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CN100553689C - Composite plant extract deodorizing additive for livestock and poultry and application thereof - Google Patents

Composite plant extract deodorizing additive for livestock and poultry and application thereof Download PDF

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Publication number
CN100553689C
CN100553689C CNB2005100490656A CN200510049065A CN100553689C CN 100553689 C CN100553689 C CN 100553689C CN B2005100490656 A CNB2005100490656 A CN B2005100490656A CN 200510049065 A CN200510049065 A CN 200510049065A CN 100553689 C CN100553689 C CN 100553689C
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livestock
poultry
volatile oil
additive
plant extract
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CN1672738A (en
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陈安国
洪奇华
杨彩梅
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Zhejiang University ZJU
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Abstract

The invention discloses a composite plant extract deodorizing additive for livestock and poultry and application thereof. It is prepared by mixing two or three of the volatile oils of pine needle, cinnamon and clove according to a proportion. On the basis of the compound feed for livestock and poultry, 0.05-2% of the composite plant extract deodorizing additive is added, and the deodorizing additive is uniformly mixed with the feed and then fed to the livestock and poultry, so that the odor emission of the livestock and poultry can be obviously reduced, the livestock and poultry breeding environment is improved, the daily gain of the livestock and poultry is increased, and the feed conversion rate is increased. The composite plant extract deodorizing additive can also be directly used in livestock and poultry manure, reduces the escape of odor and improves the preservation rate of nitrogen in the livestock and poultry manure. Through a plurality of tests and laboratory tests, the additive is high-efficient, safe and nontoxic, has no residue after long-term feeding, and the fed livestock and poultry products meet the food sanitation requirement.

Description

Composite vegetables extractive type deodorant addtives for animals or birds and uses thereof
Technical field
The present invention relates to a kind of composite vegetables extractive type deodorant addtives for animals or birds and uses thereof.
Background technology
Along with the continuous development of aquaculture, fecaluria and foul smell that aquaculture produces are also more and more serious to the influence of environment.For reducing the negative effect that aquaculture is brought, the research that reduces foul smell dischargings such as ammonia by various means has become home and abroad environment nutrition scholar's research focus.But the efficient of the urease inhibitor (as di(2-ethylhexyl)phosphate amide, tricresyl phosphate amide, tricresyl phosphate amide benzene, phosphoric acid ring Disnalon (Ferrer)., hydroxamic acid and derivant acetohrdroxamic acid thereof, xenol, benzoquinone etc.) that present domestic research is more is not high, and some also has very big harm to human body or environment.The external report that also has some plant extracts and preparation to reduce pig, poultry and milch cow gastrointestinal tract and Excreta ammonia gas level, as a kind of desert plant Hough Y. flaccida Haw. (Yucca Schidigera) extract, but, can't apply in China owing to reasons such as the plant place of production, plant extract prices.Thereby the deodorizer of research highly effective and safe has become the task of top priority.
The volatile oil that extracts from Folium Pini, Cortex Cinnamomi, Flos Caryophylli has certain effect to foul smell such as the ammonia discharging that reduces the aquaculture generation, and the existing more report of the extracting method of these active components of plants, as (1996) such as Zhang Fuwei [1]" with the research of Enzymatic Extraction pine needle volatile oil " of report, Qin Yurong etc. (2000) [2]" analysis of different cultivation areas, Guangxi Cortex Cinnamomi volatile oil is relatively " of report, Zhang Fangxia etc. (2003) [3]" extraction process of the preferred Flos Caryophylli volatile oil of orthogonal experiment " of report, existing advantages of simplicity and high efficiency extracting method, these volatile oil are played a role in foul smell dischargings such as control ammonia becomes possibility.But use a certain effect of foul smell such as ammonia discharging and not really desirable of controlling in these three kinds of volatile oil separately, therefore be necessary the factor that influences foul smell dischargings such as aquaculture ammonia is being done on the further investigation basis above-mentioned three kinds of volatile oil to be carried out the discharging that reasonable compatibility is controlled foul smell such as aquaculture ammonia.
List of references
[1] Zhang Fuwei etc., 1996, with the research of Enzymatic Extraction pine needle volatile oil, " Anshan Normal University's journal ";
[2] Qin Yurong etc., 2000, the analysis of different cultivation areas, Guangxi Cortex Cinnamomi volatile oil relatively, " Guangxi forest-science ";
[3] Zhang Fangxia etc., 2003, the extraction process of the preferred Flos Caryophylli volatile oil of orthogonal experiment, " northwest pharmaceutical journal ".
Summary of the invention
The purpose of this invention is to provide a kind of composite vegetables extractive type deodorant addtives for animals or birds and uses thereof.Reduce plant's foul smell discharging, improve livestock and poultry production performance, increase the total nitrogen content of storing in the slurry of feces and urine, promote the aquaculture sustainable development.
Composite vegetables extractive type deodorant addtives is to be processed by two kinds in the volatile oil that extracts in Folium Pini, Cortex Cinnamomi, the Flos Caryophylli or three kinds of compatibilities.
It is used for mixed feed, concentrate feed, premix material, the additive of domestic animal, poultry, perhaps directly makes an addition in the feces of livestock and poultry
Result of use of the present invention is obvious, can obviously reduce the foul smell discharging of poultry, can improve poultry daily gain, improve food conversion ratio, also can be directly used in the feces of livestock and poultry, the ease that reduces foul smell is put, and improves nitrogen storage rate in the feces of livestock and poultry.The present invention is easy to use, detects through Multitest and laboratory, and the not only efficient and safety non-toxic of this additive, long-term feeding noresidue, the animal products of being fed meets the food hygiene requirement.The present invention reduces effective behave that aquaculture pollutes environment, obtain better economic benefit for breeding enterprise technical support is provided, improve the nitrogen storage rate of feces of livestock and poultry simultaneously,, can promote the profitable agriculture development of growth of agricultural efficiency, increasing peasant income for organic agriculture provides fertilizer.
The specific embodiment
The present invention can be used for perhaps directly making an addition in the feces of livestock and poultry in the mixed feed, concentrate feed, premix material, additive of domestic animal, poultry.As according to batch gross weight meter, addition 0.01~2%.Addition is 0.1~2% in the feces of livestock and poultry.
The present invention be with derive from the volatile oil of Folium Pini, Cortex Cinnamomi, Flos Caryophylli two kinds or three kinds by a certain percentage compatibility be processed into composite vegetables extractive type deodorant addtives.Various formula proportion were as follows when composite vegetables extractive type deodorant addtives prepared:
1) portfolio ratio of two kinds of volatile oil that extract in Folium Pini and the Cortex Cinnamomi is 1: 0.1~10;
2) portfolio ratio of two kinds of volatile oil that extract in Folium Pini and the Flos Caryophylli is 1: 0.1~10;
3) portfolio ratio of two kinds of volatile oil that extract in Flos Caryophylli and the Cortex Cinnamomi is 1: 0.1~100;
4) portfolio ratio of three kinds of volatile oil that extract in Folium Pini, Cortex Cinnamomi, the Flos Caryophylli is: 1: 0.05~100: 0.1~15.
Above-mentioned compound volatile oil is used zeolite adsorption respectively, and (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains corresponding composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.The usage of composite vegetables extractive type deodorant addtives of the present invention and consumption and other feed additive are similar.As according to batch gross weight meter, addition 0.01~2%.Addition is 0.1~2% in the feces of livestock and poultry.
Composite vegetables extractive type deodorant addtives for animals or birds is Powdered, be that this powdered complex is added in mixed feed, concentrated feed, premix material or the additive during application, and carrying out uniform mixing, its addition is amounted in the mixed feed content and is counted 0.01~2%; Addition is 0.1~2% in the feces of livestock and poultry.
Embodiment 1:
Two kinds of volatile oil that extract in Folium Pini and the Cortex Cinnamomi are made up with 1: 0.1 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 2:
Two kinds of volatile oil that extract in Folium Pini and the Cortex Cinnamomi are made up with 1: 5.05 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 3:
Two kinds of volatile oil that extract in Folium Pini and the Cortex Cinnamomi are made up with 1: 10 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 4:
Two kinds of volatile oil that extract in Folium Pini and the Flos Caryophylli are made up with 1: 0.1 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 5:
Two kinds of volatile oil that extract in Folium Pini and the Flos Caryophylli are made up with 1: 5.05 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 6:
Two kinds of volatile oil that extract in Folium Pini and the Flos Caryophylli are made up with 1: 10 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 7:
Two kinds of volatile oil that extract in Flos Caryophylli and the Cortex Cinnamomi are made up with 1: 0.1 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 8:
Two kinds of volatile oil that extract in Flos Caryophylli and the Cortex Cinnamomi are made up with 1: 50 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 9:
Two kinds of volatile oil that extract in Flos Caryophylli and the Cortex Cinnamomi are made up with 1: 100 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 10:
Three kinds of volatile oil that extract in Folium Pini, Cortex Cinnamomi, the Flos Caryophylli are made up with 1: 0.05: 0.1 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 11:
Three kinds of volatile oil that extract in Folium Pini, Cortex Cinnamomi, the Flos Caryophylli are made up with 1: 0.05: 7.5 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 12:
Three kinds of volatile oil that extract in Folium Pini, Cortex Cinnamomi, the Flos Caryophylli are made up with 1: 0.05: 15 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 13:
Three kinds of volatile oil that extract in Folium Pini, Cortex Cinnamomi, the Flos Caryophylli are made up with 1: 50: 0.1 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 14:
Three kinds of volatile oil that extract in Folium Pini, Cortex Cinnamomi, the Flos Caryophylli are made up with 1: 50: 7.5 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 15:
Three kinds of volatile oil that extract in Folium Pini, Cortex Cinnamomi, the Flos Caryophylli are made up with 1: 50: 15 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 16:
Three kinds of volatile oil that extract in Folium Pini, Cortex Cinnamomi, the Flos Caryophylli are made up with 1: 100: 0.1 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 17:
Three kinds of volatile oil that extract in Folium Pini, Cortex Cinnamomi, the Flos Caryophylli are made up with 1: 100: 7.5 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Embodiment 18:
Three kinds of volatile oil that extract in Folium Pini, Cortex Cinnamomi, the Flos Caryophylli are made up with 1: 100: 15 ratio, with zeolite adsorption (compound volatile oil: zeolite=1: 10), (ethanol: bag quilt water=1: 1) obtains a kind of composite vegetables extractive type deodorant addtives to reuse 4% methylcellulose ethanol liquid.
Effect
Volatile oil complex from plant extract of the present invention is the composite vegetables extractive type deodorant addtives agent of domestic original creation, by in by the end of November, 2004, this seminar is poultry plant of family surplus priority Zhejiang Hangzhou, Ningbo, Jiaxing, Wenzhou, Taizhou, Jinhua etc. 20, with composite vegetables extractive type deodorant addtives of the present invention through 500,000 (plumage) market pigs, broiler and laying hen contrast tests, it can obviously suppress urease activity, increase the total nitrogen content that stores in the slurry of feces and urine, reduce of the discharging of foul smell such as ammonia, hydrogen sulfide, can improve the fertility performance of animal simultaneously to environment.In feces of livestock and poultry, add and show that also can increase the total nitrogen content that stores in the slurry of feces and urine, foul smell such as minimizing ammonia are to the discharging of environment.
Table 1: add of the influence of safety deodorizer in the feedstuff to child care house piglet fertility performance
Figure C20051004906500071
As can be seen from Table 1, the last anharmonic ratio matched group of test group exceeds 4.90% (P<0.05), and average daily gain improves 7.94% (P<0.01).The material anharmonic ratio of test group reduces by 4.60% (P<0.01) than matched group.
Table 2: add of the influence of safety deodorizer in the feedstuff to meat chicken production performance
Figure C20051004906500072
Figure C20051004906500081
The average end of test group is heavy, average daily gain, survival rate improve 8.74% (P<0.05), 8.91% (P<0.05) and 3.59% (P>0.05) than matched group respectively.
Table 3: add of the influence of holotype deodorizer in the peace feedstuff to the apparent digestibility of dry and crude protein
Figure C20051004906500082
As can be seen from Table 3, the diet dry substance digestibility test group of 30 ~ 54 age in days ablactational baby pig exceeds 5.94% (P<0.01) than matched group, and the crude protein digestibility improves 5.53% (P<0.01).
Table 4: add of the influence of safety deodorizer in the excrement sample to urease activity
Figure C20051004906500083
Annotate: urease activity unit per hour is the ammonia nitrogen milligram number that every gram excrement sample produces.
In the excrement sample, add safety deodorizer to excrement in the inhibition of urease activity be very significant, suppress urease activity and reach 58.32% (P<0.01).
Table 5: add of the influence of safety deodorizer in the feedstuff to urease activity in the excrement
Figure C20051004906500084
Annotate: urease activity unit per hour is the ammonia nitrogen milligram number that every gram excrement sample produces.
Add safety deodorizer in feedstuff, the test group urease activity is than matched group low by 49.91% (P<0.01).
Add of the influence (mmol/l) of safety deodorizer in table 6 daily ration to urea concentration in the slurry of feces and urine
Figure C20051004906500085
By table 6 as seen, adding deodorizer in the daily ration has a significant effect to urea concentration in the slurry of feces and urine.Urea concentration shows that than matched group low by 10.53% (P<0.01) adding safety deodorizer in the daily ration can improve animal to nitrogen use efficiency in the test group slurry of feces and urine when 0h.The urea concentration comparison is according to group difference high by 29.8% (P<0.01), 71.5% (P<0.01), 126.9% (P<0.01) and 371.4% (P<0.01) in 12h, 24h, 36h and 48h point slurry of feces and urine, show and add safety deodorizer in the daily ration, can be in external obvious inhibition urea decomposition.
Add of the influence of safety deodorizer in table 7 daily ration to total nitrogen content in the slurry of feces and urine
Figure C20051004906500091
By table 7 as seen, adding deodorizer in the daily ration has a significant effect to total nitrogen in the slurry of feces and urine.When 6h in the test group slurry of feces and urine total nitrogen content than matched group low 3.35%.The urea concentration comparison is according to group difference high by 3.38% (P<0.01), 15.68% (P<0.01), 18.86% (P<0.01) and 8.75% (P<0.01) in 12h, 24h, 36h and 48h point slurry of feces and urine, show in the daily ration and to add safety deodorizer, can be in improving slurry of feces and urine the conservation rate of total nitrogen.
Table 8: add of the influence of safety deodorizer in the daily ration to the porcine blood serum biochemical indicator
Figure C20051004906500092
By table 8 as seen, the test group total serum protein improves 10.51% (P<0.01) than matched group, and serum urea nitrogen reduces by 16.17% (P<0.01).
Productivity through 500,000 (plumage) market pigs, broiler and laying hens is used, and effect is obvious, and safety is good, remarkable in economical benefits, and plant's foul smell discharging significantly reduces.

Claims (2)

1.一种畜禽用复合植物提取物除臭添加剂,其特征在于由松针和肉桂中提取的二种挥发油组合而成,组合比例为1∶5.05,组合后将复合的挥发油用沸石吸附,沸石用量为复合挥发油的10倍,再用4%甲基纤维素乙醇液包被,其中4%甲基纤维素乙醇液中乙醇∶水为1∶1。1. A compound plant extract deodorizing additive for livestock and poultry, characterized in that it is formed by combining two kinds of volatile oils extracted from pine needles and cinnamon, and the combination ratio is 1: 5.05. After the combination, the composite volatile oil is adsorbed with zeolite, and zeolite The dosage is 10 times that of the compound volatile oil, and then coated with 4% methylcellulose ethanol solution, wherein the ratio of ethanol:water in the 4% methylcellulose ethanol solution is 1:1. 2.一种如权利要求1所述的畜禽用复合植物提取物除臭添加剂的用途,其特征在于用于家畜、家禽的配合饲料、浓缩料、预混料、添加剂中,或者直接添加于畜禽粪便中。2. a kind of purposes of compound plant extract deodorizing additive for livestock and poultry as claimed in claim 1, is characterized in that being used in the compound feed of livestock, poultry, concentrate, premix, additive, or directly adds in in livestock manure.
CNB2005100490656A 2005-02-05 2005-02-05 Composite plant extract deodorizing additive for livestock and poultry and application thereof Expired - Fee Related CN100553689C (en)

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CN101112219B (en) * 2007-08-09 2010-05-19 中国农业科学院上海兽医研究所 Composite type natural plant deodorizer
EP2453760B1 (en) * 2009-07-13 2013-09-18 Pancosma S.A. Food additive containing eugenol, cinnamaldehyde and an alliaceous extract
CN104645395A (en) * 2014-11-26 2015-05-27 彭科 Plant-source deodorant for urban garbage disposal
CN104814355A (en) * 2015-05-23 2015-08-05 昆明饲宝饲料有限责任公司 Deodorant traditional Chinese medicine feed additive for chicken, preparation method and application

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