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CN108752122A - A kind of compound fertilizer preparation method improving rice yield - Google Patents

A kind of compound fertilizer preparation method improving rice yield Download PDF

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Publication number
CN108752122A
CN108752122A CN201811017160.1A CN201811017160A CN108752122A CN 108752122 A CN108752122 A CN 108752122A CN 201811017160 A CN201811017160 A CN 201811017160A CN 108752122 A CN108752122 A CN 108752122A
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CN
China
Prior art keywords
compound fertilizer
uniformly mixed
rice yield
added
fertilizer preparation
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811017160.1A
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Chinese (zh)
Inventor
余兆琨
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Huaining Jiahe Rice Industry Co Ltd
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Huaining Jiahe Rice Industry Co Ltd
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Publication date
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Priority to CN201811017160.1A priority Critical patent/CN108752122A/en
Publication of CN108752122A publication Critical patent/CN108752122A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00Other inorganic fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/10Solid or semi-solid fertilisers, e.g. powders
    • C05G5/12Granules or flakes

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of compound fertilizer preparation methods improving rice yield, include the following steps:P-aminophenyl trimethoxy silane, calcium lignosulfonate, water are uniformly mixed, regulation system pH value is 4-4.8, is stirred, and is filtered, washing, centrifugation, it is dry, tetrahydrofuran is added and stirs evenly, maleic anhydride stirring is added, precipitation filters, and washing is dried to obtain first material;First material addition Macrogol 600 is uniformly mixed, regulation system pH value is 3-3.8, is stirred, and is centrifuged, and is filtered, and washing, vacuum drying obtains second material;Wormcast, rotted pig manure, biogas residue, sunflower seed dregs, humic acid, bastard coal mountain flour, medical stone, sawdust, bactericidal deodorant, EM bacteria agent are uniformly mixed, water is added, second material is added and is uniformly mixed, it is dry, it crushes, is granulated, drying is improved the compound fertilizer of rice yield.

Description

A kind of compound fertilizer preparation method improving rice yield
Technical field
The present invention relates to technical field of fertilizers more particularly to a kind of compound fertilizer preparation methods improving rice yield.
Background technology
With the development of science and technology, the continuous improvement of the transformation of social progress and people's life idea and living standard, People are higher and higher to the pursuit of food, clothing, housing and transportation, and green, ecological, organic, environmentally friendly life will be that following people's life must Must;Therefore organic agriculture, popularizing planting organic paddy rice, the green supply for ensureing people's dining table are greatly developed, is current and not Carry out the developing direction of agricultural production.
There are shortcomings when planting organic paddy rice for existing technology, and often fertilizer efficiency is poor, and soil is easily hardened, low output, Influence the planting benefit of farmer.
Invention content
Technical problems based on background technology, the present invention propose a kind of compound fertilizer preparation improving rice yield Method, gained compound fertilizer is not only full of nutrition, and fertilizer and water conservation capacity is strong, fabulous to the slow release effect of nutriment, Er Qiegai Kind soil hardening caused by since chemical fertilizer is used for a long time increases the permeability of soil, while can be provided for rice largely after degrading Element silicon, at low cost, increasing of quality and production significant effect.
A kind of compound fertilizer preparation method improving rice yield proposed by the present invention, includes the following steps:
S1, p-aminophenyl trimethoxy silane, calcium lignosulfonate, water are uniformly mixed, regulation system pH value is 4- 4.8, it stirs, filters, wash, centrifuge, it is dry, tetrahydrofuran is added and stirs evenly, maleic anhydride stirring is added, precipitates, filtering, Washing, is dried to obtain first material;
S2, first material addition Macrogol 600 is uniformly mixed, regulation system pH value is 3-3.8, is stirred, centrifugation, mistake Filter, washing, vacuum drying obtain second material;
S3, wormcast, rotted pig manure, biogas residue, sunflower seed dregs, humic acid, bastard coal mountain flour, medical stone, sawdust, sterilization are removed Smelly dose, EM bacteria agent be uniformly mixed, add water, second material be added and is uniformly mixed, dry, pulverize, is granulated, drying is improved rice The compound fertilizer of yield.
Preferably, in S1, regulation system pH value is 4-4.8, stirs 2-4h, and whipping temp is 10-16 DEG C.
Preferably, in S1, after maleic anhydride is added, 4-10h is stirred, whipping temp is 100-112 DEG C.
Preferably, in S1, p-aminophenyl trimethoxy silane, calcium lignosulfonate, water, tetrahydrofuran, maleic anhydride Weight ratio be 10-16:0.2-0.8:50-100:50-60:0.1-0.2.
Preferably, in S2, regulation system pH value is 3-3.8, stirs 4-10h, and whipping temp is 80-88 DEG C.
Preferably, in S2, the weight ratio of first material and Macrogol 600 is 5-8:10-16.
Preferably, in S3, it is 20-32wt% to add water to water content.
Preferably, in S3, wormcast, rotted pig manure, biogas residue, sunflower seed dregs, humic acid, bastard coal mountain flour, medical stone, wood Bits, bactericidal deodorant, EM bacteria agent, the weight ratio of second material are 100-120:32-45:10-20:15-25:2-10:1-4:2- 4:0.5-1.2:0.1-0.4:0.1-0.2:2-8.
In S1 of the present invention, p-aminophenyl trimethoxy silane prepares two-dimensional layered structure;In S2, for first material original Polyethylene glycol is inserted into position, not only increases layer structure spacing, and adsorption effect is good, can be adsorbed on surface, and fertilizer and water conservation capacity is strong, Adsorbance is high, fabulous to the slow release effect of nutriment, the fertilizer efficiency of organic additive not only can be improved, but also improve due to length Phase uses soil hardening caused by chemical fertilizer, increases the permeability of soil, while a large amount of element silicons can be provided for rice after degrading, at This low, increasing of quality and production significant effect;In S3, using wormcast, rotted pig manure, biogas residue, sunflower seed dregs, humic acid, bastard coal mountain flour, Medical stone, sawdust compounding, soil hardening and physicochemical character caused by can improving chemical fertilizer, year after year application can alleviate continuous cropping barrier significantly Hinder, increasing production of rice effect is good, and can effectively improve rice quality, and EM bacteria agent is added as fermenting microbe in cooperation, and not only nutrition is rich Richness, and can environment purification, reduce environmental pollution, while organic matter in soil can be decomposed, save fertilizers input, reduce Cost.
Specific implementation mode
In the following, technical scheme of the present invention is described in detail by specific embodiment.
Embodiment 1
A kind of compound fertilizer preparation method improving rice yield, includes the following steps:
S1,10kg p-aminophenyls trimethoxy silane, 0.8kg calcium lignosulfonates, 50kg water are uniformly mixed, use is dense It is 4-4.8 that degree, which is 5.8mol/l hydrochloric acid regulation system pH value, stirs 2h, and whipping temp is 16 DEG C, filters, washs, centrifuge, does It is dry, 50kg tetrahydrofurans are added and stir evenly, 0.2kg maleic anhydrides are added and stir 4h, whipping temp is 112 DEG C, precipitation, mistake Filter, washing, is dried to obtain first material;
S2,5kg first materials addition 16kg Macrogol 600s are uniformly mixed, are adjusted with a concentration of 1.5mol/l hydrochloric acid System pH is 3-3.8, stirs 10h, and whipping temp is 80 DEG C, centrifuges, filters, washing, vacuum drying obtains second material;
S3, by 120kg wormcasts, 32kg rotted pig manures, 20kg biogas residues, 15kg sunflower seed dregs, 10kg humic acids, 1kg coals Spoil powder, 4kg medical stones, 0.5kg sawdusts, 0.4kg bactericidal deodorants, 0.1kgEM microbial inoculums are uniformly mixed, and adding water to water content is 32wt% is added 2kg second materials and is uniformly mixed, and dry, pulverize to 100 mesh, is granulated, 45 DEG C of drying are improved rice yield Compound fertilizer.
Embodiment 2
A kind of compound fertilizer preparation method improving rice yield, includes the following steps:
S1,16kg p-aminophenyls trimethoxy silane, 0.2kg calcium lignosulfonates, 100kg water are uniformly mixed, are used A concentration of 5mol/l hydrochloric acid regulation system pH value is 4-4.8, stirs 4h, and whipping temp is 10 DEG C, filters, washs, centrifuge, does It is dry, 60kg tetrahydrofurans are added and stir evenly, 0.1kg maleic anhydrides are added and stir 10h, whipping temp is 100 DEG C, precipitation, mistake Filter, washing, is dried to obtain first material;
S2,8kg first materials addition 10kg Macrogol 600s are uniformly mixed, are adjusted with a concentration of 2.9mol/l hydrochloric acid System pH is 3-3.8, stirs 4h, and whipping temp is 88 DEG C, centrifuges, filters, washing, vacuum drying obtains second material;
S3, by 100kg wormcasts, 45kg rotted pig manures, 10kg biogas residues, 25kg sunflower seed dregs, 2kg humic acids, 4kg bastard coals Mountain flour, 2kg medical stones, 1.2kg sawdusts, 0.1kg bactericidal deodorants, 0.2kgEM microbial inoculums are uniformly mixed, and adding water to water content is 20wt% is added 8kg second materials and is uniformly mixed, and dry, pulverize to 60 mesh, is granulated, 60 DEG C of drying are improved rice yield Compound fertilizer.
Embodiment 3
A kind of compound fertilizer preparation method improving rice yield, includes the following steps:
S1,12kg p-aminophenyls trimethoxy silane, 0.6kg calcium lignosulfonates, 60kg water are uniformly mixed, use is dense It is 4-4.8 that degree, which is 5.6mol/l hydrochloric acid regulation system pH value, stirs 2.5h, and whipping temp is 14 DEG C, filters, washs, centrifuge, does It is dry, 53kg tetrahydrofurans are added and stir evenly, 0.17kg maleic anhydrides are added and stir 6h, whipping temp is 108 DEG C, precipitation, mistake Filter, washing, is dried to obtain first material;
S2,6kg first materials addition 14kg Macrogol 600s are uniformly mixed, are adjusted with a concentration of 1.8mol/l hydrochloric acid System pH is 3-3.8, stirs 8h, and whipping temp is 82 DEG C, centrifuges, filters, washing, vacuum drying obtains second material;
S3, by 115kg wormcasts, 36kg rotted pig manures, 18kg biogas residues, 18kg sunflower seed dregs, 8kg humic acids, 2kg bastard coals Mountain flour, 3.5kg medical stones, 0.6kg sawdusts, 0.3kg bactericidal deodorants, 0.13kgEM microbial inoculums are uniformly mixed, and add water to water content For 30wt%, 4kg second materials are added and are uniformly mixed, dry, pulverize to 90 mesh, be granulated, 50 DEG C of drying are improved rice production The compound fertilizer of amount.
Embodiment 4
A kind of compound fertilizer preparation method improving rice yield, includes the following steps:
S1,14kg p-aminophenyls trimethoxy silane, 0.4kg calcium lignosulfonates, 80kg water are uniformly mixed, use is dense It is 4-4.8 that degree, which is 5.2mol/l hydrochloric acid regulation system pH value, stirs 3.5h, and whipping temp is 12 DEG C, filters, washs, centrifuge, does It is dry, 57kg tetrahydrofurans are added and stir evenly, 0.13kg maleic anhydrides are added and stir 8h, whipping temp is 104 DEG C, precipitation, mistake Filter, washing, is dried to obtain first material;
S2,7kg first materials addition 12kg Macrogol 600s are uniformly mixed, are adjusted with a concentration of 2.4mol/l hydrochloric acid System pH is 3-3.8, stirs 6h, and whipping temp is 86 DEG C, centrifuges, filters, washing, vacuum drying obtains second material;
S3, by 105kg wormcasts, 40kg rotted pig manures, 12kg biogas residues, 22kg sunflower seed dregs, 4kg humic acids, 3kg bastard coals Mountain flour, 2.5kg medical stones, 1kg sawdusts, 0.2kg bactericidal deodorants, 0.17kgEM microbial inoculums are uniformly mixed, and adding water to water content is 24wt% is added 6kg second materials and is uniformly mixed, and dry, pulverize to 70 mesh, is granulated, 55 DEG C of drying are improved rice yield Compound fertilizer.
Embodiment 5
A kind of compound fertilizer preparation method improving rice yield, includes the following steps:
S1,13kg p-aminophenyls trimethoxy silane, 0.5kg calcium lignosulfonates, 70kg water are uniformly mixed, use is dense It is 4-4.8 that degree, which is 5.4mol/l hydrochloric acid regulation system pH value, stirs 3h, and whipping temp is 13 DEG C, filters, washs, centrifuge, does It is dry, 55kg tetrahydrofurans are added and stir evenly, 0.15kg maleic anhydrides are added and stir 7h, whipping temp is 106 DEG C, precipitation, mistake Filter, washing, is dried to obtain first material;
S2,6.5kg first materials addition 13kg Macrogol 600s are uniformly mixed, with a concentration of 22.1mol/l hydrochloric acid tune Section system pH is 3-3.8, stirs 7h, and whipping temp is 84 DEG C, centrifuges, filters, washing, vacuum drying obtains second material;
S3, by 110kg wormcasts, 38kg rotted pig manures, 16kg biogas residues, 20kg sunflower seed dregs, 6kg humic acids, 2.5kg coals Spoil powder, 3kg medical stones, 0.8kg sawdusts, 0.25kg bactericidal deodorants, 0.15kgEM microbial inoculums are uniformly mixed, and add water to water content For 27wt%, 5kg second materials are added and are uniformly mixed, dry, pulverize to 80 mesh, be granulated, 53 DEG C of drying are improved rice production The compound fertilizer of amount.
5 gained of embodiment is improved into the compound fertilizer of rice yield and common rice fertilizer carries out field trial, result It is as follows:
Embodiment 5 Common rice fertilizer
Average plant height, cm 124 118
Every plant of average dry weight, g 59 48
Mass of 1000 kernel, g 27.4 25.1
Yield, t/hm2 14.8 10.2
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (8)

1. a kind of compound fertilizer preparation method improving rice yield, which is characterized in that include the following steps:
S1, p-aminophenyl trimethoxy silane, calcium lignosulfonate, water being uniformly mixed, regulation system pH value is 4-4.8, Stirring is filtered, and is washed, and is centrifuged, dry, and tetrahydrofuran is added and stirs evenly, and maleic anhydride stirring is added, precipitates, and filtering is washed It washs, is dried to obtain first material;
S2, first material addition Macrogol 600 being uniformly mixed, regulation system pH value is 3-3.8, is stirred, and is centrifuged, filtering, Washing, vacuum drying obtain second material;
S3, by wormcast, rotted pig manure, biogas residue, sunflower seed dregs, humic acid, bastard coal mountain flour, medical stone, sawdust, deodorization and sterilization Agent, EM bacteria agent are uniformly mixed, and add water, and second material is added and is uniformly mixed, dry, pulverize, is granulated, and drying is improved rice production The compound fertilizer of amount.
2. improving the compound fertilizer preparation method of rice yield according to claim 1, which is characterized in that in S1, adjust body Be pH value be 4-4.8, stir 2-4h, whipping temp be 10-16 DEG C.
3. the compound fertilizer preparation method according to claim 1 or claim 2 for improving rice yield, which is characterized in that in S1, be added After maleic anhydride, 4-10h is stirred, whipping temp is 100-112 DEG C.
4. according to any one of the claim 1-3 compound fertilizer preparation methods for improving rice yield, which is characterized in that S1 In, p-aminophenyl trimethoxy silane, calcium lignosulfonate, water, tetrahydrofuran, maleic anhydride weight ratio be 10-16: 0.2-0.8:50-100:50-60:0.1-0.2.
5. according to any one of the claim 1-4 compound fertilizer preparation methods for improving rice yield, which is characterized in that S2 In, regulation system pH value is 3-3.8, stirs 4-10h, and whipping temp is 80-88 DEG C.
6. according to any one of the claim 1-5 compound fertilizer preparation methods for improving rice yield, which is characterized in that S2 In, the weight ratio of first material and Macrogol 600 is 5-8:10-16.
7. according to any one of the claim 1-6 compound fertilizer preparation methods for improving rice yield, which is characterized in that S3 In, it is 20-32wt% to add water to water content.
8. according to any one of the claim 1-7 compound fertilizer preparation methods for improving rice yield, which is characterized in that S3 In, wormcast, rotted pig manure, biogas residue, sunflower seed dregs, humic acid, bastard coal mountain flour, medical stone, sawdust, bactericidal deodorant, EM bacterium Agent, second material weight ratio be 100-120:32-45:10-20:15-25:2-10:1-4:2-4:0.5-1.2:0.1-0.4: 0.1-0.2:2-8.
CN201811017160.1A 2018-08-30 2018-08-30 A kind of compound fertilizer preparation method improving rice yield Pending CN108752122A (en)

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CN108752122A true CN108752122A (en) 2018-11-06

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005014505A1 (en) * 2003-08-06 2005-02-17 Department Of Science & Technology (Dst) A process for the manufacture of bio-release iron-manganese release fertilizer
CN103289098A (en) * 2013-05-24 2013-09-11 东莞上海大学纳米技术研究院 Organic silicon nano composite material and preparation method thereof
CN107021826A (en) * 2017-05-04 2017-08-08 全椒县王震家禽养殖专业合作社 One kind volume increase fertilizer conservation chicken manure Slow release organic fertilizer and preparation method thereof
CN107056547A (en) * 2017-05-04 2017-08-18 全椒县王震家禽养殖专业合作社 A kind of preparation method for the compound organic fertilizer for improving retention capacity of soil

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005014505A1 (en) * 2003-08-06 2005-02-17 Department Of Science & Technology (Dst) A process for the manufacture of bio-release iron-manganese release fertilizer
CN103289098A (en) * 2013-05-24 2013-09-11 东莞上海大学纳米技术研究院 Organic silicon nano composite material and preparation method thereof
CN107021826A (en) * 2017-05-04 2017-08-08 全椒县王震家禽养殖专业合作社 One kind volume increase fertilizer conservation chicken manure Slow release organic fertilizer and preparation method thereof
CN107056547A (en) * 2017-05-04 2017-08-18 全椒县王震家禽养殖专业合作社 A kind of preparation method for the compound organic fertilizer for improving retention capacity of soil

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