CN109266977A - A kind of oil fracturing pump forging process method - Google Patents
A kind of oil fracturing pump forging process method Download PDFInfo
- Publication number
- CN109266977A CN109266977A CN201811201491.0A CN201811201491A CN109266977A CN 109266977 A CN109266977 A CN 109266977A CN 201811201491 A CN201811201491 A CN 201811201491A CN 109266977 A CN109266977 A CN 109266977A
- Authority
- CN
- China
- Prior art keywords
- forging
- furnace
- quenching
- refining
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000005242 forging Methods 0.000 title claims abstract description 47
- 238000000034 method Methods 0.000 title claims abstract description 41
- 230000008569 process Effects 0.000 title claims abstract description 23
- 239000002994 raw material Substances 0.000 claims abstract description 24
- 238000004544 sputter deposition Methods 0.000 claims abstract description 18
- 229910052761 rare earth metal Inorganic materials 0.000 claims abstract description 11
- 150000002910 rare earth metals Chemical class 0.000 claims abstract description 11
- 229910001069 Ti alloy Inorganic materials 0.000 claims abstract description 6
- 238000009497 press forging Methods 0.000 claims abstract description 6
- 238000005477 sputtering target Methods 0.000 claims abstract description 6
- 239000013077 target material Substances 0.000 claims abstract description 6
- 229910052718 tin Inorganic materials 0.000 claims abstract description 6
- 229910052726 zirconium Inorganic materials 0.000 claims abstract description 6
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910052593 corundum Inorganic materials 0.000 claims abstract description 5
- 229910001845 yogo sapphire Inorganic materials 0.000 claims abstract description 5
- 238000010791 quenching Methods 0.000 claims description 50
- 230000000171 quenching effect Effects 0.000 claims description 50
- 238000007670 refining Methods 0.000 claims description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 35
- 239000002893 slag Substances 0.000 claims description 31
- 239000007921 spray Substances 0.000 claims description 26
- 238000005507 spraying Methods 0.000 claims description 24
- 238000010891 electric arc Methods 0.000 claims description 18
- 238000004321 preservation Methods 0.000 claims description 15
- 238000005496 tempering Methods 0.000 claims description 11
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 10
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 10
- 238000009749 continuous casting Methods 0.000 claims description 10
- 238000005516 engineering process Methods 0.000 claims description 10
- 239000007789 gas Substances 0.000 claims description 7
- 238000003754 machining Methods 0.000 claims description 6
- 239000005997 Calcium carbide Substances 0.000 claims description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 5
- 229910052684 Cerium Inorganic materials 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 229910052693 Europium Inorganic materials 0.000 claims description 5
- 229910052688 Gadolinium Inorganic materials 0.000 claims description 5
- 229910052777 Praseodymium Inorganic materials 0.000 claims description 5
- 229910052772 Samarium Inorganic materials 0.000 claims description 5
- 238000003723 Smelting Methods 0.000 claims description 5
- 229910052771 Terbium Inorganic materials 0.000 claims description 5
- 229910052782 aluminium Inorganic materials 0.000 claims description 5
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 5
- 229910052786 argon Inorganic materials 0.000 claims description 5
- 229910052799 carbon Inorganic materials 0.000 claims description 5
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 claims description 5
- 238000007872 degassing Methods 0.000 claims description 5
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 238000006477 desulfuration reaction Methods 0.000 claims description 5
- 230000023556 desulfurization Effects 0.000 claims description 5
- 230000003009 desulfurizing effect Effects 0.000 claims description 5
- 239000000428 dust Substances 0.000 claims description 5
- OGPBJKLSAFTDLK-UHFFFAOYSA-N europium atom Chemical compound [Eu] OGPBJKLSAFTDLK-UHFFFAOYSA-N 0.000 claims description 5
- UIWYJDYFSGRHKR-UHFFFAOYSA-N gadolinium atom Chemical compound [Gd] UIWYJDYFSGRHKR-UHFFFAOYSA-N 0.000 claims description 5
- 239000004615 ingredient Substances 0.000 claims description 5
- 238000009847 ladle furnace Methods 0.000 claims description 5
- 229910052746 lanthanum Inorganic materials 0.000 claims description 5
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims description 5
- 229910052751 metal Inorganic materials 0.000 claims description 5
- 239000002184 metal Substances 0.000 claims description 5
- 238000003801 milling Methods 0.000 claims description 5
- 230000003647 oxidation Effects 0.000 claims description 5
- 238000007254 oxidation reaction Methods 0.000 claims description 5
- 230000001590 oxidative effect Effects 0.000 claims description 5
- PUDIUYLPXJFUGB-UHFFFAOYSA-N praseodymium atom Chemical compound [Pr] PUDIUYLPXJFUGB-UHFFFAOYSA-N 0.000 claims description 5
- 238000010079 rubber tapping Methods 0.000 claims description 5
- KZUNJOHGWZRPMI-UHFFFAOYSA-N samarium atom Chemical compound [Sm] KZUNJOHGWZRPMI-UHFFFAOYSA-N 0.000 claims description 5
- GZCRRIHWUXGPOV-UHFFFAOYSA-N terbium atom Chemical compound [Tb] GZCRRIHWUXGPOV-UHFFFAOYSA-N 0.000 claims description 5
- CLZWAWBPWVRRGI-UHFFFAOYSA-N tert-butyl 2-[2-[2-[2-[bis[2-[(2-methylpropan-2-yl)oxy]-2-oxoethyl]amino]-5-bromophenoxy]ethoxy]-4-methyl-n-[2-[(2-methylpropan-2-yl)oxy]-2-oxoethyl]anilino]acetate Chemical compound CC1=CC=C(N(CC(=O)OC(C)(C)C)CC(=O)OC(C)(C)C)C(OCCOC=2C(=CC=C(Br)C=2)N(CC(=O)OC(C)(C)C)CC(=O)OC(C)(C)C)=C1 CLZWAWBPWVRRGI-UHFFFAOYSA-N 0.000 claims description 5
- 239000010936 titanium Substances 0.000 claims description 5
- 230000014759 maintenance of location Effects 0.000 claims description 4
- 230000005611 electricity Effects 0.000 claims description 3
- 238000007664 blowing Methods 0.000 claims 1
- 239000003595 mist Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 238000003860 storage Methods 0.000 abstract description 5
- 230000009471 action Effects 0.000 abstract description 2
- 230000001351 cycling effect Effects 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 230000002708 enhancing effect Effects 0.000 description 4
- 239000003208 petroleum Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 241001085205 Prenanthella exigua Species 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/16—Ferrous alloys, e.g. steel alloys containing copper
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/18—Hardening; Quenching with or without subsequent tempering
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/26—Methods of annealing
- C21D1/28—Normalising
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/005—Modifying the physical properties by deformation combined with, or followed by, heat treatment of ferrous alloys
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/002—Ferrous alloys, e.g. steel alloys containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/005—Ferrous alloys, e.g. steel alloys containing rare earths, i.e. Sc, Y, Lanthanides
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/008—Ferrous alloys, e.g. steel alloys containing tin
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/14—Ferrous alloys, e.g. steel alloys containing titanium or zirconium
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/06—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
- C23C14/14—Metallic material, boron or silicon
- C23C14/16—Metallic material, boron or silicon on metallic substrates or on substrates of boron or silicon
- C23C14/165—Metallic material, boron or silicon on metallic substrates or on substrates of boron or silicon by cathodic sputtering
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
- C23C14/35—Sputtering by application of a magnetic field, e.g. magnetron sputtering
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Forging (AREA)
Abstract
The present invention provides a kind of oil fracturing pump forging process method, comprising the following steps: (1) raw material is refined: by quality proportioning are as follows: Cu:2%-5%, Mg:2%-6%, Sn:1%-3%, Zr:0.1%-0.5%, Si0.1%-0.5%, Mn0.2%-0.6%, SiC particulate: 14%-16%, rare earth: 0.05%-0.2%, TiB3%-8%, Al2O31%-5%, the raw material that surplus is Fe are mixed, are refined；(2) blank is cast: (3) high tonnage hydraulic press forging: (4) heat treatment: (5) precision machine adds: (6) forging surface sputtering: by complete examination, qualified products storage, factory, sputtering target material is titanium alloy.The present invention improves inner surface hardness, strength and toughness is kept simultaneously, make its both antiscour, anti scuffing, it is not likely to produce seminess again under the action of cycling alternating load, and sputtered by forging surface, integral strength performance is improved, service life is extended, reduces production cost, reduce security risk in processing, is simple process, practical.
Description
Technical field
The present invention relates to oil fracturings to pump spare and accessory parts processing technique field, and specially a kind of oil fracturing pumps forging process side
Method.
Background technique
Currently, fracturing technique can effectively improve the yield of petroleum, shale gas in petroleum, shale gas exploitation field,
Fracturing pump is the key equipment in pressure break recovery process.According to the 12nd five-year-plan outline pair of national economy and social development
Manufacturing industry is promoted, optimizes structure, quality of making better products, improves fundamental technology, improves basic material R & D Level, realizing and close
The related requirement of key components technology automation etc., especially country promote production capacity to petroleum vapour well, increase yield
It is required that it is higher and higher, it is also higher and higher to the technical requirements of fracturing pump.
The performance of fracturing pump, q&r directly affect the quality and progress of pressure break implementation process, because of fracturing pump
Applying working condition it is very severe, it is desirable that fracturing pump has higher pump pressure and bigger discharge capacity, it is desirable that it is able to bear high pressure, circulation carries
Lotus effect, also require its can conveying high-pressure band medium for tempering, corroding, more require that it can reliability service be simultaneously under severe operating condition again
Keep higher service life.There is relatively high requirement particularly with Fracturing Pump Valve Box body, it is desirable that pump valve cabinet is not only wanted
The pressure of superelevation is born, and to bear higher alternating load impact force and acid-alkali-corrosive-resisting power.So to meet above-mentioned want
It asks the selection it is necessary to the material to pump valve cabinet, process for machining and manufacturing to improve, captures technical problem.
Summary of the invention
Technical problem solved by the invention is to provide a kind of oil fracturing pump forging process method, to solve above-mentioned back
The problems in scape technology.
Technical problem solved by the invention is realized using following technical scheme: a kind of oil fracturing pump forging process side
Method, comprising the following steps:
(1) raw material is refined: by quality proportioning are as follows: Cu:2%-5%, Mg:2%-6%, Sn:1%-3%, Zr:0.1%-
0.5%, Si0.1%-0.5%, Mn0.2%-0.6%, SiC particulate: 14%-16%, rare earth: 0.05%-0.2%, TiB3%-
8%, Al2O31%-5%, the raw material that surplus is Fe are mixed, are refined；
(2) blank is cast: raw material is blown after electric arc furnaces just refines and carries out pretreatment desulfurizing using converter process dephosphorizing technology
Refining is skimmed, and RH furnace vacuum circulation degassing is utilized after LF refined-smelting ladle furnace deep desulfurization, and round billet continuous casting forms continuous casting billet, and enhancing product is strong
Degree；
(3) high tonnage hydraulic press forging: using high-quality ESR ingot as raw material, forging is carried out using 8000 tons of water hydraulic presses
Three-phase forging, ensure that forging stock ingredient is uniform, even tissue is fine and close；
(4) it is heat-treated: by multiple normalizing, oil quenching, high tempering, ensure that stress sufficiently discharges and even tissue；
(5) accurate machine adds: work obtains finished product after refining, milling the accurate machining processes such as boring；
(6) forging surface sputters: first air pressure in magnetron sputtered vacuum equipment being evacuated to less than 2 × 10-3Pa is passed through argon later
Gas, turn-on flow rate meter make to close charge valve when air pressure is about 0.8Pa in vacuum chamber, sputtering bias-voltage are adjusted to -50--250V, is splashed
Radio stream is adjusted to 3-6A, deposits closing sputtering voltage and bias after 3-6h after rotating metal wheel；By complete examination, qualified products
Storage, factory, sputtering target material is titanium alloy.
Raw material refining includes: that electric arc furnaces just refines in the step (1): using slag operation is changed, the heat of oxidation terminates to flow out electric furnace
Whole oxidizing slags renew slag, it is ensured that electric arc furnaces terminal Ti≤0.0008%, P≤0.0060%；Electric arc furnaces slag free tapping；LF essence
Refining: the control of LF refining basicity of slag uses calcium carbide that carbon dust is added to be diffused deoxidation during 1.5-2.0, LF refining, and white slag is kept
Time 10-30 minute；RH vacuum refining: in vacuum degree 67Pa hereinafter, vacuum is kept for 15-20 minutes；Vacuum refining terminates first 5 points
Clock adds aluminum shot and increases Al to target value.
In the step (1) rare earth be quality proportioning lanthanum 10%, cerium 30%, praseodymium 20%, samarium 10%, europium 10%, gadolinium 10%,
Terbium 10%.
Step (4) heat treatment includes: first normalizing: workpiece being heated to 750 DEG C of heat preservations 15-20 minutes, from furnace
It takes out in air or water spray, spraying or quenching is to 200-300 DEG C；Normalizing again: workpiece is heated to 850 DEG C of heat preservations
It 15-20 minutes, is taken out from furnace in air or water spray, spraying or quenching is to 200-300 DEG C；Normalizing three times: by workpiece
950 DEG C of heat preservations 15-20 minutes are heated to, is taken out from furnace in air or water spray, spraying or quenching is to 200-300 DEG C；
Oil quenching: workpiece is heated to 920 DEG C of progress oil quenchings and is taken out from furnace in air or water spray, spraying or quenching
To 200-300 DEG C；By workpiece be heated to 780 DEG C of oil quenchings taken out from furnace in air or water spray, spraying or quenching to
200-300℃；
High tempering: after part oil quenching, 500~650 DEG C are heated to, 20-30 minutes are kept the temperature, to reduce by 20 per minute
DEG C speed be cooled to room temperature.
It is described before the sputtering of forging surface, successively forging surface is carried out by acetone, dehydrated alcohol and deionized water clear
It washes.
Be compared to open technology, there are following advantages by the present invention: the present invention improves inner surface hardness, while keeping intensity
Toughness makes its both antiscour, anti scuffing, is not likely to produce seminess again under the action of cycling alternating load, and pass through forging table
Face sputtering, improve integral strength performance, extend service life, reduce production cost, reduce processing in safety it is hidden
It is trouble, simple process, practical.
Specific embodiment
In order to make, technological means of the invention, creation characteristic, workflow, application method reach purpose and effect is easy to bright
White understanding, below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
In the description of the present invention, it should be noted that unless otherwise clearly defined and limited, term " installation ", " company ", " connection "
It shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or be integrally connected to be mechanical connection,
It is also possible to be electrically connected；It can be directly connected, can also indirectly connected through an intermediary, it can company inside two elements
It is logical, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the present invention
In embodiment, every other implementation obtained by those of ordinary skill in the art without making creative efforts
Example, shall fall within the protection scope of the present invention.
Embodiment 1
A kind of oil fracturing pump forging process method, comprising the following steps:
(1) raw material refine: by quality proportioning are as follows: Cu:2%, Mg:2%, Sn:1%, Zr:0.1%, Si0.1%,
Mn0.2%, SiC particulate: 14%, rare earth: 0.05%, TiB3%, Al2O31%, surplus is that the raw material of Fe is mixed, refined；
Electric arc furnaces just refines: for electric furnace using changing slag operation, the heat of oxidation, which terminates to flow out whole oxidizing slags, renews slag, it is ensured that and electric arc furnaces terminal Ti≤
0.0008%, P≤0.0060%；Electric arc furnaces slag free tapping；LF refining: LF refining basicity of slag is controlled in 1.5-2.0, LF refining mistake
Carbon dust is added to be diffused deoxidation using calcium carbide in journey, the white slag retention time 10-30 minutes；RH vacuum refining: in vacuum degree 67Pa
Hereinafter, vacuum is kept for 15-20 minutes；Vacuum refining terminates first 5 minutes addition aluminum shots and increases Al to target value
(2) blank is cast: raw material is blown after electric arc furnaces just refines and carries out pretreatment desulfurizing using converter process dephosphorizing technology
Refining is skimmed, and RH furnace vacuum circulation degassing is utilized after LF refined-smelting ladle furnace deep desulfurization, and round billet continuous casting forms continuous casting billet, and enhancing product is strong
Degree；
(3) high tonnage hydraulic press forging: using high-quality ESR ingot as raw material, forging is carried out using 8000 tons of water hydraulic presses
Three-phase forging, ensure that forging stock ingredient is uniform, even tissue is fine and close；
(4) it is heat-treated: by multiple normalizing, oil quenching, high tempering, ensure that stress sufficiently discharges and even tissue；Just
Secondary normalizing: being heated to 750 DEG C of heat preservations 15-20 minutes for workpiece, takes out in air or sprays water from furnace, spraying or quenching
To 200-300 DEG C；Normalizing again: being heated to 850 DEG C of heat preservations 15-20 minutes for workpiece, take out in air or spray water from furnace,
Spraying or quenching is to 200-300 DEG C；Normalizing three times: workpiece is heated to 950 DEG C of heat preservations 15-20 minutes, is taken out from furnace
In air or water spray, spraying or quenching are to 200-300 DEG C；
Oil quenching: workpiece is heated to 920 DEG C of progress oil quenchings and is taken out from furnace in air or water spray, spraying or quenching
To 200-300 DEG C；By workpiece be heated to 780 DEG C of oil quenchings taken out from furnace in air or water spray, spraying or quenching to
200-300℃；
High tempering: after part oil quenching, 500~650 DEG C are heated to, 20-30 minutes are kept the temperature, to reduce by 20 per minute
DEG C speed be cooled to room temperature.
(5) accurate machine adds: work obtains finished product after refining, milling the accurate machining processes such as boring；
(6) forging surface sputters: first air pressure in magnetron sputtered vacuum equipment being evacuated to less than 2 × 10-3Pa is passed through argon later
Gas, turn-on flow rate meter make to close charge valve when air pressure is about 0.8Pa in vacuum chamber, sputtering bias-voltage are adjusted to -50--250V, is splashed
Radio stream is adjusted to 3-6A, deposits closing sputtering voltage and bias after 3-6h after rotating metal wheel；By complete examination, qualified products
Storage, factory, sputtering target material is titanium alloy.
Rare earth is quality proportioning lanthanum 10%, cerium 30%, praseodymium 20%, samarium 10%, europium 10%, gadolinium 10%, terbium in the present embodiment
10%.It is described forging surface sputtering before, successively forging surface is cleaned by acetone, dehydrated alcohol and deionized water.
Embodiment 2
A kind of oil fracturing pump forging process method, comprising the following steps:
(1) raw material refine: by quality proportioning are as follows: Cu:5%, Mg:6%, Sn:3%, Zr:0.5%, Si0.5%,
Mn0.6%, SiC particulate: 16%, rare earth: 0.2%, TiB8%, Al2O35%, surplus is that the raw material of Fe is mixed, refined；Electricity
Arc furnace just refines: for electric furnace using changing slag operation, the heat of oxidation, which terminates to flow out whole oxidizing slags, renews slag, it is ensured that and electric arc furnaces terminal Ti≤
0.0008%, P≤0.0060%；Electric arc furnaces slag free tapping；LF refining: LF refining basicity of slag is controlled in 1.5-2.0, LF refining mistake
Carbon dust is added to be diffused deoxidation using calcium carbide in journey, the white slag retention time 10-30 minutes；RH vacuum refining: in vacuum degree 67Pa
Hereinafter, vacuum is kept for 15-20 minutes；Vacuum refining terminates first 5 minutes addition aluminum shots and increases Al to target value
(2) blank is cast: raw material is blown after electric arc furnaces just refines and carries out pretreatment desulfurizing using converter process dephosphorizing technology
Refining is skimmed, and RH furnace vacuum circulation degassing is utilized after LF refined-smelting ladle furnace deep desulfurization, and round billet continuous casting forms continuous casting billet, and enhancing product is strong
Degree；
(3) high tonnage hydraulic press forging: using high-quality ESR ingot as raw material, forging is carried out using 8000 tons of water hydraulic presses
Three-phase forging, ensure that forging stock ingredient is uniform, even tissue is fine and close；
(4) it is heat-treated: by multiple normalizing, oil quenching, high tempering, ensure that stress sufficiently discharges and even tissue；Just
Secondary normalizing: being heated to 750 DEG C of heat preservations 15-20 minutes for workpiece, takes out in air or sprays water from furnace, spraying or quenching
To 200-300 DEG C；Normalizing again: being heated to 850 DEG C of heat preservations 15-20 minutes for workpiece, take out in air or spray water from furnace,
Spraying or quenching is to 200-300 DEG C；Normalizing three times: workpiece is heated to 950 DEG C of heat preservations 15-20 minutes, is taken out from furnace
In air or water spray, spraying or quenching are to 200-300 DEG C；
Oil quenching: workpiece is heated to 920 DEG C of progress oil quenchings and is taken out from furnace in air or water spray, spraying or quenching
To 200-300 DEG C；By workpiece be heated to 780 DEG C of oil quenchings taken out from furnace in air or water spray, spraying or quenching to
200-300℃；
High tempering: after part oil quenching, 500~650 DEG C are heated to, 20-30 minutes are kept the temperature, to reduce by 20 per minute
DEG C speed be cooled to room temperature.
(5) accurate machine adds: work obtains finished product after refining, milling the accurate machining processes such as boring；
(6) forging surface sputters: first air pressure in magnetron sputtered vacuum equipment being evacuated to less than 2 × 10-3Pa is passed through argon later
Gas, turn-on flow rate meter make to close charge valve when air pressure is about 0.8Pa in vacuum chamber, sputtering bias-voltage are adjusted to -50--250V, is splashed
Radio stream is adjusted to 3-6A, deposits closing sputtering voltage and bias after 3-6h after rotating metal wheel；By complete examination, qualified products
Storage, factory, sputtering target material is titanium alloy.
Rare earth is quality proportioning lanthanum 10%, cerium 30%, praseodymium 20%, samarium 10%, europium 10%, gadolinium 10%, terbium in the present embodiment
10%.It is described forging surface sputtering before, successively forging surface is cleaned by acetone, dehydrated alcohol and deionized water.
Embodiment 3
A kind of oil fracturing pump forging process method, comprising the following steps:
(1) raw material refine: by quality proportioning are as follows: Cu:3%, Mg:4%, Sn:2%, Zr:0.3%, Si0.3%,
Mn0.5%, SiC particulate: 15%, rare earth: 0.1%, TiB5%, Al2O33%, the raw material that surplus is Fe are mixed, are refined；Electricity
Arc furnace just refines: for electric furnace using changing slag operation, the heat of oxidation, which terminates to flow out whole oxidizing slags, renews slag, it is ensured that and electric arc furnaces terminal Ti≤
0.0008%, P≤0.0060%；Electric arc furnaces slag free tapping；LF refining: LF refining basicity of slag is controlled in 1.5-2.0, LF refining mistake
Carbon dust is added to be diffused deoxidation using calcium carbide in journey, the white slag retention time 10-30 minutes；RH vacuum refining: in vacuum degree 67Pa
Hereinafter, vacuum is kept for 15-20 minutes；Vacuum refining terminates first 5 minutes addition aluminum shots and increases Al to target value
(2) blank is cast: raw material is blown after electric arc furnaces just refines and carries out pretreatment desulfurizing using converter process dephosphorizing technology
Refining is skimmed, and RH furnace vacuum circulation degassing is utilized after LF refined-smelting ladle furnace deep desulfurization, and round billet continuous casting forms continuous casting billet, and enhancing product is strong
Degree；
(3) high tonnage hydraulic press forging: using high-quality ESR ingot as raw material, forging is carried out using 8000 tons of water hydraulic presses
Three-phase forging, ensure that forging stock ingredient is uniform, even tissue is fine and close；
(4) it is heat-treated: by multiple normalizing, oil quenching, high tempering, ensure that stress sufficiently discharges and even tissue；Just
Secondary normalizing: being heated to 750 DEG C of heat preservations 15-20 minutes for workpiece, takes out in air or sprays water from furnace, spraying or quenching
To 200-300 DEG C；Normalizing again: being heated to 850 DEG C of heat preservations 15-20 minutes for workpiece, take out in air or spray water from furnace,
Spraying or quenching is to 200-300 DEG C；Normalizing three times: workpiece is heated to 950 DEG C of heat preservations 15-20 minutes, is taken out from furnace
In air or water spray, spraying or quenching are to 200-300 DEG C；
Oil quenching: workpiece is heated to 920 DEG C of progress oil quenchings and is taken out from furnace in air or water spray, spraying or quenching
To 200-300 DEG C；By workpiece be heated to 780 DEG C of oil quenchings taken out from furnace in air or water spray, spraying or quenching to
200-300℃；
High tempering: after part oil quenching, 500~650 DEG C are heated to, 20-30 minutes are kept the temperature, to reduce by 20 per minute
DEG C speed be cooled to room temperature.
(5) accurate machine adds: work obtains finished product after refining, milling the accurate machining processes such as boring；
(6) forging surface sputters: first air pressure in magnetron sputtered vacuum equipment being evacuated to less than 2 × 10-3Pa is passed through argon later
Gas, turn-on flow rate meter make to close charge valve when air pressure is about 0.8Pa in vacuum chamber, sputtering bias-voltage are adjusted to -50--250V, is splashed
Radio stream is adjusted to 3-6A, deposits closing sputtering voltage and bias after 3-6h after rotating metal wheel；By complete examination, qualified products
Storage, factory, sputtering target material is titanium alloy.
Rare earth is quality proportioning lanthanum 10%, cerium 30%, praseodymium 20%, samarium 10%, europium 10%, gadolinium 10%, terbium in the present embodiment
10%.It is described forging surface sputtering before, successively forging surface is cleaned by acetone, dehydrated alcohol and deionized water.
The above shows and describes the basic principle, main features and advantages of the invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.Claimed range of the invention by appended claims and
Its equivalent thereof.
Claims (5)
1. a kind of oil fracturing pumps forging process method, it is characterised in that: the following steps are included:
(1) raw material refine: by quality proportioning are as follows: Cu:2%-5%, Mg:2%-6%, Sn:1%-3%, Zr:0.1%-0.5%,
Si0.1%-0.5%, Mn0.2%-0.6%, SiC particulate: 14%-16%, rare earth: 0.05%-0.2%, TiB3%-8%,
Al2O31%-5%, the raw material that surplus is Fe are mixed, are refined；
(2) blank is cast: raw material is taken off after electric arc furnaces just refines and carries out pretreatment desulfurizing using the blowing of converter process dephosphorizing technology
Slag utilizes RH furnace vacuum circulation degassing after LF refined-smelting ladle furnace deep desulfurization, and round billet continuous casting forms continuous casting billet, enhances product strength；
(3) high tonnage hydraulic press forging: using high-quality ESR ingot as raw material, forging carries out three-phase using 8000 tons of water hydraulic presses
Forging, ensure that forging stock ingredient is uniform, even tissue is fine and close；
(4) it is heat-treated: by multiple normalizing, oil quenching, high tempering, ensure that stress sufficiently discharges and even tissue；
(5) accurate machine adds: work obtains finished product after refining, milling the accurate machining processes such as boring；
(6) forging surface sputters: first air pressure in magnetron sputtered vacuum equipment being evacuated to less than 2 × 10-3Pa is passed through argon gas later,
Turn-on flow rate meter makes to close charge valve when air pressure is about 0.8Pa in vacuum chamber, and sputtering bias-voltage is adjusted to -50--250V, sputtering electricity
Stream is adjusted to 3-6A, deposits closing sputtering voltage and bias after 3-6h after rotating metal wheel；By complete examination, qualified products enter
Library, factory, sputtering target material are titanium alloy.
2. a kind of oil fracturing according to claim 1 pumps forging process method, it is characterised in that: in the step (1)
Raw material refining includes: that electric arc furnaces just refines: for electric furnace using changing slag operation, the heat of oxidation, which terminates to flow out whole oxidizing slags, renews slag, it is ensured that
Electric arc furnaces terminal Ti≤0.0008%, P≤0.0060%；Electric arc furnaces slag free tapping；LF refining: the control of LF refining basicity of slag exists
1.5-2.0 uses during LF refining calcium carbide that carbon dust is added to be diffused deoxidation, and the white slag retention time 10-30 minutes；RH vacuum fine
Refining: in vacuum degree 67Pa hereinafter, vacuum is kept for 15-20 minutes；Vacuum refining terminates first 5 minutes addition aluminum shots and increases Al to target
Value.
3. a kind of oil fracturing according to claim 1 pumps forging process method, it is characterised in that: in the step (1)
Rare earth is quality proportioning lanthanum 10%, cerium 30%, praseodymium 20%, samarium 10%, europium 10%, gadolinium 10%, terbium 10%.
4. a kind of oil fracturing according to claim 1 pumps forging process method, it is characterised in that: step (4) heat
Processing includes: first normalizing: workpiece being heated to 750 DEG C of heat preservations 15-20 minutes, takes out in air or sprays water from furnace, spray
Mist or quenching are to 200-300 DEG C；Normalizing again: being heated to 850 DEG C of heat preservations 15-20 minutes for workpiece, takes out from furnace
In air or water spray, spraying or quenching are to 200-300 DEG C；Normalizing three times: workpiece is heated to 950 DEG C of heat preservation 15-20 points
Clock takes out in air from furnace or water spray, spraying or quenching is to 200-300 DEG C；
Oil quenching: by workpiece be heated to 920 ° of c carry out oil quenchings taken out from furnace in air or water spray, spraying or quenching to
200-300℃；Workpiece is heated to 780 ° of c oil quenchings to take out from furnace in air or water spray, spraying or quenching to 200-
300℃；
High tempering: after part oil quenching, 500~650 DEG C are heated to, 20-30 minutes are kept the temperature, to reduce by 20 DEG C per minute
Speed is cooled to room temperature.
5. a kind of oil fracturing according to claim 1 pumps forging process method, it is characterised in that: described on forging surface
Before sputtering, successively forging surface is cleaned by acetone, dehydrated alcohol and deionized water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811201491.0A CN109266977A (en) | 2018-10-16 | 2018-10-16 | A kind of oil fracturing pump forging process method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811201491.0A CN109266977A (en) | 2018-10-16 | 2018-10-16 | A kind of oil fracturing pump forging process method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109266977A true CN109266977A (en) | 2019-01-25 |
Family
ID=65196988
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811201491.0A Pending CN109266977A (en) | 2018-10-16 | 2018-10-16 | A kind of oil fracturing pump forging process method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109266977A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109877541A (en) * | 2019-03-25 | 2019-06-14 | 马鞍山旭阳机械有限公司 | A kind of manufacture craft of stainless steel Fracturing Pump Valve Box |
| CN111687369A (en) * | 2020-07-30 | 2020-09-22 | 江阴南工锻造有限公司 | Forging method of petroleum valve block for fracturing pump |
| CN112226700A (en) * | 2020-10-30 | 2021-01-15 | 濮阳市成豫机械配件制造有限公司 | Production process of part for fracturing of oil exploitation equipment |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1236822A (en) * | 1999-06-11 | 1999-12-01 | 武汉机械工艺研究所 | Technology for manufacturing iron- or steel-base composite material |
| CN102978579A (en) * | 2012-12-11 | 2013-03-20 | 上海工程技术大学 | Preparation method of Ta (Tantalum) film on bearing steel surface |
| CN107904486A (en) * | 2017-10-11 | 2018-04-13 | 马鞍山市天马冶金材料有限公司 | A kind of manufacturing process of fracturing pump forging |
-
2018
- 2018-10-16 CN CN201811201491.0A patent/CN109266977A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1236822A (en) * | 1999-06-11 | 1999-12-01 | 武汉机械工艺研究所 | Technology for manufacturing iron- or steel-base composite material |
| CN102978579A (en) * | 2012-12-11 | 2013-03-20 | 上海工程技术大学 | Preparation method of Ta (Tantalum) film on bearing steel surface |
| CN107904486A (en) * | 2017-10-11 | 2018-04-13 | 马鞍山市天马冶金材料有限公司 | A kind of manufacturing process of fracturing pump forging |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109877541A (en) * | 2019-03-25 | 2019-06-14 | 马鞍山旭阳机械有限公司 | A kind of manufacture craft of stainless steel Fracturing Pump Valve Box |
| CN111687369A (en) * | 2020-07-30 | 2020-09-22 | 江阴南工锻造有限公司 | Forging method of petroleum valve block for fracturing pump |
| CN111687369B (en) * | 2020-07-30 | 2022-03-01 | 江阴南工锻造有限公司 | Forging method of petroleum valve block for fracturing pump |
| CN112226700A (en) * | 2020-10-30 | 2021-01-15 | 濮阳市成豫机械配件制造有限公司 | Production process of part for fracturing of oil exploitation equipment |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108660381B (en) | A kind of low-cost manufacture method for protecting Q345B grades of steel plates of flaw detection | |
| CN102409138B (en) | A manufacturing process of alloy steel for track frogs | |
| CN113186465A (en) | Low-alloy cast steel, smelting method and heat treatment method thereof and railway locomotive part | |
| CN109266977A (en) | A kind of oil fracturing pump forging process method | |
| CN107686871B (en) | Production method of non-quenched and tempered steel | |
| CN116426812B (en) | Manufacturing method of electrolytic aluminum cathode flat steel | |
| CN113088623A (en) | Preparation method of ultrapure G102Cr18Mo stainless bearing steel | |
| CN109825762A (en) | A kind of high-speed high-performance bearing steel and preparation method thereof | |
| EP4375390A1 (en) | Hot-rolled, low-temperature-resistant, h-shaped steel with grade of yield strength of 420 mpa, and preparation method therefor | |
| CN107236894A (en) | A kind of method for making steel of low-sulfur, low titanium Aluminum steel | |
| CN109112398A (en) | A kind of chrome-bearing alloy bar and preparation method thereof | |
| CN107904486A (en) | A kind of manufacturing process of fracturing pump forging | |
| CN103627971A (en) | Alloy structural steel for large-specification soldering tools and smelting method thereof | |
| CN1995403A (en) | Double-slag converter process for producing high carbon low-phosphorus molten steel | |
| CN109161650B (en) | Low-alloy cast steel, manufacturing method and application thereof | |
| CN111485164B (en) | Casting method for enhancing wear resistance of low-chromium alloy casting | |
| CN116426827B (en) | A cast complex phase steel material suitable for semi-autogenous mill lining and preparation method thereof | |
| CN116536584A (en) | GGP300 hot-rolled round steel for load bearing shaft and preparation method thereof | |
| CN1420189A (en) | Process for vacuum induction smelting Ti-Al alloy | |
| CN111304414A (en) | Method for reducing tempering embrittlement tendency of 2.25Cr-1Mo steel | |
| CN109877541A (en) | A kind of manufacture craft of stainless steel Fracturing Pump Valve Box | |
| CN114807558B (en) | Production method of EX50V round steel for mine drill bit | |
| CN118957412A (en) | A high-strength steel hot rolling preparation process | |
| CN108842039A (en) | A kind of Roll Collar production method based on WC hard alloy | |
| CN115449704A (en) | Steel for new energy automobile hub bearing and production method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190125 |
|
| RJ01 | Rejection of invention patent application after publication |