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CN109806813A - A kind of reaction vessel - Google Patents

A kind of reaction vessel Download PDF

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Publication number
CN109806813A
CN109806813A CN201811424210.8A CN201811424210A CN109806813A CN 109806813 A CN109806813 A CN 109806813A CN 201811424210 A CN201811424210 A CN 201811424210A CN 109806813 A CN109806813 A CN 109806813A
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CN
China
Prior art keywords
bottle
volumetric bottle
volumetric
liquid
sealing element
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Application number
CN201811424210.8A
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Chinese (zh)
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CN109806813B (en
Inventor
胡学静
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Yongkang Xiaocaiya Kitchen Tools Co ltd
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Individual
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Publication of CN109806813A publication Critical patent/CN109806813A/en
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Publication of CN109806813B publication Critical patent/CN109806813B/en
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Abstract

The invention discloses a kind of quantitative reaction containers, including reaction vessel and dosing container, dosing container is set to above reaction vessel and is at least arranged two, dosing container includes liquid holding bottle and volumetric bottle, liquid holding bottle is connected to for liquid holding bottle to the first check valve of volumetric bottle one-way conduction with volumetric bottle by conducting direction, it is second one-way valve of the volumetric bottle to reaction flask that the discharge port of volumetric bottle, which is provided with conducting direction, liquid holding bottle is combined with the first pressing mechanism that liquid is pressed to volumetric bottle, volumetric bottle is provided with degassing extruder structure, degassing extruder structure includes that the exhaust gear for for will be squeezed into the liquid of volumetric bottle the expanding gas in volumetric bottle being discharged and the liquid for being used to will go into volumetric bottle are expressed into the extrusion mechanism of reaction flask from second one-way valve, the side wall of reaction flask is provided with gas outlet close to upper-end part of driving, it is set by above-mentioned It sets, the amount of reaction liquid can be accurately controlled, be easy to use, simply.

Description

A kind of reaction vessel
Technical field
The present invention relates to chemical experiment clothing arts, more particularly, to be a kind of reaction vessel.
Background technique
With the improvement of people's living standards, also can increasingly pay attention to for each health parameter in living environment, such as The standard detection etc. of certain elements etc. in water quality, food, and the extraction of this data detects, and usually passes through a series of chemistry What experiment obtained.How the reacting dose of reaction reagent is controlled, will determine the influence to experimental result accuracy.
Summary of the invention
In view of this, the object of the present invention is to provide a kind of reaction vessels of accurate control reacting dose.
To achieve the above object, realized by following technological means: a kind of quantitative reaction container, including reaction vessel and Dosing container, dosing container is set to above reaction vessel and at least setting two, and the dosing container includes liquid holding bottle and determines Measuring bottle, the liquid holding bottle are connected to for liquid holding bottle to the first check valve of volumetric bottle one-way conduction with volumetric bottle by conducting direction, It is second one-way valve of the volumetric bottle to reaction flask that the discharge port of the volumetric bottle, which is provided with conducting direction, and the liquid holding bottle is combined with Liquid is pressed to the first pressing mechanism of volumetric bottle, the volumetric bottle is provided with degassing extruder structure, the degassing extruder structure Including the exhaust gear for for the liquid of volumetric bottle will to be squeezed into the expanding gas in volumetric bottle being discharged and be used for by The liquid for entering volumetric bottle is expressed into the extrusion mechanism of reaction flask from second one-way valve, and the side wall of the reaction flask is close to upper end Position is provided with gas outlet.
Advanced optimize are as follows: the bottleneck position of the reaction vessel be provided with it is identical with volumetric bottle number to interface, it is fixed The downside of measuring bottle is screwed on to interface.
Advanced optimize are as follows: the degassing extruder structure includes a shell, be disposed in the shell discharge chamber and Extruding cavity, the discharge chamber are fixedly connected with volumetric bottle, and by being arranged on volumetric bottle between volumetric bottle and discharge chamber Gas port interconnects, and the discharge chamber sliding is connected with a sealing element, and the sealing element can in the both ends extreme position of sliding The extruding cavity and gas port are sealed, the chamber shell of the discharge chamber is provided with first row stomata, and the extrusion mechanism includes described The compressed-air system of extruding cavity and cooperation in extrusion chamber, when the sealing element seals the gas port, the compressed-air system can Gas unidirectional is pressed into volumetric bottle.
It advanced optimizes are as follows: be additionally provided with one between sealing element and the shell of volumetric bottle and drive sealing element sliding to extruding cavity The elastic component of shifting, the elastic component are provided with second row stomata, when the sealing element seals the extruding cavity, the air guide Hole, second row stomata and first row stomata are connected mutually.
It advanced optimizes are as follows: the compressed-air system includes the inflator that sliding is connected in extruding cavity, one end of the inflator It is fixed with sealing element, inflator interior slip is connected with a piston, and the other end of the piston opposing seal is provided with an operation Bar, the operating stick are pierced by extruding cavity, and it is third check valve of the inflator to gas port that conducting direction is provided on the sealing element, Conducting direction is provided on the piston to be extraneous to the 4th check valve inside inflator.
It advanced optimizes are as follows: and the conducting atmospheric pressure of the third check valve is greater than the deformation power of the elastic component.
It advanced optimizes are as follows: the elastic component is rubber bellows, and the second row stomata is set to rubber bellows On tube wall, and the both ends of the rubber bellows form sealing, the gas port and rubber wave respectively at sealing element and volumetric bottle The pore of line pipe is connected to.
It advanced optimizes are as follows: the pressing mechanism includes an air bag being connected to liquid holding bottle, is provided with and leads on the air bag Logical direction is extraneous the 5th check valve to inside air bag.
It advanced optimizes are as follows: the liquid holding bottle is provided with bottle cap, and the pressing mechanism is set on bottle cap.
It advanced optimizes are as follows: the bottom of the volumetric bottle is set as an inner concave, and the second one-way valve is set to described At inner concave.
The advantages of the present invention over the prior art are that: the liquid in liquid holding bottle can be squeezed by extruding gasbag quantitative In bottle, and scale (scale can be arranged on volumetric bottle) is wiped by pipe and control can be squeezed at any time by the amplitude of extruding gasbag Enter the amount of liquid into volumetric bottle, the liquid simultaneously entered in volumetric bottle will make the air pressure in volumetric bottle become larger, more Remaining gas can be discharged to the external world by gas port, second row stomata and first row stomata, avoid and become larger in volumetric bottle The problem of air pressure directly squeezes out liquid from second one-way valve;With same method, predetermined amount is fitted into two volumetric bottles Liquid, the liquid in volumetric bottle just then can be directly extruded by degassing extruder structure by reaction vessel, realized quantitative Reaction experiment, the variable of experiment can be precisely controlled, is easy to use, simply.
Detailed description of the invention
Fig. 1 is the entirety sectional view of embodiment quantitative reaction container (extrusion mechanism is not operating);
Fig. 2 is the entirety sectional view (extrusion mechanism movement) of embodiment quantitative reaction container;
Fig. 3 is the top view of embodiment reaction vessel;
Fig. 4 is the degassing extruder structure decomposition diagram of embodiment;
Fig. 5 is the portion the A enlarged drawing of Fig. 4;
Fig. 6 is the portion the B enlarged drawing of Fig. 4.
In figure, 1, liquid holding bottle;11, the first check valve;2, bottle cap;3, volumetric bottle;31, second one-way valve;32, gas port; 4, shell;41, extruding cavity;42, discharge chamber;421, first row stomata;5, air bag;51, the 5th check valve;6, sealing element;61, Three check valves;7, corrugated rubber pipe;71, second row stomata;8, inflator;81, piston;811, the 4th check valve;82, operating stick; 9, reaction vessel;91, gas outlet;92, to interface.
Specific embodiment
It is described in further detail with reference to the accompanying drawing and by specific embodiment to invention, following embodiment is descriptive , it is not restrictive protection scope of the present invention.
Embodiment
A kind of quantitative reaction container reaction vessel including lower section and is disposed over referring first to attached Fig. 1 and 2 Two dosing containers, it is of course possible to which, according to not allowing for reaction condition, dosing container also can be set 2 or more.Dosing container packet Liquid holding bottle 1 and volumetric bottle 3 are included, the quantifying particularly suitable for liquid reagent of volumetric bottle 1 in the present embodiment.At the bottom of liquid holding bottle 1 Portion is removably connected with volumetric bottle 3, is connected here using thread seal.The bottom of liquid holding bottle 1 is provided with the first check valve 11 For being connected to liquid holding bottle 1 and volumetric bottle 3, it is volumetric bottle 3 to the of reaction vessel 9 that the bottom surface of volumetric bottle 3, which is provided with conducting direction, Two check valves 31 are arranged at the inner concave, which is also the liquid outlet of volumetric bottle 3, in order to enable volumetric bottle 3 Interior liquid outflow is more thorough, the interior bottom of volumetric bottle 3 can be also provided with into interior concave spherical surface, and second one-way valve 31 is set Set the lowest part in the interior concave spherical surface.
It is provided with pressing mechanism on the bottle cap 2 of liquid holding bottle 1, for liquid to be pressed to volumetric bottle 3 from liquid holding bottle 1, is squeezed Mechanism includes air bag 5, and is provided with the conducting direction external world to the 5th check valve 51 inside air bag 5, to work as on air bag 5 Air pressure when extruding gasbag 5 in liquid holding bottle 1 increases, and liquid presses to volumetric bottle 3 by the first check valve 11, when release air bag After 5, air bag 5 will be restored by the deformability of itself and the air in the external world passes through the 5th check valve 51 and fills into air bag 5.And The liquid for entering volumetric bottle 3 increases the air pressure of volumetric bottle 3, excludes not in time if this increases air pressure, and it is fixed to enter Liquid in measuring bottle 3 will be directly discharged by second one-way valve 31, the effect of quantitative measurement is unable to reach, so in volumetric bottle 3 On be also combined with degassing extruder structure, it is convenient when liquid enters volumetric bottle 3 and the air pressure in volumetric bottle 3 is caused to become larger, it is more Residual air body can be discharged in time by exhaust gear.And enter the liquid in volumetric bottle 3 then can by observation scale and The amplitude of hand pinching air bag 5 controls.
Reaction vessel 9 therein referring to attached drawing 1-3, its oral area be provided with docked with volumetric bottle 3 to interface 92, can be with Connection between the two is realized in such a way that screw thread is screwed on, and is arranged in the side wall of reaction vessel 9 close to the position of oral area There is gas outlet 91, in order to which gas after reaction liquid enters reaction vessel or during the reaction is from the gas outlet Discharge, when needing to use detection reaction gas, equipment which can connect detection gas.
Degassing extruder structure therein is referring to attached drawing 4-6, the shell 4 including 3 wall surface of volumetric bottle is arranged in, shell 4 it is interior Part is extruding cavity 41 and discharge chamber 42, and the cross sectional shape of extruding cavity 41 and discharge chamber 42 therein is round and discharge chamber 42 Section radius be greater than extruding cavity 41 section radius, in discharge chamber 42 sliding be connected with sealing element 6, sealing element 6 is sliding The extreme position of left and right two extruding cavity 41 and gas port 32 can be formed sealing, certainly here in sealing element 6 and volumetric bottle 3 It is provided with corrugated rubber pipe 7 between wall surface, when sealing element 6 is drawn close to gas port 32, can first press corrugated rubber pipe 7 Contracting, is then worked by sealing element 6 and corrugated rubber pipe 7 and forms sealing between gas port 32.It should be understood that can also be with It is not provided with corrugated rubber pipe 7, forms sealing between the mode and gas port 32 of 3 wall surface of volumetric bottle that directly reclined by sealing element 6.When When sealing element 6 and extruding cavity 41 are drawn close, pass through first row stomata 421, second row stomata 71 and air guide between extraneous and volumetric bottle 3 Hole 32 is connected to, and when liquid enters volumetric bottle 3 from liquid holding bottle 1, it is fixed that extra air will be discharged by this exhaust gear Measuring bottle 3, the problem of preventing high pressure from directly squeezing out liquid out of volumetric bottle 3.
Sliding is connected with inflator 8 in extruding cavity 41, and one end of inflator 8 is directly fixed with sealing element 6, is internally provided with work Plug 81, piston rod is then reversely pierced by 41 formation operation bar 82 of extruding cavity, is provided with air guide direction on piston to be extraneous to inflator 8 The 4th internal check valve 811, it is third check valve 61 of the inflator 8 to gas port 32 that air guide direction is provided on sealing element 6, And the conducting atmospheric pressure of third check valve 61 is greater than the deformation power of the elastic component.Thus when squeezing into predetermined amount in volumetric bottle 3 Liquid after, can first push operating stick 82, inflator 8 will be moved with sealing element 6 to gas port 32 and by ripple at this time Sealing (or sealing is directly formed between gas port 32 by sealing element 6) is formed between the compression of rubber tube 7 and gas port 32, after After continuous promotion operating stick 82, the gas in inflator 8 is pressed to third check valve 61 and makes its unlatching by piston 81, and gas will pass through Gas port 32 is pressed into volumetric bottle 3, and the air pressure in volumetric bottle 3 increases the liquid in it will be discharged to instead by second one-way valve 31 It answers in container 9.It is once all projected insufficient for the liquid in volumetric bottle 3 if pushing, pullback operation bar 82, at this time gas It will be filled in inflator 8 by the 4th check valve 811 until piston 81 encounters the bottom of inflator 8, and draw catch bar, inflator 8 again at this time It retracts and retracts with sealing element 6 along discharge chamber 42, form negative pressure in volumetric bottle 3, since gas has good expansion Compressibility, it is extraneous until the position that sealing element 6 return back to first row stomata 421, second row stomata 71 is connected to gas port 32 Air will be directly added into volumetric bottle 3, then push operating stick 82 again, repeat above-mentioned extrusion step, until by volumetric bottle 3 Interior liquid all squeezes out.
Two dosing containers of the operation setting above reaction vessel 9 in the same way, may be implemented to measure quantitative The reaction liquid and then quantitative reaction liquid is discharged into reaction vessel reacts, and realizes quantitative reaction experiment, real The variable tested can be precisely controlled, is easy to use, simply.
The above is only a preferred embodiment of the present invention, protection scope of the present invention is not limited merely to above-mentioned implementation Example, all technical solutions belonged under thinking of the present invention all belong to the scope of protection of the present invention.It should be pointed out that for the art Those of ordinary skill for, several improvements and modifications without departing from the principles of the present invention, these improvements and modifications It should be regarded as protection scope of the present invention.

Claims (10)

1. a kind of quantitative reaction container, including reaction vessel and dosing container, which is characterized in that dosing container is set to reaction Container top and at least setting two, the dosing container includes liquid holding bottle and volumetric bottle, and the liquid holding bottle passes through with volumetric bottle Conducting direction is that liquid holding bottle is connected to the first check valve of volumetric bottle one-way conduction, and the discharge port of the volumetric bottle is provided with conducting Direction is second one-way valve of the volumetric bottle to reaction flask, and the liquid holding bottle is combined with the first extruder that liquid is pressed to volumetric bottle Structure, the volumetric bottle are provided with degassing extruder structure, and the degassing extruder structure includes the liquid for that will be squeezed into volumetric bottle And exhaust gear that the expanding gas in volumetric bottle is discharged and liquid for will go into volumetric bottle are unidirectional from second Valve is expressed into the extrusion mechanism of reaction flask, and the side wall of the reaction flask is provided with gas outlet close to upper-end part of driving.
2. a kind of quantitative reaction container according to claim 1, which is characterized in that the bottleneck position of the reaction vessel is set It is equipped with identical with volumetric bottle number to interface, the downside of volumetric bottle is screwed on to interface.
3. a kind of quantitative reaction container according to claim 1, which is characterized in that the degassing extruder structure includes a shell Body is disposed with discharge chamber and extruding cavity in the shell, and the discharge chamber is fixedly connected with volumetric bottle, and volumetric bottle with It is interconnected between discharge chamber by the gas port being arranged on volumetric bottle, the discharge chamber sliding is connected with a sealing element, institute The extruding cavity and gas port can be sealed in the both ends extreme position of sliding by stating sealing element, and the chamber shell of the discharge chamber is provided with One gas vent, the extrusion mechanism include the compressed-air system of the extruding cavity and cooperation in extrusion chamber, when the sealing element seals When gas port is stated in residence, gas unidirectional can be pressed to volumetric bottle by the compressed-air system.
4. a kind of quantitative reaction container according to claim 3, which is characterized in that the shell of sealing element and volumetric bottle it Between be additionally provided with an elastic component for driving sealing element to slide to extruding cavity, the elastic component is provided with second row stomata, when described When sealing element seals the extruding cavity, the gas port, second row stomata and first row stomata are connected mutually.
5. a kind of quantitative reaction container according to claim 3 or 4, which is characterized in that the compressed-air system includes sliding The inflator being connected in extruding cavity, one end and the sealing element of the inflator are fixed, and inflator interior slip is connected with a piston, described The other end of piston opposing seal is provided with an operating stick, and the operating stick is pierced by extruding cavity, is provided on the sealing element Conducting direction is third check valve of the inflator to gas port, and conducting direction is provided on the piston to be extraneous to inside inflator 4th check valve.
6. a kind of quantitative reaction container according to claim 5, which is characterized in that and the conducting gas of the third check valve Pressure is greater than the deformation power of the elastic component.
7. a kind of quantitative reaction container according to claim 4, which is characterized in that the elastic component is rubber bellows, The second row stomata is set on the tube wall of rubber bellows, and the both ends of the rubber bellows respectively at sealing element and are determined Measuring bottle forms sealing, and the gas port is connected to the pore of rubber bellows.
8. a kind of quantitative reaction container according to claim 1, which is characterized in that the pressing mechanism includes one and Sheng liquid The air bag of bottle connection, it is extraneous the 5th check valve to inside air bag that conducting direction is provided on the air bag.
9. a kind of quantitative reaction container according to claim 8, which is characterized in that the liquid holding bottle is provided with bottle cap, institute Pressing mechanism is stated to be set on bottle cap.
10. according to claim 1 or a kind of quantitative reaction container described in 9, which is characterized in that the bottom of the volumetric bottle is arranged For an inner concave, the second one-way valve is set at the inner concave.
CN201811424210.8A 2018-11-27 2018-11-27 Reaction vessel Active CN109806813B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811424210.8A CN109806813B (en) 2018-11-27 2018-11-27 Reaction vessel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811424210.8A CN109806813B (en) 2018-11-27 2018-11-27 Reaction vessel

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CN109806813A true CN109806813A (en) 2019-05-28
CN109806813B CN109806813B (en) 2021-10-26

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103543138A (en) * 2013-10-25 2014-01-29 中国华能集团清洁能源技术研究院有限公司 Experimental system combining high-temperature and high-pressure reaction system and Raman spectra analyzer
CN203425792U (en) * 2013-08-06 2014-02-12 宜兴市华联化工有限公司 Multi-kettle feeding full-automatic continuous production device
WO2015097013A1 (en) * 2013-12-23 2015-07-02 Ineos Europe Ag Process

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203425792U (en) * 2013-08-06 2014-02-12 宜兴市华联化工有限公司 Multi-kettle feeding full-automatic continuous production device
CN103543138A (en) * 2013-10-25 2014-01-29 中国华能集团清洁能源技术研究院有限公司 Experimental system combining high-temperature and high-pressure reaction system and Raman spectra analyzer
WO2015097013A1 (en) * 2013-12-23 2015-07-02 Ineos Europe Ag Process

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Effective date of registration: 20210909

Address after: 321300 Third Floor, 32 Sixth Street, Caoyuan Village, Yongkang Economic Development Zone, Jinhua City, Zhejiang Province

Applicant after: YONGKANG XIAOCAIYA KITCHEN TOOLS Co.,Ltd.

Address before: 321300 No. 118 Heng street, Hu Ku Shang Cun, Gushan Town, Yongkang City, Jinhua City, Zhejiang Province

Applicant before: Hu Xuejing

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