CN1172598C - Bactericidal and pesticidal garlic oil emulsion and its prepn. - Google Patents
Bactericidal and pesticidal garlic oil emulsion and its prepn. Download PDFInfo
- Publication number
- CN1172598C CN1172598C CNB00123966XA CN00123966A CN1172598C CN 1172598 C CN1172598 C CN 1172598C CN B00123966X A CNB00123966X A CN B00123966XA CN 00123966 A CN00123966 A CN 00123966A CN 1172598 C CN1172598 C CN 1172598C
- Authority
- CN
- China
- Prior art keywords
- essential oil
- sorbitol
- garlic essential
- temperature
- galic essential
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000839 emulsion Substances 0.000 title claims abstract description 20
- 230000000361 pesticidal effect Effects 0.000 title abstract description 4
- 230000000844 anti-bacterial effect Effects 0.000 title abstract 3
- 239000010647 garlic oil Substances 0.000 title 1
- 239000000341 volatile oil Substances 0.000 claims abstract description 33
- 239000000575 pesticide Substances 0.000 claims abstract description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000005516 engineering process Methods 0.000 claims abstract description 8
- 238000004519 manufacturing process Methods 0.000 claims abstract description 5
- 239000002994 raw material Substances 0.000 claims abstract description 4
- 238000002360 preparation method Methods 0.000 claims abstract 2
- 230000001954 sterilising effect Effects 0.000 claims description 19
- 238000003756 stirring Methods 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 230000001804 emulsifying effect Effects 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 6
- 238000001816 cooling Methods 0.000 abstract description 5
- 241000196324 Embryophyta Species 0.000 abstract description 4
- 239000000203 mixture Substances 0.000 abstract description 4
- 201000010099 disease Diseases 0.000 abstract description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 3
- 241001124076 Aphididae Species 0.000 abstract description 2
- 241000510199 Helicoverpa assulta Species 0.000 abstract description 2
- 230000002265 prevention Effects 0.000 abstract description 2
- 240000002234 Allium sativum Species 0.000 abstract 7
- 235000004611 garlic Nutrition 0.000 abstract 7
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 abstract 6
- 239000000600 sorbitol Substances 0.000 abstract 6
- 238000013019 agitation Methods 0.000 abstract 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 241000607479 Yersinia pestis Species 0.000 description 4
- 238000012856 packing Methods 0.000 description 4
- 230000000853 biopesticidal effect Effects 0.000 description 3
- 241000411851 herbal medicine Species 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- JDLKFOPOAOFWQN-VIFPVBQESA-N Allicin Natural products C=CCS[S@](=O)CC=C JDLKFOPOAOFWQN-VIFPVBQESA-N 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 241000700605 Viruses Species 0.000 description 2
- JDLKFOPOAOFWQN-UHFFFAOYSA-N allicin Chemical compound C=CCSS(=O)CC=C JDLKFOPOAOFWQN-UHFFFAOYSA-N 0.000 description 2
- 235000010081 allicin Nutrition 0.000 description 2
- 239000002689 soil Substances 0.000 description 2
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 206010035148 Plague Diseases 0.000 description 1
- 241000500437 Plutella xylostella Species 0.000 description 1
- 238000007259 addition reaction Methods 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 239000005445 natural material Substances 0.000 description 1
- 210000004681 ovum Anatomy 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 239000005871 repellent Substances 0.000 description 1
- 230000002940 repellent Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a bactericidal and pesticidal emulsion made from garlic essential oil and the technology thereof. The garlic essential oil and sorbitol T80 in accordance with medicinal standards are selected as raw materials for production, and the garlic essential oil and the sorbitol T80 in accordance with dose requirements are agitated, mixed and dissolved to react at the temperature of 38 to 42 DEG C, and then are agitated together with clear water with the temperature of 30 to 40 DEG C; the garlic essential oil and the sorbitol T80 are thoroughly mixed and emulsified, and cooled for still standing; finally, the finished products are obtained through packaging. The technical processes of the emulsion comprises the steps that the garlic essential oil and the sorbitol T80 are taken, and the sorbitol T80 is heated to the temperature of 38 to 42 DEG C to be neutralized and agitated; the clear water is heated to the temperature of 30 to 40 DEG C to be mixed in the mixture, and agitation is continued until the garlic essential oil and the sorbitol T80 are thoroughly emulsified; finally, the finished products are obtained through cooling, still standing and subpackaging. The bactericidal and pesticidal emulsion made from garlic essential oil of the present invention is used as pesticide made from pure biological preparations, and has favorable prevention and treatment effects on aphids, oriental tobacco budworms, anthracnose and root rot of plants and other epidemic diseases of the plants.
Description
The present invention relates to sterilization pesticide, relate in particular to galic essential oil sterilizing pesticide emulsion and technology thereof.
Agricultural goes up the agricultural chemicals that sterilizing pesticide is used now, mainly is chemical pesticide.Using of chemical pesticide makes the pesticide resistance of crop pests more and more stronger on the one hand, on the other hand environment polluted, and soil is damaged, and works the mischief with health.Under the situation of more and more advocating pollution-free food, green agriculture, become the task of top priority with the biopesticide substituting chemical pesticide.
The objective of the invention is to, overcome the deficiencies in the prior art part, a kind of galic essential oil that utilizes is provided, by the science compatibility, the biopesticide that the process addition reaction forms.
Galic essential oil sterilizing pesticide emulsion of the present invention and technology thereof, raw materials for production are selected galic essential oil and the sorbierite T80 that meets medicinal standard for use, the galic essential oil and the sorbierite T80 that will meet the dosage requirement stir miscible reaction under 38 ℃ to 42 ℃ temperature, stir with 30 to 40 ℃ clear water again, fully mix, through cooling, leave standstill, become finished product through packing then.Its technical process is: get galic essential oil and sorbierite T80, described sorbierite T80 heats to 38 ℃ to 42 ℃, the stirring that neutralizes, and clear water heated to 30～40 ℃ to be blended into, and continues to stir, and until fully emulsified, cooling is left standstill then, and packing becomes finished product.Galic essential oil sterilizing pesticide emulsion of the present invention, if add Chinese herbal medicine Tu Jing in process of production, insecticidal effect can be more better.The method that adds herbal medicine Tu Jing is, at first produces the solution of herbal medicine Tu Jing, blends with galic essential oil sterilizing pesticide emulsion of the present invention again.Galic essential oil sterilizing pesticide emulsion of the present invention also can add the inferior wind of dimethyl, can be used for Pesticidal and sterilizing, but impairs pure natural characteristics of the present invention like this.
Galic essential oil sterilizing pesticide emulsion of the present invention and technology thereof, with the natural material that allicin includes, the SH enzyme of oxidizing bacteria bulk-growth breeding loses activity the SH enzyme; In addition, the functional group in the allicin can destroy the cell wall structure of plant virus and bacterium, thereby produces the effect of sterilizing pesticide.The experiment proved that galic essential oil sterilizing pesticide emulsion of the present invention all has the better prevention effect to anthracnose, root rot, black rot, soft rot and other vegetable plagues of aphid, oriental tobacco budworm, Oeobia undalis, diamond-back moth and plant.
Galic essential oil sterilizing pesticide emulsion of the present invention and technology thereof, embodiment is as follows: galic essential oil sterilizing pesticide emulsion of the present invention and technology thereof, the proportioning that contains galic essential oil concentration 2% with product is an example, raw materials for production are selected 2 kilograms of galic essential oils that meet medicinal standard for use, 4 kilograms of sorbierite T80, that is to say that the content of sorbierite T80 in product is 4%, under 38 ℃ to 42 ℃ temperature, stir miscible reaction, with 94 kilograms in 30～40 ℃ clear water, promptly the content of clear water in product is 94%, adds up to double centner and stirs together again, fully mix, emulsification, through cooling, leave standstill, become finished product through packing then.Galic essential oil, sorbierite T80 and clear water three's proportioning is 2: 4: 94 in the galic essential oil sterilizing pesticide emulsion of the present invention.Here said proportioning is the optimum value of proportioning of the present invention, but is not to do such restriction, do suitable adjustment up and down and also be fine, and be the concentration height, effective, but cost is also high; Concentration reduces, and cost reduces, but effect also reduces.Its technical process is: get 4 kilograms of 2 kilograms of galic essential oils and sorbierite T80, described sorbierite T80 heats to 38 ℃ to 42 ℃, the stirring that neutralizes, with 94 kilograms in clear water, heating to 30～40 ℃ is blended into, continue to stir more than 2 hours, until fully emulsified, cooling is left standstill then, packing becomes finished product.Galic essential oil sterilizing pesticide emulsion of the present invention has repellent action preferably to crop pests, can replace existing highly toxic pesticide; The crop disease virus epidemic disease had effect a radical cure effect preferably, can spray, also can irritate by root, also can be used for the sprinkling simultaneously of ploughing, kill the insect pest in soil worm's ovum.Galic essential oil sterilizing pesticide emulsion of the present invention is pure biopesticide, to the person poultry harmless.
Claims (1)
1, the technology of preparation galic essential oil sterilizing pesticide emulsion, raw materials for production are selected galic essential oil and the sorbierite T80 that meets medicinal standard for use, it is characterized in that galic essential oil, sorbierite T80 and clear water ratio with 2: 4: 94, earlier galic essential oil and sorbierite T80 are stirred miscible emulsion reaction under 38 to 42 ℃ of temperature, stir with 30 to 40 ℃ clear water again, fully mixing and emulsifying is made galic essential oil sterilizing pesticide emulsion.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB00123966XA CN1172598C (en) | 2000-10-23 | 2000-10-23 | Bactericidal and pesticidal garlic oil emulsion and its prepn. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB00123966XA CN1172598C (en) | 2000-10-23 | 2000-10-23 | Bactericidal and pesticidal garlic oil emulsion and its prepn. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1349745A CN1349745A (en) | 2002-05-22 |
| CN1172598C true CN1172598C (en) | 2004-10-27 |
Family
ID=4590255
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB00123966XA Expired - Fee Related CN1172598C (en) | 2000-10-23 | 2000-10-23 | Bactericidal and pesticidal garlic oil emulsion and its prepn. |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1172598C (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2414912A (en) * | 2004-06-11 | 2005-12-14 | Garlic Farms | Use of garlic extract for sytematic treatment of growing crops |
| GB0507227D0 (en) * | 2005-04-09 | 2005-05-18 | Ecospray Ltd | A pesticide and repellent |
| CN101869122A (en) * | 2010-06-01 | 2010-10-27 | 刘志慧 | Garlicin plant growth promoting solution with insect disinfestation and sterilization functions |
| CN101985578B (en) * | 2010-10-30 | 2013-02-06 | 暨南大学 | A method for increasing the production of garlic essential oil |
| CN102805114B (en) * | 2012-08-30 | 2014-11-19 | 白静 | Botanical natural fungicide for fungus and preparation method thereof |
| CN103222487A (en) * | 2012-11-07 | 2013-07-31 | 湖北中烟工业有限责任公司 | Plant pesticide for preventing and controlling tobacco aphid and use thereof |
| CN104304250B (en) * | 2014-10-28 | 2016-08-24 | 青岛青知企业管理咨询有限公司 | A kind of suspending agent for preventing and treating Flos Chrysanthemi root rot |
| CN105494342A (en) * | 2016-01-12 | 2016-04-20 | 洛阳和梦科技有限公司 | Environment-friendly sterilization type insect repellent disinfectant |
| CN105724603A (en) * | 2016-02-01 | 2016-07-06 | 上海蔚科精细化工有限公司 | Emulsified garlic oil and manufacturing method thereof |
| CN111053112A (en) * | 2019-11-14 | 2020-04-24 | 北京农业智能装备技术研究中心 | Navel orange penicilliosis inhibitor and preparation method and preparation condition determination method thereof |
-
2000
- 2000-10-23 CN CNB00123966XA patent/CN1172598C/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1349745A (en) | 2002-05-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: SHANDONG PROVINCE MINAO GARLIC PRODUCTS CO., LTD. Free format text: FORMER OWNER: DENG GUANGQI Effective date: 20070105 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20070105 Address after: 272000, Shandong City, Jining province Jinxiang County rain Yuan Village Patentee after: Shandong Province Min Ao garlic products Co. Ltd. Address before: 272000 garlic oil factory in Jining, West first of Willow Village, Shizhong District, Jining, Shandong Patentee before: Deng Guangqi |
|
| DD01 | Delivery of document by public notice |
Addressee: Deng Guangqi Document name: Notification to Pay the Fees |
|
| DD01 | Delivery of document by public notice |
Addressee: Deng Guangqi Document name: Notification to Pay the Fees |
|
| DD01 | Delivery of document by public notice |
Addressee: Deng Guangqi Document name: Notification of Termination of Patent Right |
|
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20041027 Termination date: 20121023 |