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CN109576058A - A kind of cumin flavor essence and its preparation method and application for cigarette dripping pill - Google Patents

A kind of cumin flavor essence and its preparation method and application for cigarette dripping pill Download PDF

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Publication number
CN109576058A
CN109576058A CN201811564976.6A CN201811564976A CN109576058A CN 109576058 A CN109576058 A CN 109576058A CN 201811564976 A CN201811564976 A CN 201811564976A CN 109576058 A CN109576058 A CN 109576058A
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China
Prior art keywords
cumin
cigarette
flavor essence
essence
cigarettes
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Pending
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CN201811564976.6A
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Chinese (zh)
Inventor
王娜
赵国豪
熊国玺
马舒翼
肜霖
董爱君
董世良
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Priority to CN201811564976.6A priority Critical patent/CN109576058A/en
Publication of CN109576058A publication Critical patent/CN109576058A/en
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/02—Manufacture of tobacco smoke filters
    • A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
    • A24D3/0212—Applying additives to filter materials
    • A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/022—Refining
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/025—Recovery by solvent extraction

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

本发明提供的一种用于烟用滴丸的孜然风味香精及其制备方法和应用。所述茴香风味香精是由94.5‑97.9％的孜然提取物、0.1‑0.5％的枯茗醛和2.0‑5.0％的肉豆蔻酸乙酯；其中，所述孜然提取物是以孜然籽为原料，将其粉碎后加入其重量比6‑8倍量的辛癸酸甘油酯，在油浴温度120～150℃的条件下热回流1h～1.5h，之后将其超声处理10‑30min后离心取上清液过滤，得到。本发明提供的一种用于烟用滴丸的孜然风味香精，具有较好的工艺适配性，提高了孜然风味烟用滴丸的生产效率和成品率、降低其生产成本；易于在卷烟应用中，丰富了卷烟香气，赋予卷烟特征风味，具有很强的实用性和应用价值。The invention provides a cumin flavor essence for cigarette dropping pills and a preparation method and application thereof. The fennel flavor essence is composed of 94.5-97.9% cumin extract, 0.1-0.5% cuminaldehyde and 2.0-5.0% ethyl myristate; wherein, the cumin extract is cumin seed As raw materials, pulverize it and add 6-8 times its weight ratio of glyceryl caprylic acid, heat reflux for 1h-1.5h under the condition of oil bath temperature of 120-150°C, and then ultrasonically treat it for 10-30min. The supernatant was collected by centrifugation and filtered. The cumin flavor essence for cigarette dripping pills provided by the invention has good technological adaptability, improves the production efficiency and yield of cumin flavor cigarette dripping pills, and reduces the production cost; In the application of cigarettes, the aroma of cigarettes is enriched, the characteristic flavor of cigarettes is given, and it has strong practicability and application value.

Description

A kind of cumin flavor essence and its preparation method and application for cigarette dripping pill
Technical field
The present invention relates to technical field of cigarette flavors, in particular to a kind of cumin flavor essence for cigarette dripping pill And its preparation method and application.
Background technique
As cigarette consumption demand is gradually from type, enjoying type is met to novel sex reversal, the demand to cigarette is by past list One sucks hobby, gradually forms a variety of demands such as healthy, safe and environment-friendly, consumer not only focuses on the comfort of cigarette smoking With pleasant sexual experience, and with the raising of cigarette consumption structure, consumer is in terms of the novelty of cigarette, specificity, otherness Demand further enhance.
Compared with traditional cigarette flavoring technology, cigarette is to inhale not by burning in abundant cigarette with the essence that dripping pill adds It is small on the influence of cigarette entirety comfortable taste while food taste, imparting cigarette characteristic flavor on basis, it can also be achieved in smoking property of cigarette mistake What fragrance discharged in journey is artificial controllable.Meanwhile cigarette improves the experience of consumer from more sense organ dimensions such as tactile, the sense of hearing with dripping pill Sense.Cigarette is in the gesture of accelerated development with application of the dripping pill flavoring in cigarette in recent years, becomes and pulls cigarette quality, sales volume and structure The bright spot of promotion.
In the prior art, cigarette is common due to more or less having the flavor deployments such as alcohol, propylene glycol and water with dripping pill essence Solvent, technique suitability is relatively low, causes that cigarette dripping pill production efficiency is relatively low, yield rate is relatively low, production cost is universal higher etc. Problem more or less constrains the further application and development of cigarette dripping pill.Therefore, it is necessary to from improve cigarette dripping pill essence technique Suitability is started with, and the new technology of cigarette dripping pill flavor deployment is developed.
Summary of the invention
It is an object of that present invention to provide a kind of cumin flavor essence for cigarette dripping pill, abundant smoking property of cigarette taste, While assigning cigarette characteristic flavor on basis, there is preferable technique suitability, improve the production efficiency of cumin flavor cigarette dripping pill With yield rate, reduce its production cost.
The present invention is achieved through the following technical solutions: a kind of cumin flavor essence for cigarette dripping pill, It is characterized in that the fennel taste essence is by with the material composition of mass percent: the Cuminum cyminum extract of 94.5-97.9%, The ethyl myristate of the cumal of 0.1-0.5%, 2.0-5.0%；
Wherein, the Cuminum cyminum extract be using cumin seed as raw material, be added after being crushed 6-8 times of its weight ratio measure it is pungent It is by glycerol decanoate, heat reflux 1h~1.5h under conditions of 120~150 DEG C of oil bath temperature in ultrasonic power later 150-250W/L, supersonic frequency are ultrasonically treated centrifugal treating 20-30min after 10-30min under conditions of being 20-25kHz, take Clear liquid uses 0.2-0.8 microns of membrane filtration, is clarified, transparent filtrate is Cuminum cyminum extract.
The further technical solution of the present invention: the fennel taste essence of cigarette dripping pill is by with the object of mass percent Matter composition: the Cuminum cyminum extract of 96.0-97.5%, the cumal of 0.2-0.3%, 2.3-3.7% ethyl myristate.
A kind of preparation method of cumin flavor essence for cigarette dripping pill provided by the invention, it is characterised in that specific step It is rapid as follows:
(1) Glycerin, mixed triester with caprylic acid capric acid of 6-8 times of its weight is added after crushing cumin seed, then in oil bath temperature 120~150 Heat reflux 2h~2.5h under conditions of DEG C；
(2) material after hot reflow treatment in step (1) is subjected to ultrasonic treatment 10-30min, ultrasonic power 150- 250W/L, supersonic frequency 20-25kHz；
(3) material after ultrasonic treatment in step (2) is centrifuged 20-30min under conditions of revolving speed 500-2000rpm, It takes supernatant to use 0.2-0.8 microns of membrane filtration, is clarified, transparent filtrate is Cuminum cyminum extract；
(4) prepare raw material according to following mass percent formula: the Cuminum cyminum extract of 94.5-97.9%, 0.1-0.5% The ethyl myristate of cumal, 2.0-5.0%；Above-mentioned raw materials component is uniformly mixed stirring 1~3 hour, is then allowed to stand 24 Fennel taste essence is obtained after~48 hours.
The present invention preferably technical solution: the particle that cumin seed crushes as 40~80 mesh in the step (1).
The application of a kind of cumin flavor essence for cigarette dripping pill provided by the invention, it is characterised in that: will be above-mentioned diligent Right flavor essence is added in the essence tank of pill dripping machine, regulates essence pump discharge, then with the drop that is placed in pill dripping machine rubber cement tank Ball lapping and be placed in contain ball device in curing agent according to the preparation process of existing cigarette dripping pill be made weight be 3~ 10mg, crushing strength are 0.3kPa~2.0kPa, and diameter is the cigarette dripping pill of 2~5mm；In cigarette filter wire-beam forming process In, the cigarette dripping pill positioning of preparation is applied in filter rod, and cigarette is made.
The cumin is commercially available conventional food seasoning, and Glycerin, mixed triester with caprylic acid capric acid, cumal, ethyl myristate are commercially available normal See food additives.
Cumin flavor essence in the present invention selects Cuminum cyminum extract as cumin flavor main body and basis, assigns cumin wind Taste essence is strong and the pungent perfume (or spice) of natural cumin；It selects cumal to modify, increases the sense of equilibrium and the persistence of cumin flavor；Choosing Made further to increase the mellow and full sense of cumin flavor with conjunction and coordination with ethyl myristate.The cumin flavor essence assigns volume The pungent Flavor feature for the cumin that cigarette is coordinated enriches cigarette flavor, while promoting the smooth sense and pleasant feeling of flue gas.
Compared with prior art, the flavor essence for being used for cigarette dripping pill in the prior art more or less has alcohol, third The flavor deployments common solvent such as two alcohol and waters, and the alcohol, propylene glycol and water equal size in flavor essence directly affect dripping pill drop Type is made, the more low then dripping pill dripping molding effect of the alcohol, propylene glycol and water equal size in flavor essence is better, yield rate more It is high.Body material used in cumin flavor essence in the present invention is the Cuminum cyminum extract that Glycerin, mixed triester with caprylic acid capric acid directly extracts, no Spirituosity, propylene glycol and water, not spirituosity, propylene glycol and the water, and institute such as other related component cumals and ethyl myristate The not additional alcohol of cumin flavor essence, propylene glycol and water equal solvent are stated, therefore, the cumin flavor essence is in cigarette dripping pill dripping Technique suitability is good in forming process, easily package pelletization, and cracky, production are not stablized, and dripping yield rate improves 20-30%, has Effect reduces cigarette dripping pill production cost.
A kind of cumin flavor essence for cigarette dripping pill provided by the invention has preferable technique suitability, improves The production efficiency and yield rate of cumin flavor cigarette dripping pill reduce its production cost；It is easy in cigarette application, enriches volume Cigarette perfume gas assigns cigarette characteristic flavor on basis, has very strong practicability and application value.
Specific embodiment
Explanation is further explained to the present invention below with reference to embodiment.
Cuminum cyminum extract employed in following embodiments, prepares as follows:
(1) cumin seed is crushed as the particle of 40-60 mesh, weighs the cumin particle of constant weight, by weight being added 8 times It measures (weight ratio) Glycerin, mixed triester with caprylic acid capric acid (ODO), oil bath heat reflux 1.5h at 150 DEG C；
(2) material in step (1) is subjected to ultrasonic treatment 30min, ultrasonic power 250W/L, supersonic frequency 25kHz；
(3) material after ultrasonic treatment in step (2) is subjected to centrifugal treating, revolving speed 1000rpm, 20min take supernatant Liquid.The membrane filtration that supernatant is used to 0.2 micron, is clarified, transparent filtrate is Cuminum cyminum extract.
A kind of cumin flavor essence for cigarette dripping pill that embodiment 1 provides, is by the substance of following mass percent Composition: 94.5% Cuminum cyminum extract, 0.5% cumal, 5.0% ethyl myristate.The raw material of above-mentioned mass fraction Component is uniformly mixed stirring 2 hours, is then allowed to stand after 48 hours and obtains cumin flavor essence A.
The cumin flavor essence A drop that will be prepared in embodiment 1 using pill dripping machine according to the preparation process of existing cigarette dripping pill Cigarette dripping pill is made, by existing filter stick production technology, positioning applies cigarette dripping pill during cigarette filter rod wire-beam forming, and makes It is cumin flavor dripping pill cigarette at cigarette.
A kind of cumin flavor essence for cigarette dripping pill that embodiment 2 provides, is by the substance of following mass percent Composition: 96.3% Cuminum cyminum extract, 0.2% cumal, 3.5% ethyl myristate.The raw material of above-mentioned mass fraction Component is uniformly mixed stirring 2 hours, is then allowed to stand after 48 hours and obtains cumin flavor essence B.
The cumin flavor essence B drop that will be prepared in embodiment 2 using pill dripping machine according to the preparation process of existing cigarette dripping pill Cigarette dripping pill is made, by existing filter stick production technology, positioning applies cigarette dripping pill during cigarette filter rod wire-beam forming, and makes It is cumin flavor dripping pill cigarette at cigarette.
A kind of cumin flavor essence for cigarette dripping pill that embodiment 3 provides, is by the substance of following mass percent Composition: 97.5% Cuminum cyminum extract, 0.1% cumal, 2.4% ethyl myristate.The raw material of above-mentioned mass fraction Component is uniformly mixed stirring 2 hours, is then allowed to stand after 48 hours and obtains cumin flavor essence C.
The cumin flavor essence C drop that will be prepared in embodiment 3 using pill dripping machine according to the preparation process of existing cigarette dripping pill Cigarette dripping pill is made, by existing filter stick production technology, positioning applies cigarette dripping pill during cigarette filter rod wire-beam forming, and makes It is cumin flavor dripping pill cigarette at cigarette.
Comparative test 1: applicant is using being currently used in dripping pill apricot flavor essence according to technique identical with embodiment Cigarette dripping pill is prepared, and is existed for apricot flavor essence A, B, C and existing apricot flavor essence of the preparation in three embodiments Knitting technology adaptive data when preparing dripping pill is detected, and the results are shown in Table 1:
The test knot of the cumin flavor essence and existing flavor essence knitting technology suitability that are prepared in 1 three embodiments of table Fruit
Carry out the cumin flavor essence of the method preparation in the application as can be seen from Table 1 during preparing dripping pill, thereon Machine technique suitability is more preferable.
Comparative test, to cumin flavor dripping pill cigarette prepared by the embodiment of the present invention 1~3, by 7 professional sensory evaluations Personnel's reference examples blank cigarette sample (same position adds blank dripping pill) compares suction evaluation.Analyses Methods for Sensory Evaluation Results is shown in Table 2。
2 three kinds of cumin flavor dripping pill cigarette sample Analyses Methods for Sensory Evaluation Results of table
Show that the cumin flavor essence in the present invention assigns the pungent fragrant breeze for the cumin that cigarette is coordinated by smoking result in table 2 Taste feature enriches cigarette flavor, while improving the smooth sense and pleasant feeling of flue gas.
Present inventor detects for the Cuminum cyminum extract prepared in embodiment through physical index, and concrete outcome is such as Under:
By the above results it can be seen that the Cuminum cyminum extract items physical index prepared in the present invention meets cigarette perfume The index of material.
Present inventor detects for the Cuminum cyminum extract prepared in embodiment through physical index, and concrete outcome is such as Under:
Project Detected value
Appearance Clarify glassy yellow oily liquids
Fragrance The pungent perfume (or spice) of mellow, warm and natural cumin
Relative density (20/20 DEG C) 0.9425
Refraction index (20 DEG C) 1.4543
Miscible degree (25 DEG C) It can be miscible with the ODO of arbitrary volume
Lead content (mg/kg) ≤5.0
Arsenic content (mg/kg) ≤1.0
By testing result it can be seen that the cumin flavor essence items physics for cigarette dripping pill prepared in the present invention Index meets the index of flavouring essence for tobacco.

Claims (5)

1.一种用于烟用滴丸的孜然风味香精，其特征在于所述茴香风味香精是由以质量百分比的物质组成：94.5-97.9％的孜然提取物、0.1-0.5％的枯茗醛、2.0-5.0％的肉豆蔻酸乙酯；1. a cumin flavor essence for tobacco dripping pills, is characterized in that described fennel flavor essence is made up of the material with mass percentage: 94.5-97.9% cumin extract, 0.1-0.5% cumin Aldehyde, 2.0-5.0% ethyl myristate; 其中，所述孜然提取物是以孜然籽为原料，将其粉碎后加入其重量比6-8倍量的辛癸酸甘油酯，在油浴温度120～150℃的条件下热回流1h～1.5h，之后将其在超声功率为150-250W/L，超声频率为20-25kHz的条件下超声处理10-30min后离心处理20-30min，取上清液采用0.2-0.8微米的滤膜过滤，得到澄清、透明的滤液即为孜然提取物。Wherein, the cumin extract is made from cumin seeds, crushed and then added with 6-8 times the weight of caprylic acid glyceride, and refluxed under the condition of oil bath temperature of 120-150° C. for 1 hour. ~1.5h, then ultrasonically treated for 10-30min under the condition of ultrasonic power of 150-250W/L and ultrasonic frequency of 20-25kHz, then centrifuged for 20-30min, and the supernatant was taken with a filter membrane of 0.2-0.8 microns. Filtration to obtain a clear, transparent filtrate is the cumin extract. 2.根据权利要求1所述的一种用于烟用滴丸的孜然风味香精，其特征在于所述烟用滴丸的茴香风味香精是由以质量百分比的物质组成：96.0-97.5％的孜然提取物、0.2-0.3％的枯茗醛、2.3-3.7％的肉豆蔻酸乙酯。2. a kind of cumin flavor essence for cigarette dropping pills according to claim 1, is characterized in that the fennel flavor essence of described cigarette dropping pills is made up of the material with mass percentage: 96.0-97.5% Cumin extract, 0.2-0.3% cuminaldehyde, 2.3-3.7% ethyl myristate. 3.一种权利要求1中所述的用于烟用滴丸的孜然风味香精的制备方法，其特征在于具体步骤如下：3. the preparation method of the cumin flavor essence for cigarette dropping pills described in claim 1, is characterized in that concrete steps are as follows: (1)将孜然籽粉碎后加入其重量6-8倍的辛癸酸甘油酯，然后在油浴温度120～150℃的条件下热回流2h～2.5h；(1) After crushing the cumin seeds, add 6-8 times the weight of caprylic acid glyceride, and then heat under the condition of oil bath temperature of 120～150℃ for 2h～2.5h; (2)将步骤(1)中热回流处理后的物料进行超声处理10-30min，超声功率为150-250W/L，超声频率为20-25kHz；(2) carrying out ultrasonic treatment 10-30min to the material after heat reflux treatment in step (1), ultrasonic power is 150-250W/L, ultrasonic frequency is 20-25kHz; (3)将步骤(2)中超声处理后的物料在转速500-2000rpm的条件下离心20-30min，取上清液采用0.2-0.8微米的滤膜过滤，得到澄清、透明的滤液即为孜然提取物；(3) centrifuge the material after the ultrasonic treatment in step (2) for 20-30min under the condition of rotating speed 500-2000rpm, take the supernatant and filter it with a filter membrane of 0.2-0.8 microns, and obtain a clarified and transparent filtrate, which is cumin natural extract; (4)按照以下质量百分比配方准备原料：94.5-97.9％的孜然提取物、0.1-0.5％的枯茗醛、2.0-5.0％的肉豆蔻酸乙酯；将上述原料组分混合均匀搅拌1～3小时，然后静置24～48小时后即得到茴香风味香精。(4) Prepare raw materials according to the following mass percentage formula: 94.5-97.9% cumin extract, 0.1-0.5% cuminaldehyde, 2.0-5.0% ethyl myristate; mix the above-mentioned raw material components evenly and stir for 1 ～3 hours, and then stand for 24～48 hours to obtain the fennel flavor essence. 4.根据权利要求3所示的一种用于烟用滴丸的孜然风味香精的制备方法，其特征在于具体步骤如下：所述步骤(1)中孜然籽粉碎为40～80目的颗粒。4. according to a kind of preparation method of the cumin flavor essence for cigarette dropping pills shown in claim 3, it is characterized in that the concrete steps are as follows: in the described step (1), the cumin seeds are pulverized into 40～80 purpose granules . 5.一种权利要求1或2中所述的用于烟用滴丸的孜然风味香精的应用，其特征在于：将上述孜然风味香精加入滴丸机的香精罐内，调节好香精泵流量，然后与置于滴丸机胶浆罐中的滴丸包裹材料以及置于盛丸器中的固化剂按照现有烟用滴丸的制备工艺制成重量为3～10mg，压碎强度为0.3kPa～2.0kPa，直径为2～5mm的烟用滴丸；在卷烟滤嘴丝束成型过程中，将制备的烟用滴丸定位施加到滤嘴棒中，并制成卷烟。5. the application of the cumin flavor essence described in claim 1 or 2 for dropping pills for cigarettes, is characterized in that: above-mentioned cumin flavor essence is added in the essence tank of the pill dropping machine, and the essence pump is adjusted well The flow rate is then combined with the dripping pill wrapping material placed in the mortar tank of the dripping pill machine and the curing agent placed in the pill holder according to the existing preparation process of the dripping pills for cigarettes. The weight is 3～10mg, and the crushing strength is 0.3kPa～2.0kPa, 2～5mm diameter drop pills for cigarettes; in the process of forming the cigarette filter tow, the prepared drop pills for cigarettes are positioned and applied to the filter rod, and the cigarettes are made.
CN201811564976.6A 2018-12-20 2018-12-20 A kind of cumin flavor essence and its preparation method and application for cigarette dripping pill Pending CN109576058A (en)

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