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CN116735325B - Sampling and shear strength testing methods for maintaining the original structure of spoil soil - Google Patents

Sampling and shear strength testing methods for maintaining the original structure of spoil soil Download PDF

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Publication number
CN116735325B
CN116735325B CN202310967236.1A CN202310967236A CN116735325B CN 116735325 B CN116735325 B CN 116735325B CN 202310967236 A CN202310967236 A CN 202310967236A CN 116735325 B CN116735325 B CN 116735325B
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spoil
soil
acrylamide
acrylic acid
sample
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CN116735325A (en
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魏玉峰
张仕昕
陈则连
白占雄
尚海敏
裴向军
张瞳
崔圣华
梁彭
杨豪
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China Railway Design Corp
China State Railway Group Co Ltd
Chengdu Univeristy of Technology
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China Railway Design Corp
China State Railway Group Co Ltd
Chengdu Univeristy of Technology
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/36Embedding or analogous mounting of samples
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/04Acids; Metal salts or ammonium salts thereof
    • C08F220/06Acrylic acid; Methacrylic acid; Metal salts or ammonium salts thereof
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/52Amides or imides
    • C08F220/54Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
    • C08F220/56Acrylamide; Methacrylamide
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/24Investigating strength properties of solid materials by application of mechanical stress by applying steady shearing forces
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/36Embedding or analogous mounting of samples
    • G01N2001/366Moulds; Demoulding
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0001Type of application of the stress
    • G01N2203/0003Steady
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0014Type of force applied
    • G01N2203/0025Shearing

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention provides a sampling and shear strength testing method for maintaining an original structure of a waste residue soil body, belongs to the technical field of waste residue soil tests in geological engineering, and aims to adopt a copolymer material as a sealing material in a sampling process, avoid disturbance of the original structure of the original soil in the sampling process and a transportation process, and enable a deblocking process to be simpler and easier, wherein the method comprises the following steps: preparing an acrylamide-acrylic acid copolymer from a mixture consisting of pure water, glycerol, acrylamide and acrylic acid in a mass ratio of 1:2:4-8:2-4 under the condition of heating in a water bath; selecting a waste residue soil plane with a preset size and shape for leveling at a gentle part of a waste residue soil slope surface; dividing an injection adhesive tape on the flattened waste residue soil plane, and uniformly injecting a copolymer material consisting of an acrylamide-acrylic acid copolymer into the injection adhesive tape until reaching a preset depth; and after the copolymerization material is solidified, removing waste residue soil at the periphery of the adhesive tape to obtain a sealed waste residue soil sample.

Description

保持弃渣土体原状结构的取样及抗剪强度测试方法Sampling and shear strength testing methods for maintaining the original structure of spoil soil

技术领域Technical field

本发明涉及地质工程弃渣土试验技术领域,特别是涉及保持弃渣土体原状结构的取样及抗剪强度测试方法。The invention relates to the technical field of geological engineering spoil soil testing, and in particular to a sampling and shear strength testing method that maintains the original structure of the spoil soil body.

背景技术Background technique

在实际工程项目中,因工程建设开挖,造成大量工程弃渣,对弃渣土进行排水、适当措施处理是有必要的。而在对弃渣土进行处置之前,有必要对弃渣土的结构,力学性能进行测试,以选择合理的处置方法。而岩土工程中至关重要的力学参数之一为土体抗剪强度,因此,对弃渣土体的抗剪强度测试尤为必要。In actual engineering projects, a large amount of engineering waste is caused by excavation during engineering construction. It is necessary to drain the waste soil and take appropriate measures to deal with it. Before disposing of the spoil soil, it is necessary to test the structure and mechanical properties of the spoil soil to select a reasonable disposal method. One of the most important mechanical parameters in geotechnical engineering is the shear strength of soil. Therefore, it is particularly necessary to test the shear strength of spoil soil.

相关研究表明,弃渣土颗粒间相互作用和空间排列方式对弃渣土抗剪强度特征有着显著的影响,而对弃渣土力学特性的准确描述会受到颗粒间细观尺度复杂、不确定、随机性的约束。目前常规的两种抗剪强度试验方法为原位直剪试验和室内直剪试验,但在实际试验过程中均存在一定的缺陷。Relevant studies have shown that the interaction and spatial arrangement between spoil soil particles have a significant impact on the shear strength characteristics of spoil soil. However, the accurate description of the mechanical properties of spoil soil will be affected by the complexity, uncertainty and complexity of the mesoscale between particles. Constraints on randomness. At present, the two conventional shear strength test methods are in-situ direct shear test and indoor direct shear test, but both have certain defects during the actual test process.

现场原位直剪试验需要在工程现场进行,试验条件较为复杂,存在较多难以控制的环境、地质因素,此外试验设备笨重,组装复杂,会导致试验结果准确性下降。On-site in-situ direct shear tests need to be carried out at the engineering site. The test conditions are relatively complex and there are many environmental and geological factors that are difficult to control. In addition, the test equipment is bulky and complex to assemble, which will lead to a decrease in the accuracy of the test results.

而室内直剪试验获取弃渣土体抗剪强度参数主要是通过重塑土,与原状土相比,重塑土的物理指标尽管不会发生改变,但重塑土的颗粒骨架排列、颗粒接触形式、孔隙分布特征均已发生了改变,破坏了弃渣土体的初始结构,这会导致试验所得到的重塑土与原状土力学参数出现明显的差异,致使重塑土无法真实再现原状土的强度变形特征,即通过重塑土获取的抗剪强度难以表征弃渣现场的力学特性。The indoor direct shear test obtains the shear strength parameters of the spoil soil mainly through reshaped soil. Compared with the original soil, although the physical indicators of the reshaped soil will not change, the particle skeleton arrangement and particle contact of the reshaped soil will not change. The form and pore distribution characteristics have changed, destroying the initial structure of the spoil soil. This will lead to obvious differences in the mechanical parameters of the reshaped soil obtained from the test and the original soil, making the reshaped soil unable to truly reproduce the original soil. The strength and deformation characteristics of the soil, that is, the shear strength obtained by reshaping the soil, are difficult to characterize the mechanical properties of the spoil site.

发明内容Contents of the invention

有鉴于此,本发明旨在提出一种保持弃渣土体原状结构的取样及抗剪强度测试方法,以解决采用重塑土进行试验难以表征弃渣现场的力学特性的问题。In view of this, the present invention aims to propose a sampling and shear strength testing method that maintains the original structure of the spoil soil, so as to solve the problem that it is difficult to characterize the mechanical properties of the spoil site in tests using reshaped soil.

本发明实施例的第一方面,提供了一种保持弃渣土体原状结构的取样方法,包括:A first aspect of the embodiment of the present invention provides a sampling method for maintaining the original structure of spoil soil, including:

将质量比为1:2:4-8:2-4的纯水、丙三醇、丙烯酰胺以及丙烯酸组成的混合物在水浴加热条件下制备成丙烯酰胺-丙烯酸共聚物;Preparing a mixture of pure water, glycerin, acrylamide and acrylic acid with a mass ratio of 1:2:4-8:2-4 under water bath heating conditions to prepare an acrylamide-acrylic acid copolymer;

在弃渣土斜坡坡面平缓部位,选择预设尺寸形状的弃渣土平面进行平整,以方便采样;其中,所述预设尺寸形状根据对弃渣土试样的测试需求确定;In the gentle part of the spoil slope, select a spoil plane with a preset size and shape for smoothing to facilitate sampling; wherein the preset size and shape are determined based on the testing requirements for the spoil sample;

在平整后的所述弃渣土平面上划定注胶带,并向所述注胶带内均匀注入由所述丙烯酰胺-丙烯酸共聚物组成的共聚材料,直至达到预设深度;An injection tape is defined on the leveled spoil soil plane, and a copolymer material composed of the acrylamide-acrylic acid copolymer is evenly injected into the injection tape until a preset depth is reached;

待所述共聚材料凝固后,将所述注胶带外围的弃渣土挖去,得到封固的弃渣土试样。After the copolymer material solidifies, dig out the spoil soil around the injection tape to obtain a sealed spoil soil sample.

进一步地,所述预设深度为所述弃渣土试样高度的1.1-1.2倍;所述注胶带的宽度为所述弃渣土试样宽度的1/10-1/6。Further, the preset depth is 1.1-1.2 times the height of the spoil soil sample; the width of the injection tape is 1/10-1/6 of the width of the spoil soil sample.

进一步地,所述将质量比为1:2:4-8:2-4的纯水、丙三醇、丙烯酰胺以及丙烯酸组成的混合物在水浴加热条件下制备成丙烯酰胺-丙烯酸共聚物,包括:Further, the mixture of pure water, glycerol, acrylamide and acrylic acid with a mass ratio of 1:2:4-8:2-4 is prepared into an acrylamide-acrylic acid copolymer under water bath heating conditions, including :

向所述纯水中依次加入所述丙三醇、所述丙烯酸以及所述丙烯酰胺,搅拌混合得到混合液;其中,所述纯水、所述丙三醇、所述丙烯酰胺以及所述丙烯酸的质量比为1:2:4-8:2-4;Add the glycerol, the acrylic acid and the acrylamide to the pure water in sequence, stir and mix to obtain a mixed liquid; wherein the pure water, the glycerol, the acrylamide and the acrylic acid The mass ratio is 1:2:4-8:2-4;

向所述混合液中加入引发剂,搅拌后保持50~70℃的温度水浴加热10 ~20分钟,得到所述丙烯酰胺-丙烯酸共聚物;其中,所述引发剂包括过硫酸盐和偶氮化合物中的一种。An initiator is added to the mixed liquid, and after stirring, the water bath is heated at a temperature of 50 to 70°C for 10 to 20 minutes to obtain the acrylamide-acrylic acid copolymer; wherein the initiator includes persulfate and azo compounds. one of them.

进一步地,所述纯水、所述丙三醇、所述丙烯酰胺以及所述丙烯酸的质量比为1:2:6:3。Further, the mass ratio of the pure water, the glycerin, the acrylamide and the acrylic acid is 1:2:6:3.

进一步地,所述引发剂与所述丙烯酰胺的质量比为1:5-10。Further, the mass ratio of the initiator to the acrylamide is 1:5-10.

进一步地,所述向所述纯水中依次加入所述丙三醇、所述丙烯酸以及所述丙烯酰胺,搅拌混合得到混合液,包括:Further, the glycerol, the acrylic acid and the acrylamide are sequentially added to the pure water, and stirred and mixed to obtain a mixed liquid, including:

在向所述纯水中加入所述丙三醇以及所述丙烯酸后,对所述纯水进行搅拌;After adding the glycerin and the acrylic acid to the pure water, stir the pure water;

在搅拌的同时,加入所述丙烯酰胺,得到所述混合液。While stirring, add the acrylamide to obtain the mixed liquid.

进一步地,所述丙烯酰胺的纯度在99%以上,所述丙烯酸的纯度为99%以上,所述丙三醇的纯度在95%以上。Further, the purity of the acrylamide is above 99%, the purity of the acrylic acid is above 99%, and the purity of the glycerol is above 95%.

进一步地,所述向所述注胶带内均匀注入由所述丙烯酰胺-丙烯酸共聚物组成的共聚材料,直至达到预设深度,包括:Further, the copolymer material composed of the acrylamide-acrylic acid copolymer is uniformly injected into the injection tape until a preset depth is reached, including:

采用带有孔隙压力探头的注胶设备,向所述注胶带内均匀注入所述共聚材料,所述共聚材料的注入量和注入深度通过所述孔隙压力探头控制;在注胶过程中,所述注胶设备为加热状态,以保持所述共聚材料的流动性。Glue injection equipment with a pore pressure probe is used to evenly inject the copolymer material into the injection tape. The injection amount and depth of the copolymer material are controlled by the pore pressure probe; during the glue injection process, the The glue injection equipment is heated to maintain the fluidity of the copolymer material.

本发明实施例的第二方面,提供了一种抗剪强度测试方法,所述方法包括:A second aspect of the embodiment of the present invention provides a shear strength testing method, which method includes:

对上述第一方面所述的取样方法取得的封固的弃渣土试样,采用热风干燥器进行解胶;Use a hot air dryer to degumm the sealed spoil soil sample obtained by the sampling method described in the first aspect;

将解胶后的所述弃渣土试样中包含所述共聚材料的部分削去后,置于直剪仪中进行直剪试验,以测试所述弃渣土试样的抗剪强度。After the part of the degummed spoil soil sample containing the copolymer material is cut off, it is placed in a direct shear instrument to perform a direct shear test to test the shear strength of the spoil soil sample.

进一步地,所述采用热风干燥器进行解胶,包括:Further, the use of a hot air dryer for degumming includes:

围绕所述封固的弃渣土试样顺时针运行所述热风干燥器,以对所述共聚材料的各部分进行加热烘干,以使所述共聚材料失去强度。Run the hot air dryer clockwise around the sealed spoil soil sample to heat and dry each part of the copolymer material so that the copolymer material loses strength.

本发明提供的保持弃渣土体原状结构的取样方法,包括:将质量比为1:2:4-8:2-4的纯水、丙三醇、丙烯酰胺以及丙烯酸组成的混合物在水浴加热条件下制备成丙烯酰胺-丙烯酸共聚物;在弃渣土斜坡坡面平缓部位,选择预设尺寸形状的弃渣土平面进行平整,以方便采样;其中,所述预设尺寸形状根据对弃渣土试样的测试需求确定;在平整后的所述弃渣土平面上划定注胶带,并向所述注胶带内均匀注入由所述丙烯酰胺-丙烯酸共聚物组成的共聚材料,直至达到预设深度;待所述共聚材料凝固后,将所述注胶带外围的弃渣土挖去,得到封固的弃渣土试样;由此,本发明通过采用丙烯酰胺-丙烯酸共聚物在取样的过程中对弃渣土进行封固,丙烯酰胺-丙烯酸共聚物形成的共聚材料具有较高的剪切强度,因此,在运输过程中不易破损,也就避免了弃渣土试样在运输过程中的流失,同时,由于共聚材料在烘干脱水后形成薄片容易脱落,因此,可以在对弃渣土试样进行测试时直接对共聚材料进行加热烘干使弃渣土试样和共聚材料分离,使得在测试时对弃渣土试样和封固材料的分离简单易行,也避免了加热烘干后形成液体携带部分弃渣土试样造成弃渣土试样流失的问题。The sampling method provided by the invention to maintain the original structure of the spoil soil body includes: heating a mixture composed of pure water, glycerol, acrylamide and acrylic acid with a mass ratio of 1:2:4-8:2-4 in a water bath Preparation of acrylamide-acrylic acid copolymer under the conditions; in the gentle part of the spoil slope, select a spoil plane with a preset size and shape for smoothing to facilitate sampling; wherein, the preset size and shape are based on the spoil The test requirements for the soil sample are determined; an injection tape is defined on the flattened spoil soil plane, and the copolymer material composed of the acrylamide-acrylic acid copolymer is evenly injected into the injection tape until the predetermined level is reached. Set the depth; after the copolymer material is solidified, dig out the spoil soil around the injection tape to obtain a sealed spoil soil sample; thus, the present invention uses acrylamide-acrylic acid copolymer in the sample The spoil soil is sealed during the process. The copolymer material formed by acrylamide-acrylic acid copolymer has high shear strength. Therefore, it is not easy to be damaged during transportation, which avoids the waste soil sample being damaged during transportation. At the same time, since the copolymer material forms flakes that are easy to fall off after drying and dehydration, the copolymer material can be directly heated and dried when testing the spoil soil sample to separate the spoil soil sample and the copolymer material. This makes it simple and easy to separate the spoil soil sample and the sealing material during testing, and also avoids the problem of liquid carrying part of the spoil soil sample after heating and drying, causing the waste soil sample to be lost.

附图说明Description of the drawings

构成本发明的一部分的附图用来提供对本发明的进一步理解,本发明的示意性实施例及其说明用于解释本发明,并不构成对本发明的不当限定。在附图中:The drawings forming a part of the present invention are used to provide a further understanding of the present invention. The illustrative embodiments of the present invention and their descriptions are used to explain the present invention and do not constitute an improper limitation of the present invention. In the attached picture:

图1示出了本发明实施例提供的一种保持弃渣土体原状结构的取样方法的步骤流程图;Figure 1 shows a step flow chart of a sampling method for maintaining the original structure of spoil soil provided by an embodiment of the present invention;

图2示出了本发明又一实施例提供的一种保持弃渣土体原状结构的取样方法的步骤流程图;Figure 2 shows a step flow chart of a sampling method for maintaining the original structure of spoil soil provided by yet another embodiment of the present invention;

图3示出了本发明实施例提供的一种抗剪强度测试方法的步骤流程图;Figure 3 shows a step flow chart of a shear strength testing method provided by an embodiment of the present invention;

图4示出了本发明实施例提供的直剪仪的结构示意图;Figure 4 shows a schematic structural diagram of a direct shear instrument provided by an embodiment of the present invention;

图5示出了本发明实施例提供的共聚材料取样法取得的弃渣土试样和蜡封法取得的弃渣土试样的抗剪强度测试效果图;Figure 5 shows the shear strength test effect diagram of the spoil soil sample obtained by the copolymer material sampling method and the spoil soil sample obtained by the wax sealing method provided by the embodiment of the present invention;

图6示出了本发明实施例取得的弃渣土试样和重塑土试样的抗剪强度测试效果图;Figure 6 shows the shear strength test effect diagram of the spoil soil sample and the remolded soil sample obtained in the embodiment of the present invention;

图7示出了本发明实施例取得的弃渣土试样、蜡封法取得的弃渣土试样以及重塑样的抗剪强度关系曲线;Figure 7 shows the shear strength relationship curve of the spoil soil sample obtained by the embodiment of the present invention, the spoil soil sample obtained by the wax sealing method, and the reshaped sample;

附图标记说明:100、试样下剪切盒;110、下滚珠轴承;200、水平加载装置;210、拉杆;220、第一拉环;230、第二拉环;240、水平驱动电机;300、试样上剪切盒;310、上底板;320、试样上剪切盒围板;330、试样上剪切盒边板;400、试样上剪切盒连接结构;410、轴承;500、垂直加载装置;510、球头;520、加载板;530、上滚珠轴承;540、垂直驱动电机。Explanation of reference signs: 100. Lower shear box of the sample; 110. Lower ball bearing; 200. Horizontal loading device; 210. Pull rod; 220. First pull ring; 230. Second pull ring; 240. Horizontal drive motor; 300. Upper sample shear box; 310. Upper bottom plate; 320. Upper sample shear box enclosure; 330. Upper sample shear box side plate; 400. Sample upper shear box connection structure; 410. Bearing ; 500, vertical loading device; 510, ball head; 520, loading plate; 530, upper ball bearing; 540, vertical drive motor.

具体实施方式Detailed ways

需要说明的是,在不冲突的情况下,本发明中的实施例及实施例中的特征可以相互组合。It should be noted that, as long as there is no conflict, the embodiments and features in the embodiments of the present invention can be combined with each other.

目前在岩土工程的工程建设过程中,容易造成大量工程弃渣,为实现对弃渣土的科学处置,对弃渣土的结构、力学性能进行测试,依据测试出的结构及力学特征达到对弃渣土的科学处置的目的。而在岩土工程中,土体的抗剪强度是至关重要的力学参数之一。At present, during the construction process of geotechnical engineering projects, it is easy to cause a large amount of engineering waste. In order to achieve scientific disposal of waste soil, the structure and mechanical properties of the waste soil are tested, and the structural and mechanical properties of the waste soil are tested to achieve the desired results. The purpose of scientific disposal of waste soil. In geotechnical engineering, the shear strength of soil is one of the most important mechanical parameters.

相关技术中,对弃渣土进行抗剪强度测试方法包括原位直剪试验和室内直剪试验。其中,现场原位直剪试验需要在工程现场进行,试验条件较为复杂且环境、地质因素难以控制,影响试验结果的准确性。因此,目前通常采用室内直剪试验获取弃渣土体的抗剪强度参数。In related technologies, the shear strength testing methods of waste soil include in-situ direct shear tests and indoor direct shear tests. Among them, on-site direct shear tests need to be conducted at the engineering site. The test conditions are relatively complex and environmental and geological factors are difficult to control, which affects the accuracy of the test results. Therefore, indoor direct shear tests are usually used to obtain the shear strength parameters of spoil soil.

然而,室内直剪试验获取弃渣土体抗剪强度参数通过重塑土进行,其中,重塑土为原状土经烘干、碾碎,再按照原状土的密度和含水率重新制成的外形仿原状土的一种试验用土,由此,重塑土虽然物理指标并未改变,但是重塑土的颗粒骨架排列、颗粒接触形式、孔隙分布特征均已发生了改变,破坏了弃渣土体的初始结构,也就导致重塑土与原状土力学参数差异明显,其获取的抗剪强度难以表征弃渣现场的力学特性。However, the indoor direct shear test is used to obtain the shear strength parameters of the spoil soil through reshaped soil. The reshaped soil is the shape of the original soil that has been dried and crushed, and then remade according to the density and moisture content of the original soil. It is a kind of test soil that imitates the original soil. Therefore, although the physical indicators of the reshaped soil have not changed, the particle skeleton arrangement, particle contact form, and pore distribution characteristics of the reshaped soil have all changed, destroying the spoil soil body. The initial structure of the reshaped soil results in obvious differences between the mechanical parameters of the reshaped soil and the original soil, and the obtained shear strength is difficult to characterize the mechanical properties of the abandoned slag site.

当前,为取样获取原状土,通常在取样过程中采用石蜡作为封固材料以维持原状土的稳定性和颗粒骨架初始结构,然而石蜡的强度较低,无法承受运输过程中的扰动作用,极易损坏,进而导致运输过程中原状土损失;同时,在石蜡解封过程中,通常是将石蜡热熔为蜡液,使其与原状土分离,但是由于蜡液具备一定的粘性,且蜡液极易凝固,使得分离过程复杂并且原状土易流失。Currently, in order to obtain undisturbed soil for sampling, paraffin is usually used as a sealing material during the sampling process to maintain the stability of the undisturbed soil and the initial structure of the particle skeleton. However, the strength of paraffin is low and cannot withstand the disturbance during transportation, and it is easily damaged. damage, resulting in the loss of the original soil during transportation; at the same time, during the unsealing process of paraffin, the paraffin is usually hot-melted into liquid wax to separate it from the original soil. However, because the wax liquid has a certain viscosity and the wax liquid is extremely It is easy to solidify, making the separation process complicated and the undisturbed soil easy to lose.

有鉴于此,本发明提出了保持弃渣土体原状结构的取样及抗剪强度测试方法,在取样过程中采用现场制备出的共聚材料对取样部位进行封固,由此,通过在取样过程中采用共聚材料进行封固获取弃渣土试样,由于共聚材料在凝固后其抗剪强度较高,在运输过程中不易受损,避免了原状样的流失,同时,由于本发明在共聚材料制备过程中加入了纯水,在烘干过程中,共聚材料中的水被带走,使得共聚材料在烘干后形成薄片,分离过程简单且避免了原状土流失的情况发生。In view of this, the present invention proposes a sampling and shear strength testing method that maintains the original structure of the spoil soil. During the sampling process, the copolymer material prepared on site is used to seal the sampling site. Therefore, during the sampling process, The copolymer material is used for sealing to obtain the spoil soil sample. Since the copolymer material has high shear strength after solidification, it is not easily damaged during transportation and avoids the loss of the original sample. At the same time, due to the preparation of the copolymer material in the present invention Pure water is added in the process. During the drying process, the water in the copolymer material is taken away, causing the copolymer material to form flakes after drying. The separation process is simple and avoids the loss of the original soil.

下面将参考附图并结合实施例来详细说明本发明的保持弃渣土体原状结构的取样及抗剪强度测试方法。The sampling and shear strength testing method of maintaining the original structure of the spoil soil mass according to the present invention will be described in detail below with reference to the accompanying drawings and examples.

参照图1,图1示出了本发明实施例提供的保持弃渣土体原状结构的取样方法的步骤流程图,如图1所示,所述方法包括:Referring to Figure 1, Figure 1 shows a step flow chart of a sampling method for maintaining the original structure of spoil soil provided by an embodiment of the present invention. As shown in Figure 1, the method includes:

S101,将质量比为1:2:4-8:2-4的纯水、丙三醇、丙烯酰胺以及丙烯酸组成的混合物在水浴加热条件下制备成丙烯酰胺-丙烯酸共聚物。S101, prepare an acrylamide-acrylic acid copolymer from a mixture of pure water, glycerin, acrylamide and acrylic acid with a mass ratio of 1:2:4-8:2-4 under water bath heating conditions.

其中,丙烯酰胺-丙烯酸共聚物为共聚材料,共聚材料是一类亲水性强的具备三维网络结构的凝胶。由此,基于共聚材料的强亲水性,在制备过程中加入纯水能够使共聚材料处于溶胀状态;而对共聚材料加热烘干可以使原本为溶胀状态的共聚材料脱水,进而使得共聚材料干瘪形成薄片,使得共聚材料能够轻易与土样分离;此外,溶胀状态的共聚材料仍然具有较高的抗剪切强度,在原状土运输过程中不易损坏,因此,共聚材料是原状土取样过程中较佳的封固材料。Among them, acrylamide-acrylic acid copolymer is a copolymer material. The copolymer material is a type of gel with strong hydrophilicity and a three-dimensional network structure. Therefore, based on the strong hydrophilicity of the copolymer material, adding pure water during the preparation process can make the copolymer material in a swollen state; heating and drying the copolymer material can dehydrate the copolymer material that was originally in a swollen state, causing the copolymer material to dry out. Forming flakes, the copolymer material can be easily separated from the soil sample; in addition, the copolymer material in the swollen state still has high shear strength and is not easily damaged during the transportation of the undisturbed soil. Therefore, the copolymer material is more convenient during the undisturbed soil sampling process. The best sealing material.

本发明实施例中,考虑到在工程现场对弃渣土体取样的实时性,选择丙烯酰胺-丙烯酸共聚物作为原状土的封固材料。这是由于丙烯酰胺-丙烯酸能够快速制备得到且对反应条件的要求并不严格,通常,在50~70℃的温度水浴加热10~20分钟即可完成丙烯酰胺和丙烯酸的共聚过程,得到丙烯酰胺-丙烯酸共聚物,反应快速且温度较低,适用于现场作业。In the embodiment of the present invention, considering the real-time nature of sampling spoil soil at the project site, acrylamide-acrylic acid copolymer is selected as the sealing material of the undisturbed soil. This is because acrylamide-acrylic acid can be prepared quickly and the reaction conditions are not strict. Usually, the copolymerization process of acrylamide and acrylic acid can be completed by heating in a water bath at a temperature of 50 to 70°C for 10 to 20 minutes to obtain acrylamide. -Acrylic copolymer, fast reaction and low temperature, suitable for on-site operations.

同时,为避免弃渣土试样在运输过程中的损失,需要制备出抗剪切强度较高的共聚材料,因此,将纯水、丙三醇、丙烯酰胺以及丙烯酸的质量比控制在1:2:4-8:2-4之间,得到具有较高强度的丙烯酰胺-丙烯酸共聚材料。At the same time, in order to avoid the loss of spoil soil samples during transportation, it is necessary to prepare copolymer materials with higher shear strength. Therefore, the mass ratio of pure water, glycerol, acrylamide and acrylic acid is controlled at 1: Between 2:4-8:2-4, an acrylamide-acrylic acid copolymer material with higher strength is obtained.

优选地,采用质量比为1:2:6:3的纯水、丙三醇、丙烯酰胺以及丙烯酸进行共聚材料的制备,在该质量比下,制备得到的共聚材料的强度为8MPa,能够有效避免运输过程中的损坏。Preferably, pure water, glycerol, acrylamide and acrylic acid with a mass ratio of 1:2:6:3 are used to prepare the copolymer material. Under this mass ratio, the strength of the prepared copolymer material is 8MPa, which can effectively Avoid damage during transportation.

本发明实施例中对制备出的丙烯酰胺-丙烯酸共聚物的分子量不做具体要求,能够形成一定强度共聚材料即可,其中,共聚材料的强度在3MPa以上,在该强度之上,共聚材料在运输过程中不易破损进而导致弃渣土试样的流失。In the embodiments of the present invention, there are no specific requirements for the molecular weight of the prepared acrylamide-acrylic acid copolymer, as long as it can form a copolymer material with a certain strength, wherein the strength of the copolymer material is above 3 MPa, and above this strength, the copolymer material is It is not easy to be damaged during transportation, which will lead to the loss of spoil soil samples.

S102,在弃渣土斜坡坡面平缓部位,选择预设尺寸形状的弃渣土平面进行平整,以方便采样。S102. In the gentle part of the spoil slope, select a spoil plane with a preset size and shape for smoothing to facilitate sampling.

其中,所述预设尺寸形状根据对所述弃渣土试样的测试需求确定。Wherein, the preset size and shape are determined according to the testing requirements for the spoil soil sample.

具体地,在获取弃渣土试样时,根据所需试样的大小进行取样,即根据弃渣土原状样试验所需的试样大小确定取样尺寸,同时,由于需要在试样表层采用共聚材料进行封固,因此,需要预留一部分尺寸作为注胶带,因此,在选择用于采样的弃渣土平面时,需要划定弃渣土试样稍大范围的位置进行采样。其中,试样的形状同样根据测试需要确定,测试需要为圆柱形,则挖出圆柱形的弃渣土,若是需要长方体,则挖出长方体弃渣土,本发明不做具体限制。示例地,对弃渣土试样进行直剪试验,则根据测试弃渣土试样的直剪仪中剪切盒的大小来确定挖取的弃渣土试样的尺寸,进而根据该尺寸进行弃渣土试样的采集,注胶带的宽度本发明不做具体限制,能够将弃渣土试样包裹即可。Specifically, when obtaining the spoil soil sample, the sampling is carried out according to the size of the required sample, that is, the sampling size is determined based on the size of the sample required for the original spoil soil sample test. At the same time, since it is necessary to use copolymerization on the surface of the sample The material is sealed, so a part of the size needs to be reserved as a filling tape. Therefore, when selecting the spoil soil plane for sampling, it is necessary to delineate a slightly larger range of the spoil soil sample for sampling. Among them, the shape of the sample is also determined according to the test needs. If the test needs to be cylindrical, cylindrical spoil soil is dug out. If a rectangular parallelepiped is required, rectangular parallelepiped spoil soil is dug out. There is no specific limit in the present invention. For example, when performing a direct shear test on a spoil soil sample, the size of the excavated spoil soil sample is determined based on the size of the shear box in the direct shear instrument used to test the spoil soil sample, and then the test is carried out based on this size. When collecting waste soil samples, the width of the injection tape is not specifically limited in the present invention, as long as the waste soil samples can be wrapped.

S103,在平整后的所述弃渣土平面上划定注胶带,并向所述注胶带内均匀注入由所述丙烯酰胺-丙烯酸共聚物组成的共聚材料,直至达到预设深度。S103, define an injection tape on the leveled spoil soil plane, and evenly inject a copolymer material composed of the acrylamide-acrylic acid copolymer into the injection tape until a preset depth is reached.

本发明实施例中,在选择用于采样的弃渣土平面后,在弃渣土平面划定一定范围的注胶带,以通过注入的共聚材料提高注胶带内的弃渣土的强度,进而达到对试样的封固效果。In the embodiment of the present invention, after selecting the spoil soil plane for sampling, a certain range of injection tape is defined on the spoil soil plane to increase the strength of the spoil soil in the injection tape through the injected copolymer material, thereby achieving Sealing effect on the specimen.

将弃渣土试样外表层一定宽度范围作为注胶带,将液态的共聚材料均匀注入弃渣土表面,由于弃渣土为颗粒堆积的多孔隙结构,丙烯酰胺-丙烯酸共聚物可以从孔隙中渗透进入使部分弃渣土硬化,以对内部的弃渣土进行封固,避免内部弃渣土受到扰动。其中,预设深度为注胶所需达到的深度,为达到对弃渣土的封固效果,一般将预设深度设置为弃渣土试样高度的1.1-1.2倍,以将弃渣土试样侧表面完全覆盖。A certain width range of the outer surface of the spoil soil sample is used as an injection tape, and the liquid copolymer material is evenly injected onto the surface of the spoil soil. Since the spoil soil has a porous structure with accumulation of particles, the acrylamide-acrylic acid copolymer can penetrate from the pores. Enter to harden part of the spoil soil to seal the internal spoil soil and prevent the internal spoil soil from being disturbed. Among them, the preset depth is the depth required for glue injection. In order to achieve the sealing effect of the spoil soil, the preset depth is generally set to 1.1-1.2 times the height of the spoil soil sample, so that the spoil soil test The sample side surface is completely covered.

S104,待所述共聚材料凝固后,将所述注胶带外围的弃渣土挖去,得到封固的弃渣土试样。S104: After the copolymer material solidifies, dig out the spoil soil around the injection tape to obtain a sealed spoil soil sample.

具体地,丙烯酰胺-丙烯酸共聚物冷却后形成凝胶状物质,即形成固态的共聚材料,因此,在丙烯酰胺-丙烯酸未冷却凝固时就需要将其注入注胶带中,以使其能够以流体的形式填充弃渣土试样外层设定好的注胶带中,进而在丙烯酰胺-丙烯酸冷却后,使得外层注胶带硬化实现对弃渣土试样的封固。Specifically, acrylamide-acrylic acid copolymer forms a gel-like substance after cooling, that is, it forms a solid copolymer material. Therefore, when acrylamide-acrylic acid is not cooled and solidified, it needs to be injected into the injection tape so that it can be solidified as a fluid. The form is filled into the set outer layer of the injection tape of the spoil soil sample, and then after the acrylamide-acrylic acid is cooled, the outer layer of the injection tape is hardened to seal the spoil soil sample.

在共聚材料凝固后,就形成了表面有一定强度的弃渣土试样,此时,再将注胶带外围的弃渣土挖去,以得到封固的弃渣土试样。After the copolymer material solidifies, a spoil soil sample with a certain strength on the surface is formed. At this time, the spoil soil on the periphery of the injection tape is dug out to obtain a sealed spoil soil sample.

在一些实施例中,考虑到只对弃渣土侧面进行封固在运输过程中还是可能受到扰动,在挖去注胶带外围的弃渣土后,削去弃渣土试样底部的部分共聚材料,以向弃渣土试样的底面注入共聚材料,待共聚材料凝固后,将底面削平整,以对弃渣土试样的底面也进行加固。In some embodiments, considering that sealing only the side of the spoil soil may still be disturbed during transportation, after digging out the spoil soil around the injection tape, part of the copolymer material at the bottom of the spoil soil sample is cut off , to inject copolymer material into the bottom surface of the spoil soil sample. After the copolymer material solidifies, the bottom surface is smoothed to reinforce the bottom surface of the spoil soil sample.

本发明实施例提供的保持弃渣土体原状结构的取样方法,通过制备共聚材料,并在其未冷却时,将共聚材料注入试样划定的注胶带中,使其冷却后形成的固体能够将原状样完全包裹,形成封固的弃渣土试样,由此,通过采用强度较高共聚材料作为封固材料对原状样进行包裹,避免运输过程中,由于强度不足导致原状样损失的情况,同时,由于对吸水后的共聚材料烘干可直接对其脱水,进而形成干瘪的薄片,由于干瘪的薄片强度较弱,此时直接将注胶带部分的原状样挖去,即可得到保持弃渣土原状结构的试样,去除封固材料的方法简便易行,因此,采用本发明实施例提供的取样方法,在保持弃渣土体原状结构的同时,还能够避免原状样在运输过程中的损失且易于测试阶段对封固材料和原状样的分离。The sampling method provided by the embodiment of the present invention to maintain the original structure of the spoil soil body is to prepare a copolymer material, and before it is cooled, inject the copolymer material into the injection tape demarcated by the sample, so that the solid formed after cooling can The original sample is completely wrapped to form a sealed spoil soil sample. Therefore, the original sample is wrapped with a higher-strength copolymer material as the sealing material to avoid the loss of the original sample due to insufficient strength during transportation. , at the same time, since the copolymer material after absorbing water can be directly dehydrated by drying it, and then form shriveled flakes, since the shriveled flakes are weak in strength, at this time, just dig out the original part of the adhesive tape to obtain the remaining waste. For samples with the original structure of the spoil, the method of removing the sealing material is simple and easy. Therefore, using the sampling method provided by the embodiment of the present invention can maintain the original structure of the spoil and avoid the original sample being transported during transportation. loss and easy separation of the mounting material and the original sample during the testing stage.

参照图2,图2示出了本发明又一实施例提供的保持弃渣土体原状结构的取样方法的步骤流程图,如图2所示,所述方法包括:Referring to Figure 2, Figure 2 shows a step flow chart of a sampling method for maintaining the original structure of spoil soil provided by yet another embodiment of the present invention. As shown in Figure 2, the method includes:

S201,向所述纯水中依次加入所述丙三醇、所述丙烯酸以及所述丙烯酰胺,搅拌混合得到混合液。S201: Add the glycerin, the acrylic acid and the acrylamide to the pure water in sequence, stir and mix to obtain a mixed liquid.

具体地,为使多种组分充分溶解,在加入纯水、丙三醇以及丙烯酸后,持续对混合物进行搅拌,并且边搅拌边加入丙烯酰胺,以使丙烯酸和丙烯酰胺充分混合。本发明实施例中,所述丙烯酰胺的纯度在99%以上,所述丙烯酸的纯度为99%以上,所述丙三醇的纯度在95%以上。Specifically, in order to fully dissolve various components, after adding pure water, glycerol and acrylic acid, the mixture is continuously stirred, and acrylamide is added while stirring, so that acrylic acid and acrylamide are fully mixed. In the embodiments of the present invention, the purity of the acrylamide is above 99%, the purity of the acrylic acid is above 99%, and the purity of the glycerol is above 95%.

S202,向所述混合液中加入引发剂,搅拌后保持50~70℃的温度水浴加热10 ~20分钟,得到所述丙烯酰胺-丙烯酸共聚物。S202, add an initiator to the mixed solution, stir and heat in a water bath maintaining a temperature of 50 to 70°C for 10 to 20 minutes, to obtain the acrylamide-acrylic acid copolymer.

本发明实施例中,引发剂与丙烯酰胺的质量比为1:5-1:10,引发剂包括过硫酸盐、偶氮化合物中的任一种。In the embodiment of the present invention, the mass ratio of initiator to acrylamide is 1:5-1:10, and the initiator includes any one of persulfate and azo compound.

优选地,引发剂与丙烯酰胺的质量比为1:5,在能够得到强度较高的共聚材料的同时,节省材料。Preferably, the mass ratio of initiator to acrylamide is 1:5, which can obtain a copolymer material with higher strength and save materials at the same time.

优选地,控制温度在60℃,水浴加热时间以10分钟为宜,可根据丙烯酰胺含量适当增加水浴加热时间,但不宜超过20分钟。为对现场弃渣土体及时取样,在制备的过程中可以将温度控制稍高,以较快得到共聚材料,满足现场需要。Preferably, the temperature is controlled at 60°C, and the water bath heating time is preferably 10 minutes. The water bath heating time can be appropriately increased according to the acrylamide content, but it should not exceed 20 minutes. In order to sample the on-site spoil soil in a timely manner, the temperature can be controlled slightly higher during the preparation process to obtain copolymer materials quickly to meet on-site needs.

其中,生成共聚材料——丙烯酰胺-丙烯酸共聚物的过程中主要发生,丙烯酸和丙烯酰胺/>的共聚反应:Among them, the main process of generating copolymer material-acrylamide-acrylic acid copolymer, acrylic acid and acrylamide/> Copolymerization reaction:

.

S203,在弃渣土斜坡坡面平缓部位,选择预设尺寸形状的弃渣土平面进行平整,以方便采样。S203. In the gentle part of the spoil slope, select a spoil plane with a preset size and shape for smoothing to facilitate sampling.

其中,所述预设尺寸形状根据对所述弃渣土试样的测试需求确定。Wherein, the preset size and shape are determined according to the testing requirements for the spoil soil sample.

S204,在平整后的所述弃渣土平面上划定注胶带,并向所述注胶带内均匀注入由所述丙烯酰胺-丙烯酸共聚物组成的共聚材料,直至达到预设深度。S204, define an injection tape on the leveled spoil soil plane, and evenly inject a copolymer material composed of the acrylamide-acrylic acid copolymer into the injection tape until a preset depth is reached.

本发明实施例中,预设深度为注胶所需达到的深度,为达到对弃渣土的封固效果,一般将预设深度甚至为弃渣土试样高度的1.1-1.2倍,以将弃渣土试样侧表面完全覆盖;而注胶带的宽度一般为弃渣土试样宽度的1/10-1/6;在此范围内,作为封固材料的共聚材料不会太薄,使得弃渣土试样在运输过程中受到扰动,导致弃渣土试样的颗粒骨架初始结构等发生变化,也不会太厚,导致材料浪费或是共聚材料凝固时间较长。In the embodiment of the present invention, the preset depth is the depth required for glue injection. In order to achieve the sealing effect of the spoil soil, the preset depth is generally even 1.1-1.2 times the height of the spoil soil sample, so as to achieve the sealing effect of the spoil soil. The side surface of the spoil soil sample is completely covered; the width of the injection tape is generally 1/10-1/6 of the width of the spoil soil sample; within this range, the copolymer material used as the sealing material will not be too thin, so that The spoil soil sample is disturbed during transportation, which causes the initial structure of the particle skeleton of the spoil soil sample to change. It will not be too thick, resulting in material waste or a long solidification time of the copolymer material.

由于挖出的弃渣土试样以及注胶带与试验所需的试样大小有关,因此,根据试验仪器的大小来确认挖出弃渣土试样的尺寸以及注入丙烯酰胺-丙烯酸共聚物的注胶带的宽度,如在进行直剪试验时,根据直剪仪能够盛装的试样尺寸来确定。Since the excavated spoil soil sample and the injection tape are related to the size of the sample required for the test, the size of the excavated spoil soil sample and the injection of acrylamide-acrylic acid copolymer were confirmed based on the size of the test instrument. The width of the tape, such as when performing a direct shear test, is determined based on the size of the sample that the direct shear instrument can hold.

示例地,直剪剪切盒为17cm×18cm×20cm的长方体,则在取样时,选取高度在20cm以上的弃渣土斜坡,且其顶部面积在20cm×20cm以上,此时,先平整大于试样顶面尺寸的平面用于注胶,具体平整用于注胶平面的尺寸根据注胶带的大小确定,如所需注胶带的宽度为3cm,则平整平面的长度和宽度应比原状土试样宽度多出3cm,将从外表层至深度3cm位置作为注胶带,以注入丙烯酰胺-丙烯酸共聚物。由此,通过表面注入丙烯酰胺-丙烯酸共聚物提高弃渣土试样表面强度,避免内部的弃渣土受到扰动。For example, if the direct shear box is a 17cm × 18cm × 20cm rectangular parallelepiped, then when sampling, select a spoil soil slope with a height of more than 20cm, and its top area is more than 20cm × 20cm. At this time, the slope should be flattened first. The flat surface of the top surface of the sample is used for glue injection. The specific size of the flat plane used for glue injection is determined according to the size of the injection tape. If the required width of the injection tape is 3cm, the length and width of the flat plane should be larger than that of the undisturbed soil sample. The extra 3cm in width will be used as an injection tape from the outer surface to a depth of 3cm to inject acrylamide-acrylic acid copolymer. As a result, the surface strength of the spoil soil sample was increased by injecting acrylamide-acrylic acid copolymer onto the surface to prevent the internal spoil soil from being disturbed.

具体地,向弃渣土试样均匀注入液态的丙烯酰胺-丙烯酸共聚物的过程为:采用带有孔隙压力探头的注胶设备,向所述注胶带内均匀注入所述共聚材料,所述共聚材料的注入量和注入深度通过所述孔隙压力探头控制;在注胶过程中,所述注胶设备为加热状态,以保持所述丙烯酰胺-丙烯酸共聚物的流动性。Specifically, the process of uniformly injecting liquid acrylamide-acrylic acid copolymer into the spoil soil sample is: using a glue injection equipment with a pore pressure probe, uniformly injecting the copolymer material into the injection tape. The injection amount and depth of material are controlled by the pore pressure probe; during the glue injection process, the glue injection equipment is heated to maintain the fluidity of the acrylamide-acrylic acid copolymer.

示例地,在向注胶带注胶时,先将反应完成的丙烯酰胺-丙烯酸共聚物注入带有孔隙压力探头的注胶设备中;此时,丙烯酰胺-丙烯酸共聚物还未冷却,以使其能够以液体状态注入注胶设备。For example, when injecting glue into the injection tape, the reaction-completed acrylamide-acrylic acid copolymer is first injected into the glue injection equipment with a pore pressure probe; at this time, the acrylamide-acrylic acid copolymer has not yet cooled down to allow it to It can be injected into glue injection equipment in liquid state.

而后,采用该带有孔隙压力探头的注胶设备,向注胶带内均匀注入共聚材料,在注入过程中,通过孔隙压力探头监测注胶过程中,注胶带的孔隙压力变化,基于变化调节共聚材料的注入量;以及,通过孔隙压力值控制共聚材料的注入深度,以使共聚材料能够被均匀注入注胶带中,并达到预设深度。Then, the glue injection equipment with a pore pressure probe is used to evenly inject the copolymer material into the injection tape. During the injection process, the pore pressure changes of the injection tape are monitored through the pore pressure probe, and the copolymer material is adjusted based on the changes. The injection amount; and, the injection depth of the copolymer material is controlled through the pore pressure value, so that the copolymer material can be evenly injected into the injection tape and reach the preset depth.

在具体实施时,通过水平向和竖直向的孔隙压力探头在注胶带内移动,以使共聚材料能够在注胶带内扩散。需要注意的是,由于共聚材料在冷却后会凝固失去流动性,因此注胶过程中需要保持注胶设备为加热状态,以使共聚材料以液体的形式注入弃渣土孔隙中。In the specific implementation, the horizontal and vertical pore pressure probes are moved in the injection tape to enable the copolymer material to diffuse in the injection tape. It should be noted that since the copolymer material will solidify and lose fluidity after cooling, the glue injection equipment needs to be kept heated during the glue injection process so that the copolymer material can be injected into the pores of the spoil soil in the form of liquid.

S205,待所述共聚材料凝固后,将所述注胶带外围的弃渣土挖去,得到封固的弃渣土试样。S205: After the copolymer material solidifies, dig out the spoil soil around the injection tape to obtain a sealed spoil soil sample.

待丙烯酰胺-丙烯酸共聚物冷却后,形成的共聚材料——丙烯酰胺-丙烯酸共聚物支撑表面弃渣土的空隙,提高其表面强度,由此,通过丙烯酰胺-丙烯酸共聚物提高强度,避免弃渣土试样受到扰动,从而能够得到原状样。After the acrylamide-acrylic acid copolymer is cooled, the copolymer material formed - acrylamide-acrylic acid copolymer supports the voids of the surface spoil soil and improves its surface strength. Therefore, the acrylamide-acrylic acid copolymer improves the strength and avoids spoilage. The soil sample is disturbed so that the original sample can be obtained.

本发明实施例提供的保持弃渣土体原状结构的取样方法,通过制备共聚材料,并在其未冷却时,将共聚材料注入弃渣土表层注胶带中,使其冷却后形成的固体能够充填注胶带内孔隙,形成共聚材料封固的弃渣土试样,由此,通过采用强度较高共聚材料作为封固材料对弃渣土试样进行硬化包裹,避免运输过程中,由于强度不足导致原状样损失的情况,同时,由于对吸水后的共聚材料烘干可直接对其脱水,进而形成干瘪的薄片,由于干瘪的薄片强度较弱,此时直接将注胶带部分的原状样削去,即可得到保持弃渣土原状结构的试验试样,去除封固材料的方法简便易行,因此,采用本发明实施例提供的取样方法,在保持弃渣土体原状结构的同时,还能够避免原状样在运输过程中的损失且易于测试阶段对封固材料和原状样的分离。The sampling method provided by the embodiment of the present invention to maintain the original structure of the spoil soil body is to prepare a copolymer material and inject the copolymer material into the surface injection tape of the spoil soil before it is cooled, so that the solid formed after cooling can be filled The pores in the tape are filled to form a spoil soil sample sealed with a copolymer material. Therefore, the spoil soil sample is hardened and wrapped by using a higher-strength copolymer material as the sealing material to avoid damage caused by insufficient strength during transportation. In the case of loss of the original sample, at the same time, drying the copolymer material after absorbing water can directly dehydrate it, thereby forming shriveled flakes. Since the dried flakes are weak in strength, the original sample of the tape-injected part is directly cut off at this time. A test sample that maintains the original structure of the spoil soil can be obtained, and the method of removing the sealing material is simple and easy. Therefore, by using the sampling method provided by the embodiment of the present invention, while maintaining the original structure of the spoil soil, it can also avoid The original sample is lost during transportation and it is easy to separate the sealing material and the original sample during the testing stage.

参照图3,图3示出了本发明实施例提供的抗剪强度测试方法的步骤流程图,如图3所示,所述方法包括:Referring to Figure 3, Figure 3 shows a step flow chart of a shear strength testing method provided by an embodiment of the present invention. As shown in Figure 3, the method includes:

S301,将质量比为1:2:4-8:2-4的纯水、丙三醇、丙烯酰胺以及丙烯酸组成的混合物在水浴加热条件下制备成丙烯酰胺-丙烯酸共聚物。S301, prepare an acrylamide-acrylic acid copolymer from a mixture of pure water, glycerin, acrylamide and acrylic acid with a mass ratio of 1:2:4-8:2-4 under water bath heating conditions.

优选地,采用质量比为1:2:6:3的纯水、丙三醇、丙烯酰胺以及丙烯酸组成的混合物制备成丙烯酰胺-丙烯酸共聚物,其制备得到丙烯酰胺-丙烯酸共聚物的强度能够达到8MPa。Preferably, an acrylamide-acrylic acid copolymer is prepared from a mixture of pure water, glycerol, acrylamide and acrylic acid with a mass ratio of 1:2:6:3, and the strength of the acrylamide-acrylic acid copolymer obtained can be Reach 8MPa.

S302,在弃渣土斜坡坡面平缓部位,选择预设尺寸形状的弃渣土平面进行平整,以方便采样。S302. In the gentle part of the spoil slope, select a spoil plane with a preset size and shape for smoothing to facilitate sampling.

其中,所述预设尺寸形状根据对所述弃渣土试样的测试需求确定。Wherein, the preset size and shape are determined according to the testing requirements for the spoil soil sample.

S303,在平整后的所述弃渣土平面上划定注胶带,并向所述注胶带内均匀注入由所述丙烯酰胺-丙烯酸共聚物组成的共聚材料,直至达到预设深度。S303, define an injection tape on the leveled spoil soil plane, and evenly inject a copolymer material composed of the acrylamide-acrylic acid copolymer into the injection tape until a preset depth is reached.

S304,待所述共聚材料凝固后,将所述注胶带外围的弃渣土挖去,得到封固的弃渣土试样。S304: After the copolymer material solidifies, dig out the spoil soil around the injection tape to obtain a sealed spoil soil sample.

S305,对所述封固的弃渣土试样,采用热风干燥器进行解胶。S305, use a hot air dryer to degumm the sealed spoil soil sample.

本发明实施例中,由于采用的是室内直剪试验方法测试原状土的抗剪强度,在得到共聚材料封固的弃渣土试样后,将弃渣土试样运至实验室进行直剪试验,具体地,在将弃渣土试样装入运输箱时,在原状土与运输箱之间的间隔填充缓冲充气袋,以在运输过程中降低对原状土的扰动。In the embodiment of the present invention, since the indoor direct shear test method is used to test the shear strength of the undisturbed soil, after the spoil soil sample sealed with the copolymer material is obtained, the spoil soil sample is transported to the laboratory for direct shearing. During the test, specifically, when loading the spoil soil sample into the transport box, a cushioning air bag was filled in the gap between the original soil and the transport box to reduce disturbance to the original soil during transportation.

在进行测试时,先对原状样进行解胶;具体地,围绕所述共聚材料封固的弃渣土试样顺时针运行所述热风干燥器,以对所述共聚材料的各部分进行加热烘干,以使所述共聚材料失去强度。When conducting the test, the original sample is first degummed; specifically, the hot air dryer is run clockwise around the spoil soil sample sealed with the copolymer material to heat and dry each part of the copolymer material. Dry so that the copolymer material loses strength.

由于在制备共聚材料的过程中加入了纯水,实际作为封固材料的共聚材料为溶胀状态,因此,在将共聚材料加热烘干时,由于水分的流失,共聚材料会形成干瘪的薄片,此时,与共聚材料混合的部分弃渣土削去,即可得到保持原状结构的弃渣土,即弃渣土原状样,因此,解胶过程简单易行。其中,由于共聚材料为易燃材料,在对共聚材料进行加热烘干时,注意使热风干燥器与共聚材料保持一定距离,以防止引燃共聚材料。本发明实施例中,使共聚材料封固的弃渣土的表面与热风干燥器保持15cm距离,以进行加热烘干。Since pure water is added during the preparation of the copolymer material, the copolymer material actually used as a sealing material is in a swollen state. Therefore, when the copolymer material is heated and dried, the copolymer material will form dry flakes due to the loss of water. When the waste material is mixed with the copolymer material, the part of the waste soil mixed with the copolymer material can be cut off to obtain the waste soil that maintains the original structure, that is, the waste soil remains in its original shape. Therefore, the degumming process is simple and easy. Among them, since the copolymer material is a flammable material, when heating and drying the copolymer material, be careful to keep a certain distance between the hot air dryer and the copolymer material to prevent the copolymer material from igniting. In the embodiment of the present invention, the surface of the spoil soil sealed with the copolymer material is kept at a distance of 15 cm from the hot air dryer for heating and drying.

S306,将解胶后的所述弃渣土试样中包含所述共聚材料的部分削去后,置于直剪仪中进行直剪试验,以测试所述弃渣土试样的抗剪强度。S306. After cutting off the part containing the copolymer material from the degummed spoil soil sample, place it in a direct shear instrument to perform a direct shear test to test the shear strength of the spoil soil sample. .

本发明实施例中,在削去弃渣土试样中包含共聚材料的部分后,即可得到完整的、不包含杂质的弃渣土试样,以用于抗剪强度测试。In the embodiment of the present invention, after cutting off the part containing the copolymer material in the spoil soil sample, a complete spoil soil sample without impurities can be obtained for shear strength testing.

在一些实施例中,为对弃渣土试样结构等进行研究,在对弃渣土试样进行抗剪强度测试之前,可以在解胶后先进行岩土CT扫描,获取弃渣土试样的初始孔隙参数、颗粒形态以及颗粒接触关系等参数,而后再进行直剪试验,测试弃渣土试样的抗剪强度。In some embodiments, in order to study the structure of the spoil soil sample, before performing a shear strength test on the spoil soil sample, a geotechnical CT scan can be performed after degumming to obtain the spoil soil sample. The parameters such as initial pore parameters, particle morphology and particle contact relationship are then conducted, and then a direct shear test is conducted to test the shear strength of the spoil soil sample.

具体地,对弃渣土试样进行直剪试验,所述直剪试验在直剪仪中进行,具体方法包括:Specifically, a direct shear test was performed on the spoil soil sample. The direct shear test was performed in a direct shear instrument. The specific method includes:

将解胶后的弃渣土试样置于直剪剪切盒中,使得弃渣土试样底部位于试样下剪切盒中,依次安装试样上剪切盒、上剪切盖板、滚珠轴承、加载板、千斤顶活塞、承力顶板及水平加载装置;Place the degummed spoil soil sample in a direct shear shear box so that the bottom of the spoil soil sample is located in the lower shear box of the specimen. Install the upper shear box, upper shear cover plate, and Ball bearings, loading plates, jack piston, load-bearing top plate and horizontal loading device;

进行直剪试验,开始法向力和切向力的加载,记录加载过程中的切向力与切向位移;Conduct a direct shear test, start loading normal force and tangential force, and record the tangential force and tangential displacement during the loading process;

基于切向力和切向位移,确定所述弃渣土试样的抗剪强度。Based on the tangential force and tangential displacement, the shear strength of the spoil soil specimen was determined.

示例地,参照图4,图4示出了本发明实施例中用于直剪试验的直剪仪的结构示意图,如图4所示,直剪仪由试样下剪切盒100、与试样下剪切盒100连接的水平加载装置200、与试样下剪切盒100对应的试样上剪切盒300、试样上剪切盒连接结构400以及垂直加载装置500组成。For example, referring to Figure 4, Figure 4 shows a schematic structural diagram of a direct shear instrument used for a direct shear test in an embodiment of the present invention. As shown in Figure 4, the direct shear instrument consists of a sample lower shear box 100, and a test It consists of a horizontal loading device 200 connected to the lower shear box 100, an upper shear box 300 corresponding to the lower shear box 100, a connection structure 400 for the upper shear box and a vertical loading device 500.

其中,水平加载装置200包括拉杆210、第一拉环220、第二拉环230及水平驱动电机240,水平驱动电机240的一端与支撑面连接,另一端通过第一拉环220与拉杆210连接,拉杆210的另一端与第二拉环230固定,拉杆210通过第二拉环230与试样下剪切盒100外壁连接,拉杆与拉环构成的传动系统较为灵活,能够减少试验误差。The horizontal loading device 200 includes a pull rod 210, a first pull ring 220, a second pull ring 230 and a horizontal drive motor 240. One end of the horizontal drive motor 240 is connected to the support surface, and the other end is connected to the pull rod 210 through the first pull ring 220. , the other end of the pull rod 210 is fixed to the second pull ring 230, and the pull rod 210 is connected to the outer wall of the lower shear box 100 of the sample through the second pull ring 230. The transmission system composed of the pull rod and the pull ring is relatively flexible and can reduce test errors.

垂直加载装置500包括球头510、加载板520、上滚珠轴承530以及垂直驱动电机540,垂直驱动电机540上侧与支撑面固定,下侧输出端与球头510连接并可转动,球头510另一侧与加载板520顶面连接,加载板520底面与试样上剪切盒300的上底板310通过上滚珠轴承530连接。The vertical loading device 500 includes a ball head 510, a loading plate 520, an upper ball bearing 530 and a vertical drive motor 540. The upper side of the vertical drive motor 540 is fixed to the supporting surface, and the lower output end is connected to the ball head 510 and can rotate. The ball head 510 The other side is connected to the top surface of the loading plate 520, and the bottom surface of the loading plate 520 is connected to the upper bottom plate 310 of the sample upper shear box 300 through the upper ball bearing 530.

具体实施时,在安装好的试样下剪切盒100中装入解胶后的原状土试样,再组装好试样上剪切盒300的试样上剪切盒围板320、试样上剪切盒边板330,并在试样上剪切盒的内壁涂上一层矿脂。将试样上剪切盒300的试样上剪切盒边板330所在的一端开口朝下,置于试样下剪切盒100和原状样的表面,然后安装试样上剪切盒300的上底板310。During the specific implementation, the degummed undisturbed soil sample is loaded into the installed lower sample shearing box 100, and then the upper sample shearing box 300, the upper sample shearing box enclosure 320, and the sample are assembled. Upper shear box side plate 330, and coat the inner wall of the shear box with a layer of petrolatum on the sample. Place the upper shearing box 300 on the sample with the open end of the upper shearing box side plate 330 facing downward, place the lower shearing box 100 on the sample and the surface of the original sample, and then install the upper shearing box 300 on the sample. Upper base plate 310.

将装满了原状样的试样下剪切盒100与试样上剪切盒300放到下滚珠轴承110上,此时应该确保试样下剪切盒100与试样上剪切盒300正置于下滚珠轴承110上,避免由于位置误差产生偏心应力。Place the sample lower shear box 100 and the sample upper shear box 300 filled with the original sample on the lower ball bearing 110. At this time, it should be ensured that the sample lower shear box 100 and the sample upper shear box 300 are aligned. Place it on the lower ball bearing 110 to avoid eccentric stress due to position error.

将试样下剪切盒100连接至水平加载装置200上,试样上剪切盒300通过轴承410与试样上剪切盒连接结构400连接。在试样上剪切盒300的底部外侧设置加载板520和上滚珠轴承530,再连接垂直加载装置500。The lower shear box 100 of the sample is connected to the horizontal loading device 200 , and the upper shear box 300 of the sample is connected to the upper shear box connection structure 400 of the sample through the bearing 410 . A loading plate 520 and an upper ball bearing 530 are provided on the outside of the bottom of the upper shear box 300 on the sample, and then the vertical loading device 500 is connected.

安装完设备后开始直剪试验,首先卸下试样上剪切盒300的试样上剪切盒边板330,然后垂直驱动电机540加载,水平驱动电机240加载,使得试样下剪切盒100以预设的速度沿第二方向位移,其中,所述第二方向为向所述水平驱动电机240靠近的方向。After installing the equipment, start the direct shear test. First, remove the upper sample shearing box side plate 330 of the sample upper shearing box 300, then load the vertical drive motor 540, and load the horizontal drive motor 240, so that the sample lowers the shear box. 100 is displaced in a second direction at a preset speed, wherein the second direction is a direction approaching the horizontal driving motor 240 .

记录垂直驱动电机540和水平驱动电机240的功率,功率可以用来计算剪切盒的应力,并计算得到原状样的抗剪强度。Record the power of the vertical drive motor 540 and the horizontal drive motor 240. The power can be used to calculate the stress of the shear box and calculate the shear strength of the original sample.

本发明实施例中,还采用了石蜡获取弃渣土试样,对石蜡封固的弃渣土试样进行解封后,将取得的原状土采用同一直剪仪进行直剪试验,试验结果如图5所示,图中示出了分别采用石蜡封固取得的试样和采用共聚材料封固取得的试样的抗剪强度曲线;其中,水凝胶法对应的曲线为本发明实施例提供的使用共聚材料的取样方法得到的原状样对应的抗剪强度曲线。In the embodiment of the present invention, paraffin is also used to obtain the spoil soil sample. After the paraffin-sealed spoil soil sample is unsealed, the obtained undisturbed soil is subjected to a direct shear test using the same direct shear instrument. The test results are as follows As shown in Figure 5, the figure shows the shear strength curves of samples obtained by sealing with paraffin and sealing with copolymer materials; among them, the curve corresponding to the hydrogel method is provided for the embodiment of the present invention. The shear strength curve corresponding to the original sample obtained using the copolymer material sampling method.

从试验结果来看,蜡封法取样获得的弃渣土原状样,尽管保持了大部分原状样的初始结构,但直剪试验结果受到部分初始结构破坏的影响,在高剪切应力下,即300KPa以及400KPa的情况下,其抗剪强度略低于共聚材料法取得的原状样。同时由于蜡封法在解胶过程中无法完全将蜡液去除,最终会导致融化的蜡液重新凝固,在剪切后期会出现应力骤增、骤降的现象,这是因为此时剪切部分为石蜡原状土的胶结物。Judging from the test results, although the original sample of spoil soil obtained by wax sealing method maintains most of the original structure of the original sample, the direct shear test results are affected by the damage of part of the initial structure. Under high shear stress, that is, In the case of 300KPa and 400KPa, the shear strength is slightly lower than the original sample obtained by the copolymer material method. At the same time, because the wax sealing method cannot completely remove the wax liquid during the degumming process, it will eventually cause the melted wax liquid to re-solidify. In the later stage of shearing, there will be a sudden increase and decrease in stress. This is because the sheared part at this time It is the cement of paraffin undisturbed soil.

本发明实施例中,还与重塑样直剪试验进行了对比,试验结果如图6所示,图中示出了采用共聚材料封固取得的试样和重塑样的抗剪强度曲线。其中,水凝胶法对应的曲线为本发明实施例提供的使得共聚材料的取样方法得到的原状样对应的抗剪强度曲线。从试验结果来看,弃渣土重塑样因在取样和制样过程中完全破坏了弃渣土体初始结构,在剪切过程中规律性较差,峰值应力一般低于原状样的试验结果。In the embodiment of the present invention, the direct shear test of the reshaped sample was also compared. The test results are shown in Figure 6, which shows the shear strength curve of the sample sealed with copolymer material and the reshaped sample. Among them, the curve corresponding to the hydrogel method is the shear strength curve corresponding to the original sample obtained by the sampling method of the copolymer material provided in the embodiment of the present invention. Judging from the test results, the reshaped sample of spoil soil completely destroyed the initial structure of the spoil soil during the sampling and sample preparation process. The regularity during the shearing process was poor, and the peak stress was generally lower than the test results of the original sample. .

以抗剪强度(峰值应力)为纵坐标,垂直压力(法向压力)为横坐标,绘制抗剪强度与垂直压力的关系曲线。直线与横坐标的夹角为弃渣土体的内摩擦角,直线在纵坐标轴上的截距为弃渣土的黏聚力。绘制的抗剪强度关系曲线如图7所示,其中,水凝胶法对应的曲线为本发明实施例提供的使用共聚材料的取样方法得到的原状样对应的抗剪强度曲线。图中示出了采用共聚材料封固取得的试样和重塑样的抗剪强度关系曲线。从结果来看,共聚材料法取得的弃渣土体因保持了原状样的初始结构,获得的黏聚力低于蜡封法而高于重塑样、内摩擦角高于蜡封法和重塑样,这就使得在实际工程中采用共聚材料法获取原状样能够清晰的了解到土样的力学特性。Taking shear strength (peak stress) as the ordinate and vertical pressure (normal pressure) as the abscissa, draw the relationship curve between shear strength and vertical pressure. The angle between the straight line and the abscissa is the internal friction angle of the spoil soil, and the intercept of the straight line on the ordinate axis is the cohesion of the spoil soil. The plotted shear strength relationship curve is shown in Figure 7, in which the curve corresponding to the hydrogel method is the shear strength curve corresponding to the original sample obtained by the sampling method using the copolymer material provided in the embodiment of the present invention. The figure shows the shear strength relationship curve of the specimens sealed with copolymer materials and the reshaped specimens. Judging from the results, the spoil soil obtained by the copolymer material method maintains the original structure of the original sample, the cohesion obtained is lower than that of the wax sealing method but higher than that of the reshaped sample, and the internal friction angle is higher than that of the wax sealing method and the reshaped sample. This allows us to clearly understand the mechanical properties of the soil sample by using the copolymer material method to obtain the original sample in actual engineering.

本发明实施例提供的抗剪强度测试方法,将取样过程中取得的弃渣土采用共聚材料封固,得益于共聚材料较高的强度,在运输过程中可以避免原状土受到扰动,进而避免原状土在运输过程中的流失,同时,由于共聚材料在加热烘干后能够形成性脆的薄片,使得封固材料的解封过程简单易行,且解封过程中原状样不会流失,避免原状样流失的情况导致抗剪强度测试不准确,以及由于封固材料解封过程较为复杂,导致试验过程复杂,时间较长的问题。The shear strength testing method provided by the embodiment of the present invention uses copolymer material to seal the spoil soil obtained during the sampling process. Thanks to the higher strength of the copolymer material, the undisturbed soil can be prevented from being disturbed during transportation, thereby preventing The original soil is lost during transportation. At the same time, because the copolymer material can form brittle flakes after heating and drying, the unsealing process of the sealing material is simple and easy, and the original soil will not be lost during the unsealing process, which avoids The loss of the original sample leads to inaccurate shear strength testing, and the complicated unsealing process of the sealing material results in a complicated and long test process.

以上所述仅为本发明的较佳实施例而已,并不用以限制本发明,凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内;The above descriptions are only preferred embodiments of the present invention and are not intended to limit the present invention. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention shall be included in the present invention. within the scope of protection;

对于方法实施例,为了简单描述,故将其都表述为一系列的动作组合,但是本领域技术人员应该知悉,本发明并不受所描述的动作顺序的限制,因为依据本发明,某些步骤可以采用其他顺序或者同时进行。其次,本领域技术人员也应该知悉,说明书中所描述的实施例均属于优选实施例,所涉及的动作和部件并不一定是本发明所必须的。For the method embodiments, for the sake of simple description, they are all expressed as a series of action combinations. However, those skilled in the art should know that the present invention is not limited by the described action sequence, because according to the present invention, some steps Other orders or simultaneous steps are possible. Secondly, those skilled in the art should also know that the embodiments described in the specification are all preferred embodiments, and the actions and components involved are not necessarily necessary for the present invention.

以上对本发明所提供的保持弃渣土体原状结构的取样及抗剪强度测试方法进行了详细介绍,本文中应用了具体个例对本发明的原理及实施方式进行了阐述,以上实施例的说明只是用于帮助理解本发明的方法及其核心思想;同时,对于本领域的一般技术人员,依据本发明的思想,在具体实施方式及应用范围上均会有改变之处,综上所述,本说明书内容不应理解为对本发明的限制。The above is a detailed introduction to the sampling and shear strength testing methods for maintaining the original structure of the waste soil body provided by the present invention. Specific examples are used in this article to illustrate the principles and implementation methods of the present invention. The description of the above embodiments is only It is used to help understand the method and its core idea of the present invention; at the same time, for those of ordinary skill in the field, there will be changes in the specific implementation and application scope according to the idea of the present invention. In summary, this The content of the description should not be construed as limiting the invention.

Claims (9)

1.一种保持弃渣土体原状结构的取样方法,其特征在于,所述方法包括:1. A sampling method that maintains the original structure of spoil soil, characterized in that the method includes: 将质量比为1:2:4-8:2-4的纯水、丙三醇、丙烯酰胺以及丙烯酸组成的混合物在水浴加热条件下制备成丙烯酰胺-丙烯酸共聚物;Preparing a mixture of pure water, glycerin, acrylamide and acrylic acid with a mass ratio of 1:2:4-8:2-4 under water bath heating conditions to prepare an acrylamide-acrylic acid copolymer; 在弃渣土斜坡坡面平缓部位,选择预设尺寸形状的弃渣土平面进行平整,以方便采样;其中,所述预设尺寸形状根据对弃渣土试样的测试需求确定;In the gentle part of the spoil slope, select a spoil plane with a preset size and shape for smoothing to facilitate sampling; wherein the preset size and shape are determined based on the testing requirements for the spoil sample; 在平整后的所述弃渣土平面上划定注胶带,并向所述注胶带内均匀注入由所述丙烯酰胺-丙烯酸共聚物组成的共聚材料,直至达到预设深度;An injection tape is defined on the leveled spoil soil plane, and a copolymer material composed of the acrylamide-acrylic acid copolymer is evenly injected into the injection tape until a preset depth is reached; 待所述共聚材料凝固后,将所述注胶带外围的弃渣土挖去,得到封固的弃渣土试样;其中,所述向所述注胶带内均匀注入由所述丙烯酰胺-丙烯酸共聚物组成的共聚材料,直至达到预设深度,包括:After the copolymer material solidifies, dig out the spoil soil around the injection tape to obtain a sealed spoil soil sample; wherein, the acrylamide-acrylic acid is uniformly injected into the injection tape. Copolymer materials composed of copolymers up to a preset depth including: 采用带有孔隙压力探头的注胶设备,向所述注胶带内均匀注入所述共聚材料,所述共聚材料的注入量和注入深度通过所述孔隙压力探头控制;在注胶过程中,所述注胶设备为加热状态,以保持所述共聚材料的流动性。Glue injection equipment with a pore pressure probe is used to evenly inject the copolymer material into the injection tape. The injection amount and depth of the copolymer material are controlled by the pore pressure probe; during the glue injection process, the The glue injection equipment is heated to maintain the fluidity of the copolymer material. 2.根据权利要求1所述的保持弃渣土体原状结构的取样方法,其特征在于,所述预设深度为所述弃渣土试样高度的1.1-1.2倍;所述注胶带的宽度为所述弃渣土试样宽度的1/10-1/6。2. The sampling method for maintaining the original structure of the spoil soil according to claim 1, characterized in that the preset depth is 1.1-1.2 times the height of the spoil soil sample; the width of the injection tape is It is 1/10-1/6 of the width of the spoil soil sample. 3.根据权利要求1所述的保持弃渣土体原状结构的取样方法,其特征在于,所述将质量比为1:2:4-8:2-4的纯水、丙三醇、丙烯酰胺以及丙烯酸组成的混合物在水浴加热条件下制备成丙烯酰胺-丙烯酸共聚物,包括:3. The sampling method for maintaining the original structure of the waste soil body according to claim 1, characterized in that the mass ratio of pure water, glycerol, and propylene is 1:2:4-8:2-4. A mixture of amide and acrylic acid is prepared into an acrylamide-acrylic acid copolymer under water bath heating conditions, including: 向所述纯水中依次加入所述丙三醇、所述丙烯酸以及所述丙烯酰胺,搅拌混合得到混合液;其中,所述纯水、所述丙三醇、所述丙烯酰胺以及所述丙烯酸的质量比为1:2:4-8:2-4;Add the glycerol, the acrylic acid and the acrylamide to the pure water in sequence, stir and mix to obtain a mixed liquid; wherein the pure water, the glycerol, the acrylamide and the acrylic acid The mass ratio is 1:2:4-8:2-4; 向所述混合液中加入引发剂,搅拌后保持50~70℃的温度水浴加热10 ~20分钟,得到所述丙烯酰胺-丙烯酸共聚物;其中,所述引发剂包括过硫酸盐和偶氮化合物中的一种。An initiator is added to the mixed liquid, and after stirring, the water bath is heated at a temperature of 50 to 70°C for 10 to 20 minutes to obtain the acrylamide-acrylic acid copolymer; wherein the initiator includes persulfate and azo compounds. one of them. 4.根据权利要求1或3所述的保持弃渣土体原状结构的取样方法,其特征在于,所述纯水、所述丙三醇、所述丙烯酰胺以及所述丙烯酸的质量比为1:2:6:3。4. The sampling method for maintaining the original structure of spoil soil according to claim 1 or 3, characterized in that the mass ratio of the pure water, the glycerol, the acrylamide and the acrylic acid is 1 :2:6:3. 5.根据权利要求3所述的保持弃渣土体原状结构的取样方法,其特征在于,所述引发剂与所述丙烯酰胺的质量比为1:5-10。5. The sampling method for maintaining the original structure of spoil soil according to claim 3, characterized in that the mass ratio of the initiator to the acrylamide is 1:5-10. 6.根据权利要求3所述的保持弃渣土体原状结构的取样方法,其特征在于,所述向所述纯水中依次加入所述丙三醇、所述丙烯酸以及所述丙烯酰胺,搅拌混合得到混合液,包括:6. The sampling method for maintaining the original structure of the spoil soil according to claim 3, characterized in that the glycerin, the acrylic acid and the acrylamide are sequentially added to the pure water and stirred. Mix to obtain a mixture including: 在向所述纯水中加入所述丙三醇以及所述丙烯酸后,对所述纯水进行搅拌;After adding the glycerol and the acrylic acid to the pure water, stir the pure water; 在搅拌的同时,加入所述丙烯酰胺,得到所述混合液。While stirring, add the acrylamide to obtain the mixed liquid. 7.根据权利要求3所述的保持弃渣土体原状结构的取样方法,其特征在于,所述丙烯酰胺的纯度在99%以上,所述丙烯酸的纯度为99%以上,所述丙三醇的纯度在95%以上。7. The sampling method for maintaining the original structure of the spoil soil according to claim 3, characterized in that the purity of the acrylamide is above 99%, the purity of the acrylic acid is above 99%, and the purity of the glycerol is above 99%. The purity is above 95%. 8.一种抗剪强度测试方法,其特征在于,所述方法包括:8. A shear strength testing method, characterized in that the method includes: 对上述权利要求1-7任一所述的取样方法取得的封固的弃渣土试样,采用热风干燥器进行解胶;The sealed spoil soil sample obtained by the sampling method described in any one of claims 1 to 7 is degummed using a hot air dryer; 将解胶后的所述弃渣土试样中包含共聚材料的部分削去后,置于直剪仪中进行直剪试验,以测试所述弃渣土试样的抗剪强度。After the degummed spoil soil sample contains the part containing the copolymer material, it is placed in a direct shear instrument to perform a direct shear test to test the shear strength of the spoil soil sample. 9.根据权利要求8所述的抗剪强度测试方法,其特征在于,所述采用热风干燥器进行解胶,包括:9. The shear strength testing method according to claim 8, characterized in that the use of a hot air dryer for degumming includes: 围绕所述封固的弃渣土试样顺时针运行所述热风干燥器,以对所述共聚材料的各部分进行加热烘干,以使所述共聚材料失去强度。Run the hot air dryer clockwise around the sealed spoil soil sample to heat and dry each part of the copolymer material so that the copolymer material loses strength.
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