technology, comprising a device cover, a device base and a water-cooled tray, the water-cooled chassis comprising a water-cooled outer ring, a water-cooled middle ring and a water-cooled inner circle which are sequentially sleeved from the outside to the inside, the water-cooled outer ring is fixed on the top of the device base, a lifting mechanism is arranged in the control chamber, an inlet and outlet are arranged on the top of the device base, a ring mold shell is detachably installed on the top surface of the water-cooled middle ring, a heating rod located at the center of the ring mold shell is installed on the top surface of the water-cooled inner circle, the device cover is fixed on the water-cooled outer ring and covered outside the ring mold shell, a heating body is arranged on the inner wall of the device cover, and a pouring cup is arranged on the top of the device cover. The heating rod and the heating body can improve the temperature gradient during the solidification process of the casting, so that the grain orientation of the casting is good, and it is not easy to produce broken crystals and miscellaneous crystals. Under the action of the water-cooled tray, especially the water-cooled inner circle, the solid-liquid interface morphology can be improved and the generation of defects can be reduced.
Description
技术领域Technical Field
本发明涉及金属铸造技术领域,特别是涉及一种定向或单晶铸件晶粒生长方向控制设备及其控制方法。The invention relates to the technical field of metal casting, and in particular to a device for controlling the grain growth direction of a directional or single crystal casting and a control method thereof.
背景技术Background technique
定向柱晶叶片和单晶叶片由于消除了横向晶界,其纵向力学性得到了明显提高,因此通常被用来作为航机和燃机关键的热端部件铸件。该类叶片主要通过快速凝固法(HRS)来制备,虽然工艺成熟稳定,但其温度梯度低,并且随着抽拉距离的增加,下降很快,导致铸件的晶粒取向偏离轴向增大甚至出现等轴晶。同时,在实际生产中,由于模壳结构的不同,模壳出现阴面和阳面,铸件固液界面弯曲变形,极易导致铸件出现晶粒取向偏差增加和断头晶,严重降低了铸件的综合使用性能。Directed columnar crystal blades and single crystal blades have significantly improved their longitudinal mechanical properties due to the elimination of transverse grain boundaries, so they are usually used as key hot end castings for aircraft and gas turbines. This type of blade is mainly prepared by rapid solidification (HRS). Although the process is mature and stable, its temperature gradient is low and drops rapidly with the increase of the pulling distance, causing the grain orientation of the casting to deviate from the axial direction and even the appearance of equiaxed crystals. At the same time, in actual production, due to the different mold shell structures, the mold shell has negative and positive surfaces, and the solid-liquid interface of the casting is bent and deformed, which can easily lead to increased grain orientation deviation and broken crystals in the casting, seriously reducing the comprehensive performance of the casting.
发明内容Summary of the invention
本发明的目的是解决上述技术问题,提供一种定向或单晶铸件晶粒生长方向控制设备及其控制方法,在加热棒和加热体作用下,浇注时可以为铸件的内外侧提供热量进行保温,提高定向凝固过程中铸件的温度梯度,使其生长中的组织得到细化,性能提高,生产定向和单晶铸件晶粒取向好,不易产生断头晶和杂晶,在水冷托盘作用下,尤其是水冷内圆对铸件中心进行降温,能够保持铸件固液界面稳定不倾斜,改善固液界面形貌,降低单晶铸件大平台边角出现不同取向晶粒的几率,提高定向或单晶铸件的合格率,降低缺陷的产生。The purpose of the present invention is to solve the above-mentioned technical problems and provide a device for controlling the grain growth direction of a directional or single crystal casting and a control method thereof. Under the action of a heating rod and a heating body, heat can be provided to the inner and outer sides of the casting for insulation during pouring, thereby increasing the temperature gradient of the casting during directional solidification, refining its growing structure, improving performance, producing directional and single crystal castings with good grain orientation, and not prone to producing broken crystals and miscellaneous crystals. Under the action of a water-cooled tray, especially a water-cooled inner circle, the center of the casting is cooled, the solid-liquid interface of the casting can be kept stable and not tilted, the solid-liquid interface morphology can be improved, the probability of differently oriented grains appearing at the edges and corners of large platforms of single crystal castings can be reduced, the qualified rate of directional or single crystal castings can be improved, and the generation of defects can be reduced.
为实现上述目的,本发明提供了如下方案:本发明公开了一种定向或单晶铸件晶粒生长方向控制设备,包括设备外罩、内设有控制腔室的设备底座以及轴线竖向设置的水冷托盘,所述水冷底盘包括由外至内依次紧密套设的水冷外环、水冷中环以及水冷内圆,所述水冷外环固定连接在所述设备底座的顶部,所述控制腔室内设有用于独立驱使所述水冷中环和所述水冷内圆升降的升降机构,所述设备底座的顶部设有供所述水冷中环和所述水冷内圆进出所述控制腔室的进出口,所述水冷中环的顶面可拆卸的安装有环形模壳,所述水冷内圆的顶面安装有同轴位于所述环形模壳中心的加热棒,所述设备外罩固定在所述水冷外环上并罩设在所述环形模壳外,所述设备外罩的内壁上设有位于所述环形模壳四周的加热体,所述设备外罩的顶部安装有用于向所述环形模壳内浇注的浇口杯。To achieve the above-mentioned purpose, the present invention provides the following scheme: The present invention discloses a device for controlling the grain growth direction of directional or single crystal castings, comprising a device cover, a device base with a control chamber therein, and a water-cooled tray with an axis vertically arranged, the water-cooled chassis comprising a water-cooled outer ring, a water-cooled middle ring and a water-cooled inner circle which are tightly sleeved from the outside to the inside in sequence, the water-cooled outer ring is fixedly connected to the top of the device base, a lifting mechanism for independently driving the water-cooled middle ring and the water-cooled inner circle to rise and fall is arranged in the control chamber, an inlet and outlet for the water-cooled middle ring and the water-cooled inner circle to enter and exit the control chamber is arranged on the top of the device base, an annular mold shell is detachably mounted on the top surface of the water-cooled middle ring, a heating rod coaxially located at the center of the annular mold shell is mounted on the top surface of the water-cooled inner circle, the device cover is fixed on the water-cooled outer ring and is covered outside the annular mold shell, a heating body located around the annular mold shell is arranged on the inner wall of the device cover, and a pouring cup for pouring into the annular mold shell is mounted on the top of the device cover.
优选地,所述加热棒为石墨加热棒。Preferably, the heating rod is a graphite heating rod.
优选地,所述设备外罩的内壁上设有保温层。Preferably, a heat-insulating layer is provided on the inner wall of the equipment housing.
优选地,其特征在于,所述加热体为磁加热体,所述设备外罩的外壁上设有为所述磁加热体提供感应磁场的加热线圈。Preferably, it is characterized in that the heating body is a magnetic heating body, and a heating coil for providing an induced magnetic field for the magnetic heating body is provided on the outer wall of the device cover.
优选地,所述水冷中环和所述水冷内圆通过锁止机构互锁。Preferably, the water-cooled middle ring and the water-cooled inner circle are interlocked by a locking mechanism.
优选地,所述锁止机构包括锁紧螺栓和对应设置在所述水冷中环和所述水冷内圆上的螺栓耳板。Preferably, the locking mechanism comprises locking bolts and bolt ear plates correspondingly arranged on the water-cooled middle ring and the water-cooled inner circle.
优选地,所述升降机构包括能够上下升降的抽拉杆,所述水冷内圆的底壁同轴连接有一个所述抽拉杆,所述水冷中环的底壁连接有分设在其轴线两侧的两个所述抽拉杆。Preferably, the lifting mechanism comprises a pull-out rod capable of being lifted up and down, the bottom wall of the water-cooled inner circle is coaxially connected to one of the pull-out rods, and the bottom wall of the water-cooled middle ring is connected to two pull-out rods arranged on both sides of its axis.
优选地,所述抽拉杆为中空杆,所述水冷内圆的抽拉杆一端与所述水冷内圆连通,另一端设有冷却水门,所述水冷中环的两个抽拉杆一端与所述水冷中环连通,另一端分别设有冷却水进口和冷却水出口。Preferably, the pull-out rod is a hollow rod, one end of the pull-out rod of the water-cooled inner circle is connected to the water-cooled inner circle, and the other end is provided with a cooling water gate, and one end of the two pull-out rods of the water-cooled middle ring are connected to the water-cooled middle ring, and the other end is respectively provided with a cooling water inlet and a cooling water outlet.
还公开了一种定向或单晶铸件晶粒生长方向控制方法,包括以下步骤:Also disclosed is a method for controlling the grain growth direction of a directional or single crystal casting, comprising the following steps:
S1、将上述的定向或单晶铸件晶粒生长方向控制设备安装在保温炉内,将浇口杯与熔炼室连通;S1. Install the above-mentioned directional or single crystal casting grain growth direction control device in a holding furnace, and connect the pouring cup with the melting chamber;
S2、对保温炉和熔炼室进行抽真空,熔炼室进行熔炼,并安预设保温时间保温,将熔炼的合金液通过浇口杯浇注到环形模壳内,加热体和加热棒进行加热保温,浇注完后安预设静置时间静置,然后关闭加热棒和加热体;S2, the holding furnace and the smelting chamber are evacuated, the smelting chamber is smelted, and the smelting time is set to keep the temperature, the molten alloy liquid is poured into the annular mold shell through the pouring cup, the heating body and the heating rod are heated and kept warm, and after the pouring is completed, the preset rest time is set to stand, and then the heating rod and the heating body are turned off;
S3、水冷外环、水冷中环以及水冷内圆内注入冷却水,水冷中环先下降,待铸件抽拉结束,水冷内圆再下降到与所述水冷中环同一水平位置,待所述环形模壳温度冷却到预设冷却温度以下后,将所述环形模壳取出,获得定向铸件或单晶铸件。S3, cooling water is injected into the water-cooled outer ring, the water-cooled middle ring and the water-cooled inner circle. The water-cooled middle ring descends first. After the casting is pulled out, the water-cooled inner circle descends to the same horizontal position as the water-cooled middle ring. After the temperature of the annular mold shell is cooled to below the preset cooling temperature, the annular mold shell is taken out to obtain a directional casting or a single crystal casting.
优选地,熔炼时温度控制在1500-1570℃,预设保温时间为3-5min;浇注时温度控制在1480-1550℃,预设静置时间为2-5min;所述预设冷却温度为100℃。Preferably, the temperature during smelting is controlled at 1500-1570°C, and the preset insulation time is 3-5 minutes; the temperature during pouring is controlled at 1480-1550°C, and the preset standing time is 2-5 minutes; the preset cooling temperature is 100°C.
本发明相对于现有技术取得了以下技术效果:Compared with the prior art, the present invention has achieved the following technical effects:
本发明的控制设备中,加热棒和加热体可以为铸件的内外侧提供热量进行保温,提高了铸件在定向凝固过程中的温度梯度,使其生长中的组织得到细化,性能提高,用此技术生产的定向和单晶铸件晶粒取向好,不易产生断头晶和杂晶,水冷托盘中的水冷内圆能够对铸件的中心降温,使得铸件的固液界面稳定不倾斜,改善固液界面形貌,降低单晶铸件大平台边角出现不同取向晶粒的几率,提高定向或单晶铸件的合格率,降低缺陷的产生。In the control device of the present invention, the heating rod and the heating body can provide heat for the inner and outer sides of the casting for insulation, thereby improving the temperature gradient of the casting during the directional solidification process, refining the growing structure, and improving the performance. The directional and single crystal castings produced by this technology have good grain orientation and are not prone to broken crystals and mixed crystals. The water-cooled inner circle in the water-cooled tray can cool the center of the casting, making the solid-liquid interface of the casting stable and not tilted, improving the solid-liquid interface morphology, reducing the probability of differently oriented grains appearing at the edges and corners of large platforms of single crystal castings, improving the qualified rate of directional or single crystal castings, and reducing the occurrence of defects.
附图说明BRIEF DESCRIPTION OF THE DRAWINGS
为了更清楚地说明本发明实施例或现有技术中的技术方案,下面将对实施例中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本发明的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required for use in the embodiments will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative work.
图1为定向或单晶铸件晶粒生长方向控制设备的内部结构示意图;FIG1 is a schematic diagram of the internal structure of a device for controlling the grain growth direction of a directional or single crystal casting;
图2为水冷托盘的仰视结构示意图;FIG2 is a schematic diagram of the structure of the water cooling tray when viewed from above;
图3为控制设备(水冷中环先下降)的运动过程示意图;Figure 3 is a schematic diagram of the motion process of the control device (the water-cooled middle ring descends first);
图4为控制设备(水冷中环和水冷内圆同步下降)的运动过程示意图;FIG4 is a schematic diagram of the motion process of the control device (the water-cooled middle ring and the water-cooled inner circle descend synchronously);
图5为不同工艺下铸件的固液界面(a加热棒加热和中心水冷冷却,b加热棒加热,c传统HRS法);Figure 5 shows the solid-liquid interface of the casting under different processes (a heating with heating rod and central water cooling, b heating with heating rod, c traditional HRS method);
图6为不同工艺下铸件的晶粒取向(a加热棒加热和中心水冷冷却,b加热棒加热,c传统HRS法)。Figure 6 shows the grain orientation of the castings under different processes (a heating with heating rod and central water cooling, b heating with heating rod, c traditional HRS method).
附图标记说明:1、设备外罩;2、设备底座;3、水冷外环;4、水冷中环;5、水冷内圆;6、环形模壳;7、加热棒;8、加热体;9、加热线圈;10、浇口杯;11、抽拉杆;12、保温层;13、隔热垫;14、伸缩缸;15、连接架;16、导向架;17、锁紧螺栓;18、定位座。Explanation of the accompanying drawings: 1. Equipment cover; 2. Equipment base; 3. Water-cooled outer ring; 4. Water-cooled middle ring; 5. Water-cooled inner circle; 6. Ring-shaped mold shell; 7. Heating rod; 8. Heating body; 9. Heating coil; 10. Pouring cup; 11. Pull rod; 12. Insulation layer; 13. Insulation pad; 14. Telescopic cylinder; 15. Connecting frame; 16. Guide frame; 17. Locking bolt; 18. Positioning seat.
具体实施方式Detailed ways
下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
实施例1Example 1
本实施例提供了一种定向或单晶铸件晶粒生长方向控制设备,如图1至图6所示,包括设备外罩1、设备底座2以及水冷托盘。水冷托盘的轴线竖向设置,水冷托盘主要由水冷外环3、水冷中环4以及水冷内圆5构成,水冷外环3、水冷中环4以及水冷内圆5由外至内依次套设且相互贴合。其中水冷外环3的底面固定连接在设备底座2的顶部。设备底座2内设有控制腔室,控制腔室内设有升降机构,升降机构用于独立驱动水冷中环4和水冷内圆5升降,即可分别控制水冷中环4和水冷内圆5升降,也可以同步控制水冷中环4和水冷内圆5升降。设备底座2的顶部设有与控制腔室连通的进出口,水冷中环4和水冷内圆5在升降机构驱动下升降时,可通过进出口进出控制腔室。水冷中环4的顶面可拆卸的安装有环形模壳6,水冷内圆5的顶面安装有加热棒7,优选地,加热棒7也可以采用可拆卸的安装方式,如在水冷内圆5上设置一个定位座18,定位座18上设有定位孔,供加热棒7插接。加热棒7竖向设置且位于环形模壳6的中心。设备外罩1固定连接在水冷外环3的顶面上,且设备外罩1将环形模壳6罩入其中,设备外罩1的顶部安装有浇口杯10,通过浇口杯10可向环形模壳6内浇注的金属熔液,作为优选地,浇口杯10可拆卸的安装在设备外罩1的顶部,如在设备外罩1上设置一个卡扣装置,来卡住浇口杯10。设备外罩1的内壁上设有若干加热体8,若干加热体8围设在环形模壳6的四周。The present embodiment provides a device for controlling the grain growth direction of directional or single crystal castings, as shown in Figures 1 to 6, including a device housing 1, a device base 2, and a water-cooled tray. The axis of the water-cooled tray is arranged vertically, and the water-cooled tray is mainly composed of a water-cooled outer ring 3, a water-cooled middle ring 4, and a water-cooled inner circle 5. The water-cooled outer ring 3, the water-cooled middle ring 4, and the water-cooled inner circle 5 are sequentially arranged from the outside to the inside and fit each other. The bottom surface of the water-cooled outer ring 3 is fixedly connected to the top of the device base 2. A control chamber is provided in the device base 2, and a lifting mechanism is provided in the control chamber. The lifting mechanism is used to independently drive the water-cooled middle ring 4 and the water-cooled inner circle 5 to rise and fall, which can control the water-cooled middle ring 4 and the water-cooled inner circle 5 to rise and fall respectively, and can also control the water-cooled middle ring 4 and the water-cooled inner circle 5 to rise and fall synchronously. An inlet and outlet connected to the control chamber are provided at the top of the device base 2. When the water-cooled middle ring 4 and the water-cooled inner circle 5 are lifted and lowered under the drive of the lifting mechanism, they can enter and exit the control chamber through the inlet and outlet. The top surface of the water-cooled middle ring 4 is detachably mounted with an annular mold shell 6, and the top surface of the water-cooled inner circle 5 is mounted with a heating rod 7. Preferably, the heating rod 7 can also be detachably mounted, such as providing a positioning seat 18 on the water-cooled inner circle 5, and providing a positioning hole on the positioning seat 18 for the heating rod 7 to be plugged in. The heating rod 7 is vertically arranged and located at the center of the annular mold shell 6. The equipment cover 1 is fixedly connected to the top surface of the water-cooled outer ring 3, and the equipment cover 1 covers the annular mold shell 6 therein. A pouring cup 10 is installed on the top of the equipment cover 1, and the molten metal can be poured into the annular mold shell 6 through the pouring cup 10. Preferably, the pouring cup 10 is detachably mounted on the top of the equipment cover 1, such as providing a snap device on the equipment cover 1 to clamp the pouring cup 10. A plurality of heating bodies 8 are arranged on the inner wall of the equipment cover 1, and the plurality of heating bodies 8 are arranged around the annular mold shell 6.
工作原理:working principle:
将本控制设备安装在保温炉内,将浇口杯10与熔炼室连通,对保温炉和熔炼室进行抽真空,熔炼坩埚进行金属熔炼,熔炼结束后将合金液通过浇口杯10浇注到环形模壳6中,合金液到环形模壳6后,加热棒7和加热体8将会对环形模壳6中的合金液体保温,并静置一定时间后,关闭加热棒7和加热体8完成浇注,然后对水冷外环3、水冷中环4以及水冷内圆5内注入冷却水,然后水冷中环4先下降,水冷内圆5保持不动,水冷中环4带动环形模壳6下降,对铸件形成抽拉,抽拉过程中水冷内圆5会对铸件中心进行冷却,待铸件抽拉结束,水冷内圆5再下降到与水冷中环4同一水平位置,然后待环形模壳6温度冷却到预设冷却温度以下后,将环形模壳6取出,获得定向铸件或单晶铸件。优选的,水冷中环4和水冷内圆5下降时,以恒定速率下降。The control device is installed in a heat-insulating furnace, the pouring cup 10 is connected to the smelting chamber, the heat-insulating furnace and the smelting chamber are evacuated, and the smelting crucible is used to smelt the metal. After the smelting is completed, the alloy liquid is poured into the annular mold shell 6 through the pouring cup 10. After the alloy liquid reaches the annular mold shell 6, the heating rod 7 and the heating body 8 will keep the alloy liquid in the annular mold shell 6 warm. After standing for a certain period of time, the heating rod 7 and the heating body 8 are turned off to complete the pouring, and then cooling water is injected into the water-cooled outer ring 3, the water-cooled middle ring 4 and the water-cooled inner circle 5. Then, the water-cooled middle ring 4 first descends, and the water-cooled inner circle 5 remains stationary. The water-cooled middle ring 4 drives the annular mold shell 6 to descend, and the casting is pulled. During the pulling process, the water-cooled inner circle 5 will cool the center of the casting. After the casting is pulled, the water-cooled inner circle 5 will descend to the same horizontal position as the water-cooled middle ring 4. Then, after the temperature of the annular mold shell 6 is cooled to below the preset cooling temperature, the annular mold shell 6 is taken out to obtain a directional casting or a single crystal casting. Preferably, the water-cooled middle ring 4 and the water-cooled inner circle 5 descend at a constant rate.
加热棒7对环形模壳6中心进行加热保温,加热体8可以为环形模壳6外围进行加热保温,可改善环形模壳6阴面和阳面的温度场,提高铸件阴面的温度梯度,高代次单晶合金和定向柱晶合金难溶元素增加,而温度梯度提高不仅可以降低元素偏析,也可以使铸件在选晶段的竞争生长过程中,更有利于取向晶粒生长,改善晶体的生长方向,减少铸件表面的断头晶。通过水冷托盘中的水冷内圆5对铸件中心进行冷却,可让铸件的固液界面保持水平,不倾斜,改善固液界面形貌,降低单晶铸件大平台边角出现不同取向晶粒的几率,提高定向或单晶铸件的合格率,降低缺陷的产生。The heating rod 7 heats and insulates the center of the annular mold shell 6, and the heating body 8 can heat and insulate the periphery of the annular mold shell 6, which can improve the temperature field of the negative and positive surfaces of the annular mold shell 6, improve the temperature gradient of the negative surface of the casting, increase the refractory elements of the high-generation single crystal alloy and the oriented columnar crystal alloy, and the increase in temperature gradient can not only reduce element segregation, but also make the casting more conducive to oriented grain growth during the competitive growth process of the crystal selection section, improve the growth direction of the crystal, and reduce the broken crystals on the surface of the casting. The water-cooled inner circle 5 in the water-cooled tray cools the center of the casting, which can keep the solid-liquid interface of the casting horizontal and not tilted, improve the solid-liquid interface morphology, reduce the probability of different oriented grains appearing at the corners of the large platform of the single crystal casting, improve the qualified rate of oriented or single crystal castings, and reduce the generation of defects.
对照实验:Control experiment:
实验1:抽真空,熔炼合金温度控制在1500-1570℃,保温时间3-5min,浇注温度为1480-1550℃,加热棒7和加热体8进行加热保温,静置时间2-5min,浇注完成后,水冷中环4先以一定的速率同步下降,水冷内圆5保持不动,当铸件完全抽拉结束之后,将水冷内圆5快速抽拉到与水冷中环4同一水平位置,待环形模壳6温度降到100℃以下,将环形模壳6取下,浇注过程结束,获得定向铸件或单晶铸件,得到的铸件固液界面如图5中的a所示,晶粒取向如图6中的a所示。Experiment 1: Vacuuming, the temperature of the molten alloy is controlled at 1500-1570℃, the holding time is 3-5min, the pouring temperature is 1480-1550℃, the heating rod 7 and the heating body 8 are heated and kept warm, and the standing time is 2-5min. After the pouring is completed, the water-cooled middle ring 4 first descends synchronously at a certain rate, and the water-cooled inner circle 5 remains motionless. When the casting is completely pulled out, the water-cooled inner circle 5 is quickly pulled to the same horizontal position as the water-cooled middle ring 4. When the temperature of the annular mold shell 6 drops below 100℃, the annular mold shell 6 is removed, the pouring process is completed, and a directional casting or a single crystal casting is obtained. The solid-liquid interface of the obtained casting is shown in a of Figure 5, and the grain orientation is shown in a of Figure 6.
实验2:抽真空,熔炼合金温度控制在1500-1570℃,保温时间3-5min,浇注温度为1480-1550℃,加热棒7和加热体8进行加热保温,静置时间2-5min,浇注完成后,水冷中环4和水冷内圆5以一定的速率同步下降,当铸件完全抽拉结束之后,待环形模壳6温度降到100℃以下,将环形模壳6取下,浇注过程结束,获得定向铸件或单晶铸件,得到的铸件固液界面如图5中的b所示,晶粒取向如图6中的b所示。Experiment 2: Vacuuming, the temperature of the smelting alloy is controlled at 1500-1570℃, the holding time is 3-5min, the pouring temperature is 1480-1550℃, the heating rod 7 and the heating body 8 are heated and kept warm, and the standing time is 2-5min. After the pouring is completed, the water-cooled middle ring 4 and the water-cooled inner circle 5 are synchronously lowered at a certain rate. When the casting is completely pulled out, the temperature of the annular mold shell 6 drops below 100℃, the annular mold shell 6 is removed, the pouring process is completed, and a directional casting or a single crystal casting is obtained. The solid-liquid interface of the obtained casting is shown in b in Figure 5, and the grain orientation is shown in b in Figure 6.
实验3:Experiment 3:
抽真空,熔炼合金温度控制在1500-1570℃,保温时间3-5min,浇注温度为1480-1550℃,加热体8进行加热保温,加热棒7不启动,静置时间2-5min,浇注完成后,水冷中环4和水冷内圆5以一定的速率同步下降,当铸件完全抽拉结束之后,待环形模壳6温度降到100℃以下,将环形模壳6取下,浇注过程结束,获得定向铸件或单晶铸件,得到的铸件固液界面如图5中的c所示,晶粒取向如图6中的c所示。Evacuate the casting, control the temperature of the smelting alloy at 1500-1570°C, keep warm for 3-5 minutes, and set the pouring temperature at 1480-1550°C. Heat the heating body 8 and keep warm. Do not start the heating rod 7. Leave it to stand for 2-5 minutes. After the pouring is completed, the water-cooled middle ring 4 and the water-cooled inner circle 5 drop synchronously at a certain rate. When the casting is completely pulled out, wait for the temperature of the annular mold shell 6 to drop below 100°C, remove the annular mold shell 6, and the pouring process is completed to obtain a directional casting or a single crystal casting. The solid-liquid interface of the casting is shown in c in Figure 5, and the grain orientation is shown in c in Figure 6.
综上,从图5中可以看出,实验3(传统HRS法)的固液界面倾斜角偏大,而实验1通过添加水冷系统和在环形模壳6中间增设加热棒7,固液界面明显平缓。同时,还可以看出三个实验中实验1(中心加热加中心水冷工艺)的糊状区(即TL和TS中间区域)长度最短。在液相和固体之间有一层半液体半固体的区域,这个区域被称为糊状区。结晶温度区间与合金成分和工艺有关,因此,使用同一种合金时,加热棒7加中心水冷温度梯度最大。固液界面处温度梯度可以通过公式GL=(TL-TS)/L获得,其中TL代表固液界面前沿液相温度,TS代表已凝固固体温度,L代表糊状区长度。从图6中可以看出,实验1(中心加热加中心水冷工艺)中,生长取向小于15°的晶粒占比最多,其晶粒取向较好。实验2(仅设置了中心加热工艺)中,增大了晶粒取向偏差。而实验3(传统HRS法)中,其晶粒取向普遍超过15°。因此,加热棒7加中心水冷工艺不仅改变了固液界面形貌,也增加了固液界面前沿的温度梯度,同时,优化了晶粒的生长方向,降低了缺陷的形成几率。In summary, it can be seen from Figure 5 that the inclination angle of the solid-liquid interface in Experiment 3 (traditional HRS method) is too large, while in Experiment 1, by adding a water cooling system and adding a heating rod 7 in the middle of the annular mold shell 6, the solid-liquid interface is significantly flat. At the same time, it can also be seen that the length of the mushy zone (i.e., the middle area between TL and TS) in Experiment 1 (central heating plus central water cooling process) is the shortest among the three experiments. There is a semi-liquid and semi-solid area between the liquid phase and the solid, which is called the mushy zone. The crystallization temperature range is related to the alloy composition and process. Therefore, when the same alloy is used, the temperature gradient of the heating rod 7 plus central water cooling is the largest. The temperature gradient at the solid-liquid interface can be obtained by the formula GL=(TL-TS)/L, where TL represents the liquid phase temperature at the solid-liquid interface front, TS represents the solidified solid temperature, and L represents the length of the mushy zone. It can be seen from Figure 6 that in Experiment 1 (central heating plus central water cooling process), the proportion of grains with a growth orientation less than 15° is the largest, and its grain orientation is better. In Experiment 2 (only the central heating process is set), the grain orientation deviation is increased. In Experiment 3 (traditional HRS method), the grain orientation generally exceeds 15°. Therefore, the heating rod 7 plus the center water cooling process not only changes the solid-liquid interface morphology, but also increases the temperature gradient at the solid-liquid interface front, and at the same time, optimizes the growth direction of the grains and reduces the probability of defect formation.
进一步,本实施例中,如图1至图6所示,环形模壳6处的温度通过温度传感器监测,温度传感器安装在环形模壳6的外壁上。Further, in this embodiment, as shown in FIGS. 1 to 6 , the temperature at the annular formwork 6 is monitored by a temperature sensor, and the temperature sensor is installed on the outer wall of the annular formwork 6 .
进一步,本实施例中,如图1至图6所示,水冷外环3、水冷中环4以及水冷内圆5均为铜材质制作而成。Furthermore, in this embodiment, as shown in FIG. 1 to FIG. 6 , the water-cooled outer ring 3 , the water-cooled middle ring 4 and the water-cooled inner ring 5 are all made of copper.
本实施例中,如图1至图6所示,加热棒7为石墨加热棒。In this embodiment, as shown in FIG. 1 to FIG. 6 , the heating rod 7 is a graphite heating rod.
本实施例中,如图1至图6所示,设备外罩1的内壁上设有保温层12。In this embodiment, as shown in FIG. 1 to FIG. 6 , a heat-insulating layer 12 is provided on the inner wall of the equipment housing 1 .
进一步,本实施例中,如图1至图6所示,设备底座2的顶面设有隔热垫13,加热体8和保温层12安装在隔热垫13上,将加热体8和保温层12与设备底座2隔开。Furthermore, in this embodiment, as shown in Figures 1 to 6, a thermal insulation pad 13 is provided on the top surface of the device base 2, and the heating body 8 and the thermal insulation layer 12 are installed on the thermal insulation pad 13 to separate the heating body 8 and the thermal insulation layer 12 from the device base 2.
本实施例中,如图1至图6所示,加热体8为磁加热体。设备外罩1的外壁上设有加热线圈9。加热线圈9为磁加热体提供感应磁场,磁加热体感应到磁场后会产生涡流,转化成电阻加热。In this embodiment, as shown in Figures 1 to 6, the heating body 8 is a magnetic heating body. A heating coil 9 is provided on the outer wall of the device housing 1. The heating coil 9 provides an induced magnetic field for the magnetic heating body. When the magnetic heating body senses the magnetic field, eddy currents are generated and converted into resistance heating.
本实施例中,如图1至图6所示,水冷中环4和水冷内圆5通过锁止机构互锁,通过锁止机构锁住水冷中环4和水冷内圆5,更有利于水冷中环4和水冷内圆5同步升降,当不需要水冷中环4和水冷内圆5同步升降时,解锁锁止机构即可。In this embodiment, as shown in Figures 1 to 6, the water-cooled middle ring 4 and the water-cooled inner circle 5 are interlocked by a locking mechanism. Locking the water-cooled middle ring 4 and the water-cooled inner circle 5 by the locking mechanism is more conducive to the synchronous lifting of the water-cooled middle ring 4 and the water-cooled inner circle 5. When the water-cooled middle ring 4 and the water-cooled inner circle 5 do not need to be lifted and lowered synchronously, the locking mechanism can be unlocked.
进一步,本实施例中,如图1至图6所示,锁止机构包括锁紧螺栓17和螺栓耳板(未画出)。水冷中环4和水冷内圆5上对应设有螺栓耳板,将锁紧螺栓17拧入水冷中环4上的螺栓耳板和水冷内圆5上相对应的螺栓耳板,即可锁住水冷中环4和水冷内圆5,将锁紧螺栓17拧下来即可解锁水冷中环4和水冷内圆5。Further, in this embodiment, as shown in Figures 1 to 6, the locking mechanism includes a locking bolt 17 and a bolt ear plate (not shown). The water-cooled middle ring 4 and the water-cooled inner circle 5 are provided with bolt ear plates correspondingly. The locking bolt 17 is screwed into the bolt ear plate on the water-cooled middle ring 4 and the corresponding bolt ear plate on the water-cooled inner circle 5 to lock the water-cooled middle ring 4 and the water-cooled inner circle 5. The locking bolt 17 is screwed off to unlock the water-cooled middle ring 4 and the water-cooled inner circle 5.
本实施例中,如图1至图6所示,升降机构包括抽拉杆11,抽拉杆11能够上下升降。水冷内圆5的底壁同轴连接有一个抽拉杆11。水冷中环4的底壁连接有两个抽拉杆11,两个抽拉杆11分设在水冷中环4的轴线两侧。同时下拉三个抽拉杆11,即可实现水冷中环4和水冷内圆5同步下降。抽拉杆11升降可通过伸缩缸14实现,即伸缩缸14的缸体固定在设备底座2的控制腔室内,伸缩缸14的活塞杆上固定连接有连接架15,连接架15与抽拉杆11固定连接,通过伸缩缸14的活塞杆伸缩,实现抽拉杆11的升降。具体的,伸缩缸14可采用气动缸、液压缸或者电动缸。In this embodiment, as shown in Figures 1 to 6, the lifting mechanism includes a pull rod 11, and the pull rod 11 can be lifted up and down. A pull rod 11 is coaxially connected to the bottom wall of the water-cooled inner circle 5. Two pull rods 11 are connected to the bottom wall of the water-cooled middle ring 4, and the two pull rods 11 are arranged on both sides of the axis of the water-cooled middle ring 4. By pulling down the three pull rods 11 at the same time, the water-cooled middle ring 4 and the water-cooled inner circle 5 can be synchronously lowered. The lifting and lowering of the pull rod 11 can be achieved by a telescopic cylinder 14, that is, the cylinder body of the telescopic cylinder 14 is fixed in the control chamber of the equipment base 2, and a connecting frame 15 is fixedly connected to the piston rod of the telescopic cylinder 14. The connecting frame 15 is fixedly connected to the pull rod 11, and the lifting and lowering of the pull rod 11 is achieved by the extension and retraction of the piston rod of the telescopic cylinder 14. Specifically, the telescopic cylinder 14 can be a pneumatic cylinder, a hydraulic cylinder or an electric cylinder.
本实施例中,如图1至图6所示,抽拉杆11为中空杆。水冷内圆5上的抽拉杆11一端与水冷内圆5连通,另一端设有冷却水门,通过冷却水门送入和排出冷却液。水冷中环4的两个抽拉杆11一端与水冷中环4连通,另一端分别设有冷却水进口和冷却水出口,冷却液由其中一个抽拉杆11的冷却水进口进入,然后由另一个抽拉杆11的冷却水出口排出。In this embodiment, as shown in FIGS. 1 to 6 , the pull rod 11 is a hollow rod. One end of the pull rod 11 on the water-cooled inner circle 5 is connected to the water-cooled inner circle 5, and the other end is provided with a cooling water gate, through which the coolant is fed in and discharged. One end of the two pull rods 11 of the water-cooled middle ring 4 is connected to the water-cooled middle ring 4, and the other end is provided with a cooling water inlet and a cooling water outlet, respectively. The coolant enters through the cooling water inlet of one of the pull rods 11, and then is discharged through the cooling water outlet of the other pull rod 11.
进一步,本实施例中,如图1至图6所示,设备底座2的控制腔室内安装有导向架16,导向架16上设有三个导向孔,导向孔的轴线竖向设置,三个导向孔位置与三个抽拉杆11位置相对应,三个抽拉杆11分别插在三个导向孔内,以保证抽拉杆11稳定的竖向升降。Furthermore, in this embodiment, as shown in Figures 1 to 6, a guide frame 16 is installed in the control chamber of the equipment base 2, and three guide holes are provided on the guide frame 16. The axes of the guide holes are vertically arranged, and the positions of the three guide holes correspond to the positions of the three pull-out rods 11. The three pull-out rods 11 are respectively inserted into the three guide holes to ensure stable vertical lifting of the pull-out rods 11.
实施例2Example 2
本实施例提供了一种定向或单晶铸件晶粒生长方向控制方法,如图1至图6所示,包括以下步骤:This embodiment provides a method for controlling the grain growth direction of a directional or single crystal casting, as shown in FIGS. 1 to 6 , comprising the following steps:
S1、将实施例1中的定向或单晶铸件晶粒生长方向控制设备安装在保温炉内,将浇口杯10与熔炼室连通;S1. Install the directional or single crystal casting grain growth direction control device in Example 1 in a holding furnace, and connect the pouring cup 10 with the melting chamber;
S2、对保温炉和熔炼室进行抽真空,熔炼室进行熔炼,并安预设保温时间保温,将熔炼的合金液通过浇口杯10浇注到环形模壳6内,加热体8和加热棒7进行加热保温,浇注完后安预设静置时间静置,然后关闭加热体8和加热棒7;S2, the holding furnace and the smelting chamber are evacuated, the smelting chamber is smelted, and the smelting is kept warm for a preset holding time, the molten alloy liquid is poured into the annular mold shell 6 through the pouring cup 10, the heating body 8 and the heating rod 7 are heated and kept warm, and after the pouring is completed, the preset standing time is set to stand, and then the heating body 8 and the heating rod 7 are turned off;
S3、水冷中环4先下降,待铸件抽拉结束,水冷内圆5再下降到与水冷中环4同一水平位置,水冷外环3、水冷中环4以及水冷内圆5注入冷却水,待环形模壳6温度冷却到预设冷却温度以下后,将环形模壳6取出,获得定向铸件或单晶铸件。S3, the water-cooled middle ring 4 descends first, and when the casting is pulled out, the water-cooled inner circle 5 descends to the same horizontal position as the water-cooled middle ring 4, and cooling water is injected into the water-cooled outer ring 3, the water-cooled middle ring 4 and the water-cooled inner circle 5. After the temperature of the annular mold shell 6 is cooled to below the preset cooling temperature, the annular mold shell 6 is taken out to obtain a directional casting or a single crystal casting.
本控制方法,提高了定向凝固过程中铸件的温度梯度,使其生长中的组织得到细化,性能提高,用此技术生产的定向和单晶铸件晶粒取向好,不易产生断头晶和杂晶,固液界面稳定不倾斜,固液界面形貌可有效改善,定向或单晶铸件合格率高,缺陷少。相关证明可参考实施例1中的对照实验。This control method improves the temperature gradient of the casting during directional solidification, refines the growing structure, and improves the performance. The directional and single crystal castings produced by this technology have good grain orientation, are not prone to broken crystals and miscellaneous crystals, have a stable solid-liquid interface without tilting, and can effectively improve the solid-liquid interface morphology. The qualified rate of directional or single crystal castings is high and the defects are few. For relevant proof, refer to the control experiment in Example 1.
进一步,本实施例中,熔炼时温度控制在1500-1570℃,预设保温时间为3-5min;浇注时温度控制在1480-1550℃,预设静置时间为2-5min;预设冷却温度为100℃,即待100℃以下时,将环形模壳6取出。当然以上参数仅为参考数值,可根据具体需求进行调整。Further, in this embodiment, the temperature during smelting is controlled at 1500-1570°C, and the preset holding time is 3-5 minutes; the temperature during pouring is controlled at 1480-1550°C, and the preset standing time is 2-5 minutes; the preset cooling temperature is 100°C, that is, when the temperature is below 100°C, the annular mold shell 6 is taken out. Of course, the above parameters are only reference values and can be adjusted according to specific needs.
本发明中应用了具体个例对本发明的原理及实施方式进行了阐述,以上实施例的说明只是用于帮助理解本发明的方法及其核心思想;同时,对于本领域的一般技术人员,依据本发明的思想,在具体实施方式及应用范围上均会有改变之处。综上所述,本说明书内容不应理解为对本发明的限制。The present invention uses specific examples to illustrate the principles and implementation methods of the present invention. The above examples are only used to help understand the method and core ideas of the present invention. At the same time, for those skilled in the art, according to the ideas of the present invention, there will be changes in the specific implementation methods and application scope. In summary, the content of this specification should not be understood as limiting the present invention.
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