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CN109203155A - A kind of preparation method of asepsis environment-protecting wood veneer preservative - Google Patents

A kind of preparation method of asepsis environment-protecting wood veneer preservative Download PDF

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Publication number
CN109203155A
CN109203155A CN201811154539.7A CN201811154539A CN109203155A CN 109203155 A CN109203155 A CN 109203155A CN 201811154539 A CN201811154539 A CN 201811154539A CN 109203155 A CN109203155 A CN 109203155A
Authority
CN
China
Prior art keywords
parts
added
preservative
wood veneer
powder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201811154539.7A
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Chinese (zh)
Inventor
钱雪峰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Huzhou Yun Gao Wood Industry Co Ltd
Original Assignee
Huzhou Yun Gao Wood Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Huzhou Yun Gao Wood Industry Co Ltd filed Critical Huzhou Yun Gao Wood Industry Co Ltd
Priority to CN201811154539.7A priority Critical patent/CN109203155A/en
Publication of CN109203155A publication Critical patent/CN109203155A/en
Withdrawn legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52Impregnating agents containing mixtures of inorganic and organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/007Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process employing compositions comprising nanoparticles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment
    • B27K2240/20Removing fungi, molds or insects

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Chemical And Physical Treatments For Wood And The Like (AREA)

Abstract

The invention discloses a kind of preparation methods of asepsis environment-protecting wood veneer preservative, and each raw material is in terms of mass parts, comprising the following steps: A, clean to cloves, rosemary respectively and dry, ball milling obtains Ground Cloves and rosemary powder;B, deionized water is added in blender and is used as bottom water, fatty alcohol polyoxyethylene ether and Lauryl Diethanolamine is added, is dispersed with stirring;C, trimethylborate, butyl carbamate, imidacloprid and Traditional Chinese medicine bacteriostatic agent are sequentially added into blender, are stirred, ultrasonic disperse;D, Ground Cloves and rosemary powder, stirring are added in heating process for heating water bath;E, the mixed solution in step D is cooled to room temperature, ultrasonic disperse, stands, obtains preservative finished product.The present invention has the advantages that environmental friendliness height, concise in technology, at low cost.

Description

A kind of preparation method of asepsis environment-protecting wood veneer preservative
Technical field
The present invention relates to wood preservation technical field, especially a kind of preparation side of asepsis environment-protecting wood veneer preservative Method.
Background technique
The preservative pervasive environments friendliness having currently on the market is poor, has micro toxicity for the human body, especially It is to directly influence indoor air quality coated in the preservative on the surfacings such as wood veneer, with the development of the times, The preservative of asepsis environment-protecting is a general orientation of current preservative development, and the preparation side of asepsis environment-protecting wood veneer preservative Innovation of the law develops at present relatively delays, and existing timber preservative preparation process is relatively complicated, and higher cost, in preparation process In be easy to produce pollution environment by-product.Therefore, a kind of preparation method of asepsis environment-protecting wood veneer preservative is needed, to make Standby asepsis environment-protecting wood veneer preservative.
Summary of the invention
The object of the present invention is to provide a kind of preparation methods of asepsis environment-protecting wood veneer preservative.It has environment Friendliness height, concise in technology, advantage at low cost.
Technical solution of the present invention: a kind of preparation method of asepsis environment-protecting wood veneer preservative, each raw material is with mass parts Meter, comprising the following steps:
A, respectively cloves, rosemary clean and be dried, with 200-240r/min ball milling 2-3h, obtain Ground Cloves and fan Repeatedly face powder;
B, 150 parts of deionized waters are added in blender and are used as bottom water, while 5 parts of fatty alcohol polyoxyethylene ether and 7 are added Part Lauryl Diethanolamine, is heated to 40-46 DEG C, is dispersed with stirring, mixing speed 2200-2600r/min, and when stirring is a length of 30-40min;
C, 40 parts of trimethylborates, 8 parts of butyl carbamates are sequentially added into blender, in 16 parts of imidacloprids and 10 parts Medicine bacteriostatic agent is heated to 48-52 DEG C after being all added, and stirs 25-35min with the mixing speed of 2500-3000r/min, Then ultrasonic disperse 15-20min;
D, the mixed solution in step C is poured out to glass container, water is carried out to glass container using 55-60 DEG C of temperature Bath is heated, and 4 parts of Ground Cloves obtained in step A and 6 parts of rosemary powder is slowly added in heating process, with 2000-2400r/ The mixing speed of min stirs 35-45min;
E, the mixed solution in step D is cooled to room temperature, ultrasonic disperse 5-10min, stand 2-3h, obtain preservative at Product.
In a kind of preparation method of asepsis environment-protecting wood veneer preservative above-mentioned, 4 parts of Ground Cloves and 6 in the step D First mixed-powder is added to glass container again after mixing for part rosemary powder.
In a kind of preparation method of asepsis environment-protecting wood veneer preservative above-mentioned, the Traditional Chinese medicine bacteriostatic agent includes micro-nano Coptis root powder, diatomite and cinnamon oil.
In a kind of preparation method of asepsis environment-protecting wood veneer preservative above-mentioned, the micro-nano coptis root powder, diatom The weight part ratio of soil and cinnamon oil is 2:5:8.
Compared with prior art, the present invention is with trimethylborate, rosemary powder, Ground Cloves, fatty alcohol polyoxyethylene ether, the moon Osmanthus base diethanol amine, Traditional Chinese medicine bacteriostatic agent, imidacloprid, butyl carbamate and deionized water are to prepare raw material, first will be in blender Middle addition water, fatty alcohol polyoxyethylene ether and Lauryl Diethanolamine, form a kind of solution with certain consistency, sequentially add Trimethylborate, butyl carbamate, imidacloprid and Traditional Chinese medicine bacteriostatic agent, above-mentioned material inherently have good deinsectization sterilization effect Fruit, preservative set obtained is a variety of a little after being mixed in a certain ratio, and heating is improved mixing speed, made using ultrasonic disperse Solution mixing is more uniform, then Ground Cloves and rosemary powder is added down to glass container heating water bath in above-mentioned mixed solution, can So that adding the wood veneer after preservative produced by the present invention increases delicate fragrant, wood veneer is not necessarily to after adding preservative It stands and carries out dissipating taste for a period of time, can accomplish to produce and sell, finally carry out ultrasonic disperse again, stand to obtain preservative finished product, Whole preparation process concise in technology, at low cost, raw material of the present invention is environmentally protective, and whole preparation process does not generate pollution environment By-product, through preservative produced by the present invention be similarly green, asepsis environment-protecting.
To sum up, the present invention has the advantages that environmental friendliness height, concise in technology, at low cost.
Specific embodiment
Below with reference to embodiment, the present invention is further illustrated, but is not intended as the foundation limited the present invention.
Embodiment 1: a kind of preparation method of asepsis environment-protecting wood veneer preservative, each raw material in terms of mass parts, including with Lower step:
A, respectively cloves, rosemary clean and be dried, with 200r/min ball milling 2h, obtain Ground Cloves and rosemary Powder;
B, 150 parts of deionized waters are added in blender and are used as bottom water, while 5 parts of fatty alcohol polyoxyethylene ether and 7 are added Part Lauryl Diethanolamine, is heated to 40 DEG C, is dispersed with stirring, mixing speed 2200r/min, when stirring a length of 30min;
C, 40 parts of trimethylborates, 8 parts of butyl carbamates are sequentially added into blender, in 16 parts of imidacloprids and 10 parts Medicine bacteriostatic agent is heated to 48 DEG C after being all added, and stirs 25min with the mixing speed of 2500r/min, then ultrasonic disperse 15min;
D, the mixed solution in step C is poured out to glass container, water-bath is carried out to glass container using 55 DEG C of temperature It heats, 4 parts of Ground Cloves obtained in step A and 6 parts of rosemary powder is slowly added in heating process, with stirring for 2000r/min Mix speed stirring 35min;
E, the mixed solution in step D is cooled to room temperature, ultrasonic disperse 5min, stands 2h, obtains preservative finished product.
Mixed-powder is first added to glass again after mixing and holds by 4 parts of Ground Cloves and 6 parts of rosemary powder in the step D Device.
The Traditional Chinese medicine bacteriostatic agent includes micro-nano coptis root powder, diatomite and cinnamon oil.
The weight part ratio of the micro-nano coptis root powder, diatomite and cinnamon oil is 2:5:8.
Embodiment 2: a kind of preparation method of asepsis environment-protecting wood veneer preservative, each raw material in terms of mass parts, including with Lower step:
A, respectively cloves, rosemary clean and be dried, with 240r/min ball milling 3h, obtain Ground Cloves and rosemary Powder;
B, 150 parts of deionized waters are added in blender and are used as bottom water, while 5 parts of fatty alcohol polyoxyethylene ether and 7 are added Part Lauryl Diethanolamine, is heated to 46 DEG C, is dispersed with stirring, mixing speed 2600r/min, when stirring a length of 40min;
C, 40 parts of trimethylborates, 8 parts of butyl carbamates are sequentially added into blender, in 16 parts of imidacloprids and 10 parts Medicine bacteriostatic agent is heated to 52 DEG C after being all added, and stirs 35min with the mixing speed of 3000r/min, then ultrasonic disperse 20min;
D, the mixed solution in step C is poured out to glass container, water-bath is carried out to glass container using 60 DEG C of temperature It heats, 4 parts of Ground Cloves obtained in step A and 6 parts of rosemary powder is slowly added in heating process, with stirring for 2400r/min Mix speed stirring 45min;
E, the mixed solution in step D is cooled to room temperature, ultrasonic disperse 10min, stands 3h, obtains preservative finished product.
Mixed-powder is first added to glass again after mixing and holds by 4 parts of Ground Cloves and 6 parts of rosemary powder in the step D Device.
The Traditional Chinese medicine bacteriostatic agent includes micro-nano coptis root powder, diatomite and cinnamon oil.
The weight part ratio of the micro-nano coptis root powder, diatomite and cinnamon oil is 2:5:8.
Embodiment 3: a kind of preparation method of asepsis environment-protecting wood veneer preservative, each raw material in terms of mass parts, including with Lower step:
A, respectively cloves, rosemary clean and be dried, with 220r/min ball milling 2.5h, obtain Ground Cloves and rosemary Powder;
B, 150 parts of deionized waters are added in blender and are used as bottom water, while 5 parts of fatty alcohol polyoxyethylene ether and 7 are added Part Lauryl Diethanolamine, is heated to 43 DEG C, is dispersed with stirring, mixing speed 2400r/min, when stirring a length of 35min;
C, 40 parts of trimethylborates, 8 parts of butyl carbamates are sequentially added into blender, in 16 parts of imidacloprids and 10 parts Medicine bacteriostatic agent is heated to 50 DEG C after being all added, and stirs 30min with the mixing speed of 2800r/min, then ultrasonic disperse 18min;
D, the mixed solution in step C is poured out to glass container, water-bath is carried out to glass container using 57 DEG C of temperature It heats, 4 parts of Ground Cloves obtained in step A and 6 parts of rosemary powder is slowly added in heating process, with stirring for 2200r/min Mix speed stirring 40min;
E, the mixed solution in step D is cooled to room temperature, ultrasonic disperse 8min, stands 2.5h, obtains preservative finished product.
Mixed-powder is first added to glass again after mixing and holds by 4 parts of Ground Cloves and 6 parts of rosemary powder in the step D Device.
The Traditional Chinese medicine bacteriostatic agent includes micro-nano coptis root powder, diatomite and cinnamon oil.
The weight part ratio of the micro-nano coptis root powder, diatomite and cinnamon oil is 2:5:8.
The present invention with trimethylborate, rosemary powder, Ground Cloves, fatty alcohol polyoxyethylene ether, Lauryl Diethanolamine, in Medicine bacteriostatic agent, imidacloprid, butyl carbamate and deionized water are to prepare raw material, and water, fatty alcohol will first be added in blender Polyoxyethylene ether and Lauryl Diethanolamine form a kind of solution with certain consistency, sequentially add trimethylborate, amino Butyl formate, imidacloprid and Traditional Chinese medicine bacteriostatic agent, above-mentioned material inherently have good deinsectization bactericidal effect, mix by a certain percentage Preservative set obtained is a variety of a little after conjunction, and heating improves mixing speed, keeps solution mixing more equal using ultrasonic disperse It is even, then Ground Cloves and rosemary powder is added down to glass container heating water bath in above-mentioned mixed solution, the addition present invention can be made Wood veneer after preservative obtained increases delicate fragrant, wood veneer after add preservative without stand for a period of time into The scattered taste of row can be accomplished to produce and sell, finally carry out ultrasonic disperse again, stand to obtain preservative finished product, whole preparation process work Skill is succinct, at low cost, and raw material of the present invention is environmentally protective, and whole preparation process does not generate the by-product of pollution environment, through this It invents preservative obtained and is similarly green, asepsis environment-protecting.
A kind of wood veneer preservative of asepsis environment-protecting, comprises the following components in parts by weight: trimethylborate, 40 parts, fan Repeatedly face powder, 6 parts, Ground Cloves, 4 parts, fatty alcohol polyoxyethylene ether, 5 parts, Lauryl Diethanolamine, 7 parts, Traditional Chinese medicine bacteriostatic agent, 10 Part, imidacloprid, 16 parts, butyl carbamate, 8 parts, deionized water, 150 parts.
The Traditional Chinese medicine bacteriostatic agent includes micro-nano coptis root powder, diatomite and cinnamon oil.
The weight part ratio of the micro-nano coptis root powder, diatomite and cinnamon oil is 2:5:8.

Claims (4)

1. a kind of preparation method of asepsis environment-protecting wood veneer preservative, which is characterized in that each raw material in terms of mass parts, including with Lower step:
A, respectively cloves, rosemary clean and be dried, with 200-240r/min ball milling 2-3h, obtain Ground Cloves and rosemary Powder;
B, 150 parts of deionized waters are added in blender and are used as bottom water, while 5 parts of fatty alcohol polyoxyethylene ether and 7 parts months are added Osmanthus base diethanol amine, is heated to 40-46 DEG C, is dispersed with stirring, mixing speed 2200-2600r/min, when stirring a length of 30- 40min;
C, 40 parts of trimethylborates, 8 parts of butyl carbamates, 16 parts of imidacloprids and 10 parts of Chinese medicine suppressions are sequentially added into blender Microbial inoculum is heated to 48-52 DEG C after being all added, and stirs 25-35min with the mixing speed of 2500-3000r/min, then Ultrasonic disperse 15-20min;
D, the mixed solution in step C is poured out to glass container, water-bath is carried out to glass container using 55-60 DEG C of temperature and is added Heat is slowly added to 4 parts of Ground Cloves obtained in step A and 6 parts of rosemary powder in heating process, with 2000-2400r/min's Mixing speed stirs 35-45min;
E, the mixed solution in step D is cooled to room temperature, ultrasonic disperse 5-10min, stands 2-3h, obtains preservative finished product.
2. a kind of preparation method of asepsis environment-protecting wood veneer preservative according to claim 1, it is characterised in that: described First mixed-powder is added to glass container again after mixing for 4 parts of Ground Cloves and 6 parts of rosemary powder in step D.
3. a kind of preparation method of asepsis environment-protecting wood veneer preservative according to claim 1, it is characterised in that: described Traditional Chinese medicine bacteriostatic agent includes micro-nano coptis root powder, diatomite and cinnamon oil.
4. a kind of preparation method of asepsis environment-protecting wood veneer preservative according to claim 3, it is characterised in that: described The weight part ratio of micro-nano coptis root powder, diatomite and cinnamon oil is 2:5:8.
CN201811154539.7A 2018-09-30 2018-09-30 A kind of preparation method of asepsis environment-protecting wood veneer preservative Withdrawn CN109203155A (en)

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CN201811154539.7A CN109203155A (en) 2018-09-30 2018-09-30 A kind of preparation method of asepsis environment-protecting wood veneer preservative

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Application Number Priority Date Filing Date Title
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002052935A3 (en) * 2001-01-05 2002-10-03 Kop Coat Inc Synergistic combination of fungicides to protect wood and wood-based products from fungal decay, mold and mildew
CN106553244A (en) * 2015-09-24 2017-04-05 牛誉博 A kind of non-toxic, environmental friendly timber preservative and preparation method thereof
CN106665673A (en) * 2015-11-09 2017-05-17 阜南县宏泰工艺品有限公司 Wood preservative and preparation method thereof
CN107813389A (en) * 2017-11-13 2018-03-20 常州麒通国际贸易有限公司 A kind of timber preservative and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002052935A3 (en) * 2001-01-05 2002-10-03 Kop Coat Inc Synergistic combination of fungicides to protect wood and wood-based products from fungal decay, mold and mildew
CN106553244A (en) * 2015-09-24 2017-04-05 牛誉博 A kind of non-toxic, environmental friendly timber preservative and preparation method thereof
CN106665673A (en) * 2015-11-09 2017-05-17 阜南县宏泰工艺品有限公司 Wood preservative and preparation method thereof
CN107813389A (en) * 2017-11-13 2018-03-20 常州麒通国际贸易有限公司 A kind of timber preservative and preparation method thereof

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Application publication date: 20190115

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