[go: up one dir, main page]

CN1073997A - Dyeing method for bulk cotton fibres - Google Patents

Dyeing method for bulk cotton fibres Download PDF

Info

Publication number
CN1073997A
CN1073997A CN 91112719 CN91112719A CN1073997A CN 1073997 A CN1073997 A CN 1073997A CN 91112719 CN91112719 CN 91112719 CN 91112719 A CN91112719 A CN 91112719A CN 1073997 A CN1073997 A CN 1073997A
Authority
CN
China
Prior art keywords
cotton
minutes
water
dyeing
dye
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN 91112719
Other languages
Chinese (zh)
Other versions
CN1025964C (en
Inventor
扬雪涛
施兴德
张建英
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiufeng Dyeing Mill Co., Ltd., Yuyao
Original Assignee
JIUFENG DYEING FACTORY YUYAO
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=4911044&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CN1073997(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by JIUFENG DYEING FACTORY YUYAO filed Critical JIUFENG DYEING FACTORY YUYAO
Priority to CN 91112719 priority Critical patent/CN1025964C/en
Publication of CN1073997A publication Critical patent/CN1073997A/en
Application granted granted Critical
Publication of CN1025964C publication Critical patent/CN1025964C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/58Material containing hydroxyl groups
    • D06P3/60Natural or regenerated cellulose
    • D06P3/62Natural or regenerated cellulose using direct dyes
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/58Material containing hydroxyl groups
    • D06P3/60Natural or regenerated cellulose
    • D06P3/6025Natural or regenerated cellulose using vat or sulfur dyes

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Coloring (AREA)

Abstract

A kind of dyeing method for bulk cotton fibres changes over traditional after stain cotton spinning of spinning earlier to dye the back spinning process earlier.The water boiling-off that cotton is put into refining agent RAS-1 is earlier cleaned with heat, cold water, changes next procedure dyeing again, uses warm water cleaning after the dyeing.For making cotton fiber soft and anti-crisp, carry out spinnability after the dyeing again and handle.This method is not wanted special installation and just can be produced, therefore suitable especially small enterprise produces, look cotton look, light cylinder difference that this method is produced are little, soft, bulk, substantially solved loose colour, faded, problem such as staining, cotton knot, COLOR FASTNESS, reduced and returned yarn, winder multiple tracks iterative process is for market increases bright and colourful clothes and lining.

Description

Dyeing method for bulk cotton fibres
The present invention relates to a kind of processing method, dyeing method for bulk cotton fibres.(cotton is meant skin rod cotton or saw ginned cotton).
Coat is because of good water absorption in the all-cotton knitting, and gas permeability is strong, and is antistatic, easily decontamination, and the quality softness, fashionable whole international market, existing cotton sportswear more is subjected to people's favor, the process of after stain makes but the many employings of commercially available knitwear are knitted earlier.Thereby the color dullness, designs and varieties are few, and technical process is longer, and cotton is spun into a yarn through the cotton mill, and the shape of completion strand more just can go dyeing, and dying needs again fall a yarn for weaving cotton cloth or doing knitwear usefulness strand shape after good.It is more to repeat operation back and forth, and time-consuming, effort causes unnecessary waste, and easily causes defective product when yarn-dyed, piece dyeing.
The object of the present invention is to provide a kind of dyeing method for bulk cotton fibres, the process that traditional elder generation's spinning is dyeed again changes over the process of directly spinning again with cotton dyeing, and the horn of plenty people's lives provide the more clothes and the garment material of multi-color kind.
The present invention is achieved in that
1. to the bulk cotton fibres boiling-off: put cotton into bath raio 1: 15 at normal temperatures, contain in the water of 3~4 gram/every premium on currency refining agents, be warmed up to 100 ℃ of insulations 30~60 minutes, bleed off whole pin water, water cleans.
2. dyeing: earlier dyestuff has been put into accelerant glauber salt 5~15%(bulk cotton fibres percentage by weight); bath raio 1: 15~20; in the dye vat that temperature is 40~60 ℃; the bulk cotton fibres of putting into again after the boiling-off is warmed up to 90~100 ℃, be incubated 60 minutes, bleeds off whole pin water after the cooling; change water and clean up; remain on room temperature~60 and ℃ add glacial acetic acid, reach color-fixing agent (Y) 5~8% or detergent (105) 2%, be incubated 20~30 minutes and clean up with warm water.
3. spinnability is handled: just add 0.5~1% peregal zero and maybe will dye look cotton after good with warm water cleaning and put into the aqueous solution that is mixed with 40 ℃ by peregal 0 0.5~1%, softener 2~3%, urea 1%, turkey red oil 2~7% with bathing to handle then when fixation, be warmed up to 55~70 ℃ of insulations 20 minutes.
Fig. 1. cotton boiling-off heating curve figure of the present invention.
Fig. 2. dyeing course heating curve figure of the present invention.
Fig. 3. spinnability is handled heating curve figure.
Below in conjunction with accompanying drawing embodiments of the invention are further described.
Contain a lot of commensals in the cotton fiber, as wax, nitrogenous thing, pectin thing, mineral and natural colouring matter, seed coat etc., the existence of these commensals will badly influence the wettability of cotton fiber, makes road, back dyeing difficulty, so must at first remove.Select the unidirectional circulation that opening is big, easy to operate, penetrability is strong for use, bath raio is applicable to the Nc464B type flock dyeing machine operation that cotton fiber dyes greatly under loose condition (of surface).Select existing clean result for use, have the multiple function of infiltration, emulsification again concurrently, not only satisfy the dyeing requirement, and reduce the cotton loss, shorten the RAS-1 refining agent of process time.
1. at first to the bulk cotton fibres boiling-off, at normal temperatures cotton being lifted up into dye vat discharges water by regulating the bath amount at 1: 15 again, add refining agent RAS-1 in 3~4 gram/every premium on currency ratios, and turn on pump closes vapour insulation 30~60 minutes after opening vapour and being warmed up to 100 ℃ to the cotton boiling-off, bleed off whole pin water after cooked, clean behind the secondary again to clean up to the pH value of refining liquid with 85~90 ℃ hot water and reach 7~8 for extremely near neutrality with cold water.
2. dyeing: with direct dyeing (dying bright red, pink, purplish red), with sulfur dyeing (dye coffee, dark blue, first look, blackish green, grass green etc.).
A. direct dyes select for use the fast scarlet 4 BS dyestuff to dye large red.Glauber salt (Na 2SO 4) 10~15%, glacial acetic acid (HAC content 89%) 0.6~1%, color-fixing agent (Y) 5~8%, with warm water making beating, boiling water impulsive motion, dye bath ratio 1: 15 is too small to cause uneven dyeing dyestuff, and excessive then look shallow.Cotton after the boiling-off put into above-mentioned raw materials and put the dye solution of 1/2 glauber salt earlier, temperature is controlled at 60 ℃, and be warmed up to 100 ℃ with 1 ℃/minute speed, again 1/2 glauber salt is added in the dye solution after spending 5 minutes, play the short effect of dying, be incubated 60 minutes, be cooled to 80 ℃, pin water is given out light, washing prevents that totally residual glauber salt or salt from causing color-fixing agent to lose efficacy, make temperature be controlled at 60 ℃ again, regulate pH value before the fixation, use color-fixing agent (Y) 5~8% to carry out fixation again 6~6.5, to improve wet colour fastness, add glacial acetic acid (HAC) 0.6~1% again, be incubated 30 minutes, with Warm Wash cleared-out cylinder.
This method dye bright red bulk cotton fibres, technology is easy to control, Dry Sack is even, the cylinder difference is little, price is low, finished product is soft.
B. SULPHUR DYES is dyed coffee color:
Raw material sulfur red brown b3r, sulfur yellow brown 6g, sulphur black BR consumption are decided on shade, total amount be 8~14% earlier with turkey red oil with dyestuff furnishing pulpous state, being dissolved in 90 ℃ of sulfur-bearing cholines (akali sulphide is 1~2 times of SULPHUR DYES consumption) and 2~3% soda ash (is softening of water, prevents H 2The S gaseous contamination) in the dye liquor, dye bath ratio was controlled at 1: 20, to hang in above-mentioned prescription initial temperature through the cotton of boiling-off and be to soak after 10 minutes in 40 ℃ the dye liquor and add 5~10% glauber salt, cross that the speed with 1 ℃ of per minute is warmed up to 90 ℃ after 10 minutes, be incubated and reduce to 70 ℃ after 60 minutes and bleed off whole pin water, changing water cleans because of sulfur red brown b3r dyeing rear oxidation speed needs eccysis more slowly and dyes akali sulphide on the thing, at room temperature handle 10 minutes removal loose colours with glacial acetic acid 2~3%, add detergent (105) 2% again, speed with 2 ℃ of per minutes was warmed up to 60 ℃ of soap boilings after 20 minutes, the cooling washing is clean, removes loose colour.Use glacial acetic acid HAC oxidation fastness to descend with sulphur red brown and seldom can carry out fixation.
Cotton fiber is through boiling-off, wax, fat have been removed, dyeing under alkali condition again, make that the cotton fiber feel is coarse hardens, drying room temperature and moisture regain control is improper also to cause cotton knot in the cotton spinning process, broken end is many brings difficulty to spinning, therefore carries out the short liquor ratio softness in cotton dyeing back and oils and contaminate and anti-crisp processing at once.
3. spinnability is handled:
A. use direct dyes: in fixation, add 0.5~1% peregal zero bath processing together, then with going out cylinder behind 50 ℃ of Warm Wash secondaries.
B. use SULPHUR DYES: 2~7%(directly pours into by turkey red oil), softener (HC) 2~3%(elder generation cold water making beating boiling water impulsive motion), urea 1%(makes SULPHUR DYES do anti-crisp processing) be mixed with spinnability solution.The above-mentioned solution softness that the look cotton is put into 40 ℃ of the initial temperatures dip dyeing treatment that oils, and rise to 55 ℃ of insulations with the speed of 1 ℃ of per minute and cylinder in 20 minutes again through dewatering, break into pieces by hand, under 55~70 ℃ temperature, dry with R456 cylinder suction-type dryer, cotton dyeing is all finished, and the color relation that becoming you needs can change next procedure over to.
The present invention is compared with prior art: it does not need special equipment just can produce, therefore the especially suitable small enterprise of the method produces, the cotton look of the look that this method is produced, light cylinder difference is little, soft, bulk, basically solved loose colour, fade and staining, cotton knot, the problems such as color fastness, traditional after stain cotton spinning of spinning is earlier changed over and dyes earlier rear spinning process, for a blank has been filled up in textile industry, for improving the people's livelihood, increase varieties and designs and produce bright and colourful knitted underwear and coat or garment material, but also can reduce yarn-dyed, the piece dyeing defective product improves the feel of finished product, has reduced and has returned yarn, winder multiple tracks technology, reduce cost, shorten the process-cycle, look cotton loss improves the utilization rate of cotton than I, and very big economic benefit and social benefit are arranged.

Claims (6)

1, a kind of processing method dyeing method for bulk cotton fibres is characterized in that:
One. to the bulk cotton fibres boiling-off: put cotton into bath raio 1: 15 at normal temperatures, contain in the water of 3~4 gram/every premium on currency refining agents, be warmed up to 100 ℃ of insulations 30~60 minutes, bleed off whole pin water, water cleans.
Two. dyeing: earlier dyestuff has been put into accelerant glauber salt 5~15% (bulk cotton fibres percentage by weight); bath raio 1: 15~20; in the dye vat that temperature is 40~60 ℃; the bulk cotton fibres of putting into again after the boiling-off is warmed up to 90~100 ℃, is incubated 60 minutes, bleeds off whole pin water after the cooling; change water and clean up; remain on room temperature~60 ℃, add glacial acetic acid and color-fixing agent (y) 5~8% or detergent (105) 2%, be incubated 20~30 minutes and clean up with warm water.
Three. spinnability is handled: just add 0.5~1% paregal O and put into the spinnability solution that is mixed with 40 ℃ by paregal O 0.5~1%, softener 2~3%, urea 1%, turkey red oil 2~7% with bathing the look cotton of handling after maybe will dying with warm water cleaning then when fixation, be warmed up to 50~55 ℃ of insulations 20 minutes.
2, colouring method according to claim 1 is characterized in that refining agent is RAS-1, bleeds off whole pin water after the boiling-off, cleans the pH value that cleans up to refining liquid with cold water again behind the secondary with 85~90 ℃ hot water and reaches till 7~8 near neutrality.
3, colouring method according to claim 1, its feature dyestuff selects for use direct dyes fast scarlet 4 BS x% to dye large red, glauber salt (Na2SO4) 10~15% puts 1/2 earlier, glacial acetic acid (HAC of 89% content) 0.6~1%, color-fixing agent (Y) 5~8%; bath raio 1: 15; cotton after the boiling-off is put into above-mentioned dye solution; temperature is controlled at 60 ℃ and be warmed up to 100 ℃ with 1 ℃/minute speed; cross again will be other after 5 minutes 1/2 glauber salt add in the dye solution; be incubated 60 minutes and is cooled to 80 ℃, bleed off pin water and clean up, keeps the preceding adjusting of 60 ℃ of fixation pH value 6~6.5; to use color-fixing agent (Y) 5~8% fixation; add glacial acetic acid 0.6~1% again, be incubated 30 minutes, use warm water cleaning.
4, colouring method according to claim 1, it is characterized in that dyestuff selects SULPHUR DYES for use, sulfur red brown b3r, sulfur yellow brown 6g, sulphur black BR total amount is that 8~14%(dyes coffee color), earlier with turkey red oil with dyestuff furnishing pulpous state, be dissolved in the dye liquor of 90 ℃ of sulfur-bearing cholines and 2~3% soda ash, dye bath ratio was controlled at 1: 20, to put into initial temperature through the cotton of boiling-off is to add 5~10% glauber salt after 40 ℃ dye liquor soaks 10 minutes, cross after 10 minutes and to be warmed up to 90 ℃ of insulations with 1 ℃/minute speed and to reduce to 70 ℃ after 60 minutes and bleed off whole pin water, changing water cleans, adding glacial acetic acid 2~3% at room temperature handled 10 minutes, add detergent (105) 2% again, be warmed up to 60 ℃ of soap boilings after 20 minutes with 2 ℃/minute speed, the cooling washing is clean.
5,, when fixation, just add 0.5~1% peregal zero bath processing together when it is characterized in that adopting direct dyeing, then with going out cylinder behind 50 ℃ of Warm Wash secondaries according to claim 1 or 3 described colouring methods.
6, according to claim 1 or 4 described colouring methods, the look cotton that it is characterized in that adopting sulfur dyeing is put into the spinnability solution softness dip dyeing treatment that oils, and rises to 55 ℃ of insulations 20 minutes with 1 ℃/minute speed.
CN 91112719 1991-12-31 1991-12-31 Cotton loose fiber processing method Expired - Fee Related CN1025964C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 91112719 CN1025964C (en) 1991-12-31 1991-12-31 Cotton loose fiber processing method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 91112719 CN1025964C (en) 1991-12-31 1991-12-31 Cotton loose fiber processing method

Publications (2)

Publication Number Publication Date
CN1073997A true CN1073997A (en) 1993-07-07
CN1025964C CN1025964C (en) 1994-09-21

Family

ID=4911044

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 91112719 Expired - Fee Related CN1025964C (en) 1991-12-31 1991-12-31 Cotton loose fiber processing method

Country Status (1)

Country Link
CN (1) CN1025964C (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101514304B (en) * 2009-04-08 2011-05-11 宋子奎 Colored textile hyperchromic washing agent
CN103643366A (en) * 2013-12-09 2014-03-19 常熟市梦迪安家饰用品有限公司 Method for producing cotton fiber colored spun yarn
CN103911782A (en) * 2014-03-19 2014-07-09 绍兴国周纺织新材料有限公司 Loose fiber dyeing process
CN103981734A (en) * 2014-05-16 2014-08-13 苏州市吴中区大明针织漂染有限公司 Fiber staining method
CN107217500A (en) * 2017-07-27 2017-09-29 合肥远科服装设计有限公司 A kind of colouring method of cotton fabric
CN113334870A (en) * 2021-06-07 2021-09-03 红豆集团无锡红豆童装有限公司 Double-layer yarn-dyed fabric based on organic cotton and preparation method thereof

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1324176C (en) * 2003-05-08 2007-07-04 宁波百隆纺织有限公司 Dyeing and spinning method for loose cotton fiber
CN1687500B (en) * 2005-04-30 2010-05-26 浙江华孚色纺有限公司 Soft cotton dyed yarn and production method thereof

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101514304B (en) * 2009-04-08 2011-05-11 宋子奎 Colored textile hyperchromic washing agent
CN103643366A (en) * 2013-12-09 2014-03-19 常熟市梦迪安家饰用品有限公司 Method for producing cotton fiber colored spun yarn
CN103911782A (en) * 2014-03-19 2014-07-09 绍兴国周纺织新材料有限公司 Loose fiber dyeing process
CN103911782B (en) * 2014-03-19 2016-03-30 绍兴国周纺织新材料有限公司 A kind of loose stock dyeing technique
CN103981734A (en) * 2014-05-16 2014-08-13 苏州市吴中区大明针织漂染有限公司 Fiber staining method
CN107217500A (en) * 2017-07-27 2017-09-29 合肥远科服装设计有限公司 A kind of colouring method of cotton fabric
CN113334870A (en) * 2021-06-07 2021-09-03 红豆集团无锡红豆童装有限公司 Double-layer yarn-dyed fabric based on organic cotton and preparation method thereof

Also Published As

Publication number Publication date
CN1025964C (en) 1994-09-21

Similar Documents

Publication Publication Date Title
CN101525851A (en) Reactive dye ultra-short rapid dyeing and fixation technology method
CN1865559B (en) Milk protein fiber or its filament or its blended fabric weaving and dyeing method
CN101407983B (en) Method for dyeing real silk fabric cheese
CN106939515B (en) The preparation of ball warp mercerization and efficient silkete penetrating agent in a kind of production of denim fabric
CN101748601B (en) Aging processing method for colored fabric
CN111188208A (en) Printing and dyeing process of cloth
CN1285799C (en) Soybean fiber loose-stock dyeing and processing method
CN1025964C (en) Cotton loose fiber processing method
CN106917302A (en) A kind of dyeing of silk fabrics
CN110042650A (en) The water-saving pre-treating technology of polyester woven fabric and its application
CN102619112A (en) Dyeing method of acrylic fiber fabric
CN103215713B (en) Production method of bastose wet spinning yarn
CN1091819C (en) Cotton loose-stock dyeing method
CN111088705A (en) Production method of dark knitwear with high color fastness to washing
KR100513084B1 (en) Improvements in dyeing and finishing of cellulosic fabric
CN100485113C (en) Dyeing method of copper ammonia fiber and tencel interwoven fabric
CN110055773B (en) Two-bath Dyeing Process of PLA/PHBV Blended Silk/Tencel Interwoven Fabric
CN107354774A (en) A kind of dyeing and finishing technology for improving the mutual dyefastness of blending brushed fabrics spliced together
CN111172786A (en) Green efficient ecological printing and dyeing method
CN104452364A (en) Machine washable dyeing method for jacquard fabric of wool / acrylic fiber blended yarn
CN110184805A (en) A kind of anti-return of inflaming retarding fabric dye jigger slurry is stained with technique
CN1528975A (en) Cotton loose fiber dyeing method
CN108193530A (en) A kind of people cotton and the colouring method of beautiful color blended yarn weaved fabric
CN1397681A (en) Method for dyeing cotton loose fibers by indigo dye
CN1250830A (en) Method for dyeing animal protein fibre, such as wool,with cationic dye

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C53 Correction of patent for invention or patent application
COR Change of bibliographic data

Free format text: CORRECT: PATENTEE; FROM: YUYAO JIUFENG DYEING FACTORY TO: YUYAO JIUFENG DYEING PLANT CO., LTD.

CP01 Change in the name or title of a patent holder

Patentee after: Jiufeng Dyeing Mill Co., Ltd., Yuyao

Patentee before: Jiufeng Dyeing Factory, Yuyao

C15 Extension of patent right duration from 15 to 20 years for appl. with date before 31.12.1992 and still valid on 11.12.2001 (patent law change 1993)
OR01 Other related matters
ASS Succession or assignment of patent right

Owner name: YUYAO JIUFENG DYEING PLANT CO., LTD.; YUYAO JIANI

Free format text: FORMER OWNER: YUYAO JIUFENG DYEING PLANT CO., LTD.

Effective date: 20031010

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20031010

Patentee after: Jiufeng Dyeing Mill Co., Ltd., Yuyao

Patentee after: Yuyao Jiani color cotton Co. Ltd.

Patentee before: Jiufeng Dyeing Mill Co., Ltd., Yuyao

ASS Succession or assignment of patent right

Owner name: YUYAO JIUFENG DYEING PLANT CO., LTD.

Free format text: FORMER OWNER: YUYAO JIUFENG DYEING PLANT CO., LTD.; YUYAO JIANI COLOR COTTON CO., LTD.

Effective date: 20070615

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20070615

Address after: 315400 No. 358 East Street, Yuyao, Zhejiang

Patentee after: Jiufeng Dyeing Mill Co., Ltd., Yuyao

Address before: 315400 Sanjiang mouth, Yuyao, Zhejiang

Co-patentee before: Yuyao Jiani color cotton Co. Ltd.

Patentee before: Jiufeng Dyeing Mill Co., Ltd., Yuyao

C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee