CN114806699A - Method for improving hardness of beef tallow based on strengthening internal structure of fat crystal - Google Patents
Method for improving hardness of beef tallow based on strengthening internal structure of fat crystal Download PDFInfo
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- CN114806699A CN114806699A CN202210459202.7A CN202210459202A CN114806699A CN 114806699 A CN114806699 A CN 114806699A CN 202210459202 A CN202210459202 A CN 202210459202A CN 114806699 A CN114806699 A CN 114806699A
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- Prior art keywords
- fat
- tallow
- oil
- beef tallow
- cooling
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/02—Refining fats or fatty oils by chemical reaction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/10—Refining fats or fatty oils by adsorption
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Edible Oils And Fats (AREA)
- Fats And Perfumes (AREA)
Abstract
本发明公开了基于强化脂肪晶体内部结构的牛油硬度改良方法,包括以下步骤:S1,预处理;S2,熔炼过滤;S3,精炼;S4,均质:将精制牛油与脂肪结晶改良剂混合引入至反应釜中,在80℃‑90℃的条件下,控制搅拌速度在45‑55r/min下搅拌35min‑50min,得到均匀的精制牛油‑脂肪结晶改良剂混合物,将混合物引至暂存罐,在65℃条件下进行暂存;S5,冷却结晶:将暂存后的精制牛油‑脂肪结晶改良剂混合物导入冷却装置中,通过程序降温后灌装得到固体成品牛油,形成更加紧密有序、空间填充度大的结晶网络,并在相应的剪切力的作用下,与牛油中的脂肪晶体进行充分交联混合,使脂肪晶体相互聚集,并形成具有特定方式排列的三维网络晶体结构,以增加其晶体结构的尺寸,使结晶网络进一步密集化,从而增加牛油的硬度。
The invention discloses a method for improving the hardness of tallow based on strengthening the internal structure of fat crystals, comprising the following steps: S1, pretreatment; S2, smelting and filtering; S3, refining; Introduce into the reaction kettle, under the condition of 80 ℃-90 ℃, control the stirring speed to stir at 45-55r/min for 35min-50min, obtain a uniform refined tallow-fat crystallization modifier mixture, and lead the mixture to temporary storage Tank, temporarily stored at 65°C; S5, cooling crystallization: the temporarily stored refined tallow-fat crystallization modifier mixture is introduced into the cooling device, and the solid finished tallow is obtained by filling after cooling through the program, forming a more compact Ordered and space-filled crystalline network, and under the action of the corresponding shear force, fully cross-linking and mixing with the fat crystals in the tallow, so that the fat crystals aggregate each other and form a three-dimensional network arranged in a specific way crystal structure to increase the size of its crystal structure, further densifying the crystalline network, thereby increasing the hardness of the tallow.
Description
| Temperature gradient/. degree.C | Example 1 | Example 2 | Commercial beef tallow |
| 10 | 66.81±0.63 | 70.82±1.1 | 62.69±0.86 |
| 20 | 48.69±0.82 | 53.56±0.91 | 43.54±0.17 |
| 30 | 29.42±0.45 | 34.68±0.7 | 24.07±0.55 |
| 40 | 12.93±0.97 | 17.70±0.56 | 9.06±0.17 |
| 50 | 4.68±0.09 | 10.54±0.24 | 0 |
| Categories | Example 1 | Example 2 | Commercial beef tallow |
| Melting Point (. degree.C.) | 45.8±0.54 | 48.6±0.91 | 41.5±0.83 |
| Form of beta' (%) | 97.88±0.08 | 98.58±0.12 | 92.88±0.06 |
| Hardness (g) | 147.47±4.75 | 153.47±5.25 | 110.56±3.50 |
Claims (5)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210459202.7A CN114806699B (en) | 2022-04-27 | 2022-04-27 | Butter hardness improvement method based on strengthening fat crystal internal structure |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210459202.7A CN114806699B (en) | 2022-04-27 | 2022-04-27 | Butter hardness improvement method based on strengthening fat crystal internal structure |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN114806699A true CN114806699A (en) | 2022-07-29 |
| CN114806699B CN114806699B (en) | 2023-09-08 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210459202.7A Active CN114806699B (en) | 2022-04-27 | 2022-04-27 | Butter hardness improvement method based on strengthening fat crystal internal structure |
Country Status (1)
| Country | Link |
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| CN (1) | CN114806699B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114874856A (en) * | 2022-04-29 | 2022-08-09 | 广汉市迈德乐食品有限公司 | Transesterification method for improving hardness of beef tallow |
| CN114933930A (en) * | 2022-05-16 | 2022-08-23 | 广汉市迈德乐食品有限公司 | Beef tallow hardness improving method based on compound gel factor |
Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4127597A (en) * | 1977-04-14 | 1978-11-28 | The United States Of America As Represented By The Secretary Of Agriculture | Continuous fractionation of tallow and production of a cocoa butter-like plastic fat |
| CN104302749A (en) * | 2012-05-18 | 2015-01-21 | J-制油株式会社 | Crystallization accelerator |
| JP2016077175A (en) * | 2014-10-10 | 2016-05-16 | 株式会社Adeka | Manufacturing method of hard butter |
| CN105638932A (en) * | 2016-01-08 | 2016-06-08 | 广州南侨食品有限公司 | Butter character like low-trans-fatty acid base material oil and preparation method thereof |
| CN105794997A (en) * | 2014-12-29 | 2016-07-27 | 丰益(上海)生物技术研发中心有限公司 | Oil composition replacing beef tallow and preparation method thereof |
| CN106497674A (en) * | 2016-11-08 | 2017-03-15 | 江南大学 | A kind of high strength supersonic is coupled the method that emulsifying agent promotes fat crystals |
| CN106857882A (en) * | 2017-02-28 | 2017-06-20 | 江南大学 | A kind of preparation and application of trans-fatty acid-free crisp skin oil |
| CN112694943A (en) * | 2020-08-21 | 2021-04-23 | 重庆市帅克食品有限公司 | Low-cholesterol low-saturated-fat hotpot beef tallow and preparation method thereof |
| CN112868820A (en) * | 2021-02-21 | 2021-06-01 | 中粮东海粮油工业(张家港)有限公司 | Butter-like oil base and butter, and preparation method and application thereof |
| CN112931636A (en) * | 2021-03-10 | 2021-06-11 | 江南大学 | Beef fat substitute, preparation method thereof and application thereof in hotpot condiment |
| CN114190538A (en) * | 2021-12-21 | 2022-03-18 | 郑州轻工业大学 | A kind of grease crystallizer for promoting the formation of β' crystal form and its application |
-
2022
- 2022-04-27 CN CN202210459202.7A patent/CN114806699B/en active Active
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4127597A (en) * | 1977-04-14 | 1978-11-28 | The United States Of America As Represented By The Secretary Of Agriculture | Continuous fractionation of tallow and production of a cocoa butter-like plastic fat |
| CN104302749A (en) * | 2012-05-18 | 2015-01-21 | J-制油株式会社 | Crystallization accelerator |
| JP2016077175A (en) * | 2014-10-10 | 2016-05-16 | 株式会社Adeka | Manufacturing method of hard butter |
| CN105794997A (en) * | 2014-12-29 | 2016-07-27 | 丰益(上海)生物技术研发中心有限公司 | Oil composition replacing beef tallow and preparation method thereof |
| CN105638932A (en) * | 2016-01-08 | 2016-06-08 | 广州南侨食品有限公司 | Butter character like low-trans-fatty acid base material oil and preparation method thereof |
| CN106497674A (en) * | 2016-11-08 | 2017-03-15 | 江南大学 | A kind of high strength supersonic is coupled the method that emulsifying agent promotes fat crystals |
| CN106857882A (en) * | 2017-02-28 | 2017-06-20 | 江南大学 | A kind of preparation and application of trans-fatty acid-free crisp skin oil |
| CN112694943A (en) * | 2020-08-21 | 2021-04-23 | 重庆市帅克食品有限公司 | Low-cholesterol low-saturated-fat hotpot beef tallow and preparation method thereof |
| CN112868820A (en) * | 2021-02-21 | 2021-06-01 | 中粮东海粮油工业(张家港)有限公司 | Butter-like oil base and butter, and preparation method and application thereof |
| CN112931636A (en) * | 2021-03-10 | 2021-06-11 | 江南大学 | Beef fat substitute, preparation method thereof and application thereof in hotpot condiment |
| CN114190538A (en) * | 2021-12-21 | 2022-03-18 | 郑州轻工业大学 | A kind of grease crystallizer for promoting the formation of β' crystal form and its application |
Non-Patent Citations (2)
| Title |
|---|
| 孟宗;刘元法;胡鹏;徐振波;王兴国;: "牛油基起酥油起砂原因分析(Ⅱ)――结晶动力学、晶体形态", 中国粮油学报, no. 03, pages 62 - 65 * |
| 池娟娟;孟宗;李进伟;王兴国;金青哲;刘元法;: "棕榈油基基料油相容性及结晶形态的研究", 中国油脂, no. 05, pages 16 - 21 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114874856A (en) * | 2022-04-29 | 2022-08-09 | 广汉市迈德乐食品有限公司 | Transesterification method for improving hardness of beef tallow |
| CN114874856B (en) * | 2022-04-29 | 2024-04-02 | 广汉市迈德乐食品有限公司 | Transesterification method for improving hardness of beef tallow |
| CN114933930A (en) * | 2022-05-16 | 2022-08-23 | 广汉市迈德乐食品有限公司 | Beef tallow hardness improving method based on compound gel factor |
| CN114933930B (en) * | 2022-05-16 | 2024-03-15 | 广汉市迈德乐食品有限公司 | Butter hardness improving method based on compound gel factor |
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| Publication number | Publication date |
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| CN114806699B (en) | 2023-09-08 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A method for improving the hardness of butter based on strengthening the internal structure of fat crystals Granted publication date: 20230908 Pledgee: Industrial Bank Co.,Ltd. Deyang Branch Pledgor: GUANGHAN MAIDELE FOOD Co.,Ltd. Registration number: Y2024980011490 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20230908 Pledgee: Industrial Bank Co.,Ltd. Deyang Branch Pledgor: GUANGHAN MAIDELE FOOD Co.,Ltd. Registration number: Y2024980011490 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A method for improving the hardness of butter based on strengthening the internal structure of fat crystals Granted publication date: 20230908 Pledgee: Industrial Bank Co.,Ltd. Deyang Branch Pledgor: GUANGHAN MAIDELE FOOD Co.,Ltd. Registration number: Y2025510000179 |