CN107603736A - Fragrant line ambrein and its application in a kind of ramuscule filter stick - Google Patents

Abstract

The invention belongs to the technical field of slim cigarette filter rod production, and in particular relates to a patent application for an ambergris essence used for incense thread in a slim filter rod and its application. In terms of mass percentage, it consists of the following components: 2.0~5.0% ambrox, 0.2~0.5% muskone, 0.5~1.0% rose oil, 0.5~1.0% vetiver oil, 1.0~2.0% 0.2-0.5% isopropanol, 0.2-0.5% ionone, 0.2-0.5% decanal, 89.5-95.4% caprylic glyceride. This application not only provides a kind of ambergris essence with special flavor for slim cigarette medium incense thread, but also improves the smoking effect of slim cigarettes with the improvement of the filter rod structure of slim cigarettes, and the improvement effect is obvious. Good practical value, while enriching the types of cigarette products, has good demonstration, promotion and application significance for the design, development, production and sales of new slim cigarettes.

Description

A kind of ambergris essence and its application

technical field

The invention belongs to the technical field of slim cigarette filter rod production, and in particular relates to a patent application for an ambergris essence used for incense thread in a slim filter rod and its application.

Background technique

With the continuous improvement of people's living standards, there are more and more varieties of cigarettes on the cigarette market, which also provides consumers with more choices, and slim cigarettes are a typical example. Judging from the actual sales effect, slim cigarettes have conquered more and more consumers with their unique charm.

Judging from the quality of cigarettes, the tar content of slim cigarettes is generally lower than that of ordinary cigarettes, and the taste is also lighter, so it is more in line with the needs of specific consumers, especially urban women who pursue fashion, elegance and avant-garde life. special favor. With the rapid development of low-tar cigarettes, the advantages of slim cigarettes in "reducing tar and maintaining flavor" have attracted special attention.

Due to the inherent advantages of small cigarette volume and relatively low tar release, slim cigarettes also have problems such as light smoke and insufficient aroma, which also limits their popularization and application. For this reason, existing cigarette manufacturers are also solving this technical problem by reducing the pressure drop of filter rods and optimizing the structure of shredded tobacco.

Focusing on the flavor enhancement of slim cigarettes, in the existing technical ideas, flavor granules and flavor capsules are mainly used to supplement or increase the flavor of cigarettes. Short, poor coordination with smoke and other defects, so that the effect of improving the fragrance is not obvious enough. Therefore, it is extremely necessary to further improve the uniformity, stability and coordination of aroma enhancement through comprehensive means such as flavor formula and improvement of aroma enhancement methods on the basis of existing aroma enhancement methods.

Contents of the invention

The purpose of the present invention is to provide an ambergris essence for the fragrance thread in slim filter sticks, and at the same time cooperate with the improvement of the structure of the slim filter sticks to further improve the flavor-enhancing effect of slim cigarettes while enriching the types of slim cigarettes .

The technical scheme adopted by this application is described in detail as follows.

A kind of ambergris essence for fragrance thread in fine-branched filter sticks, which is composed of the following components in terms of mass percentage:

2.0~5.0% ambrox, 0.2~0.5% muscone, 0.5~1.0% rose oil,

0.5~1.0% vetiver oil, 1.0~2.0% isopropanol, 0.2~0.5% ionone, 0.2~0.5% decanal,

89.5~95.4% caprylic capric acid glyceride.

Described rose oil, can adopt finished product, or prepare with reference to following preparation method:

(1) After the dried rose is crushed, pass through a 50-60 mesh sieve to obtain rose powder;

(2) Take a certain amount of rose powder and put it into a distillation flask, add a certain amount of distilled water, and steam distill for 4~5 hours to obtain a distillate with oil and water layers;

(3) Extract the oil phase in the distillate with dichloromethane, and dry it with anhydrous sodium sulfate;

(4) After filtering the oil agent obtained in step (3), the solvent was evaporated in a water bath at 55°C to obtain rose essential oil.

The ambergris essence used for the incense thread in the thin filter stick, the specific formula is, for example: 3.0% ambrox, 0.3% muskone, 0.8% rose oil, 0.8% vetiver oil, 1.5% iso Propanol, 0.4% Ionone, 0.3% Capric Aldehyde, 92.9% Caprylic Capric Glycerides.

The application of the ambergris flavoring essence for thin filter rods in cigarettes is used for fine cigarette filter rods.

A thin composite filter rod with built-in ambergris flavor and fragrance thread, the composite filter rod is wrapped with molding paper outside, and the inside is composed of ordinary acetate fiber filter rod section and built-in ambergris flavor and fragrance thread acetate fiber filter rod section, Among them, the built-in ambergris essence fragrance line acetate fiber filter rod section is close to the cut tobacco section;

Ordinary acetate filter rod section and built-in ambergris flavoring thread acetate fiber filter rod section, the cross-sectional shape of the acetate fiber tow used is Y-shaped, and the tow specification requirements are: single denier: 6.0den~11.0den, total denier: 15000den ~17000den;

The length ratio of the ordinary acetate filter rod section to the built-in ambergris fragrance thread acetate filter rod section can be adjusted according to the suction resistance or aroma enhancement requirements, and the specific length ratio is, for example, 1:1;

The built-in ambergris essence fragrance thread acetate fiber filter rod section has a built-in fragrance thread in the middle, and the fragrance thread is adsorbed with ambergris essence; its preparation process can be prepared according to the existing technology, specifically: after the fragrance thread comes out of the thread roll Before entering the filter rod forming machine, the fragrance is applied through the fragrance system equipped with a certain concentration of ambergris essence;

The specific specifications of the composite filter rod are, for example: the length is 120mm, the circumference is 16.90mm, and the pressure drop is 2600Pa~4200Pa.

The amount of essence applied to a single filter stick of the fine-branched incense thread filter stick is 10 mg to 30 mg.

Slim cigarettes are prepared by utilizing the slim composite filter stick with built-in ambergris essence and fragrance thread.

In the present invention, an ambergris-flavored essence with a special fragrance is firstly prepared by independently designing the essence formula, which is used as an aroma-enhancing additive in the fine-branched incense thread filter rod, and a thin-branch composite filter rod with ambergris fragrance is prepared. . Because ambergris has the effects of resuscitating phlegm, promoting blood circulation and promoting qi, the present application can partially reduce the harmfulness of tobacco to human health while enriching the types of existing essence products.

Preliminary application shows that when the composite filter rod of slim incense thread is used in slim cigarettes, it not only improves the uniformity of flavor application and the stability of release, but also improves the coordination between aroma and product sensory quality. Since the applied ambergris flavor is obtained from natural substances, these aroma substances can further highlight the "roasted sweet" aroma of cigarettes after entering the cigarette smoke, improve the aroma fullness and fullness of slim cigarettes, and then improve Its smoking quality and sensory comfort.

Compared with the existing perfuming technology, the main advantages of the present invention are:

(1) The process is simple: the preparation process of the present invention is simple, no need to make significant adjustments to the current production process and equipment, no need for large-scale equipment and expensive reagents, simple operation and easy control;

(2) Safe and hygienic: the raw and auxiliary materials adopted in the present invention are widely used in the field of food processing, and there is no problem of toxic reagent residue, so they are safe and reliable;

(3) Stable release: The compound filter stick with built-in incense thread used in the present invention helps to slow down the loss of aroma while avoiding direct contact with the incense thread in the mouth.

In general, while providing a kind of ambergris essence with special flavor for the fragrance thread of slim cigarettes, the application can better improve the smoking effect of slim cigarettes and improve the The effect is obvious, and it has good practical value. While enriching the types of cigarette products, it has good demonstration, popularization and application significance for the design, development, production and sales of new slim cigarettes.

Description of drawings

Fig. 1 is the structural representation of the thin composite filter stick with built-in ambergris essence fragrance thread provided by the present invention;

Fig. 2 is a schematic diagram of the structure of a slim cigarette prepared by using a slim composite filter stick with a built-in ambergris flavor thread.

detailed description

The present application will be further explained below in conjunction with the embodiments. Before introducing the specific examples, it should be noted that the ambrox, muscone, rose oil, vetiver oil, isopropanol, ionone, decanal, caprylic glyceride, etc. used in the following examples The materials are all products of Shanghai Huabao Biotechnology Co., Ltd.; incense sticks, fine filter rods, etc. are also produced according to the existing technology.

Example 1

The ambergris essence for fine filter stick medium incense thread provided in this embodiment is composed of the following components in terms of mass percentage:

2.0% Ambrox, 0.2% Muscone, 0.5% Rose Oil, 0.5% Vetiver Oil, 1.0% Isopropanol, 0.2% Ionone, 0.2% Decylaldehyde, 95.4% Octyl Glyceryl caprate.

According to the prior art, a fine-branched composite filter stick with built-in ambergris flavor and fragrance thread is prepared, as shown in Figures 1 and 2, the prepared composite filter stick 3 is wrapped with molding paper on the outside, and the inside is made of ordinary acetate fiber filter stick section 2 and The built-in ambergris essence fragrance thread vinegar fiber filter rod section 1 is compounded, and the built-in ambergris essence fragrance thread vinegar fiber filter rod section 1 is close to the shredded tobacco section 4;

Ordinary acetate fiber filter rod section 2, the cross-sectional shape of the acetate fiber tow used is Y-shaped, and the specification of the tow is: 6.0Y/17000 (den/den);

Built-in ambergris essence fragrance thread acetate filter rod section 2, the cross-sectional shape of the acetate tow used is Y-shaped, and the tow specification requirement is: 8.0Y/15000 (den/den);

The length ratio of the common acetate filter stick section to the built-in ambergris flavor thread acetate filter stick section is 1:1; the specific specifications of the composite filter stick are: the length is 120 mm, and the circumference is 16.90 mm (in Fig. 2 , in actual use, the length of the filter tip is 30mm (that is, the structural length of part 1+2 in Figure 2)).

When preparing the fine-branched composite filter stick with built-in ambergris flavor and fragrance thread, it is carried out according to the existing filter rod production process, firstly, the fragrance thread with ambergris flavor added is put into the center of the filter rod through a filter rod forming machine to make a fragrance thread The filter stick is then formed into a fine-branched incense thread binary composite filter rod (the fine-branched composite filter rod with built-in ambergris essence fragrance thread) by a filter rod compound machine and an ordinary cellulose acetate filter rod. After molding, the measurement results show that the amount of ambergris essence for incense thread in each composite filter stick is about 20mg (that is, the amount of 120mm long filter stick is 20mg).

According to the existing technology, the thin composite filter stick with the built-in ambergris flavor and fragrance thread is wound with the tobacco sample to form a thin cigarette sample as the test sample, and a blank control sample is set at the same time (blank fragrance thread is added at the same position of the filter stick) As a control sample, 7 professional sensory evaluators conducted detection and suction evaluation on the test sample and the control sample respectively. For specific smoke test results and specific smoking evaluation scores, see the table below.

The results of smoking evaluation show that after the addition of ambergris flavor, the cigarette sample has a significant aroma of "ambergris", the richness of the aroma of the smoke is improved, the irritation is reduced, the miscellaneous gas is reduced, the fineness of the smoke is improved, and the aftertaste is strong. improved.

Example 2

The ambergris essence for fine filter stick medium incense thread provided in this embodiment is composed of the following components in terms of mass percentage:

3.0% Ambrox, 0.3% Muscone, 0.8% Rose Oil, 0.8% Vetiver Oil, 1.5% Isopropanol, 0.4% Ionone, 0.3% Decylaldehyde, 92.9% Octyl Glyceryl caprate.

With the filter stick specifications of Example 1, a thin composite filter stick with built-in ambergris essence and fragrance thread was prepared. After molding, the measurement results show that the amount of ambergris essence applied for incense thread in each composite filter stick is about 20 mg.

The slim composite filter stick with the built-in ambergris flavor line and the tobacco sample were coiled into a slim cigarette sample as a test sample, and the smoking evaluation was carried out.

The results of the smoking evaluation show that after adding ambergris flavor, the "ambergris" of the cigarette samples is more obvious, the aroma richness of the smoke is significantly increased, the irritation is significantly reduced, the miscellaneous gas is reduced, the fineness of the smoke is significantly improved, and the aftertaste Significant improvement.

Example 3

The ambergris essence for fine filter stick medium incense thread provided in this embodiment is composed of the following components in terms of mass percentage:

5.0% Ambrox, 0.5% Muscone, 1.0% Rose Oil, 1.0% Vetiver Oil, 2.0% Isopropanol, 0.5% Ionone, 0.5% Decylaldehyde, 89.5% Octyl Glyceryl caprate.

With the filter stick specifications of Example 1, a thin composite filter stick with built-in ambergris essence and fragrance thread was prepared. After molding, the measurement results show that the amount of ambergris essence applied for incense thread in each composite filter stick is about 20 mg.

The slim composite filter stick with the built-in ambergris flavor line and the tobacco sample were coiled into a slim cigarette sample as a test sample, and the smoking evaluation was carried out.

The results of smoking evaluation show that after adding ambergris flavor, the "ambergris" of the cigarette samples is very obvious, the aroma coordination of the smoke is reduced, the irritation is increased, the miscellaneous gas is reduced, the coordination of the smoke is poor, and there is an unpleasant smell. Comfortable sweetness, aftertaste is not as good as normal cigarettes (compared with control cigarettes).

The composite filter sticks prepared in different examples were tested. In addition, the total particulate matter and tar in the mainstream smoke of cigarettes were determined according to the method of "GB/T 19609-2004 Determination of total particulate matter and tar by smoking machine for routine analysis of cigarettes". Indicators such as tar, nicotine and moisture were tested, and the specific results are shown in the table below.

Table 1, the detection results of the thin composite filter sticks with built-in ambergris fragrance thread prepared in different embodiments:

;

Table 2. Physical indicators and mainstream smoke test results of different cigarette samples:

.

It can be seen from the data in Table 1 above that, compared with the normal cellulose acetate tow filter stick, there is no significant difference in the physical indicators of the filter stick with the ambergris thread placed there. It can be seen from the data in Table 2 that, compared with the normal cigarettes of the control example, the mainstream smoke of the ambergris cigarettes did not change significantly, and the key indicators affecting the sense of cigarettes such as tar and nicotine did not change significantly.

Table 3, the sensory quality evaluation results of different cigarette samples:

.

From the results in Table 3, it can be seen that the sensory quality of cigarettes can be significantly improved by using the composite filter stick of ambergris flavor and flavor thread. Great reduction.

To sum up, through the targeted design of flavor formulas for incense filter sticks with specific flavors and applying them to cigarettes, the aroma characteristics of cigarettes can be significantly improved when smoking, and the smoking experience can be enriched and enhanced. The thread filter stick can avoid the rapid loss of conventional incense thread filter sticks, and is safe and hygienic at the same time. Therefore, this application, as a novel ambergris-flavored fine-branched incense thread composite filter stick that highlights the "ambergris" fragrance of cigarettes and improves smoking quality, has certain promotion and application value in the industry.

Claims (5)

1. Ambergris essence for fragrant thread in a thin filter stick, it is characterized in that, by mass percentage, it is made up of following components: 2.0~5.0% ambrox, 0.2~0.5% muscone, 0.5~1.0% rose oil, 0.5~1.0% vetiver oil, 1.0~2.0% isopropanol, 0.2~0.5% ionone, 0.2~0.5% decanal, 89.5~95.4% caprylic capric acid glyceride. 2. as claimed in claim 1, the ambergris essence for incense sticks in fine filter sticks is characterized in that the specific formula is: 3.0% ambrox, 0.3% muscone, 0.8% rose oil, 0.8% Vetiver oil, 1.5% isopropanol, 0.4% ionone, 0.3% decanal, 92.9% caprylic glyceride; Or: 5.0% ambrox, 0.5% muscone, 1.0% rose oil, 1.0% vetiver oil, 2.0% isopropanol, 0.5% ionone, 0.5% decanal, 89.5 % caprylic capric acid glyceride; Or: 2.0% ambrox, 0.2% muscone, 0.5% rose oil, 0.5% vetiver oil, 1.0% isopropanol, 0.2% ionone, 0.2% decanal, 95.4 % caprylic capric glycerides. 3. The application of the ambergris flavoring essence for the thin filter stick middle-flavor thread according to claim 1 or 2 in cigarettes, characterized in that it is used for the fine-count cigarette filter stick middle-flavor thread. 4. A thin composite filter stick with built-in ambergris flavor and fragrance thread, characterized in that, the composite filter rod is wrapped with molding paper outside, and the inside is filtered by ordinary acetate fiber filter rod section and built-in ambergris essence and fragrance thread vinegar fiber The stick section is compounded, and the built-in ambergris flavor and fragrance fiber acetate filter stick section is close to the tobacco section; Ordinary acetate filter rod section and built-in ambergris flavoring thread acetate fiber filter rod section, the cross-sectional shape of the acetate fiber tow used is Y-shaped, and the tow specification requirements are: single denier: 6.0den~11.0den, total denier: 15000den ~17000den; The length of the ordinary acetate filter rod section and the built-in ambergris fragrance thread acetate filter rod section is 1:1; The built-in ambergris essence fragrance thread acetate filter stick section has a built-in fragrance thread in the middle, and the fragrance thread is adsorbed with ambergris essence. 5. The slim cigarettes prepared by using the slim composite filter stick with built-in ambergris flavor and fragrance thread according to claim 4, characterized in that the amount of flavor applied to a single filter stick is 10 mg to 30 mg.