CN107792551A - A kind of triisopropyl borate ester storage device - Google Patents
A kind of triisopropyl borate ester storage device Download PDFInfo
- Publication number
- CN107792551A CN107792551A CN201610770239.6A CN201610770239A CN107792551A CN 107792551 A CN107792551 A CN 107792551A CN 201610770239 A CN201610770239 A CN 201610770239A CN 107792551 A CN107792551 A CN 107792551A
- Authority
- CN
- China
- Prior art keywords
- tank
- sealed shell
- control device
- borate ester
- triisopropyl borate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- -1 triisopropyl borate ester Chemical class 0.000 title claims abstract description 22
- 239000000498 cooling water Substances 0.000 claims abstract description 20
- 238000005057 refrigeration Methods 0.000 claims abstract description 8
- 238000006073 displacement reaction Methods 0.000 claims description 16
- 230000008859 change Effects 0.000 claims description 10
- 238000004891 communication Methods 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 3
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 3
- 239000004327 boric acid Substances 0.000 description 3
- 229910052796 boron Inorganic materials 0.000 description 3
- 238000004880 explosion Methods 0.000 description 3
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 208000021760 high fever Diseases 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 238000002207 thermal evaporation Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D88/00—Large containers
- B65D88/74—Large containers having means for heating, cooling, aerating or other conditioning of contents
- B65D88/744—Large containers having means for heating, cooling, aerating or other conditioning of contents heating or cooling through the walls or internal parts of the container, e.g. circulation of fluid inside the walls
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D90/00—Component parts, details or accessories for large containers
- B65D90/22—Safety features
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D90/00—Component parts, details or accessories for large containers
- B65D90/22—Safety features
- B65D90/38—Means for reducing the vapour space or for reducing the formation of vapour within containers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D90/00—Component parts, details or accessories for large containers
- B65D90/48—Arrangements of indicating or measuring devices
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
Abstract
The present invention discloses a kind of triisopropyl borate ester storage device, including a sealed shell of tank and the control device on sealed shell of tank, and the top of the sealed shell of tank is provided with feed tube, and its underpart is provided with drain pipe, sealed valve is mounted on feed tube and drain pipe；The bottom of described sealed shell of tank is additionally provided with cooling water pipeline, and the cooling water pipeline reaches the outer circulating pump by setting of sealed shell of tank and forms cooling water circulation passage, and the cooling water pipeline approach one refrigeration pond.The present invention is provided with the cooling-water duct of circulation in sealed shell of tank, the cooling-water duct passes through from refrigeration pond, the temperature in sealed shell of tank can be effectively reduced, sealed shell of tank is reached a metastable temperature range, ensures the stability of triisopropyl borate ester.
Description
Technical field
The present invention relates to triisopropyl borate ester manufacture to store, specifically a kind of triisopropyl borate ester storage device.
Background technology
Triisopropyl borate ester is without colourless transparent liquid, and as solvent, semiconductor boron diffusion source, being that one kind is very important has
Machine boron fine chemical material.Steam after triisopropyl borate ester heat is steamed can form explosive mixture with air, meet naked light, high fever
It can cause combustion explosion；It can be reacted with oxidant.If meet high fever high-temperature condition, container internal pressure increase, have cracking and it is quick-fried
Fried danger；Therefore requirement of the storage of triisopropyl borate ester to temperature is higher；And existing storage device is usually not set
The preferable cooling system of effect, while the equipment for being also not provided with the temperature and tank body pressure for monitoring, thus there is compared with
High potential safety hazard.
The content of the invention
The purpose of the present invention is in view of the deficienciess of the prior art, providing a kind of triisopropyl borate ester storage device.
Technical scheme：It is of the present invention solve the problems, such as used by technical scheme be：A kind of triisopropyl borate ester storage device, bag
A sealed shell of tank and the control device on sealed shell of tank are included, the top of the sealed shell of tank is provided with feed tube, its underpart
Drain pipe is installed, sealed valve is mounted on feed tube and drain pipe；The bottom of described sealed shell of tank is additionally provided with cold
But waterpipe, the cooling water pipeline reach the outer circulating pump by setting of sealed shell of tank and form cooling water circulation passage, and should
The refrigeration of cooling water pipeline approach one pond.
The arc-shaped elasticity inwall of inside lateral bend is additionally provided with inside the tank skin of described sealed shell of tank；Sealed shell of tank
Displacement transducer is also equipped with the inside of tank skin, the displacement transducer can sense its own change in displacement between elastic inwall；
The displacement transducer is connected with control device.
Further, pressure sensor and temperature sensor are also equipped with described sealed shell of tank；Described pressure passes
Sensor and temperature sensor are connected with control device.
Further, in addition to refrigerating plant, described refrigerating plant is by pipeline communication to sealed shell of tank, and freezes
Device is connected with control device.
Further, in addition to vacuum extractor；Described vacuum extractor by pipeline communication to sealed shell of tank, and
The vacuum extractor is connected with control device.
Further, it is provided with magnetic valve on the connecting pipe of described refrigerating plant and vacuum extractor；The electromagnetism
Valve is connected with control device.
Beneficial effect：The invention has the advantages that：
(1) present invention in sealed shell of tank be provided with circulation cooling-water duct, the cooling-water duct from refrigeration Chi Zhongtong
Cross, the temperature in sealed shell of tank can be effectively reduced, sealed shell of tank is reached a metastable temperature range, ensure boron
The stability of sour three isopropyl esters；
(2) the elastic inwall of arc is provided with the tank skin of sealed shell of tank of the invention, and is also provided with displacement sensing
Device monitors the change in displacement of elastic inwall, and when the pressure in sealed shell of tank changes, can extrude elastic inwall makes elastic inwall
Displacement change, therefore can be used to monitor the pressure change in tank body, and pressure sensing is also provided with sealed shell of tank
Device and temperature sensor, changed by the pressure and temp in three aspect close supervision sealed shell of tank；Increase safety coefficient；
(3) present invention is also provided with standby refrigerating plant；Cause in the hot weather such as summer or generation fire residence accident
When temperature in sealed shell of tank steeply rises, when pressure sensor and temperature sensor experience temperature and pressure change,
Control refrigerating plant to freeze by control device, cold air is drained into sealed shell of tank, make the reduction of its temperature, prevent boric acid three
Isopropyl ester evaporation mixes with air, explodes；
(4) present invention is also provided with standby vacuum extractor, if when the temperature of the triisopropyl borate ester in sealed shell of tank
Degree now controls vacuum extractor by tank because the other reasonses such as fire have occurred that the situation of thermal evaporation by control device
Internal air is extracted out, then controls closed electromagnetic valve, prevents triisopropyl borate ester and air mixed explosion, increases safety system
Number.
Brief description of the drawings
Fig. 1 is schematic structural view of the invention.
Embodiment
Below in conjunction with the accompanying drawings and specific embodiment, the present invention is furture elucidated, and the present embodiment is with technical solution of the present invention
Premised under implemented, it should be understood that these embodiments are only illustrative of the invention and is not intended to limit the scope of the invention.
As shown in figure 1, a kind of triisopropyl borate ester storage device, including a sealed shell of tank 1 and on sealed shell of tank 1
Control device 2, the top of the sealed shell of tank 1 is provided with feed tube 3, and its underpart is provided with drain pipe 4, feed tube 3 and goes out liquid
Sealed valve 5 is mounted on pipe 4；The bottom of described sealed shell of tank 1 is additionally provided with cooling water pipeline 6, the cooling water pipeline 6
Reach the outer circulating pump 7 by setting of sealed shell of tank 1 and form cooling water circulation passage, and the approach one of cooling water pipeline 5 is made
Cold drop 8.
The arc-shaped elasticity inwall 9 of inside lateral bend is additionally provided with inside the tank skin of described sealed shell of tank 1；Sealed shell of tank
Displacement transducer 10 is also equipped with the inside of 1 tank skin, the displacement transducer 10 can sense its own position between elastic inwall 9
Move change；The displacement transducer 10 is connected with control device 2.
Pressure sensor 11 and temperature sensor 12 are also equipped with described sealed shell of tank 1；Described pressure sensor
11 and temperature sensor 12 be connected with control device 2.
Also include refrigerating plant 13, described refrigerating plant 13 is by pipeline communication to sealed shell of tank 1, and refrigerating plant
13 are connected with control device 2.
Also include vacuum extractor 14；Described vacuum extractor 14 is by pipeline communication to sealed shell of tank 1, and this is taken out
Vacuum plant 14 is connected with control device 2；Magnetic valve is provided with the connecting pipe of refrigerating plant 13 and vacuum extractor 14
15；The magnetic valve 15 is connected with control device 2.
The present invention in sealed shell of tank be provided with circulation cooling-water duct, the cooling-water duct from refrigeration pond in by,
The temperature in sealed shell of tank can be effectively reduced, sealed shell of tank is reached a metastable temperature range, ensures boric acid
The stability of three isopropyl esters；
The elastic inwall of arc is provided with the tank skin of the sealed shell of tank of the present invention, and is also provided with displacement transducer prison
The change in displacement of elastic inwall is controlled, when the pressure in sealed shell of tank changes, can extrude elastic inwall makes the position of elastic inwall
Shifting changes, therefore can be used to monitor the pressure change in tank body, and be also provided with sealed shell of tank pressure sensor and
Temperature sensor, changed by the pressure and temp in three aspect close supervision sealed shell of tank；Increase safety coefficient.
The present invention is also provided with standby refrigerating plant；Cause to seal in the hot weather such as summer or generation fire residence accident
When temperature in tank body steeply rises, when pressure sensor and temperature sensor experience temperature and pressure change, pass through
Control device control refrigerating plant refrigeration, cold air is drained into sealed shell of tank, makes the reduction of its temperature, prevents the isopropyl of boric acid three
Ester evaporation mixes with air, explodes.
The present invention is also provided with standby vacuum extractor, if when the triisopropyl borate ester in sealed shell of tank temperature by
The situation of thermal evaporation is had occurred that in other reasonses such as fire, vacuum extractor is now controlled by tank body by control device
Air extract out, then control closed electromagnetic valve, prevent triisopropyl borate ester and air mixed explosion, increase safety coefficient.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (5)
- A kind of 1. triisopropyl borate ester storage device, it is characterised in that：Including a sealed shell of tank (1) and installed in sealed shell of tank (1) control device (2) on, the top of the sealed shell of tank (1) are provided with feed tube (3), and its underpart is provided with drain pipe (4), Sealed valve (5) is mounted on feed tube (3) and drain pipe (4)；The bottom of described sealed shell of tank (1) is additionally provided with cooling Waterpipe (6), the cooling water pipeline (6) reach sealed shell of tank (1) and form cooling water circulation by the circulating pump (7) of setting outside Passage, and cooling water pipeline (5) approach one refrigeration pond (8)；The arc-shaped elasticity inwall (9) of inside lateral bend is additionally provided with inside the tank skin of described sealed shell of tank (1)；Sealed shell of tank (1) displacement transducer (10) is also equipped with the inside of tank skin, the displacement transducer (10) can sense its own and elastic inwall (9) Between change in displacement；The displacement transducer (10) is connected with control device (2).
- A kind of 2. triisopropyl borate ester storage device according to claim 1, it is characterised in that：Described sealed shell of tank (1) pressure sensor (11) and temperature sensor (12) are also equipped with；Described pressure sensor (11) and temperature sensor (12) it is connected with control device (2).
- A kind of 3. triisopropyl borate ester storage device according to claim 1, it is characterised in that：Also include refrigerating plant (13), described refrigerating plant (13) is interior by pipeline communication to sealed shell of tank (1), and refrigerating plant (13) and control device (2) it is connected.
- A kind of 4. triisopropyl borate ester storage device according to claim 1, it is characterised in that：Also include vacuum extractor (14)；Described vacuum extractor (14) is interior by pipeline communication to sealed shell of tank (1), and the vacuum extractor (14) and control Device (2) is connected.
- A kind of 5. triisopropyl borate ester storage device according to claim 3 or 4, it is characterised in that：Described refrigeration dress Put and magnetic valve (15) is provided with the connecting pipe of (13) and vacuum extractor (14)；The magnetic valve (15) and control device (2) it is connected.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610770239.6A CN107792551A (en) | 2016-08-30 | 2016-08-30 | A kind of triisopropyl borate ester storage device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610770239.6A CN107792551A (en) | 2016-08-30 | 2016-08-30 | A kind of triisopropyl borate ester storage device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107792551A true CN107792551A (en) | 2018-03-13 |
Family
ID=61528258
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610770239.6A Pending CN107792551A (en) | 2016-08-30 | 2016-08-30 | A kind of triisopropyl borate ester storage device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107792551A (en) |
Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62216751A (en) * | 1986-03-19 | 1987-09-24 | Canon Inc | Detector for residual amount of ink |
| CN2164036Y (en) * | 1993-04-13 | 1994-05-04 | 任顺平 | Displacement measuring pressure sensor |
| CN2831067Y (en) * | 2005-07-20 | 2006-10-25 | 徐名勇 | Displacement pressure sensor |
| CN101006897A (en) * | 2007-02-07 | 2007-08-01 | 张亚晨 | Pressure type electric water kettle |
| CN201194732Y (en) * | 2008-03-28 | 2009-02-18 | 符井然 | Electric pressure cooker |
| CN202244841U (en) * | 2011-08-12 | 2012-05-30 | 南通烟滤嘴有限责任公司 | Filter stick glyceride centralized supply temperature control device |
| CN103210363A (en) * | 2010-09-12 | 2013-07-17 | 深圳纽迪瑞科技开发有限公司 | Displacement sensing touch panel and touch screen using the same |
| CN204297389U (en) * | 2014-11-14 | 2015-04-29 | 浙江巨圣氟化学有限公司 | A kind of monomer storage tank being applied to polytetrafluoroethylene |
| CN204896359U (en) * | 2015-08-05 | 2015-12-23 | 南通鸿志化工有限公司 | Storage device of three isopropyl esters of boric acid |
| CN205049267U (en) * | 2015-09-30 | 2016-02-24 | 福建上润精密仪器有限公司 | Non-contact pressure detection device |
| CN205169398U (en) * | 2015-11-26 | 2016-04-20 | 高超 | Volatile chemical engineering liquid material storing device |
| CN105730885A (en) * | 2016-03-16 | 2016-07-06 | 哈尔滨宏万智科技开发有限公司 | Vacuum sealing tank |
-
2016
- 2016-08-30 CN CN201610770239.6A patent/CN107792551A/en active Pending
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62216751A (en) * | 1986-03-19 | 1987-09-24 | Canon Inc | Detector for residual amount of ink |
| CN2164036Y (en) * | 1993-04-13 | 1994-05-04 | 任顺平 | Displacement measuring pressure sensor |
| CN2831067Y (en) * | 2005-07-20 | 2006-10-25 | 徐名勇 | Displacement pressure sensor |
| CN101006897A (en) * | 2007-02-07 | 2007-08-01 | 张亚晨 | Pressure type electric water kettle |
| CN201194732Y (en) * | 2008-03-28 | 2009-02-18 | 符井然 | Electric pressure cooker |
| CN103210363A (en) * | 2010-09-12 | 2013-07-17 | 深圳纽迪瑞科技开发有限公司 | Displacement sensing touch panel and touch screen using the same |
| CN202244841U (en) * | 2011-08-12 | 2012-05-30 | 南通烟滤嘴有限责任公司 | Filter stick glyceride centralized supply temperature control device |
| CN204297389U (en) * | 2014-11-14 | 2015-04-29 | 浙江巨圣氟化学有限公司 | A kind of monomer storage tank being applied to polytetrafluoroethylene |
| CN204896359U (en) * | 2015-08-05 | 2015-12-23 | 南通鸿志化工有限公司 | Storage device of three isopropyl esters of boric acid |
| CN205049267U (en) * | 2015-09-30 | 2016-02-24 | 福建上润精密仪器有限公司 | Non-contact pressure detection device |
| CN205169398U (en) * | 2015-11-26 | 2016-04-20 | 高超 | Volatile chemical engineering liquid material storing device |
| CN105730885A (en) * | 2016-03-16 | 2016-07-06 | 哈尔滨宏万智科技开发有限公司 | Vacuum sealing tank |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105066504A (en) | Refrigeration device of cooling suit | |
| CN105448357A (en) | Containment shell cooling system of floating nuclear power plant | |
| CN204297389U (en) | A kind of monomer storage tank being applied to polytetrafluoroethylene | |
| CN107792551A (en) | A kind of triisopropyl borate ester storage device | |
| CN107799188A (en) | A kind of containment pressure supression system | |
| WO2025162110A1 (en) | Cryogenic full containment tank | |
| CN203950555U (en) | There is after the nuclear power plant accident of heat conduction reactor pit exterior wall fused mass gaseous-waste holdup system in heap | |
| CN104648850A (en) | Alcohol storage tank | |
| CN205026985U (en) | Cooling suit refrigerating plant | |
| CN206786329U (en) | Ammonia tank thermal insulation system | |
| CN221334105U (en) | Safety interlocking control system of reaction kettle | |
| CN212492860U (en) | Jacket steam drum heating reactor system for experimental device | |
| CN209198961U (en) | A kind of chemical industry equipment temperature control device with warning device | |
| CN106264853A (en) | There is the automatic freeze therapy unit of heat insulation circulation line | |
| CN208997705U (en) | A kind of high security liquid chlorine gasification device | |
| CN208344999U (en) | A kind of transfer accumulating tank of propylene oxide | |
| CN209500855U (en) | A kind of Chinese materia medica preparation chemical component purity check distillation crystallization apparatus | |
| CN204214135U (en) | A kind of conduction oil loop heating system for enamel jacket type evaporating kettle | |
| CN205065281U (en) | Cold volume recovery unit of liquid chlorine complete evaporation | |
| CN114604868A (en) | Graphite purification furnace | |
| CN206738936U (en) | A kind of liquid carbon dioxide release device | |
| CN205718533U (en) | A kind of steam recycling device | |
| CN207235310U (en) | A kind of electric cabinet cooling system | |
| CN204237041U (en) | Temperature control system in a kind of high-purity phosphorus oxychloride liquid-supplying system | |
| CN206483169U (en) | Haplo-effect concentrator |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180313 |
|
| RJ01 | Rejection of invention patent application after publication |