CN100394910C - Production of improved water-free hand eluate - Google Patents
Production of improved water-free hand eluate Download PDFInfo
- Publication number
- CN100394910C CN100394910C CNB2006100284598A CN200610028459A CN100394910C CN 100394910 C CN100394910 C CN 100394910C CN B2006100284598 A CNB2006100284598 A CN B2006100284598A CN 200610028459 A CN200610028459 A CN 200610028459A CN 100394910 C CN100394910 C CN 100394910C
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- CN
- China
- Prior art keywords
- worm gear
- reaction thing
- phase reaction
- minutes
- gear mixer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 22
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000007788 liquid Substances 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229920002125 Sokalan® Polymers 0.000 claims abstract description 9
- XEFQLINVKFYRCS-UHFFFAOYSA-N Triclosan Chemical compound OC1=CC(Cl)=CC=C1OC1=CC=C(Cl)C=C1Cl XEFQLINVKFYRCS-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229960001631 carbomer Drugs 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 229960003500 triclosan Drugs 0.000 claims abstract description 9
- CBTVGIZVANVGBH-UHFFFAOYSA-N aminomethyl propanol Chemical compound CC(C)(N)CO CBTVGIZVANVGBH-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 8
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 8
- 238000001816 cooling Methods 0.000 claims abstract description 4
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 18
- 238000002360 preparation method Methods 0.000 claims description 15
- 239000006185 dispersion Substances 0.000 claims description 4
- 238000005406 washing Methods 0.000 abstract description 4
- 239000000203 mixture Substances 0.000 abstract description 3
- 238000002156 mixing Methods 0.000 abstract 3
- 235000011187 glycerol Nutrition 0.000 abstract 2
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical compound CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000009775 high-speed stirring Methods 0.000 abstract 1
- 238000004659 sterilization and disinfection Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- 229910000831 Steel Inorganic materials 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 239000006184 cosolvent Substances 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 229940111630 tea tree oil Drugs 0.000 description 2
- 239000010677 tea tree oil Substances 0.000 description 2
- 239000000080 wetting agent Substances 0.000 description 2
- -1 Ka Bobo Substances 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- MHIRBEIOVZPIDF-UHFFFAOYSA-N [O].ClC1=CC=CC=C1 Chemical compound [O].ClC1=CC=CC=C1 MHIRBEIOVZPIDF-UHFFFAOYSA-N 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
- Detergent Compositions (AREA)
Abstract
An improved hand-washing liquid without water is prepared from alcohol, carbomer, deionized water, aminomethyl propanol, propanediol, triclosan and glycerin proportionally through mixing carbomer with deionized water, stirring while heating, cooling, mixing with alcohol, adding aminomethyl propanol to obtain phase A, high-speed stirring, mixing it with the mixture of triclosan and propanediol while stirring, slow stirring, and adding glycerin.
Description
Technical field
The present invention relates to handwashing liquid, particularly a kind of preparation method of modified model non-water hand cleanser.
Background technology
Chinese patent literature CN1596877A discloses a kind of water washing avoiding disinfection handwashing liquid and preparation method thereof, in handwashing liquid main assembly compositions such as ethanol, tea tree oil, Ka Bobo, cosolvent, wetting agent, take by weighing each component by formula proportion, in adding a cover reaction pot, rustless steel adds the pure water that accounts for handwashing liquid gross weight 20% earlier, Ka Bobo divided join in the pure water lentamente 3～5 times, the limit edged stirs, carried out mechanical agitation 150 minutes with 80～100 rev/mins speed, fully disperse an even muddy dispersion, standing over night, fully swelling makes first liquid.Add a cover in the reaction pot at another rustless steel and to add the ethanol that accounts for handwashing liquid gross weight 10%, add 5-chloro-2-(2, the two chlorobenzene oxygen of 4-) phenol then, mixed dissolution carried out mechanical agitation 10 minutes with 50～80 rev/mins speed, until the liquid clear, make second liquid, airtight preservation is standby.Second liquid is poured in the first liquid, and added surplus and get ethanol, stir 30 minutes mix homogeneously with 50～80 rev/mins speed.Add skin protectant, tea tree oil, wetting agent, cosolvent, mixed dissolution then successively.Fully stir 10 minutes to homodisperse with 80～100 rev/mins speed, add the pH value regulator and regulate pH value 6.7～8.7, add essence again, replenish pure water restir 20 minutes to the capacity, promptly get this handwashing liquid.
The preparation process of this kind water washing avoiding disinfection handwashing liquid is comparatively loaded down with trivial details, complicated process of preparation.
Summary of the invention
Task of the present invention provides a kind of modified model anhydrous hand cleaner liquid and preparation method thereof, and the preparation process that it has solved existing water washing avoiding disinfection handwashing liquid is loaded down with trivial details, the problem of complicated process of preparation.
Technical solution of the present invention is as follows:
A kind of anhydrous hand cleaner liquid and preparation method thereof, each component that will comprise ethanol, carbomer, deionized water, aminomethyl propanol, propylene glycol, triclosan, glycerol follows these steps to assembly:
(1) carbomer and deionized water are being heated with stirring to dispersion fully under 40～45 ℃ in vacuum worm gear mixer; Cooling subsequently adds ethanol, mixes 5 minutes; Add aminomethyl propanol again, become A phase reaction thing between the solution pH value is transferred to 6～7; With this A phase reaction thing with vacuum worm gear mixer blade quick rotation;
(2) in another blender, triclosan is added propylene glycol and fully dissolve, become B phase reaction thing; Pour B phase reaction thing into A phase reaction thing, in vacuum worm gear mixer, mixed 5 minutes, and vacuum worm gear mixer is turned round with maximal rate;
(3) make the slow-down of vacuum worm gear mixer then, add glycerol, mixed 3 minutes, become C phase product; At room temperature C phase product is taken out from machine.
By modified model anhydrous hand cleaner liquid and preparation method thereof of the present invention, preparation technology and preparation process are simple.The modified model non-water hand cleanser that makes through preparation method of the present invention is a kind of renewal product, and it is little to skin irritation, action temperature and, strong detergency has played the effect of disinfection.
The specific embodiment
The present invention is a kind of modified model anhydrous hand cleaner liquid and preparation method thereof, and each component of this non-water hand cleanser is: ethanol, carbomer (carbomer), deionized water, aminomethyl propanol, propylene glycol, triclosan (triclosan), glycerol.
Above-mentioned each component of the present invention's assembly as follows:
(1) carbomer and deionized water are being heated with stirring to dispersion fully under 40～45 ℃ in vacuum worm gear mixer.Cooling subsequently adds ethanol, mixes 5 minutes.Add aminomethyl propanol again, the solution pH value is transferred between 6～7.With this A phase reaction thing with vacuum worm gear mixer blade quick rotation.
(2) in another blender, triclosan is added propylene glycol and fully dissolve, become B phase reaction thing.Pour B phase reaction thing into A phase reaction thing, in vacuum worm gear mixer, mixed 5 minutes, and vacuum worm gear mixer is turned round with maximal rate.
(3) make the slow-down of vacuum worm gear mixer then, add glycerol, mixed 3 minutes, become C phase product.At room temperature C phase product is taken out from machine at last.
Certainly, those skilled in the art in the present technique field will be appreciated that, the foregoing description only is to be used for illustrating the present invention, and be not as limitation of the invention, as long as in connotation scope of the present invention, all will drop in the scope of claim of the present invention variation, the modification of the foregoing description.
Claims (1)
1. an anhydrous hand cleaner liquid and preparation method thereof is characterized in that, each component that will comprise ethanol, carbomer, deionized water, aminomethyl propanol, propylene glycol, triclosan, glycerol follows these steps to assembly:
(1) carbomer and deionized water are being heated with stirring to dispersion fully under 40～45 ℃ in vacuum worm gear mixer; Cooling subsequently adds ethanol, mixes 5 minutes; Add aminomethyl propanol again, become A phase reaction thing between the solution pH value is transferred to 6～7; With this A phase reaction thing with vacuum worm gear mixer blade quick rotation;
(2) in another blender, triclosan is added propylene glycol and fully dissolve, become B phase reaction thing; Pour B phase reaction thing into A phase reaction thing, in vacuum worm gear mixer, mixed 5 minutes, and vacuum worm gear mixer is turned round with maximal rate;
(3) make the slow-down of vacuum worm gear mixer then, add glycerol, mixed 3 minutes, become C phase product; At room temperature C phase product is taken out from machine.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100284598A CN100394910C (en) | 2006-06-30 | 2006-06-30 | Production of improved water-free hand eluate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100284598A CN100394910C (en) | 2006-06-30 | 2006-06-30 | Production of improved water-free hand eluate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1895204A CN1895204A (en) | 2007-01-17 |
| CN100394910C true CN100394910C (en) | 2008-06-18 |
Family
ID=37607942
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006100284598A Expired - Fee Related CN100394910C (en) | 2006-06-30 | 2006-06-30 | Production of improved water-free hand eluate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100394910C (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107714538A (en) * | 2017-10-19 | 2018-02-23 | 浙江雅颜生物科技有限公司 | Lemon glue hand cleanser and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5869061A (en) * | 1996-06-04 | 1999-02-09 | Brugh; Bettie Sue | Protective hand lotion of aloe vera gel and vitamin E gel |
| CN1312069A (en) * | 2000-12-29 | 2001-09-12 | 徐玉笙 | Composition and and preparation of disinfecting skin care hand cleaning liquid |
| CN1432640A (en) * | 2002-01-15 | 2003-07-30 | 叶汉华 | Water-free bacteriostatic hand-washing agent |
| US6783766B2 (en) * | 2002-03-06 | 2004-08-31 | Dow Global Technologies Inc. | Process for preparing a cosmetic formulation |
| CN1596877A (en) * | 2003-09-16 | 2005-03-23 | 上海拜耳科生物科技有限公司 | Antiseptic hand cleaning liquid with out water cleaning and its preparation method |
-
2006
- 2006-06-30 CN CNB2006100284598A patent/CN100394910C/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5869061A (en) * | 1996-06-04 | 1999-02-09 | Brugh; Bettie Sue | Protective hand lotion of aloe vera gel and vitamin E gel |
| CN1312069A (en) * | 2000-12-29 | 2001-09-12 | 徐玉笙 | Composition and and preparation of disinfecting skin care hand cleaning liquid |
| CN1432640A (en) * | 2002-01-15 | 2003-07-30 | 叶汉华 | Water-free bacteriostatic hand-washing agent |
| US6783766B2 (en) * | 2002-03-06 | 2004-08-31 | Dow Global Technologies Inc. | Process for preparing a cosmetic formulation |
| CN1596877A (en) * | 2003-09-16 | 2005-03-23 | 上海拜耳科生物科技有限公司 | Antiseptic hand cleaning liquid with out water cleaning and its preparation method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1895204A (en) | 2007-01-17 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20080618 |