CN107616545A - Fragrant line cassia bark essence and its application in a kind of ramuscule filter stick - Google Patents

Abstract

The invention belongs to ramuscule cigarette filter rod production technical field, and in particular to fragrant line cassia bark essence and its patent application of application in a kind of ramuscule filter stick.It is calculated in mass percent, it is composed of the following components：10.0 ~ 15.0% cassia oil, 1.0 ~ 2.0% bay leaves oil, 0.5 ~ 1.0% acetic acid cassia bark ester, 0.5 ~ 1.0% acetic acid, 0.2 ~ 0.5% eugenol, 0.2 ~ 0.5% linalool, 80.0 ~ 87.6% Glycerin, mixed triester with caprylic acid capric acid.The application is while fragrant line is with cassia bark essence in providing a kind of ramuscule cigarette with peat-reek, coordinate the improvement of ramuscule cigarette filter rod structure, ramuscule cigarette can preferably be improved sucks effect, and improvement effect is obvious, with preferable practical value, while abundant cigarette product type, design, exploitation and production and sales for new ramuscule cigarette have preferable Demonstration And Extension application value.

Description

A kind of cinnamon essence for fine filter stick medium incense thread and its application

technical field

The invention belongs to the technical field of slim cigarette filter rod production, and in particular relates to a patent application for a cinnamon essence for incense thread in a slim filter rod and its application.

Background technique

With the continuous improvement of people's living standards, there are more and more varieties of cigarettes on the cigarette market, which also provides consumers with more choices, and slim cigarettes are a typical example. Judging from the actual sales effect, slim cigarettes have conquered more and more consumers with their unique charm.

Judging from the quality of cigarettes, the tar content of slim cigarettes is generally lower than that of ordinary cigarettes, and the taste is also lighter, so it is more in line with the needs of specific consumers, especially urban women who pursue fashion, elegance and avant-garde life. special favor. With the rapid development of low-tar cigarettes, the advantages of slim cigarettes in "reducing tar and maintaining flavor" have attracted special attention.

Due to the inherent advantages of small cigarette volume and relatively low tar release, slim cigarettes also have problems such as light smoke and insufficient aroma, which also limits their popularization and application. For this reason, existing cigarette manufacturers are also solving this technical problem by reducing the pressure drop of filter rods and optimizing the structure of shredded tobacco.

Focusing on the flavor enhancement of slim cigarettes, in the existing technical ideas, flavor granules and flavor capsules are mainly used to supplement or increase the flavor of cigarettes. Short, poor coordination with smoke and other defects, so that the effect of improving the fragrance is not obvious enough. Therefore, it is extremely necessary to further improve the uniformity, stability and coordination of aroma enhancement through comprehensive means such as flavor formula and improvement of aroma enhancement methods on the basis of existing aroma enhancement methods.

Contents of the invention

The purpose of the present invention is to provide a kind of cinnamon essence for the fragrance thread in the slim filter stick, and cooperate with the improvement of the structure of the slim filter stick to further improve the flavoring effect of the slim cigarette while enriching the types of the slim cigarette.

The technical solution adopted by this application is described in detail as follows.

A kind of cinnamon essence for incense sticks in fine filter sticks, in terms of mass percentage, consists of the following components:

10.0~15.0% cinnamon oil, 1.0~2.0% laurel leaf oil,

0.5~1.0% cinnamon acetate, 0.5~1.0% acetic acid, 0.2~0.5% eugenol, 0.2~0.5% linalool,

80.0~87.6% caprylic capric acid glyceride.

Described cassia bark oil, can adopt finished product, or prepare with reference to following preparation method:

(1) After the dried cinnamon is crushed, pass through a 50-60 mesh sieve to obtain cinnamon powder;

(2) Take a certain amount of cinnamon powder and put it into a distillation flask, add a certain amount of distilled water, and steam distill for 4~5 hours to obtain a distillate with oil and water layers;

(3) Extract the oil phase in the distillate with dichloromethane, and dry it with anhydrous sodium sulfate;

(4) After filtering the oil obtained in step (3), the solvent was evaporated in a water bath at 55° C. to obtain cinnamon essential oil.

Described osmanthus leaf oil, can adopt finished product, or prepare with reference to following preparation method:

(1) Crush the dried osmanthus leaves and pass through a 50-60 mesh sieve to obtain osmanthus leaf powder;

(2) Take a certain amount of cinnamon leaf powder and put it into a distillation flask, add a certain amount of distilled water, and steam distill for 4~5 hours to obtain a distillate with oil and water layers;

(3) Extract the oil phase in the distillate with dichloromethane, and dry it with anhydrous sodium sulfate;

(4) After filtering the oil agent obtained in step (3), the solvent was evaporated in a water bath at 55° C. to obtain bay leaf essential oil.

The cinnamon essence used for the incense thread in the thin filter stick, the specific formula is, for example: 13.0% cinnamon oil, 1.5% cinnamon leaf oil, 0.8% cinnamon acetate, 0.8% acetic acid, 0.3% eugenol, 0.3 % linalool, 83.3% caprylic capric glyceride.

The application of the cinnamon essence for thin filter rods in cigarettes is used for fine cigarette filter rods.

A thin composite filter rod with built-in cinnamon essence and fragrance thread. The composite filter rod is wrapped with molding paper outside, and the inside is composed of ordinary acetate fiber filter rod section and built-in cinnamon essence and fragrance thread acetate fiber filter rod section. The cinnamon flavor and fragrance line acetate fiber filter rod section is close to the cut tobacco section;

Ordinary acetate filter rod section and acetate fiber filter rod section with built-in cinnamon flavor and fragrance thread, the section shape of the acetate fiber tow used is Y-shaped, and the tow specification requirements are: single denier is 6.0den~11.0den, and total denier is 15000den~ 17000den;

The length ratio of the ordinary acetate filter rod section to the built-in cinnamon essence and fragrance thread acetate filter rod section can be adjusted according to the suction resistance or the demand for flavor enhancement. The specific length ratio is, for example, 1:1;

The built-in cinnamon essence fragrance thread acetate fiber filter rod section has a built-in fragrance thread in the middle, and the fragrance thread is adsorbed with cinnamon essence; its preparation process can be prepared according to the existing technology, specifically: the fragrant thread enters the filter rod after coming out of the thread roller. Before the stick forming machine, the flavor is applied through the flavoring system equipped with a certain concentration of cinnamon flavor;

The specific specifications of the composite filter rod are, for example: the length is 120mm, the circumference is 16.90mm, and the pressure drop is 2600Pa~4200Pa.

The amount of essence applied to a single filter stick of the fine-branched incense thread filter stick is 10 mg to 30 mg.

Slim cigarettes are prepared by using the slim composite filter stick with built-in cinnamon essence and fragrance thread.

The present invention firstly prepares a cinnamon-flavored essence with a special fragrance by independently designing the essence formula, and uses it as an aroma-enhancing additive in the fine-branched incense thread filter rod to prepare a fine-branch composite filter rod with the cinnamon-flavored filter rod. Because cinnamon bark contains phenylacrylic acid compounds, it has a therapeutic effect on benign prostatic hyperplasia, and can increase the blood flow of prostate tissue and promote the improvement of local tissue blood supply; at the same time, cinnamon bark also has medicinal effects. Traditional Chinese medicine believes that cinnamon bark is hot in nature and has the effect of warming the stomach. It has the functions of dispelling cold, activating blood and relaxing tendons, dredging channels, relieving pain and relieving diarrhea. Therefore, the flavor provided by this application can partially reduce the harm of tobacco products to human health while enriching the types of flavors.

Preliminary application shows that when the composite filter rod of slim incense thread is used in slim cigarettes, it not only improves the uniformity of flavor application and the stability of release, but also improves the coordination between aroma and product sensory quality. Since the cinnamon essence applied is obtained from natural substances, these aroma substances can further highlight the "roasted sweet" aroma of cigarettes after entering the cigarette smoke, improve the aroma fullness and fullness of slim cigarettes, and then improve its quality. Smoking quality and sensory comfort.

Compared with the existing perfuming technology, the main advantages of the present invention are:

(1) The process is simple: the preparation process of the present invention is simple, no need to make significant adjustments to the current production process and equipment, no need for large-scale equipment and expensive reagents, simple operation and easy control;

(2) Safe and hygienic: the raw and auxiliary materials adopted in the present invention are widely used in the field of food processing, and there is no problem of toxic reagent residue, so they are safe and reliable;

(3) Stable release: The compound filter stick with built-in incense thread used in the present invention helps to slow down the loss of aroma while avoiding direct contact with the incense thread in the mouth.

In general, while providing a cinnamon essence with a special flavor for the incense thread in slim cigarettes, this application can better improve the smoking effect of slim cigarettes, and improve the effect Obviously, it has good practical value. While enriching the types of cigarette products, it has good demonstration, promotion and application significance for the design, development, production and sales of new slim cigarettes.

Description of drawings

Fig. 1 is the structural representation of the thin composite filter stick with built-in cinnamon essence fragrance thread provided by the present invention;

Fig. 2 is a schematic diagram of the structure of slim cigarettes prepared by using the slim composite filter stick with built-in cinnamon essence and flavor thread.

detailed description

The present application will be further explained below in conjunction with the embodiments. Before introducing specific examples, it should be noted that the materials used in the following examples, such as cinnamon oil, laurel leaf oil, cinnamon acetate, acetic acid, eugenol, linalool, caprylic glyceride, etc. The products of Treasure Biotechnology Co., Ltd.; incense sticks, fine filter sticks, etc. are also produced according to the existing technology.

Example 1

The cinnamon essence for the incense thread in the thin filter stick provided in this embodiment is composed of the following components in terms of mass percentage:

10.0% cinnamon oil, 1.0% laurel leaf oil, 0.5% cinnamon acetate, 0.5% acetic acid, 0.2% eugenol, 0.2% linalool, 87.6% caprylic capric acid glyceride.

According to the prior art, a thin composite filter stick with built-in cinnamon essence and fragrance thread is prepared, as shown in Figures 1 and 2, the prepared composite filter stick 3 is wrapped with molding paper on the outside, and the inside is composed of ordinary acetate fiber filter stick section 2 and built-in filter stick. The cinnamon essence, fragrance thread and vinegar fiber filter rod section 1 is compounded, and the cinnamon essence and fragrance thread acetate fiber filter rod section 1 is built close to the shredded tobacco section 4;

Ordinary acetate fiber filter rod section 2, the cross-sectional shape of the acetate fiber tow used is Y-shaped, and the specification of the tow is: 6.0Y/17000 (den/den);

Built-in cinnamon essence fragrance thread acetate filter rod section 2, the cross-sectional shape of the acetate tow used is Y-shaped, and the specification of the tow is: 8.0Y/15000 (den/den);

The length ratio of the ordinary acetate filter stick section to the built-in cinnamon essence fragrance thread acetate filter stick section is 1:1; the specific specifications of the composite filter stick are: the length is 120mm, and the circumference is 16.90mm (in Fig. 2, In actual use, the length of the filter tip is 30mm (that is, the structural length of part 1+2 in Figure 2)).

When preparing the fine-branched composite filter stick with built-in cinnamon essence and fragrance thread, it is carried out according to the existing filter rod production process. First, the fragrance thread applied with cinnamon essence is inserted into the center of the filter rod through a filter rod forming machine to make a fragrance thread filter rod. , and then through the filter stick compound machine and ordinary cellulose acetate filter sticks, it is formed into a fine-branched incense thread binary composite filter stick (the fine-branched composite filter stick with built-in cinnamon essence and fragrance thread). After molding, the measurement results show that the amount of cinnamon essence for incense thread in each composite filter stick is about 20mg (that is, the amount of 120mm long filter stick is 20mg).

According to the existing technology, the thin composite filter stick with built-in cinnamon flavor and fragrance thread is wound with the tobacco sample to form a thin cigarette sample as a test sample, and a blank control sample (blank fragrance thread is added at the same position of the filter stick) is used as a test sample. For the control sample, 7 professional sensory evaluators conducted detection and suction evaluation on the test sample and the control sample respectively. For specific smoke test results and specific smoking evaluation scores, see the table below.

The results of smoking evaluation show that after adding cinnamon essence, the "cinnamon" aroma of the cigarette sample is obvious, the aroma richness of the smoke is improved to a certain extent, the irritation is reduced, the miscellaneous gas is reduced, the fineness of the smoke is improved, and the aftertaste is improved .

Example 2

The cinnamon essence for the incense thread in the thin filter stick provided in this embodiment is composed of the following components in terms of mass percentage:

13.0% cinnamon oil, 1.5% laurel leaf oil, 0.8% cinnamon acetate, 0.8% acetic acid, 0.3% eugenol, 0.3% linalool, 83.3% caprylic capric acid glycerides.

With the filter stick specifications of Example 1, a thin composite filter stick with built-in cinnamon essence and fragrance thread was prepared. After molding, the measurement results show that the application amount of cinnamon essence for incense thread in each composite filter stick is about 20 mg.

The slim composite filter stick with the built-in cinnamon flavor and fragrance thread and the tobacco sample were rolled into a slim cigarette sample as a test sample, and the smoking evaluation was carried out.

The results of smoking evaluation show that after adding cinnamon essence, the "cinnamon aroma" of the cigarette sample is more obvious, the aroma richness of the smoke is significantly increased, the irritation is significantly reduced, the miscellaneous gas is reduced, the fineness of the smoke is significantly improved, and the aftertaste is significantly improved .

Example 3

The cinnamon essence for the incense thread in the thin filter stick provided in this embodiment is composed of the following components in terms of mass percentage:

15.0% cinnamon oil, 2.0% laurel leaf oil, 1.0% cinnamon acetate, 1.0% acetic acid, 0.5% eugenol, 0.5% linalool, 80.0% caprylic capric acid glyceride.

With the filter stick specifications of Example 1, a thin composite filter stick with built-in cinnamon essence and fragrance thread was prepared. After molding, the measurement results show that the application amount of cinnamon essence for incense thread in each composite filter stick is about 20 mg.

The slim composite filter stick with the built-in cinnamon flavor and fragrance thread and the tobacco sample were rolled into a slim cigarette sample as a test sample, and the smoking evaluation was carried out.

The results of smoking evaluation show that after adding cinnamon essence, the "cinnamon aroma" of the cigarette samples is very obvious, the smoke aroma coordination is reduced, the irritation is increased, the miscellaneous gas is reduced, the smoke coordination is poor and there is an uncomfortable smell. Sweet and greasy, the aftertaste is not as good as normal cigarettes (compared with control cigarettes).

The composite filter sticks prepared in different examples were tested. In addition, the total particulate matter and tar in the mainstream smoke of cigarettes were determined according to the method of "GB/T 19609-2004 Determination of total particulate matter and tar by smoking machine for routine analysis of cigarettes". Indicators such as tar, nicotine and moisture were tested, and the specific results are shown in the table below.

Table 1, the detection results of the thin composite filter sticks with built-in cinnamon essence and fragrance thread prepared in different embodiments:

;

Table 2. Physical indicators and mainstream smoke test results of different cigarette samples:

;

As can be seen from the data in Table 1 above, compared with normal cellulose acetate tow filter sticks, there is no significant difference in the physical indicators of the filter sticks with cinnamon sticks. It can be seen from the data in Table 2 that, compared with the normal cigarettes of the control example, the mainstream smoke of the cinnamon-flavored cigarettes did not change significantly, and the key indicators affecting the senses of the cigarettes did not change significantly, such as tar and nicotine.

Table 3, the sensory quality evaluation results of different cigarette samples:

.

From the results in Table 3, it can be seen that the sensory quality of cigarettes can be significantly improved by using the composite filter stick of cinnamon flavor and fragrance thread. reduce.

To sum up, through the targeted design of flavor formulas for incense filter sticks with specific flavors and applying them to cigarettes, the aroma characteristics of cigarettes can be significantly improved when smoking, and the smoking experience can be enriched and enhanced. The thread filter stick can avoid the rapid loss of conventional incense thread filter sticks, and is safe and hygienic at the same time. Therefore, this application, as a novel cinnamon-flavored thin incense thread composite filter stick that highlights the "cinnamon bark" fragrance of cigarettes and improves smoking quality, has a certain promotion and application value in the industry.

Claims (5)

1. A kind of 1. fragrant line cassia bark essence in ramuscule filter stick, it is characterised in that it is calculated in mass percent, it is composed of the following components：

   10.0 ~ 15.0% cassia oil, 1.0 ~ 2.0% bay leaves oil,

   0.5 ~ 1.0% acetic acid cassia bark ester, 0.5 ~ 1.0% acetic acid, 0.2 ~ 0.5% eugenol, 0.2 ~ 0.5% linalool,

   80.0 ~ 87.6% Glycerin, mixed triester with caprylic acid capric acid.
2. 2. fragrant line cassia bark essence in ramuscule filter stick as claimed in claim 1, it is characterised in that specific formula is：13.0% osmanthus Skin oil, 1.5% bay leaves oil, 0.8% acetic acid cassia bark ester, 0.8% acetic acid, 0.3% eugenol, 0.3% linalool, 83.3% Glycerin, mixed triester with caprylic acid capric acid；

   Or it is：15.0% cassia oil, 2.0% bay leaves oil, 1.0% acetic acid cassia bark ester, 1.0% acetic acid, 0.5% cloves Phenol, 0.5% linalool, 80.0% Glycerin, mixed triester with caprylic acid capric acid；

   Or it is：10.0% cassia oil, 1.0% bay leaves oil, 0.5% acetic acid cassia bark ester, 0.5% acetic acid, 0.2% cloves Phenol, 0.2% linalool, 87.6% Glycerin, mixed triester with caprylic acid capric acid.
3. 3. application of the fragrant line with cassia bark essence in cigarette in the ramuscule filter stick of claim 1 or 2, it is characterised in that be used for Fragrant line in ramuscule cigarette filter rod.
4. 4. a kind of ramuscule composite filter of built-in cassia bark essence perfume (or spice) line, it is characterised in that the composite filter outer wrap has into Type paper, inside is combined by common vinegar fibre filter rod segments and built-in cassia bark essence perfume (or spice) line vinegar fibre filter rod segments, wherein built-in cassia bark is fragrant The fragrant line vinegar fibre filter rod segments of essence are close to pipe tobacco section；

   Common vinegar fibre filter rod segments and built-in cassia bark essence perfume (or spice) line vinegar fibre filter rod segments, the cross sectional shape of diacetate fiber used are Y types, silk Beam specification requires：Single-strand is 6.0den ~ 11.0den, and total denier is 15000den ~ 17000den；

   The length ratio of common vinegar fibre filter rod segments and built-in cassia bark essence perfume (or spice) line vinegar fibre filter rod segments is 1:1；

   The built-in cassia bark essence perfume (or spice) line vinegar fibre filter rod segments, its middle part are built-in with fragrant line, and fragrant line is adsorbed with cassia bark essence.
5. 5. existed using ramuscule cigarette, its feature prepared by the ramuscule composite filter of built-in cassia bark essence perfume (or spice) line described in claim 4 In the essence applied amount of single branch filter stick is 10mg ~ 30mg.