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CN109126681A - Pipeline vibrating material reaction unit - Google Patents

Pipeline vibrating material reaction unit Download PDF

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Publication number
CN109126681A
CN109126681A CN201811203465.1A CN201811203465A CN109126681A CN 109126681 A CN109126681 A CN 109126681A CN 201811203465 A CN201811203465 A CN 201811203465A CN 109126681 A CN109126681 A CN 109126681A
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China
Prior art keywords
reactor
reaction device
dynamic formula
material reaction
formula material
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Application number
CN201811203465.1A
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Chinese (zh)
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CN109126681B (en
Inventor
欧阳晓平
毛评生
鲍瑞
毛亮程
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Hainan Walker New Material Technology Co ltd
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Hunan Trailblazer Environmental Protection Technology Co ltd
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Priority to CN201811203465.1A priority Critical patent/CN109126681B/en
Publication of CN109126681A publication Critical patent/CN109126681A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/28Moving reactors, e.g. rotary drums
    • B01J19/285Shaking or vibrating reactors; reactions under the influence of low-frequency vibrations or pulsations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a pipeline vibration type material reaction device which comprises a reactor and a vibration component connected with the reactor and driving the reactor to vibrate, wherein the reactor is provided with a reaction channel for materials to pass through, and the reaction channel is provided with a feeding hole and a discharging hole. The pipeline vibration type material reaction device has the advantages of high production efficiency, good environmental protection, low production cost, more sufficient and uniform material reaction and the like.

Description

A kind of pipe Vibration dynamic formula material reaction device
Technical field
The present invention relates to hydrometallurgys and chemical engineering to produce equipment technology field, and in particular to a kind of pipe Vibration dynamic formula object Expect reaction unit.
Background technique
In actual industrial production, common reaction is mostly the reaction that solid phase participates in, such as solid-liquid reaction, solid-solid reaction With gas-solid reaction etc..Solid-liquid reaction refers to the reaction occurred between solid and liquid.Some products are dissolved in liquid phase, such as metal Oxide is dissolved in acid;Some products form coating on solid-phase reactant, such as the reaction of zinc displacement copper.As product dissolves in liquid Phase, then liquid phase has an opportunity to touch reaction solid.Solid-solid reaction carries out anti-in solid form for two or more reactants It answers, reaction is usually to be taken place by the contact surface between solid phase, and reaction rate is controlled by interfacial reaction.Either where Reaction type is planted, the reaction between solid phase interface is extremely important, it will will affect the rate and progress entirely reacted.
In the prior art, the consersion unit that solid phase participates in reaction is generally the consersion unit of static fixation, by anti- Should during increase the method for material stirring or ball milling solid phase and react contact area between phase, and then raising two with other Reaction rate between phase.But either stirring or ball grinding method, all can exist to stir and uneven or insufficient show As, or even there is the phenomenon that stirring dead angle.It is contacted so as to cause between the solid phase and other reaction phases at position each in consersion unit Area energy imbalance causes local reaction incomplete, and product quality is difficult to ensure.
Summary of the invention
The technical problem to be solved in the present invention is to overcome the shortcomings of the prior art, provides a kind of high production efficiency, ring Guarantor property is good, production cost is low, material reaction can be made more abundant and uniform pipe Vibration dynamic formula material reaction device.
In order to solve the above technical problems, the invention adopts the following technical scheme:
A kind of pipe Vibration dynamic formula material reaction device, the vibration for being connected including reactor and with reactor and reactor being driven to vibrate Component, the reaction utensil have the reaction channel for passing through for material, and the reaction channel is equipped with inlet port and outlet port.
As a further improvement of the above technical scheme:
Above-mentioned pipe Vibration dynamic formula material reaction device, it is preferred that gradually downward from reaction channel described in feed inlet to discharge port Inclination extends.
Above-mentioned pipe Vibration dynamic formula material reaction device, it is preferred that the reaction channel is the pipeline for curling up into multi-turn.
Above-mentioned pipe Vibration dynamic formula material reaction device, it is preferred that the feed inlet and/or discharge port are equipped with and can be opened and closed simultaneously It is adjustable the valve of flow.
Above-mentioned pipe Vibration dynamic formula material reaction device, it is preferred that the vibration component includes pedestal and is mounted on pedestal On more than one vibratory drive mechanism, the reactor by elastic floating supporting mechanism install on the base, the vibration Driving mechanism is connected with the reactor.
Above-mentioned pipe Vibration dynamic formula material reaction device, it is preferred that there are the vibration component more than two vibrations to drive altogether Motivation structure, the vibration frequency and amplitude of all vibratory drive mechanisms are equal.
Above-mentioned pipe Vibration dynamic formula material reaction device, it is preferred that the vibratory drive mechanism includes rotary drive, passes The driving end of moving axis and vibrating shaft, the rotary drive is connected with the transmission shaft, and the transmission shaft passes through universal joint and vibration Moving axis is connected, and the vibrating shaft is equipped with several eccentric blocks, and the vibrating shaft is connected with reactor.
Above-mentioned pipe Vibration dynamic formula material reaction device, it is preferred that the transmission shaft includes that the first transmission segment and second pass Dynamic section, the driving end of the rotary drive are connected with the first transmission segment, and first transmission segment and the second transmission segment are with can be Axially with respect to moving and the mode being driven connects, second transmission segment is connected by universal joint with vibrating shaft.
Above-mentioned pipe Vibration dynamic formula material reaction device, it is preferred that first transmission segment is passed by splined shaft and second Dynamic section connection;The rotary drive is motor, and the output shaft of the motor is connected by connecting flange with the first transmission segment, or The output shaft of motor described in person is connected by chain-drive mechanism with the first transmission segment.
Above-mentioned pipe Vibration dynamic formula material reaction device, it is preferred that the elastic floating supporting mechanism includes several connections Bearing spring between pedestal and reactor, several bearing springs are evenly arranged in the four of more than one vibratory drive mechanism Week.
Compared with the prior art, the advantages of the present invention are as follows: pipe Vibration dynamic formula material reaction device of the invention will react Chamber is set as dynamic stationary state, and overcoming the consersion unit that solid phase participates in reaction in the prior art is usually static fixation Technology prejudice provides vibration supporting way for reaction chamber, realizes the mass motion of consersion unit chamber.Using vibration group Part drives reactor to vibrate, and the material in reaction channel can be made constantly to be stir-fried, be mixed, and the contact of material is more abundant, thus Keep the reaction of material more full and uniform.Meanwhile continuous production can be realized using the reaction channel of duct type, to mention significantly High efficiency, and material is reacted in the reaction channel of relative closure, and the feature of environmental protection might as well.Using the pipe Vibration dynamic formula Material reaction device can be very good to solve the problems, such as that traditional equipment participates in reacting in solid phase.
Detailed description of the invention
Fig. 1 is the structure schematic diagram of pipe Vibration dynamic formula material reaction device.
Fig. 2 is the schematic perspective view of coiled pipeline.
Fig. 3 is the side structure schematic view of coiled pipeline.
Marginal data:
1, reactor;11, reaction channel;111, feed inlet;112, discharge port;113, valve;12, shell;2, pedestal;3, it rotates Actuator;4, transmission shaft;41, the first transmission segment;42, the second transmission segment;43, connecting flange;44, splined shaft;5, vibrating shaft;6, Universal joint;7, eccentric block;9, spring is supported;10, fixed deformation bearing.
Specific embodiment
The present invention is described in further detail below in conjunction with the drawings and specific embodiments.
As shown in Figure 1 to Figure 3, the pipe Vibration dynamic formula material reaction device of the present embodiment, including reactor 1 and vibration group Part, vibration component are connected with reactor 1 and reactor 1 are driven to vibrate, and reactor 1 has the reaction channel for passing through for material 11, reaction channel 11 be equipped with feed inlet 111 and discharge port 112, from feed inlet 111 to 112 reaction channel 11 of discharge port gradually to Lower inclination extends.When work, reaction channel 11 is added from feed inlet 111 in material, and exports from discharge port 112, and material is passing through It is reacted during reaction channel 11.Reaction chamber is set dynamic fixing shape by the pipe Vibration dynamic formula material reaction device State overcomes the technology prejudice that the consersion unit that solid phase participates in reacting in the prior art is usually static fixation, is reaction chamber Vibration supporting way is provided, the mass motion of consersion unit chamber is realized.Reactor 1 is driven to vibrate using vibration component, The material in reaction channel 11 can be made constantly to be stir-fried, be mixed, the contact of material is more abundant, to make the reaction of material more It is full and uniform.Meanwhile continuous production can be realized using the reaction channel of duct type 11, so that production efficiency is greatly improved, and And material is reacted in the reaction channel 11 of relative closure, the feature of environmental protection might as well.High temperature and pressure leaching device of the invention can The problem of reacting is participated in solid phase with very good solution traditional equipment.
In the present embodiment, reaction channel 11 is the pipeline for curling up into multi-turn, 11 occupied space of reaction channel of this kind of form It is small, structural compactness can be greatly improved.Preferably, the both ends of pipeline are respectively that feed inlet 111 arrives discharge port 112.Pipeline is Circular pipe, conducive to the full and uniform stir-frying of material, mixing.
In the present embodiment, pipeline is the coiled pipeline curled up around a vertical centerline, and feed inlet 111 is located at discharge port 112 top, and be gradually increased from feed inlet 111 to the radial spacing of 112 coiled pipeline of discharge port and vertical centerline, it should Kind pipeline is conducive to material stir-frying, is more fully mixed uniformly, and passes through reaction channel 11 conducive to material is smooth.It is above-mentioned curl up into it is more The reaction channel 11 of circle can be various shape, such as can also be round perhaps ellipse but be not limited only to round or ellipse It is round.
In the present embodiment, discharge port 112, which is equipped with, can be opened and closed and be adjustable the valve 113 of flow, can be with by the valve 113 Discharge port 112 is opened or closed, while can also adjust the flow that material reaction product is flowed out from discharge port 112, thus realization pair The control of reaction rate substantially increases the controllability and using flexible of pipe Vibration dynamic formula material reaction device.In other realities It applies in example, valve 113 only can also be set in feed inlet 111, it is logical to enter reaction by the control material of valve 113 of feed inlet 111 The flow in road 11 can also control reaction rate.Also valve 113 can be respectively provided in feed inlet 111 and discharge port 112.
In the present embodiment, vibration component includes more than one the vibratory drive mechanism of pedestal 2 and installation on the base 2, instead Device 1 is answered to install on the base 2 by elastic floating supporting mechanism, vibratory drive mechanism is connected with reactor 1.Due to reactor 1 On the base 2 by the installation of elastic floating supporting mechanism, reactor 1 can elastic floating on the base 2, make vibratory drive mechanism Can drive response device 1 vibrate, and reactor 1 vibrate stability it is good.The structure of this kind of vibration component is simple, at low cost, work Make reliable and stable.
In the present embodiment, vibration component has altogether there are two vibratory drive mechanism, the vibration frequency of all vibratory drive mechanisms It is equal with amplitude, good resonance effect can be generated in this way, keeps stirring more violent, and material contact is more abundant, and reaction is more Add uniformly.Preferably, Liang Ge vibratory drive mechanism is symmetrical relative to the vertical centerline of coiled pipeline, resonance effect More preferably, the stress of reactor 1 is also more evenly.In other embodiments, the quantity of the had vibratory drive mechanism of vibration component is also It can be one or three or more, when vibration component tool is there are three the above vibratory drive mechanism, all vibratory drive mechanisms The vertical centerline of drum tubular conduit is uniformly distributed, and resonance effect can be made more preferable, and the stress of reactor 1 is more evenly.
In the present embodiment, vibratory drive mechanism includes rotary drive 3, transmission shaft 4 and vibrating shaft 5, rotary drive 3 Driving end is connected with transmission shaft 4, and transmission shaft 4 is connected by universal joint 6 with vibrating shaft 5, and vibrating shaft 5 is equipped with several eccentric blocks 7, Vibrating shaft 5 is connected with reactor 1.When rotary drive 3 drives transmission shaft 4 to rotate, transmission shaft 4 drives vibration by universal joint 6 Axis 5 rotates, and since vibrating shaft 5 is equipped with eccentric block 7, eccentric block 7 can make vibrating shaft 5 generate vibration when rotating with vibrating shaft 5, from And it is vibrated with reactor 1.The structure of the vibratory drive mechanism is simple, it is at low cost, stable and reliable in work, be easily installed maintenance.
Preferably, it is 500 ~ 6000r/min that rotary drive 3, which drives the revolving speed of transmission shaft 4,.There are two being set on vibrating shaft 5 Between eccentric block 7, two eccentric blocks 7 are divided into the opposite sides of vibrating shaft 5, and two eccentric blocks 7 are on 5 axis direction of vibrating shaft Every setting.
In the present embodiment, reactor 1 includes the reaction channel 11 of 12 sum of shell, and reaction channel 11 is mounted on shell 12, The vibrating shaft 5 of each vibratory drive mechanism is connected with shell 12.Vibrating shaft 5 is connect with reactor 1: being covered on vibrating shaft 5 If at least one fixed deformation bearing 10, fixed deformation bearing 10 includes the inner ring body and outer ring body of rotation connection, wherein inner ring Body is sleeved on vibrating shaft 5, and outer ring body is mounted in the installation sleeve being fixedly arranged on shell 12.
In the present embodiment, transmission shaft 4 includes the first transmission segment 41 and the second transmission segment 42, the driving end of rotary drive 3 It is connected with the first transmission segment 41, the first transmission segment 41 and the second transmission segment 42 are moved and are driven can be axially relative to Mode connect, the second transmission segment 42 is connected by universal joint 6 with vibrating shaft 5.Due to reactor 1 vibrate when and environment temperature Can generate axial stress when variation, the first transmission segment 41 and the second transmission segment 42 can relative motion in the axial direction, can play and disappear Except the effect of the axial stress, the service life of pipe Vibration dynamic formula material reaction device is improved.
In the present embodiment, the first transmission segment 41 is connect by splined shaft 44 with the second transmission segment 42;Rotary drive 3 is electricity The output shaft of machine, motor is connected by connecting flange 43 with the first transmission segment 41 or the output shaft of motor passes through chain conveyer machine Structure is connected with the first transmission segment 41.
In the present embodiment, elastic floating supporting mechanism includes several bearing springs being connected between pedestal 2 and reactor 1 9, several bearing springs 9 are evenly arranged in the surrounding of all vibratory drive mechanisms, and the reliable and stable of the vibration of reactor 1 can be improved Property, and the structure of the elastic floating supporting mechanism it is simple, it is at low cost, be easy to make.
Pipe Vibration dynamic formula material reaction device of the invention can also flow according to material and reaction time, to reaction channel The structural parameters such as 11 diameter are adjusted, to meet real reaction requirement.
The above is only a preferred embodiment of the present invention, protection scope of the present invention is not limited merely to above-mentioned implementation Example.To those of ordinary skill in the art, obtained improvement and change in the case where not departing from the technology of the present invention concept thereof It changes and also should be regarded as protection scope of the present invention.

Claims (10)

1. a kind of pipe Vibration dynamic formula material reaction device, it is characterised in that: be connected simultaneously including reactor (1) and with reactor (1) The vibration component for driving reactor (1) to vibrate, the reactor (1) have the reaction channel (11) for passing through for material, institute Reaction channel (11) are stated equipped with feed inlet (111) and discharge port (112).
2. pipe Vibration dynamic formula material reaction device according to claim 1, it is characterised in that: from feed inlet (111) to out Material mouth (112) reaction channel (11) tilts extension gradually downward.
3. pipe Vibration dynamic formula material reaction device according to claim 2, it is characterised in that: the reaction channel (11) is Curl up into the pipeline of multi-turn.
4. pipe Vibration dynamic formula material reaction device according to claim 1, it is characterised in that: the feed inlet (111) and/ Or discharge port (112) is equipped with the valve (113) that can be opened and closed and be adjustable flow.
5. pipe Vibration dynamic formula material reaction device according to any one of claim 1 to 4, it is characterised in that: the vibration Dynamic component includes pedestal (2) and more than one the vibratory drive mechanism being mounted on pedestal (2), and the reactor (1) passes through bullet Property Floatable supporting mechanism is mounted on pedestal (2), and the vibratory drive mechanism is connected with the reactor (1).
6. pipe Vibration dynamic formula material reaction device according to claim 5, it is characterised in that: the vibration component has altogether More than two vibratory drive mechanisms, the vibration frequency and amplitude of all vibratory drive mechanisms are equal.
7. pipe Vibration dynamic formula material reaction device according to claim 5, it is characterised in that: vibratory drive mechanism packet Include rotary drive (3), transmission shaft (4) and vibrating shaft (5), the driving end and the transmission shaft (4) of the rotary drive (3) It is connected, the transmission shaft (4) is connected by universal joint (6) with vibrating shaft (5), and the vibrating shaft (5) is equipped with several eccentric blocks (7), the vibrating shaft (5) is connected with reactor (1).
8. pipe Vibration dynamic formula material reaction device according to claim 7, it is characterised in that: the transmission shaft (4) includes The driving end of first transmission segment (41) and the second transmission segment (42), the rotary drive (3) is connected with the first transmission segment (41), First transmission segment (41) is connected in a manner of it can be axially relative to move and be driven with the second transmission segment (42), Second transmission segment (42) is connected by universal joint (6) with vibrating shaft (5).
9. pipe Vibration dynamic formula material reaction device according to claim 8, it is characterised in that: first transmission segment (41) It is connect by splined shaft (44) with the second transmission segment (42);The rotary drive (3) is motor, and the output shaft of the motor is logical Cross connecting flange (43) be connected with the first transmission segment (41) or the output shaft of the motor by chain-drive mechanism with first biography Dynamic section (41) are connected.
10. pipe Vibration dynamic formula material reaction device according to claim 5, it is characterised in that: the elastic floating support Mechanism includes several bearing springs (9) being connected between pedestal (2) and reactor (1), and several bearing springs (9) are evenly arranged In the surrounding of more than one vibratory drive mechanism.
CN201811203465.1A 2018-10-16 2018-10-16 A pipeline vibration type material reaction device Active CN109126681B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112058209A (en) * 2020-08-03 2020-12-11 湖北航鹏化学动力科技有限责任公司 a continuous action system
CN113019300A (en) * 2019-12-09 2021-06-25 上海合全药业股份有限公司 Vibrating peripheral, pipeline reaction device and application thereof

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Publication number Priority date Publication date Assignee Title
CN113019300A (en) * 2019-12-09 2021-06-25 上海合全药业股份有限公司 Vibrating peripheral, pipeline reaction device and application thereof
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Inventor after: Mao Pingsheng

Inventor after: Bao Rui

Inventor after: Mao Liangcheng

Inventor before: OuYang Xiaoping

Inventor before: Mao Pingsheng

Inventor before: Bao Rui

Inventor before: Mao Liangcheng