CN109666879A - A kind of space flight and aviation ZK61M magnesium alloy - Google Patents
A kind of space flight and aviation ZK61M magnesium alloy Download PDFInfo
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- CN109666879A CN109666879A CN201910131231.9A CN201910131231A CN109666879A CN 109666879 A CN109666879 A CN 109666879A CN 201910131231 A CN201910131231 A CN 201910131231A CN 109666879 A CN109666879 A CN 109666879A
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- forging
- rolling
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- magnesium alloy
- aviation
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- 229910000861 Mg alloy Inorganic materials 0.000 title claims abstract description 45
- 238000005242 forging Methods 0.000 claims abstract description 77
- 238000005096 rolling process Methods 0.000 claims abstract description 56
- 238000005266 casting Methods 0.000 claims abstract description 24
- 230000032683 aging Effects 0.000 claims abstract description 14
- 238000005098 hot rolling Methods 0.000 claims abstract description 13
- 239000011777 magnesium Substances 0.000 claims abstract description 10
- 238000011282 treatment Methods 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims description 18
- 239000011825 aerospace material Substances 0.000 abstract description 2
- 238000003483 aging Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 description 10
- 238000004519 manufacturing process Methods 0.000 description 5
- 238000005728 strengthening Methods 0.000 description 5
- 239000000956 alloy Substances 0.000 description 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- LQHZJYFIRFRDKF-UHFFFAOYSA-N gold magnesium Chemical compound [Mg].[Au] LQHZJYFIRFRDKF-UHFFFAOYSA-N 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000003672 processing method Methods 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 230000035882 stress Effects 0.000 description 1
- 230000010415 tropism Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/06—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of magnesium or alloys based thereon
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- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Forging (AREA)
- Metal Rolling (AREA)
Abstract
A kind of space flight and aviation ZK61M magnesium alloy, it is through the following steps that be prepared: (1) forge: the ZK61M circle ingot casting that will meet YS/T 627-2013 deformed Mg and magnesium alloy circle ingot casting standard carries out heats forged, and when forging carries out the forging in length, three width, height directions；(2) hot rolling: carrying out steering rolling for the forging plate that step (1) obtains, and the rolling of small working modulus multi-pass is then carried out at 345-355 DEG C of temperature, finally obtains the hot rolled plate that total plus power is 26-27%；(3) timeliness: the hot rolled plate that step (2) is obtained carries out 170-180 DEG C of ageing treatment 22-26h, obtains space flight and aviation ZK61M magnesium alloy.The present invention exceeds needed for aerospace material by forging, hot rolling and ageing treatment, the magnesium alloy three-dimensional performance produced, good can be applied to space flight and aviation military industry.
Description
Technical field
The invention belongs to alloy manufacturing technology fields, and in particular to a kind of space flight and aviation ZK61M magnesium alloy.
Background technique
Magnesium alloy is the smallest metal of specific gravity in light metal, this material is particularly suitable for applications in space flight and aviation.But because
ZK61M materials hot working temperature range is relatively narrow, only 50 degree or so, is difficult to complete hot rolling within this range, therefore lead to not
Plate is produced, domestic at present also without any standard about plate, only production forging (only forge at present by ZK61M magnesium alloy
Part standard), but the performance of forging standard is not able to satisfy the material property of space flight and aviation application.ZK61M forging standard and space flight boat
Sky standard is as shown in table 1.
Note: H112 is natural cooling state in table, is national forging standard (country is without ZK61M plates specifications), parantheses in parantheses
It is the mechanical property of aerospace plate requirement outside.
Current any magnesium alloy materials mechanical property does not have three-dimensional requirement, and strip requires longitudinal performance；It squeezes and requires longitudinal direction
Performance；Forging requires longitudinal and transverse two performances.However whatsoever standard, material do not require high Xiang Xingneng, but space flight and aviation
The three-dimensional performance of material is required with plate, and every to all beyond standard regulation.The high tropism energy tensile strength of ZK61M is extremely difficult to
220N/mm2, it is specified that disproportional strength is extremely difficult to 120N/mm2；For this reason, it may be necessary to a kind of novel ZK61M magnesium alloy is researched and developed,
To realize the material property of space flight and aviation application, industry blank is filled up.
Summary of the invention
The object of the invention is that providing a kind of space flight and aviation ZK61M magnesium conjunction to solve the deficiencies in the prior art
Gold.
The purpose of the present invention is what is realized with following technical proposals:
A kind of space flight and aviation ZK61M magnesium alloy, it is through the following steps that be prepared:
(1) it forges: the ZK61M circle ingot casting for meeting YS/T 627-2013 deformed Mg and magnesium alloy circle ingot casting standard is heated
Forging, heating temperature are 420-430 DEG C, and heating time 13-16 hour carries out when forging in length, width, highly three directions
Forging, final forging temperature be not less than 350 DEG C, obtain forging plate；
(2) hot rolling: then the forging plate that step (1) is obtained carries out steering rolling, is rolled in 400-420 DEG C of heating 6-9h
Then making sheet A carries out the rolling of small working modulus multi-pass at 345-355 DEG C of temperature, finally obtaining total plus power is 26-27%'s
Hot rolled plate；
(3) timeliness: the hot rolled plate that step (2) is obtained carries out 170-180 DEG C of ageing treatment 22-26h, obtains space flight and aviation use
ZK61M magnesium alloy.
The forging ratio that three step (1) length, width, height directions are all made of 10-20 is forged.
Step (1) ZK61M circle ingot diameters are Φ 300-500mm, length 600-700mm, are finally forged to
The circle ingot casting that length is 600-700mm is first forged and pressed to 300-400mm when forging, then again will by the forging plate of 150-155mm thickness
The flat forging and stamping of circle forging and stamping are rectangle, then are forged in three length, width, height directions.
It is 22-23% that the step (2), which turns to the milled sheet A working modulus obtained after rolling, and it is more then to carry out small working modulus again
The rolling of passage finally obtains the hot rolled plate that total plus power is 26-27%.
The step (2) turns to rolling concrete operations are as follows: is first thickness 137- by the forging plate axial rolling of 150-155mm thickness
The plate of 141mm then turns to the plate that transverse rolling is thickness 126-130mm, turns again to the plate that axial rolling is thickness 119-123mm, finally
Turn to transverse rolling be thickness 114-116mm milled sheet A, then carry out the rolling of small working modulus multi-pass, roll for a thickness of
The milled sheet of 109-112mm.
Passage number is not less than 6-8 passage in the rolling of the small working modulus multi-pass.
The present invention is first by the ZK61M circle ingot casting for meeting YS/T 627-2013 deformed Mg and magnesium alloy circle ingot casting standard first
First to be forged, the blank interior tissue after forging becomes worked structure from cast sturcture, and hot-working relatively easily rolls,
Also, in order to meet final material performance, when forging, will carry out three directions forging and stamping, and it is more that small-power is then finally carried out when hot rolling
The rolling of passage, it is ensured that three-dimensional performance, finally by ageing treatment, the magnesium alloy three-dimensional performance produced exceeds aviation boat
Needed for its material, good it can be applied to space flight and aviation military industry.
Specific embodiment
Embodiment 1
A kind of space flight and aviation ZK61M magnesium alloy, it is through the following steps that be prepared:
(1) it forges: the ZK61M circle ingot casting for meeting YS/T 627-2013 deformed Mg and magnesium alloy circle ingot casting standard is heated
Forging, heating temperature are 420-430 DEG C, and heating time 13-16 hour carries out when forging in length, width, highly three directions
Forging, final forging temperature be not less than 350 DEG C, obtain forging plate；Three preferred length, width, height directions are all made of 10-20's
Forging ratio is forged.Available ZK61M circle cast ingot dimension be diameter be Φ 300-500mm, length 600-
700mm first forges and presses the circle ingot casting that length is 600-700mm to 300-400mm when forging, then forges and presses again as rectangle, then
It is forged in three length, width, height directions, is finally forged to the forging plate of 150-155mm thickness；
(2) hot rolling: then the forging plate that step (1) is obtained carries out steering rolling, is rolled in 400-420 DEG C of heating 6-9h
Then making sheet A carries out the rolling of small working modulus multi-pass at 345-355 DEG C of temperature, finally obtaining total plus power is 26-27%'s
Hot rolled plate；An available concrete operation step are as follows: be first thickness 137-141mm by the forging plate axial rolling of 150-155mm thickness
Plate, then turn to transverse rolling be thickness 126-130mm plate, turn again to axial rolling be thickness 119-123mm plate, be ultimately steering to cross
The milled sheet A for thickness 114-116mm is rolled, milled sheet A working modulus is 22-23%；Then the rolling of small working modulus multi-pass is carried out
(plate of sauntering), passage number is 6-8 passage in the rolling of the small working modulus multi-pass, is rolled as with a thickness of 109-112mm's
Milled sheet；
(3) timeliness: the hot rolled plate that step (2) is obtained carries out 170-180 DEG C of ageing treatment 22-26h, obtains space flight and aviation use
ZK61M magnesium alloy.
The present invention can not to the higher index request of plate three-dimensional mechanical property, single rolling or forging processing method
Touch the mark the performance of requirement, and the rectangle ingot production of ZK61M is difficult, and ingot casting is also not easy hot rolling, but in the blank after forging
Portion's tissue becomes worked structure from cast sturcture, and hot-working relatively easily rolls, also, in order to meet final material
Can, when forging, will carry out three directions forging and stamping, and when hot rolling finally carries out plate of sauntering, therefore the present invention uses forging+hot rolling group
Conjunction processing method is equipped with necessary aging strengthening model again and can be only achieved aerospace material requested performance.
Embodiment 2
A kind of space flight and aviation ZK61M magnesium alloy, it is through the following steps that be prepared:
(1) it forges: the ZK61M circle ingot casting for meeting YS/T 627-2013 deformed Mg and magnesium alloy circle ingot casting standard is heated
Forging, circle cast ingot dimension be diameter be Φ 450mm, length 700mm, heating temperature be 420 DEG C, heating time 16 hours, forging
First the circle ingot casting that length is 700mm is forged and pressed to 400mm when making, is then forged and pressed again for rectangle, then in length, width, height
The forging ratio that three directions are all made of 15 is forged, and final forging temperature is 350 DEG C, is finally forged to the forging plate of 150mm thickness；?
It materialses on the plate of 150mm thickness, room-temperature mechanical property such as table 2(test data three times).
As seen from Table 2, user's technology is not satisfied in the magnesium alloy tensile strength after forging, regulation disproportional intensity three-dimensional performance
Index request, and three-dimensional is uneven, elongation percentage three-dimensional, which also has, is unsatisfactory for aerospace user requirement.So primary forging life
The big plate of the magnesium alloy of production is not able to satisfy aerospace user requirement.
(2) hot rolling: then the forging plate that step (1) is obtained carries out steering rolling, first by 150mm in 400 DEG C of heating 8h
The plate that thick forging plate axial rolling is thickness 139mm, then turns to the plate that transverse rolling is thickness 128mm, and turning again to axial rolling is thickness
The plate of 121mm is ultimately steering to the milled sheet A that transverse rolling is thickness 115mm, and milled sheet A working modulus is 23%, then carries out small processing
The rolling of 6 passage of rate rolls as the forging plate with a thickness of 110mm, and always plus power is 26%.
Finishing temperature is also used to carry out the rolling of small working modulus multi-pass to having a competition for 360 DEG C, 370 DEG C in experimentation
It tests, other steps are identical, materials on the 110mm plate rolled at different temperatures；Room-temperature mechanical property such as table 3(is tested three times
Data).
As seen from Table 3, the rolling performance of 350 DEG C of small working modulus multi-pass on milling train is better than 360 DEG C and 370 DEG C, and rolling is thick
Degree is the ZK61M plate of 110mm, and by the change of process flow, length three-dimensional is forged, rolls test, and it is reasonable to determine
Forging and rolling mode, optimize the technological parameter of forging and rolling, produce the qualified products for meeting customer performance requirements.
But to effectively eliminate magnesium plate internal stress, also to pass through aging strengthening model.
(3) timeliness: the hot rolled plate that step (2) is obtained carries out 180 DEG C of ageing treatments for 24 hours, obtains space flight and aviation ZK61M
Magnesium alloy.
Also use aging strengthening model temperature for 190 DEG C of aging strengthening model comparative test in experimentation, other step phases
Together, the hot rolled plate obtained at different temperatures is materialsed, room-temperature mechanical property such as table 4(test data twice).
As seen from Table 4, ZK61M plate after 180 DEG C of aging strengthening models is micro- to have mentioned product tensile strength, the ZK61M plate of production
It is able to satisfy aerospace magnesium alloy materials requirement.
Embodiment 3
A kind of space flight and aviation ZK61M magnesium alloy, it is through the following steps that be prepared:
(1) it forges: the ZK61M circle ingot casting for meeting YS/T 627-2013 deformed Mg and magnesium alloy circle ingot casting standard is heated
Forging, it be Φ 300mm length is 650mm that circle cast ingot dimension, which is diameter, and heating temperature is 420 DEG C, heating time 14 hours, forging
When first the circle ingot casting that length is 650mm is forged and pressed to 300mm, then circle is forged and pressed for rectangle, then in length, width, height again
It spends three directions to be forged using 11 forging ratio, final forging temperature is 350 DEG C, is finally forged to the forging plate of 150mm thickness；
(2) hot rolling: then the forging plate that step (1) is obtained carries out steering rolling in 400 DEG C of heating 7h, first that 150mm is thick
The plate that plate axial rolling is thickness 138mm is forged, the plate that transverse rolling is thickness 127mm is then turned to, turning again to axial rolling is thickness 120mm's
Plate is ultimately steering to the milled sheet A that transverse rolling is thickness 115mm, and milled sheet A working modulus is 23%, then carries out small 8 passage of working modulus
Rolling, roll as the forging plate with a thickness of 110mm, always plus power is 26%；
(3) timeliness: the hot rolled plate that step (2) is obtained carries out 180 DEG C of ageing treatment 23h, obtains the conjunction of space flight and aviation ZK61M magnesium
Gold, performance is as shown in table 5, meets aerospace user requirement.
Embodiment 4
A kind of space flight and aviation ZK61M magnesium alloy, it is through the following steps that be prepared:
(1) it forges: the ZK61M circle ingot casting for meeting YS/T 627-2013 deformed Mg and magnesium alloy circle ingot casting standard is heated
Forging, it be Φ 350mm length is 680mm that circle cast ingot dimension, which is diameter, and heating temperature is 420 DEG C, heating time 15 hours, forging
When first the circle ingot casting that length is 680mm is forged and pressed to 320mm, the then garden Zai Jiang forging and stamping are rectangle, then in length, width, height
It spends three directions to be forged using 12 forging ratio, final forging temperature is 350 DEG C, is finally forged to the forging plate of 150mm thickness；
(2) hot rolling: then the forging plate that step (1) is obtained carries out steering rolling in 400 DEG C of heating 7h, first that 150mm is thick
The plate that plate axial rolling is thickness 138mm is forged, the plate that transverse rolling is thickness 127mm is then turned to, turning again to axial rolling is thickness 120mm's
Plate is ultimately steering to the milled sheet A that transverse rolling is thickness 116mm, and milled sheet A working modulus is 22.6%, then carries out small working modulus 7
Secondary rolling rolls as the forging plate with a thickness of 109mm, and always plus power is 27%；
(3) timeliness: the hot rolled plate that step (2) is obtained carries out 182 DEG C of ageing treatment 23h, obtains the conjunction of space flight and aviation ZK61M magnesium
Gold, performance is as shown in table 6, meets aerospace user requirement.
Claims (6)
1. a kind of space flight and aviation ZK61M magnesium alloy, it is characterised in that it is through the following steps that be prepared:
(1) it forges: the ZK61M circle ingot casting for meeting YS/T 627-2013 deformed Mg and magnesium alloy circle ingot casting standard is heated
Forging, heating temperature are 420-430 DEG C, and heating time 13-16 hour carries out when forging in length, width, highly three directions
Forging, final forging temperature be not less than 350 DEG C, obtain forging plate；
(2) hot rolling: then the forging plate that step (1) is obtained carries out steering rolling, is rolled in 400-420 DEG C of heating 6-9h
Then making sheet A carries out the rolling of small working modulus multi-pass at 345-355 DEG C of temperature, finally obtaining total plus power is 26-27%'s
Hot rolled plate；
(3) timeliness: the hot rolled plate that step (2) is obtained carries out 170-180 DEG C of ageing treatment 22-26h, obtains space flight and aviation use
ZK61M magnesium alloy.
2. space flight and aviation as described in claim 1 ZK61M magnesium alloy, it is characterised in that step (1) length, width,
The forging ratio that highly three directions are all made of 10-20 is forged.
3. space flight and aviation as described in claim 1 ZK61M magnesium alloy, it is characterised in that step (1) the ZK61M circle ingot casting
Diameter is Φ 300-500mm, length 600-700mm, is finally forged to the forging plate of 150-155mm thickness, and when forging will first be grown
Degree is that the circle ingot casting of 600-700mm is forged and pressed to 300-400mm, then again will circle forging and stamping are flat forges and presses for rectangle, then in length, width
Three degree, height directions are forged.
4. space flight and aviation as described in claim 1 ZK61M magnesium alloy, it is characterised in that after the step (2) turns to rolling
The milled sheet A working modulus of acquisition is 22-23%, then carries out the rolling of small working modulus multi-pass again, finally obtains always plus power is
The hot rolled plate of 26-27%.
5. space flight and aviation as claimed in claim 3 ZK61M magnesium alloy, it is characterised in that the step (2) turns to rolling tool
Gymnastics as: the plate for being first thickness 137-141mm by the thick forging plate axial rolling of 150-155mm, then turning to transverse rolling is thickness
The plate of 126-130mm turns again to the plate that axial rolling is thickness 119-123mm, is ultimately steering to the rolling that transverse rolling is thickness 114-116mm
Then plate A carries out the rolling of small working modulus multi-pass, roll as the milled sheet with a thickness of 109-112mm.
6. space flight and aviation as claimed in claim 5 ZK61M magnesium alloy, it is characterised in that the small working modulus multi-pass rolls
Passage number is not less than 6-8 passage in system.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910131231.9A CN109666879B (en) | 2019-02-22 | 2019-02-22 | ZK61M magnesium alloy for aerospace |
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| CN201910131231.9A CN109666879B (en) | 2019-02-22 | 2019-02-22 | ZK61M magnesium alloy for aerospace |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115323296A (en) * | 2022-08-25 | 2022-11-11 | 中铝洛阳铜加工有限公司 | Processing method of wide-width high-performance magnesium alloy plate |
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| CN102321836A (en) * | 2011-10-12 | 2012-01-18 | 中南大学 | Method for preparing high-strength heat-resistant magnesium alloy sheet |
| CN105951010A (en) * | 2016-05-06 | 2016-09-21 | 江苏科技大学 | High-strength high-damping-performance magnesium alloy sheet and preparation method thereof |
| CN107649628A (en) * | 2017-09-19 | 2018-02-02 | 陕西华镁特材科技有限公司 | A kind of processing method of ZK61 high-strength magnesium alloys forging |
| WO2018132134A1 (en) * | 2017-01-11 | 2018-07-19 | The Boeing Company | Calcium-bearing magnesium and rare earth element alloy and method for manufacturing the same |
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2019
- 2019-02-22 CN CN201910131231.9A patent/CN109666879B/en active Active
Patent Citations (5)
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| JP2010116618A (en) * | 2008-11-14 | 2010-05-27 | Univ Of Electro-Communications | Method for manufacturing magnesium alloy material |
| CN102321836A (en) * | 2011-10-12 | 2012-01-18 | 中南大学 | Method for preparing high-strength heat-resistant magnesium alloy sheet |
| CN105951010A (en) * | 2016-05-06 | 2016-09-21 | 江苏科技大学 | High-strength high-damping-performance magnesium alloy sheet and preparation method thereof |
| WO2018132134A1 (en) * | 2017-01-11 | 2018-07-19 | The Boeing Company | Calcium-bearing magnesium and rare earth element alloy and method for manufacturing the same |
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| WANG XIN ET.AL: "Microstructure refining and property improvement of ZK60 magnesium alloy by hot rolling", 《TRANS. NONFERROUS MET. SOC. CHINA》 * |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115323296A (en) * | 2022-08-25 | 2022-11-11 | 中铝洛阳铜加工有限公司 | Processing method of wide-width high-performance magnesium alloy plate |
| CN115323296B (en) * | 2022-08-25 | 2024-03-12 | 中铝洛阳铜加工有限公司 | Processing method of wide magnesium alloy plate |
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Effective date of registration: 20220701 Address after: 471000 Room 201, building 1, No. 22, Binhe Road, high tech Industrial Development Zone, Luoyang area, China (Henan) pilot Free Trade Zone, Luoyang City, Henan Province Patentee after: Luoyang MAG Magnesium Industry Co.,Ltd. Address before: Economic Development Zone, Yiyang County, Luoyang City, Henan Province Patentee before: LUOYANG HUA LING MAGNESIUM INDUSTRY CO.,LTD. |
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