CN101536636B - Method for reducing nicotine content from mixture - Google Patents
Method for reducing nicotine content from mixture Download PDFInfo
- Publication number
- CN101536636B CN101536636B CN2008100470815A CN200810047081A CN101536636B CN 101536636 B CN101536636 B CN 101536636B CN 2008100470815 A CN2008100470815 A CN 2008100470815A CN 200810047081 A CN200810047081 A CN 200810047081A CN 101536636 B CN101536636 B CN 101536636B
- Authority
- CN
- China
- Prior art keywords
- mixture
- malonic acid
- spray
- heteroauxin
- grams
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 29
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 title claims abstract description 22
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 title claims abstract description 22
- 229960002715 nicotine Drugs 0.000 title claims abstract description 22
- 238000000034 method Methods 0.000 title claims abstract description 18
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims abstract description 38
- SEOVTRFCIGRIMH-UHFFFAOYSA-N indole-3-acetic acid Chemical compound C1=CC=C2C(CC(=O)O)=CNC2=C1 SEOVTRFCIGRIMH-UHFFFAOYSA-N 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000007921 spray Substances 0.000 claims abstract description 14
- 238000005507 spraying Methods 0.000 claims abstract description 8
- 238000002360 preparation method Methods 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims abstract description 6
- 238000004140 cleaning Methods 0.000 claims abstract description 4
- 235000014347 soups Nutrition 0.000 claims description 5
- 235000019504 cigarettes Nutrition 0.000 claims description 3
- 238000011017 operating method Methods 0.000 claims description 3
- 239000003643 water by type Substances 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 22
- 241000208125 Nicotiana Species 0.000 abstract description 21
- 239000003617 indole-3-acetic acid Substances 0.000 abstract 4
- SIKJAQJRHWYJAI-UHFFFAOYSA-N Indole Chemical compound C1=CC=C2NC=CC2=C1 SIKJAQJRHWYJAI-UHFFFAOYSA-N 0.000 abstract 2
- 241000196324 Embryophyta Species 0.000 abstract 1
- 244000061176 Nicotiana tabacum Species 0.000 abstract 1
- PZOUSPYUWWUPPK-UHFFFAOYSA-N indole Natural products CC1=CC=CC2=C1C=CN2 PZOUSPYUWWUPPK-UHFFFAOYSA-N 0.000 abstract 1
- RKJUIXBNRJVNHR-UHFFFAOYSA-N indolenine Natural products C1=CC=C2CC=NC2=C1 RKJUIXBNRJVNHR-UHFFFAOYSA-N 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 235000020097 white wine Nutrition 0.000 abstract 1
- 229930013930 alkaloid Natural products 0.000 description 3
- 150000003797 alkaloid derivatives Chemical class 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000779 smoke Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000000618 nitrogen fertilizer Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- VYPKFHFVKFKHMK-UHFFFAOYSA-N 2-(1h-indol-2-yl)butanoic acid Chemical compound C1=CC=C2NC(C(C(O)=O)CC)=CC2=C1 VYPKFHFVKFKHMK-UHFFFAOYSA-N 0.000 description 1
- 239000005982 Indolylbutyric acid Substances 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 231100000989 no adverse effect Toxicity 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
一种用混合物降低烟碱含量的方法，其操作步骤如下：A、混合物的配制：使用10mg/kg至50mg/kg吲哚乙酸+40mg/kg至80mg/kg丙二酸配制混合物，称量吲哚乙酸7.5克和丙二酸60克，按1公顷喷施量配制；用375毫升白酒溶解前述吲哚乙酸，用少许水溶解丙二酸，备用；B、用水定容：按每公顷用水750千克，将水加入上述配制好的吲哚乙酸+丙二酸混合物中定容，备用；C、田间喷施：将上述备制好的混合物药液装入喷雾器内，当天下午4点后赴田间，按每株喷药液0.75千克在烟株叶面喷施一次；若6小时内下雨，再补喷一次；D、清洗：清洗喷雾器，除去残留药液，以备后用。本发明推广前景广阔，为我国烟草行业对烟碱的调控提供了一种新的方法，可广泛应用于生产烟叶的地区和行业。A method for reducing nicotine content with a mixture, the operation steps are as follows: A. Preparation of the mixture: use 10mg/kg to 50mg/kg indole acetic acid + 40mg/kg to 80mg/kg malonic acid to prepare the mixture, weigh the indole 7.5 grams of indoleacetic acid and 60 grams of malonic acid are prepared according to the spraying rate of 1 hectare; dissolve the aforementioned indoleacetic acid with 375 milliliters of white wine, and dissolve malonic acid with a little water for subsequent use; Kg, add water to the above-mentioned prepared indole acetic acid+malonic acid mixture to make a constant volume, and set aside; C, field spraying: put the above-mentioned prepared mixture liquid into the sprayer, and go to the field after 4 o'clock in the afternoon on the same day , Spray once on the leaf surface of the tobacco plant according to 0.75 kg of spray liquid per plant; if it rains within 6 hours, spray again; D, cleaning: clean the sprayer and remove the residual liquid for future use. The present invention has broad promotion prospects, provides a new method for regulating nicotine in my country's tobacco industry, and can be widely used in regions and industries producing tobacco leaves.
Description
Technical field
The present invention relates to a kind of regulate and control method of tobacco smoke alkaloid content, particularly relate to a kind of method that reduces nicotine content with mixture.
Background technology
Nicotine is the important chemical composition in the tobacco, and it is higher commonplace that present China produces tobacco leaf upper leaf nicotine content, has a strong impact on the upper leaf availability, restricted the foundation and the development of national brand.The tobacco planting brainstrust is devoted to carry out the regulation and control of tobacco smoke alkaloid always, and major measure (1) control nitrogenous fertilizer usage amount attempts by reducing tobacco the absorption of nitrogenous fertilizer to be reduced the synthetic of nicotine, is subjected to the influence of soil, DeGrain.With time control nitrogen yield of tobacco is descended, reduced tobacco grower's income, promote very difficult; (2) increase planting density: density increases, and the yield of tobacco quality descends, and the tobacco grower takes in minimizing, promotes difficulty; (3) postponement is pinched, gathered in advance: the tobacco leaf presentation quality descends, and the tobacco grower takes in reduction; Other measure such as drought resisting, balanced nutrients etc. are subjected to the influence of basic condition restriction and the tobacco grower's technical quality difficulty that operates very big.
Summary of the invention
Purpose of the present invention is exactly in order to overcome the deficiencies in the prior art, by inventor's concentrating on studies and repetition test for many years, provide a kind of and can regulate and control tobacco smoke alkaloid content, science practicality, be easy to promote the method with mixture reduction nicotine content of no negative interaction.
To achieve these goals, a kind of method that the present invention relates to mixture reduction nicotine content, its technical method case is such:
The operating procedure of this method is as follows:
The preparation of A, mixture: use 10mg/kg to 50mg/kg heteroauxin+40mg/kg to 80mg/kg malonic acid (promptly 10～50 mg/kg heteroauxins (IAA) add 40～80 mg/kg malonic acid) preparating mixture, with general utility balance difference weighing heteroauxin 7.5 grams and malonic acid 60 grams, by the 1 hectare of amount of spraying preparation; Dissolve aforementioned heteroauxin (heteroauxin is water insoluble) with 375 milliliters of liquor, with little water (to the negligible minor amount of water of 750 kg water described later) dissolving malonic acid, standby;
B, water constant volume: by 750 kilograms of per hectare waters, water is added constant volume in the above-mentioned heteroauxin for preparing+malonic acid mixture, standby;
C, field spray: the above-mentioned mixture soup for preparing is packed in the sprayer, go to the field after 4 of that afternoons, by 0.75 kilogram of every strain spraying liquid at cigarette strain foliage-spray once; If rain in 6 hours, fill spray once again, otherwise soup no longer fill spray.
D, cleaning: clean sprayer, remove residual liquor, for future use.
A kind of method with mixture reduction nicotine content that the present invention is alleged, when using 7.5 gram heteroauxins (IAA) to add 60 gram malonic acid mixtures, its effect that reduces nicotine content is more obvious.
The alleged a kind of mixture of the present invention reduces the method for nicotine content, has easy and simple to handlely, is easy to grasp, cost is lower, the tobacco leaf output value, output are had no adverse effect, environment is not had characteristics such as negative effect, behind use the present invention, it is obvious that nicotine content of tobacco leaves is reduced effect.For example: not using tobacco upper leaf nicotine content of the present invention is 6.87%, use the present invention, after 7.5 gram heteroauxins (IAA) add 60 gram malonic acid mixture process, the upper leaf nicotine content is 3.45%, contrast nicotine content 6.87%, reduce by 3.42 percentage points in nicotine, the range of decrease is 49.78%.Promotion prospect of the present invention is wide, for China's tobacco business provides a kind of new thinking and method to the regulation and control of nicotine; The present invention can be widely used in producing the area and the industry of tobacco leaf.
Embodiment
The present invention is described in detail as follows to its technical scheme in conjunction with specific embodiments: a kind of method with reducing nicotine content from chemical that the present invention is alleged is made of following operating procedure:
The preparation of A, mixture: by the 1 hectare of amount of spraying preparation,, with 375 milliliters of liquor dissolving heteroauxins, dissolve malonic acid again with little water with balance difference weighing indolylbutyric acid 7.5 grams and malonic acid 60 grams, standby;
B, water constant volume: by 750 kilograms of waters of per hectare water, water is added constant volume in the above-mentioned heteroauxin for preparing+malonic acid mixture, standby;
C, field spray: the above-mentioned mixture soup for preparing is packed in the sprayer, go to the field after 4 of that afternoons, by 0.75 kilogram of every strain spraying liquid at cigarette strain foliage-spray once; If rain in 6 hours, fill spray once again, otherwise soup no longer fill spray.
D, cleaning: clean sprayer, remove residual liquor, for future use.
Claims (2)
1. one kind is reduced the method for nicotine content with mixture, it is characterized in that the operating procedure of this method is as follows:
The preparation of A, mixture: use 10mg/kg to 50mg/kg heteroauxin+40mg/kg to 80mg/kg malonic acid preparating mixture, with general utility balance difference weighing heteroauxin 7.5 grams and malonic acid 60 grams, by the 1 hectare of amount of spraying preparation; Dissolve aforementioned heteroauxin with 375 milliliters of liquor, dissolve malonic acid with little water, standby;
B, water constant volume: by 750 kilograms of per hectare waters, water is added constant volume in the above-mentioned heteroauxin for preparing+malonic acid mixture, standby;
C, field spray: the above-mentioned mixture soup for preparing is packed in the sprayer, go to the field after 4 of that afternoons, by 0.75 kilogram of every strain spraying liquid at cigarette strain foliage-spray once; If rain in 6 hours, fill spray again once;
D, cleaning: clean sprayer, remove residual liquor, for future use.
2. according to the described a kind of method of claim 1, it is characterized in that adding 60 gram malonic acid preparating mixtures with 7.5 gram heteroauxins with mixture reduction nicotine content.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100470815A CN101536636B (en) | 2008-03-17 | 2008-03-17 | Method for reducing nicotine content from mixture |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100470815A CN101536636B (en) | 2008-03-17 | 2008-03-17 | Method for reducing nicotine content from mixture |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101536636A CN101536636A (en) | 2009-09-23 |
| CN101536636B true CN101536636B (en) | 2011-04-20 |
Family
ID=41120210
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008100470815A Expired - Fee Related CN101536636B (en) | 2008-03-17 | 2008-03-17 | Method for reducing nicotine content from mixture |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101536636B (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1039530A (en) * | 1987-02-10 | 1990-02-14 | R.J.雷诺兹烟草公司 | cigarette |
| CN1157126C (en) * | 2000-12-29 | 2004-07-14 | 钱刚 | Method for producing cigarette without public hazard |
-
2008
- 2008-03-17 CN CN2008100470815A patent/CN101536636B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1039530A (en) * | 1987-02-10 | 1990-02-14 | R.J.雷诺兹烟草公司 | cigarette |
| CN1157126C (en) * | 2000-12-29 | 2004-07-14 | 钱刚 | Method for producing cigarette without public hazard |
Non-Patent Citations (1)
| Title |
|---|
| 许萍等.添加有机酸钾对卷烟焦油量的影响.《合肥工业大学学报》.1999,第22卷(第3期),88-93. * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101536636A (en) | 2009-09-23 |
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