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CN109092115B - Laboratory solution automatic stirring device - Google Patents

Laboratory solution automatic stirring device Download PDF

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Publication number
CN109092115B
CN109092115B CN201811188347.8A CN201811188347A CN109092115B CN 109092115 B CN109092115 B CN 109092115B CN 201811188347 A CN201811188347 A CN 201811188347A CN 109092115 B CN109092115 B CN 109092115B
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China
Prior art keywords
solution
processing unit
shell
rotating shaft
driving motor
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Application number
CN201811188347.8A
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Chinese (zh)
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CN109092115A (en
Inventor
张然
袁巍
王跃
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Anhui Yu'an Laboratory Equipment Co ltd
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Anhui Yu'an Laboratory Equipment Co ltd
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Priority to CN201811188347.8A priority Critical patent/CN109092115B/en
Publication of CN109092115A publication Critical patent/CN109092115A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/60Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
    • B01F27/70Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/19Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/191Stirrers with two or more mixing elements mounted in sequence on the same axis with similar elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/20Measuring; Control or regulation
    • B01F35/21Measuring
    • B01F35/213Measuring of the properties of the mixtures, e.g. temperature, density or colour
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/23Mixing of laboratory samples e.g. in preparation of analysing or testing properties of materials

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The invention provides an automatic stirring device for laboratory solution, which comprises: the device comprises a shell, a rotary stirring mechanism, a driving motor, a sampling tube, an electric pump, a spectrophotometer and a control module; the control module comprises a spectrum curve drawing unit, a processing unit and an execution control unit; the spectral curve drawing unit is connected with the spectrophotometer, the processing unit is connected with the spectral curve drawing unit, the execution control unit is connected with the processing unit and the driving motor, and the execution control unit is used for controlling the driving motor to work according to the judging result of the processing unit. According to the invention, the light transmittance of the solution output at different moments in the shell is subjected to linear analysis, so that the change of the light transmittance of the solution at different moments in the shell can be more intuitively obtained, and the uniformity degree in the solution mixing process can be judged. According to the invention, the stirring operation of the solution is automatically controlled according to the uniformity of the solution, which is beneficial to improving the stirring efficiency and effect of the solution.

Description

Laboratory solution automatic stirring device
Technical Field
The invention relates to the technical field of experimental equipment, in particular to an automatic stirring device for laboratory solutions.
Background
At present, along with the development of industry, most of the preparation processes of materials need to process various raw materials, the stirring device is often used for uniformly mixing the raw materials due to the fact that the stirring device has larger stirring power, whether the raw materials are uniformly mixed cannot be judged in the stirring process, and due to the fact that the stirring speed of the stirring device is higher in the stirring process, the power supply of the stirring device is stopped to observe the mixing condition, so that the processing time is greatly wasted, and the stirring device capable of safely observing the stirring state while the power supply is not turned off is needed; on the other hand, the stirring rod in the current stirring device has only one stirring function, a large-power stirring device is often required to be added for stirring the thick liquid of the raw materials, and the stirring rod cannot stir the raw materials adhered to the inner wall of the stirring device.
Disclosure of Invention
Based on the technical problems in the background technology, the invention provides an automatic stirring device for laboratory solution.
The invention provides an automatic stirring device for laboratory solution, which comprises: the device comprises a shell, a rotary stirring mechanism, a driving motor, a sampling tube, an electric pump, a spectrophotometer and a control module;
the rotary stirring mechanism is rotatably arranged in the shell, the driving motor is arranged outside the shell, and the driving motor is connected with the rotary stirring mechanism and used for driving the rotary stirring mechanism to rotate;
the two sides of the shell, which are opposite to the rotating plane of the rotating stirring mechanism, are respectively provided with a sampling port and a reflux port; the first end of the sampling tube is communicated with the sampling port, the second end of the sampling tube passes through the sample chamber of the spectrophotometer to be communicated with the reflux port, and the electric pump is arranged on the sampling tube;
the control module comprises a spectrum curve drawing unit, a processing unit and an execution control unit;
the spectrum curve drawing unit is connected with the spectrophotometer and is used for acquiring the light transmittance detection value of the spectrophotometer on the sample in the sample chamber in real time and drawing a spectrum curve;
the processing unit is connected with the spectrum curve drawing unit and is used for obtaining the maximum value N of the spectrum curve in the latest preset time period max And a minimum value N min Average value N of (2) ave The method is used for judging the uniformity degree of the solution according to the comparison result of the spectrum curve and the average value in the latest preset time period;
the execution control unit is connected with the processing unit and the driving motor, and is used for controlling the driving motor to work according to the judging result of the processing unit.
Preferably, the processing unit works in the following manner: the processing unit is based on the average value N ave And a preset float value f x Drawing a reference interval, wherein the reference interval is N as an upper limit value on the latest preset time period ave +f x And the lower limit value is N ave -f x Is a rectangular region of (2); the processing unit is used for calculating the area value of the spectrum curve positioned outside the reference interval in the latest preset time period and judging the uniformity degree of the solution according to the calculation result.
Preferably, the processing unit is configured to measure the uniformity of the solution according to the following formula:
r=A×S 1 /S 0 wherein A is a calculation constant, A is more than or equal to 10 and less than or equal to 100, S 1 For the area value of the spectral curve lying outside the reference interval for the latest preset time period, S 0 The area value of the reference section.
Preferably, the processing unit is further adapted to compare the maximum value N of the spectral curve max And a minimum value N min The processing unit is used for judging the next solution uniformity degree after the reference time is delayed by a preset time period.
Preferably, the processing unit periodically performs the solution uniformity degree judgment.
Preferably, the execution control unit is preset with a multi-stage working mode, and the working power of the driving motor in the multi-stage working mode is sequentially increased; each stage of working mode is associated with a corresponding uniform degree interval range, and the execution control unit is used for adjusting the working mode of the driving motor according to the uniform degree acquired by the processing unit.
Preferably, the shell is of a circular tube structure which is horizontally arranged, the rotary stirring mechanism consists of a rotating shaft and scraping plates arranged on the rotating shaft, and the axis of the rotating shaft is positioned on or parallel to the plane where any scraping plate is positioned; the projections of the scrapers on the axis of the rotating shaft are connected into a straight line, and a gap is reserved between any two adjacent scrapers; the rotating shaft is arranged in the shell in parallel to the axis of the shell, and the sampling port and the reflux port are positioned at two opposite ends of the rotating shaft.
Preferably, the shaft is offset downwardly from the housing axis, and the housing bottom is located on the rotational path of the scraper.
Preferably, the sampling port and the reflux port are both positioned above the rotating shaft.
Preferably, two groups of scrapers are arranged on the rotating shaft, the two groups of scrapers are respectively and evenly distributed on a first straight line and a second straight line which are parallel to the rotating shaft, and the scrapers on the first straight line and the second straight line are staggered along the extending direction of the rotating shaft.
According to the automatic laboratory solution stirring device provided by the invention, under the working state of the electric pump, the solution in the shell flows through the sampling tube from the sample chamber of the spectrophotometer, and the solution in the shell enters the sampling tube from the sampling port and flows back into the shell from the backflow port, so that the real-time measurement of the transmittance of the solution in the shell by the spectrophotometer is realized, and the mixing uniformity degree of the solution is judged according to the change trend of the transmittance output by the spectrophotometer. Meanwhile, the solution in the shell circularly flows along the direction of the rotating shaft of the rotating stirring mechanism through the sampling pipe, so that the mixing of the solutions at two opposite sides of the rotating plane of the rotating stirring mechanism is facilitated, and the layering of the solution in the shell is avoided.
According to the invention, the light transmittance of the solution output at different moments in the shell is subjected to linear analysis, so that the change of the light transmittance of the solution at different moments in the shell can be more intuitively obtained, and the uniformity degree in the solution mixing process can be judged. According to the invention, the stirring operation of the solution is automatically controlled according to the uniformity of the solution, which is beneficial to improving the stirring efficiency and effect of the solution.
Drawings
FIG. 1 is a diagram showing a construction of an automatic laboratory solution stirring device according to the present invention;
fig. 2 is a control block diagram of fig. 1.
The diagram is: the device comprises a shell 1, a sampling port 11, a backflow port 12, a rotary stirring mechanism 2, a rotating shaft 21, a scraper 22, a driving motor 3, a sampling tube 4, an electric pump 5 and a spectrophotometer 6.
Detailed Description
Referring to fig. 1, the automatic laboratory solution stirring device provided by the invention comprises: the device comprises a shell 1, a rotary stirring mechanism 2, a driving motor 3, a sampling tube 4, an electric pump 5, a spectrophotometer 6 and a control module.
The rotary stirring mechanism 2 is rotatably arranged in the shell 1, the driving motor 3 is arranged outside the shell 1, and the driving motor 3 is connected with the rotary stirring mechanism 2 and used for driving the rotary stirring mechanism 2 to rotate so as to stir the solution in the shell 1.
The two opposite sides of the shell 1, which are positioned on the rotating plane of the rotary stirring mechanism 2, are respectively provided with a sampling port 11 and a reflux port 12. The first end of the sampling tube 4 is communicated with the sampling port 11, the second end of the sampling tube passes through the sample chamber of the spectrophotometer 6 to be communicated with the reflux port 12, and the electric pump 5 is arranged on the sampling tube 4. In this way, under the working state of the electric pump 5, the solution in the shell 1 flows through the sampling tube 4 from the sample chamber of the spectrophotometer 6, and the solution in the shell 1 enters the sampling tube 4 from the sampling port 11 and flows back into the shell 1 from the backflow port 12, so that the real-time measurement of the transmittance of the solution in the shell 1 by the spectrophotometer 6 is realized, and the degree of uniformity of the solution mixing is judged according to the change trend of the transmittance output by the spectrophotometer 6.
Meanwhile, in the present embodiment, the solution in the housing 1 is circulated in the direction along the rotation axis of the rotary stirring mechanism 2 by the sampling tube 4, which is advantageous for mixing the solutions at both sides opposite to the rotation plane of the rotary stirring mechanism 2, thereby avoiding the delamination of the solution in the housing 1.
The control module comprises a spectrum curve drawing unit, a processing unit and an execution control unit.
The spectrum curve drawing unit is connected with the spectrophotometer 6 and is used for acquiring the light transmittance detection value of the spectrophotometer 6 on the sample in the sample chamber in real time and drawing a spectrum curve. In this way, in the present embodiment, the light transmittance of the solution output at different times in the housing 1 is linearly analyzed, which is favorable for more intuitively obtaining the light transmittance change of the solution at different times in the housing 1, so as to determine the uniformity degree in the solution mixing process.
The processing unit is connected with the spectrum curve drawing unit and is used for obtaining the maximum value N of the spectrum curve in the latest preset time period max And a minimum value N min Average value N of (2) ave And is used for judging the uniformity degree of the solution according to the comparison result of the spectrum curve and the average value in the latest preset time period.
In practice, the maximum value N can be passed max Difference from average or minimum value N min And average value N ave And judging the uniformity of the solution.
In this embodiment, the processing unit operates in the following manner: the processing unit is based on the average value N ave And a preset float value f x Drawing a reference interval, wherein the reference interval is N as an upper limit value on the latest preset time period ave +f x And the lower limit value is N ave -f x Is a rectangular region of the panel. The processing unit is used for calculating the area value of the spectrum curve positioned outside the reference interval in the latest preset time period and judging the uniformity degree of the solution according to the calculation result. I.e. the greater the area value of the spectral curve over the most recent preset time period outside the reference interval, the lower the degree of homogeneity of the solution.
The execution control unit is connected with the processing unit and the driving motor 3, and is used for controlling the driving motor 3 to work according to the judging result of the processing unit. For example, if the degree of uniformity of the solution reaches the standard, the execution control unit controls the driving motor 3 to stop operating to stop stirring the solution; if the solution uniformity is low, the execution control unit controls the driving motor 3 to continue to work so as to further stir the solution to improve the solution uniformity.
Specifically, in the present embodiment, the execution control unit is preset with a plurality of operation modes, and the operation power of the driving motor 3 in the plurality of operation modes is sequentially increased. Each stage of working mode is associated with a corresponding uniform degree interval range, and the execution control unit is used for adjusting the working mode of the driving motor 3 according to the uniform degree acquired by the processing unit.
In this way, when the processing unit determines that the solution uniformity is lower, the execution control unit controls the driving motor 3 to work in a higher-power working mode so as to drive the rotary stirring mechanism 2 to stir at a higher rotating speed, thereby being beneficial to improving the solution stirring efficiency. And along with the improvement of the uniformity degree of the solution, the rotating speed of the rotary stirring mechanism 2 is gradually reduced, so that excessive stirring is avoided, and redundant energy consumption is avoided.
Specifically, in this embodiment, the processing unit is configured to measure the uniformity of the solution according to the following formula:
r=A×S 1 /S 0 wherein A is a calculation constant, A is more than or equal to 10 and less than or equal to 100, S 1 For the area value of the spectral curve lying outside the reference interval for the latest preset time period, S 0 The area value of the reference section.
Thus, the solution uniformity is quantized by calculating the magnitude r, thereby being beneficial to the imaging judgment of the solution uniformity and facilitating the accurate control of the driving motor 3.
In this embodiment, the processing unit is further configured to compare the maximum value N of the spectrum curve max And a minimum value N min The processing unit is used for judging the next solution uniformity degree after the reference time is delayed by a preset time period. Therefore, the time for judging each spectrum curve of the processing unit is accurately controlled, real-time detection of the uniformity of the solution is realized, redundant work is reduced, the workload of the processing unit is reduced, and the working efficiency is improved. In specific implementation, the processing unit may also periodically determine the uniformity of the solution.
In this embodiment, the casing 1 is a horizontally arranged circular tube structure, the rotary stirring mechanism 2 is composed of a rotating shaft 21 and a scraper 22 installed on the rotating shaft 21, and the axis of the rotating shaft 21 is located on or parallel to the plane where any scraper 22 is located, so that the maximum stirring area of the scraper 22 can be ensured in the rotating process of the rotating shaft 21, and the stirring effect is improved. The projections of each scraper 22 on the axis of the rotating shaft 21 are connected in a straight line, and a gap is reserved between any two adjacent scrapers 22. In this way, not only is the overall stirring within the application environment achieved, but also the convection of the solution is achieved through the gap between two adjacent scrapers 22, thereby facilitating the improvement of the stirring effect. In this embodiment, two sets of scrapers 22 are disposed on the rotating shaft 21, and the two sets of scrapers 22 are respectively and evenly distributed on a first straight line and a second straight line parallel to the rotating shaft 21, and the scrapers 22 on the first straight line and the second straight line are staggered along the extending direction of the rotating shaft 21.
In the present embodiment, the rotary shaft 21 is installed inside the housing 1 in parallel to the axis of the housing 1, and the sampling port 11 and the return port 12 are located at opposite ends of the rotary shaft 21.
Specifically, in the present embodiment, the rotation shaft 21 is offset downward from the axis of the housing 1, and the bottom of the housing 1 is located on the rotation track of the scraper 22. In this way, precipitation may occur at the bottom of the surface housing 1. In this embodiment, the sampling port 11 and the return port 12 are both located above the rotation shaft 21.
The foregoing is only a preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be able to apply equivalents and modifications to the technical solution and the inventive concept thereof within the scope of the present invention.

Claims (9)

1. An automatic laboratory solution stirring device, comprising: the device comprises a shell (1), a rotary stirring mechanism (2), a driving motor (3), a sampling tube (4), an electric pump (5), a spectrophotometer (6) and a control module;
the rotary stirring mechanism (2) is rotatably arranged in the shell (1), the driving motor (3) is arranged outside the shell (1), and the driving motor (3) is connected with the rotary stirring mechanism (2) and used for driving the rotary stirring mechanism (2) to rotate;
the two opposite sides of the rotation plane of the rotation stirring mechanism (2) on the shell (1) are respectively provided with a sampling port (11) and a reflux port (12); the first end of the sampling tube (4) is communicated with the sampling port (11), the second end of the sampling tube passes through a sample chamber of the spectrophotometer (6) to be communicated with the reflux port (12), and the electric pump (5) is arranged on the sampling tube (4);
the control module comprises a spectrum curve drawing unit, a processing unit and an execution control unit;
the spectrum curve drawing unit is connected with the spectrophotometer (6) and is used for acquiring the light transmittance detection value of the spectrophotometer (6) on the sample in the sample chamber in real time and drawing a spectrum curve;
the processing unit is connected with the spectrum curve drawing unit and is used for obtaining the maximum value N of the spectrum curve in the latest preset time period max And a minimum value N min Average value N of (2) ave The method is used for judging the uniformity degree of the solution according to the comparison result of the spectrum curve and the average value in the latest preset time period;
the execution control unit is connected with the processing unit and the driving motor (3) and is used for controlling the driving motor (3) to work according to the judgment result of the processing unit;
the working mode of the processing unit is as follows: the processing unit is based on the average value N ave And a preset float value f x Drawing a reference section, referring toThe upper limit value on the preset time period with the latest interval is N ave +f x And the lower limit value is N ave -f x Is a rectangular region of (2); the processing unit is used for calculating the area value of the spectrum curve positioned outside the reference interval in the latest preset time period and judging the uniformity degree of the solution according to the calculation result.
2. The laboratory solution automatic stirring device according to claim 1, wherein the processing unit is configured to measure the degree of homogeneity of the solution according to the following formula:
r=A×S 1 /S 0 wherein A is a calculation constant, A is more than or equal to 10 and less than or equal to 100, S 1 For the area value of the spectral curve lying outside the reference interval for the latest preset time period, S 0 The area value of the reference section.
3. The laboratory solution automatic stirring device according to claim 1, wherein the processing unit is further configured to compare the maximum value N of the spectral curve max And a minimum value N min The processing unit is used for judging the next solution uniformity degree after the reference time is delayed by a preset time period.
4. The laboratory solution automatic stirring device according to claim 1, wherein the processing unit periodically performs the solution uniformity degree judgment.
5. The laboratory solution automatic stirring device according to any one of claims 1 to 4, wherein a multistage operation mode is preset in the execution control unit, and the operation power of the driving motor (3) in the multistage operation mode is sequentially increased; each stage of working mode is associated with a corresponding uniform degree interval range, and the execution control unit is used for adjusting the working mode of the driving motor (3) according to the uniform degree acquired by the processing unit.
6. The automatic laboratory solution stirring device according to claim 1, wherein the shell (1) is of a horizontally arranged circular tube structure, the rotary stirring mechanism (2) consists of a rotating shaft (21) and scrapers (22) arranged on the rotating shaft (21), and the axis of the rotating shaft (21) is positioned on or parallel to the plane of any scraper (22); the projections of the scrapers (22) on the axis of the rotating shaft (21) are connected into a straight line, and a gap is reserved between any two adjacent scrapers (22); the rotating shaft (21) is arranged in the shell (1) in parallel to the axis of the shell (1), and the sampling port (11) and the reflux port (12) are positioned at two opposite ends of the rotating shaft (21).
7. The laboratory solution automatic stirring device according to claim 6, wherein the rotating shaft (21) is downwardly offset from the axis of the housing (1), and the bottom of the housing (1) is located on the rotation locus of the scraper (22).
8. The laboratory solution automatic stirring device according to claim 7, wherein the sampling port (11) and the return port (12) are both located above the rotation shaft (21).
9. The automatic laboratory solution stirring device according to claim 6, wherein two groups of scrapers (22) are arranged on the rotating shaft (21), the two groups of scrapers (22) are respectively and evenly distributed on a first straight line and a second straight line which are parallel to the rotating shaft (21), and the scrapers (22) on the first straight line and the second straight line are staggered along the extending direction of the rotating shaft (21).
CN201811188347.8A 2018-10-12 2018-10-12 Laboratory solution automatic stirring device Active CN109092115B (en)

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CN109092115B true CN109092115B (en) 2024-03-22

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Publication number Priority date Publication date Assignee Title
CN114931878A (en) * 2022-07-21 2022-08-23 山东福尔特种设备有限公司 Strong magnetic coupling stirring autoclave with good stability
CN116510665A (en) * 2023-05-10 2023-08-01 浙江茶博士生物科技有限公司 Separation equipment and method for separating theanine from tea
CN116351313B (en) * 2023-05-31 2023-07-28 广东奔富之堡智能家电工程技术研究中心有限公司 Intelligent control system of food mixer based on computer control

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CN101206463A (en) * 2007-11-30 2008-06-25 深圳先进技术研究院 A method and system for on-line monitoring of drug production and mixing process
CN104923094A (en) * 2015-05-29 2015-09-23 安徽育安实验室装备有限公司 Solution blending device
CN207153502U (en) * 2017-07-12 2018-03-30 绍兴柯桥宏灏纺织有限公司 A kind of agitator for preventing dye precipitated
CN108357321A (en) * 2017-12-28 2018-08-03 合肥长天信息技术有限公司 A kind of bus heating equipment control method

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