System and method for testing porosity of in-situ coal body by using magnetic fluid
Technical Field
The invention relates to the technical field of mine gas extraction and utilization, in particular to a system and a method for testing in-situ coal porosity by using magnetic fluid.
Background
Coal seam gas is an efficient clean energy source and is also an important dangerous source in the coal mine production process. The efficient extraction of the coal bed gas can help the national 'double carbon' target to be realized, and the occurrence of mine gas disaster accidents can be effectively prevented. The coal contains dual porous media of cracks and pores, the complex pore structure of the coal is used as a gas occurrence space and a migration channel, and the accurate test of the porosity and the crack rate of the coal body is of great significance in grasping the occurrence form and the migration state of the coal bed gas.
The common coal porosity testing methods comprise mercury compression, gas adsorption, nuclear magnetic resonance and the like, have the characteristics of repeatability, sample size, testing range, testing precision and the like, and basically the testing methods are used for sampling on site, so that the sampling process causes secondary disturbance destruction of a coal sample, the primary pore-crack structure of the coal is destroyed, the test result deviates from a true value, the sampling process releases the complex stress state of the coal sample, and even if the laboratory condition considers the stress effect, the actual pore-crack structure of the coal under the in-situ stress constraint condition cannot be truly described.
Disclosure of Invention
Aiming at the technical defects, the invention aims to provide a system and a method for testing the porosity of an in-situ coal body by using magnetic fluid, wherein a sampling unit and a heating unit are arranged in a shell, and electric energy is provided by a battery pack to drive motors in the heating unit and the sampling unit, so that asphalt to be sampled is extracted and heated, the fluidity of the asphalt is ensured, and the manual operation and transportation are facilitated.
In order to solve the technical problems, the invention adopts the following technical scheme:
The invention provides a system for testing the porosity of an in-situ coal body by utilizing magnetic fluid, which comprises a supply subsystem and a test subsystem, wherein the supply subsystem comprises a crusher for inputting coal mine waste iron into a vacuum evaporator and a grinding mill, a surfactant storage tank for inputting surfactant into the vacuum evaporator and the grinding mill, and a base carrier liquid storage tank for inputting base carrier liquid into the vacuum evaporator and the grinding mill;
the testing subsystem comprises a plurality of magnetic fluid targeting control drilling holes which are arranged in an annular array and are arranged in a target coal layer, a magnetic fluid conveying drilling hole is formed in the center of the annular array, and a medium-large-grain-size magnetic fluid storage tank and a small-grain-size magnetic fluid storage tank are communicated with the magnetic fluid conveying drilling hole and are used for transfusion.
Preferably, the distance between the magnetic fluid targeting control drilling holes and the magnetic fluid conveying drilling holes is smaller than or equal to 5m, and the number of the magnetic fluid targeting control drilling holes is not smaller than 8.
The electromagnetic hole sealing device comprises a hollow push rod and a high-power electromagnetic rod which are sequentially and fixedly connected, wherein the high-power electromagnetic rod is close to the bottom of a hole, a protective rubber sleeve is sleeved on the outer wall of the high-power electromagnetic rod, the hollow push rod is fixedly clamped in the hole through two hole sealing plugs sleeved on the outer wall of the hollow push rod, a gas drainage pipe and a magnetic fluid conveying pipe are reserved on the hole sealing plugs, and a grouting hole opening is reserved on a hole sealing section of the hollow push rod between the two hole sealing plugs.
Preferably, the insulated wire connected with the high-power electromagnetic rod passes through the hollow push rod and is electrically connected with the controller.
The invention also provides a using method of the system for testing the porosity of the in-situ coal body by using the magnetic fluid, which comprises the following steps:
S1, putting coal mine waste iron into a crusher, putting tailings into a vacuum evaporator and a grinding mill, and simultaneously adding a surfactant and a base carrier liquid into the vacuum evaporator and the grinding mill through a surfactant storage tank and a base carrier liquid storage tank respectively;
s2, starting a vacuum evaporator and a grinding machine, wherein the vacuum evaporator produces small-particle-size magnetic fluid and stores the small-particle-size magnetic fluid in a small-particle-size magnetic fluid storage tank, the middle-large-particle-size magnetic fluid crude liquid produced by the grinding machine is conveyed into a centrifugal machine to be centrifuged to obtain middle-large-particle-size magnetic fluid and stored in the middle-large-particle-size magnetic fluid storage tank, and the centrifuged large-particle-size magnetic fluid is conveyed into the grinding machine to be re-ground;
s3, constructing magnetic fluid targeting control drilling holes and magnetic fluid conveying drilling holes into the target coal seam, sealing holes in the stratum sections of the drilling holes, and communicating gas drainage pipes in the drilling holes with a gas drainage pipeline to pre-drain gas in the coal seam;
s4, when the change of the gas flow rate of the drilling hole is stable, closing a gas drainage pipe in the magnetic fluid conveying drilling hole, opening the magnetic fluid conveying pipe in the magnetic fluid conveying drilling hole, and injecting the magnetic fluid with small particle size into the annular array inner area, namely the target test area through the magnetic fluid storage tank with small particle size;
s5, when the magnetic fluid flows out of the gas drainage pipe and the magnetic fluid conveying pipe in the magnetic fluid targeting control drilling hole, closing the gas drainage pipe in the magnetic fluid targeting control drilling hole, and starting the high-power electromagnetic rod in the magnetic fluid conveying drilling hole to recover the magnetic fluid with small particle size to the magnetic fluid storage tank with small particle size;
S6, repeating the steps S4-S5, injecting the medium-large particle size magnetic liquid into the target test area through the medium-large particle size magnetic liquid storage tank, recovering the medium-large particle size magnetic liquid, recording the accumulated injection volume V 2, and calculating the porosity of the in-situ coal body based on the twice magnetic liquid injection volumes.
Preferably, in the step S1, water is selected as the base carrier liquid, and oleic acid is selected as the surfactant.
Preferably, the medium-large particle size magnetic liquid and the small particle size magnetic liquid contain iron particle body with the integral number of more than or equal to 30 percent, the volume fraction of the surfactant is more than or equal to 20 percent, and the rest components are base carrier liquid.
Preferably, the particle size of the iron particles in the small-particle-size magnetic liquid is less than or equal to 100nm, and the particle size of the iron particles in the medium-large-particle-size magnetic liquid is greater than or equal to 100nm.
Preferably, in step S6, the calculation formula of the in-situ coal body pore is as follows,
Wherein phi is the total porosity of the coal body, phi f is the fracture rate of the coal body, phi m is the porosity of the coal body matrix, r is the diameter of a target test area circle, and H is the average coal seam thickness.
The method has the advantages that the method utilizes the characteristics of small viscosity of magnetic fluid, strong controllability under an electric field and controllable particle size as a nanoscale probe in a pore test process to realize in-situ coal body diffusion pore-seepage fracture full-scale porosity test, utilizes electromagnet targeting traction magnetic fluid to fully fill the coal body pore fracture, avoids the problem that a traditional high-pressure fluid pressure injection damages a pore fracture structure, realizes low-loss and accurate test of the diffusion pore-seepage fracture full-scale porosity under complex in-situ stress conditions of the coal body, solves the problem that the conventional test method induces secondary damage of the original pore-fracture structure of the coal body in the in-situ sampling and testing process, is difficult to reproduce loaded stress of complex in-situ conditions of the coal body under laboratory test conditions, leads to detachment of constraint stress of the coal body pore fracture, and cannot represent the actual condition in-situ, so that the method realizes the porosity test under the in-situ stress conditions of the coal body porosity, and ensures the reliability, practicability and authenticity of the reference provided for engineering practice by the porosity test result.
Drawings
In order to more clearly illustrate the embodiments of the invention or the technical solutions in the prior art, the drawings that are required in the embodiments or the description of the prior art will be briefly described, it being obvious that the drawings in the following description are only some embodiments of the invention, and that other drawings may be obtained according to these drawings without inventive effort for a person skilled in the art.
Fig. 1 is a schematic diagram of connection relation of a system for testing in-situ coal porosity by using magnetic fluid according to an embodiment of the present invention.
Fig. 2 is a schematic structural diagram of an electromagnetic hole sealing device according to an embodiment of the present invention.
In the figure, 1-coal mine waste iron, 2-surfactant storage tank, 3-base carrier liquid storage tank, 4-vacuum evaporator, 5-crusher, 6-mill, 7-centrifuge, 8-medium and large particle size magnetic liquid storage tank, 9-small particle size magnetic liquid storage tank, 10-target coal seam, 11-magnetic fluid targeting control drilling, 12-target test area, 13-magnetic fluid conveying drilling, 14-rock stratum, 15-gas drainage pipe, 16-magnetic fluid conveying pipe, 17-insulated wire, 18-grouting orifice, 19-hole sealing plug, 20-hollow push rod, 21-protective rubber sleeve and 22-high power electromagnetic rod.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
As shown in fig. 1 to 2, a system for testing the porosity of an in-situ coal body by using magnetic fluid comprises a multi-stage particle size magnetic fluid supply subsystem and an in-situ coal body porosity testing subsystem, which are hereinafter referred to as the supply subsystem and the testing subsystem;
The feeding subsystem comprises a crusher 5 for inputting coal mine waste iron 1 to a vacuum evaporator 4 and a grinding machine 6, a surfactant storage tank 2 for inputting surfactant to the vacuum evaporator 4 and the grinding machine 6, and a base carrier liquid storage tank 3 for inputting base carrier liquid to the vacuum evaporator 4 and the grinding machine 6, wherein an outlet of the vacuum evaporator 4 is communicated with a small-particle-size magnetic liquid storage tank 9, the grinding machine 6 is also communicated with a centrifugal machine 7, and an outlet of the centrifugal machine 7 is communicated with a medium-large-particle-size magnetic liquid storage tank 8;
The testing subsystem comprises a plurality of magnetic fluid targeting control drilling holes 11 which are arranged in an annular array and are arranged in a target coal seam 10, a magnetic fluid conveying drilling hole 13 is formed in the center of the annular array, and a medium-large-particle-size magnetic fluid storage tank 8 and a small-particle-size magnetic fluid storage tank 9 are communicated with the magnetic fluid conveying drilling hole 13 and are used for transfusion.
The distance between the magnetic fluid targeting control drilling holes 11 and the magnetic fluid conveying drilling holes 13 is smaller than or equal to 5m, and the number of the magnetic fluid targeting control drilling holes 11 is not smaller than 8.
The magnetic fluid targeting control drilling hole 11 and the magnetic fluid conveying drilling hole 13 are internally provided with electromagnetic hole sealing devices, each electromagnetic hole sealing device comprises a hollow push rod 20 and a high-power electromagnetic rod 22 which are sequentially and fixedly connected, the high-power electromagnetic rod 22 is close to the hole bottom, the outer wall of the high-power electromagnetic rod is sleeved with a protective rubber sleeve 21, the hollow push rod 20 is fixedly clamped in a hole through two hole sealing plugs 19 sleeved on the outer wall, a gas drainage pipe 15 and a magnetic fluid conveying pipe 16 are reserved on the hole sealing plugs 19, and a grouting hole 18 is reserved on a hole sealing section of the hollow push rod 20 between the two hole sealing plugs 19.
The insulated wire 17 connected with the high-power electromagnetic rod 22 passes through the hollow push rod 20 and is electrically connected with the controller.
The embodiment of the invention also provides a using method of the system for testing the porosity of the in-situ coal body by using the magnetic fluid, which comprises the following steps:
S1, putting coal mine waste iron 1 into a crusher 5, putting tailings into a vacuum evaporator 4 and a grinding mill 6, and simultaneously adding a surfactant and a base carrier liquid into the vacuum evaporator 4 and the grinding mill 6 through a surfactant storage tank 2 and a base carrier liquid storage tank 3 respectively;
S2, starting the vacuum evaporator 4 and the grinding machine 6, wherein the vacuum evaporator 4 produces small-particle-size magnetic fluid and stores the small-particle-size magnetic fluid in a small-particle-size magnetic fluid storage tank 9, the medium-large-particle-size magnetic fluid crude fluid produced by the grinding machine 6 is conveyed into a centrifugal machine 7 to be centrifuged to obtain medium-large-particle-size magnetic fluid and stored in a medium-large-particle-size magnetic fluid storage tank 8, and the centrifuged large-particle-size magnetic fluid is conveyed into the grinding machine 6 to be re-ground;
s3, constructing a magnetic fluid targeting control drilling hole 11 and a magnetic fluid conveying drilling hole 13 into the target coal seam 10, sealing holes of all drilling holes in a rock stratum 14 section, and communicating a gas drainage pipe 15 in each drilling hole with a gas drainage pipeline to pre-drain gas in the coal seam;
S4, when the change of the gas flow rate of the drilling hole is stable, closing a gas drainage pipe 15 in the magnetic fluid conveying drilling hole 13, opening a magnetic fluid conveying pipe 16 in the magnetic fluid conveying drilling hole 13, and injecting small-particle-size magnetic fluid into the annular array inner area, namely the target test area 12 through a small-particle-size magnetic fluid storage tank 9;
S5, when the magnetic fluid flows out of the gas drainage pipe 15 and the magnetic fluid conveying pipe 16 in the magnetic fluid targeting control drilling hole 11, closing the gas drainage pipe 15 in the magnetic fluid targeting control drilling hole 11, and starting the high-power electromagnetic rod 22 in the magnetic fluid conveying drilling hole 13 to recover the magnetic fluid with small particle size to the magnetic fluid storage tank 9 with small particle size;
s6, repeating the steps S4-S5, injecting the medium-large particle size magnetic liquid into the target test area 12 through the medium-large particle size magnetic liquid storage tank 8, recovering, recording the accumulated injection volume V 2, and calculating the porosity of the in-situ coal body based on the two magnetic liquid injection volumes.
In the step S1, water is selected as the base carrier liquid, and oleic acid is selected as the surfactant.
The magnetic liquid with medium and large particle sizes and the magnetic liquid with small particle sizes contain iron particle body with the integral number of more than or equal to 30 percent, the volume fraction of the surfactant with the volume fraction of more than or equal to 20 percent, and the rest components are base carrier liquid.
The particle size of the iron particles in the small-particle-size magnetic liquid is smaller than or equal to 100nm, and the particle size of the iron particles in the medium-large-particle-size magnetic liquid is larger than or equal to 100nm.
In the step S6, the calculation formula of the in-situ coal body pore is as follows,
Wherein phi is the total porosity of the coal body, phi f is the fracture rate of the coal body, phi m is the porosity of the coal body matrix, r is the diameter of a target test area circle, and H is the average coal seam thickness.
The invention uses the characteristics of small viscosity of the magnetic fluid, strong controllability under an electric field and controllable particle size of particles as the nano probe in the pore test process, realizes the low-loss and accurate test of the pore and fracture rate of the coal under the in-situ stress condition, and ensures the reliability, the practicability and the authenticity of the reference provided by the porosity test result for engineering practice.
It will be apparent to those skilled in the art that various modifications and variations can be made to the present invention without departing from the spirit or scope of the invention. Thus, it is intended that the present invention also include such modifications and alterations insofar as they come within the scope of the appended claims or the equivalents thereof.