CN1028604C - Prepn. of Chinese herb-fresh bamboo-juice - Google Patents
Prepn. of Chinese herb-fresh bamboo-juice Download PDFInfo
- Publication number
- CN1028604C CN1028604C CN 90105836 CN90105836A CN1028604C CN 1028604 C CN1028604 C CN 1028604C CN 90105836 CN90105836 CN 90105836 CN 90105836 A CN90105836 A CN 90105836A CN 1028604 C CN1028604 C CN 1028604C
- Authority
- CN
- China
- Prior art keywords
- alcohol
- water
- bamboo stem
- bright bamboo
- fresh bamboo
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 55
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 55
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 55
- 241001330002 Bambuseae Species 0.000 claims abstract description 53
- 239000011425 bamboo Substances 0.000 claims abstract description 53
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 27
- 238000000034 method Methods 0.000 claims abstract description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 15
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 239000003814 drug Substances 0.000 claims abstract description 11
- 238000002360 preparation method Methods 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000007788 liquid Substances 0.000 claims description 13
- 239000000243 solution Substances 0.000 claims description 8
- 244000025254 Cannabis sativa Species 0.000 claims description 4
- 241000543826 Sinobambusa Species 0.000 claims description 4
- 241000745988 Phyllostachys Species 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 3
- 230000001476 alcoholic effect Effects 0.000 claims description 3
- 238000009835 boiling Methods 0.000 claims description 3
- 238000010790 dilution Methods 0.000 claims description 3
- 239000012895 dilution Substances 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 10
- 235000011389 fruit/vegetable juice Nutrition 0.000 abstract description 4
- 239000000835 fiber Substances 0.000 abstract description 3
- 238000003908 quality control method Methods 0.000 abstract description 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 abstract 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 4
- 238000010923 batch production Methods 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 238000005325 percolation Methods 0.000 description 4
- 208000026435 phlegm Diseases 0.000 description 4
- 241000209128 Bambusa Species 0.000 description 3
- 206010011224 Cough Diseases 0.000 description 3
- 150000001413 amino acids Chemical class 0.000 description 3
- 229940079593 drug Drugs 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 2
- 206010036790 Productive cough Diseases 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 239000003125 aqueous solvent Substances 0.000 description 2
- LHGVFZTZFXWLCP-UHFFFAOYSA-N guaiacol Chemical compound COC1=CC=CC=C1O LHGVFZTZFXWLCP-UHFFFAOYSA-N 0.000 description 2
- 240000003323 Centaurea nigra Species 0.000 description 1
- 235000002505 Centaurea nigra Nutrition 0.000 description 1
- 206010008190 Cerebrovascular accident Diseases 0.000 description 1
- 206010010904 Convulsion Diseases 0.000 description 1
- RGHNJXZEOKUKBD-UHFFFAOYSA-N D-gluconic acid Natural products OCC(O)C(O)C(O)C(O)C(O)=O RGHNJXZEOKUKBD-UHFFFAOYSA-N 0.000 description 1
- 241000202807 Glycyrrhiza Species 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 240000005827 Phyllostachys nigra Species 0.000 description 1
- 235000010717 Phyllostachys nigra Nutrition 0.000 description 1
- 229920001131 Pulp (paper) Polymers 0.000 description 1
- 208000006011 Stroke Diseases 0.000 description 1
- 244000273928 Zingiber officinale Species 0.000 description 1
- 235000006886 Zingiber officinale Nutrition 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000036461 convulsion Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003172 expectorant agent Substances 0.000 description 1
- 230000003419 expectorant effect Effects 0.000 description 1
- 239000011094 fiberboard Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 235000008397 ginger Nutrition 0.000 description 1
- 235000012208 gluconic acid Nutrition 0.000 description 1
- 239000000174 gluconic acid Substances 0.000 description 1
- 229960001867 guaiacol Drugs 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 239000011021 lapis lazuli Substances 0.000 description 1
- 239000006187 pill Substances 0.000 description 1
- UAJTZZNRJCKXJN-UHFFFAOYSA-M sodium;2-dodecoxy-2-oxoethanesulfonate Chemical compound [Na+].CCCCCCCCCCCCOC(=O)CS([O-])(=O)=O UAJTZZNRJCKXJN-UHFFFAOYSA-M 0.000 description 1
- 208000024794 sputum Diseases 0.000 description 1
- 210000003802 sputum Anatomy 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to a preparation method of fresh bamboo juice as a traditional Chinese medicine, which takes fresh bamboo stalks as a raw material. The fresh bamboo stalks are cut into pieces at normal temperature and are soaked in water or the water containing 10 to 50% of alcohol (any one in methanol, etanol, propanol and normal butyl alcohol); next, after the fresh bamboo stalks are extracted in a heating mode and filtered at 50 to 120 DEG C, the fresh bamboo juice which is light yellow to a light red umber is obtained (for alcohol-containing extract, alcohol can be recovered in a heating mode). The method has the characteristics of high yield, good quality, low production cost, little device investment, simple method, convenient factory production, convenient quality control, etc. Bamboo fibers obtained by extracting the fresh bamboo juice can also be comprehensively used and has good economical and social benefits.
Description
The present invention is a kind of preparation method of Chinese medicine fresh Succus Bambusae.
Fresh Succus Bambusae is a Chinese medicine, has the effect of removing heat-phlegm.Be used for the treatment of illness such as cough due to lung-heat's abundant expectoration, uncomfortable in chest, the apoplexy stiff tongue of asthma, accumulation and obstruction of sputum, the hot infantile convulsion of children's's expectorant clinically.Commercially available fresh Succus Bambusae is to be that raw material adopts traditional method that scorches [being Pharmacopoeia of People's Republic of China (an one) version regulation in 1977] to produce with the Phyllostachys bamboo.The method method that bamboo in addition alive is got Succus Bambusae except that scorching method for preparing fresh Succus Bambusae (is seen " Zhejiang Chinese medicine " the 1st phase in 1976, " production process of phyllostachys nigra (lodd.ex lindl.) munro var.henonis (miff.) spapf et rendle liquid and process introduction " one literary composition and see " Chinese Hospitals pharmaceutical journal " 2 phases in 1987 " Sucus bambusae is followed the example of " literary composition) and the report of percolation (seeing " Shandong medical industry " 2 phases in 1987, " discussion of fresh Succus Bambusae extraction process " literary composition) extraction Succus Bambusae.The method of scorching is that bright bamboo stem is cut into 30～50cm length, and joint is removed at two ends, rives, and erects, and the middle part scorches with fire, and the faint yellow extremely light red brown liquid that the two ends drop goes out promptly is a fresh Succus Bambusae.This legal system is got Succus Bambusae yield low (be about former bamboo weight 3%), and the production cost height is not easy to quality control and batch production production, needs to cut down a large amount of bamboos aborning, and the waste bamboo resource has destroyed bamboo fibre, is not easy to bamboo resource is fully utilized.It is in boring on the bamboo that lives or after removing a joint bamboo tail bamboo to be stooped the method for getting fresh Succus Bambusae that the bamboo that lives is got the Succus Bambusae method.This genealogy of law dispersibility manual operations, get Succus Bambusae be subjected to multiple condition restriction (as rain, the Heavenly Stems, hot summer and severe winter all can not get Succus Bambusae), its gained fresh Succus Bambusae yield is low, be not easy to batch production production and control of product quality and management.Percolation is to be contained in the percolation pipe after bright bamboo stem is cut into slices, and with cold water soak and percolation, collects a certain amount of percolate and is fresh Succus Bambusae.It is to carry out at normal temperatures that this legal system is got fresh Succus Bambusae, and preparation time is long, and product is easily corrupt rotten, and uncontrollable quality, so this method only is in the laboratory test stage can not drop into batch production and produce and implement.
The objective of the invention is the shortcoming that exists at existing fresh Succus Bambusae preparation method, propose a kind of yield height, quality is good, method for making is easy, cost the is low method for preparing fresh Succus Bambusae.
The present invention realizes by following approach, with the bright bamboo stem of grass is raw material, after chopping, be soaked in water or contain 10～50% alcohol (methanol, ethanol, propanol, in the n-butyl alcohol any) in the water, bright bamboo stem raw material and water or the solid-liquid weight ratio that contains the water of above-mentioned alcohol are 1: 1.5～8, after it is soaked 0.5～2 hour at normal temperatures, heat again to 50～120 ℃ of following heat and carry 2～8 hours, thereafter filter bright bamboo stem extracting solution (should reclaim alcohol with heating means according to the boiling point of alcohol) to the extracting solution that contains above-mentioned alcohol, again through adding cold clear water dilution or heating concentrated extracting solution, the weight that makes this solution is 1～3 times of bright bamboo stem raw material weight, obtains having faint yellow to light red brown fresh Succus Bambusae at last.
This method is raw materials used to be the bright bamboo stem of the various Sinobambusas of grass, and wherein the raw material that more preferably adopts is the bright bamboo stem of Sinocalamus, bitter bamboo genus, Phyllostachys, Thorny Sinobambusa.The bright bamboo stem of above-mentioned four kinds of Sinobambusas has rich in natural resources in China, the fresh Succus Bambusae quality height that price is low, produce.This method prepares its bright bamboo stem raw material of fresh Succus Bambusae and water or contains in the water of 10-50% alcohol (in methanol, ethanol, propanol, the n-butyl alcohol any), and bright bamboo stem raw material and above-mentioned water or the preferred solid-liquid weight ratio of aqueous solvent that contains above-mentioned alcohol are 1: 2～3.To more help the amino acid whose extraction of fresh Succus Bambusae active ingredient through the bright bamboo stem soak at room temperature after the chopping in water or contain in the alcoholic acid water of 10-50% 1～2 hour and carry out heat again and carry.
Adopt this method to prepare fresh Succus Bambusae, the yield of its fresh Succus Bambusae is 100～300% of a bright bamboo weight, be to scorch 30～90 times of method yield, the active ingredient amino acids content of eliminating phlegm and stopping cough is to scorch more than the octuple of method, and other useful component guaiacol, gluconic acid etc. are also than scorching method content height.Adopt this method to prepare fresh Succus Bambusae and do not need to cut down a large amount of bamboos, production cost is low, equipment investment is few, constant product quality, impurity are few, be easy to batch production production and control of product quality and management, bamboo fibre behind the extracted from bamboo juice also can be used for making paper pulp and bamboo fiberboard etc., has improved the comprehensive utilization value and the economic benefit of bamboo resource.As add an amount of antiseptic with after the fresh Succus Bambusae dilution, boiling, checking, bottling to make fresh bamboo trickle liquid; Fresh Succus Bambusae is added adjuvant also can be made into Chinese medicine single preparation bamboo trickle paste, bamboo drop plate; Can be made into Chinese patent medicine compound recipe fresh Succus Bambusae with drug matchings such as Herba Houttuyniae, Rhizoma Pinelliae, fresh ginger, Folium Eriobotryae, Radix Platycodonis, peppermints; Can be made into Chinese patent medicine Succus Bambusae phlegm-resolving pill with drug matchings such as Radix Scutellariae, Pericarpium Citri Reticulatae, Rhizoma Pinelliae Preparatum, Lapis Micae Aureus (forging), Lignum Aquilariae Resinatum, Radix Et Rhizoma Rhei, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizaes.Fresh Succus Bambusae also can be used with other drug matching in prescription.
Through adopting the inventive method trial production fresh bamboo trickle liquid to prove that the production cost of producing fresh bamboo trickle liquid than the method that scorches hangs down 40 times, the efficacy component amino acids content ratio of eliminating phlegm and stopping cough scorches high ten times of methods.
Embodiment
Example 1: with the bright bar 0.5kg chopping of cizu or bitter bamboo, be 1: 2～3 by the solid-liquid weight ratio, it was soaked 1～2 hour at normal temperatures that heat and carry 2～8 hours to 50～120 ℃ of heat, filtration can get light red brown fresh Succus Bambusae 1～1.5kg with cold water.
Example 2: the bright bamboo stem 0.5kg chopping that will press from both sides bamboo or hardhead bambusa textilt in vain, is 1: 4～6 with containing 50% alcoholic acid aqueous solvent by the solid-liquid weight ratio, it was soaked 1～2 hour at normal temperatures, heat again to 50～80 ℃ of heat and carry 2～4 hours, filter, get bright bamboo stem extracting solution, heating extraction liquid can get flaxen fresh Succus Bambusae 1～1.5kg after reclaiming ethanol.
Claims (4)
1, a kind of preparation method of Chinese medicine fresh Succus Bambusae, it is characterized in that this method is a raw material with the bright bamboo stem of grass, after chopping, be soaked in water or contain 10-50% alcohol (methanol, ethanol, propanol, any in the n-butyl alcohol) in the water, bright bamboo stem raw material and water or the solid-liquid weight ratio that contains the water of above-mentioned alcohol are 1: 1.5～8, after it is soaked 0.5～2 hour at normal temperatures, heat again to 50～120 ℃ of heat and carry 2～8 hours, thereafter filter bright bamboo stem extracting solution (should reclaim alcohol with heating means according to the boiling point of alcohol) to the extracting solution that contains above-mentioned alcohol, again through adding cold clear water dilution or heating concentrated extracting solution, the weight that makes this liquid is 1～3 times of bright bamboo stem raw material weight, can have faint yellow to light red brown fresh Succus Bambusae subsequently.
2, preparation method according to claim 1 is characterized in that the bright bamboo stem of grass is the bright bamboo stem of Sinocalamus, Phyllostachys, bitter bamboo genus, Thorny Sinobambusa.
3, preparation method according to claim 1, the solid-liquid weight ratio that it is characterized in that bright bamboo stem raw material and water or contain the water of 10-50% alcohol (in methanol, ethanol, propanol, the n-butyl alcohol any) is 1: 2～3.
4,, it is characterized in that the bright bamboo stem after chopping is soak at room temperature in water or contains in the alcoholic acid water of 10-50% 1～2 hour and carry out heat again and carry according to claim 1 or 2 or 3 described preparation methoies.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90105836 CN1028604C (en) | 1990-06-13 | 1990-06-13 | Prepn. of Chinese herb-fresh bamboo-juice |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90105836 CN1028604C (en) | 1990-06-13 | 1990-06-13 | Prepn. of Chinese herb-fresh bamboo-juice |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1057196A CN1057196A (en) | 1991-12-25 |
| CN1028604C true CN1028604C (en) | 1995-05-31 |
Family
ID=4879637
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 90105836 Expired - Fee Related CN1028604C (en) | 1990-06-13 | 1990-06-13 | Prepn. of Chinese herb-fresh bamboo-juice |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1028604C (en) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1042093C (en) * | 1993-06-09 | 1999-02-17 | 罗正都 | Bamboo juice and series nutrition health care food |
| CN1053357C (en) * | 1994-11-04 | 2000-06-14 | 张仲安 | Method for preparing bamboo juice |
| CN1052649C (en) * | 1996-07-17 | 2000-05-24 | 蒋道友 | Bamboo juice extraction method |
| CN1082374C (en) * | 1997-06-04 | 2002-04-10 | 中国医学科学院药物研究所 | Traditional Chinese medicinal composition with reducing-blood-sugar activity |
| US20040185124A1 (en) * | 2002-10-24 | 2004-09-23 | Hiromichi Hayashi | Health food and antitumor agent |
| US7972632B2 (en) | 2003-02-28 | 2011-07-05 | Unigen Pharmaceuticals, Inc. | Identification of Free-B-Ring flavonoids as potent COX-2 inhibitors |
| US7108868B2 (en) | 2002-03-22 | 2006-09-19 | Unigen Pharmaceuticals, Inc. | Isolation of a dual cox-2 and 5-lipoxygenase inhibitor from acacia |
| US8034387B2 (en) | 2002-04-30 | 2011-10-11 | Unigen, Inc. | Formulation of a mixture of free-B-ring flavonoids and flavans for use in the prevention and treatment of cognitive decline and age-related memory impairments |
| BRPI0309689B1 (en) | 2002-04-30 | 2021-06-29 | Unigen, Inc | COMPOSITIONS COMPRISING A MIXTURE OF B-RING-FREE FLAVONOIDS AND FLAVANES AND USES THEREOF |
| CN1798568B (en) | 2003-04-04 | 2011-05-11 | 尤尼根制药公司 | Formulation of dual cycloxygenase (cox) and lipoxygenase (lox) inhibitors for mammal skin care |
| CN1304041C (en) * | 2004-05-13 | 2007-03-14 | 湖南正清制药集团股份有限公司 | Method of PH gradient extracting bamboo juice |
| CN100473408C (en) * | 2005-01-21 | 2009-04-01 | 四川奥邦药业有限公司 | Heat-clearing and phlegm-resolving medicine composition, preparation and use thereof |
| KR100761248B1 (en) | 2006-10-12 | 2007-10-04 | 주식회사 유니젠 | Composition for the treatment of atopic dermatitis containing bamboo and golden extract as active ingredients |
| CN104749282A (en) * | 2015-04-07 | 2015-07-01 | 湖北端正药业股份有限公司 | Method for determining content of guaiacol in fresh bamboo juice |
| CN112316068A (en) * | 2020-11-04 | 2021-02-05 | 江西中竹生物质科技有限公司 | Method for extracting fresh bamboo juice by using ultrasonic waves |
| CN114982950A (en) * | 2022-06-10 | 2022-09-02 | 重庆升升药业有限公司 | Preparation method of fresh bamboo juice red yeast rice oral liquid |
-
1990
- 1990-06-13 CN CN 90105836 patent/CN1028604C/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1057196A (en) | 1991-12-25 |
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