CN107136558B - A kind of preparation method of chu chrysanthemum flavored type cigarette filter - Google Patents
A kind of preparation method of chu chrysanthemum flavored type cigarette filter Download PDFInfo
- Publication number
- CN107136558B CN107136558B CN201710530558.4A CN201710530558A CN107136558B CN 107136558 B CN107136558 B CN 107136558B CN 201710530558 A CN201710530558 A CN 201710530558A CN 107136558 B CN107136558 B CN 107136558B
- Authority
- CN
- China
- Prior art keywords
- chu chrysanthemum
- chrysanthemum
- cigarette filter
- type cigarette
- chu
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 235000007516 Chrysanthemum Nutrition 0.000 title claims abstract description 54
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 244000189548 Chrysanthemum x morifolium Species 0.000 title 1
- 241000723353 Chrysanthemum Species 0.000 claims abstract description 55
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 34
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 24
- 239000002071 nanotube Substances 0.000 claims abstract description 16
- 229920001661 Chitosan Polymers 0.000 claims abstract description 15
- 239000000654 additive Substances 0.000 claims abstract description 14
- 230000000996 additive effect Effects 0.000 claims abstract description 14
- 150000001875 compounds Chemical class 0.000 claims abstract description 13
- 239000000463 material Substances 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 9
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000203 mixture Substances 0.000 claims abstract description 6
- 239000002893 slag Substances 0.000 claims abstract description 5
- 238000000605 extraction Methods 0.000 claims abstract description 4
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 4
- 238000001035 drying Methods 0.000 claims abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 239000012153 distilled water Substances 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 4
- 238000007796 conventional method Methods 0.000 claims description 3
- 239000000284 extract Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 1
- 206010013786 Dry skin Diseases 0.000 claims 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- 240000007594 Oryza sativa Species 0.000 claims 1
- 235000007164 Oryza sativa Nutrition 0.000 claims 1
- 229960000583 acetic acid Drugs 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 238000004321 preservation Methods 0.000 claims 1
- 235000009566 rice Nutrition 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 8
- 238000001027 hydrothermal synthesis Methods 0.000 abstract description 4
- 230000003110 anti-inflammatory effect Effects 0.000 abstract description 3
- 230000003340 mental effect Effects 0.000 abstract description 3
- 230000015572 biosynthetic process Effects 0.000 abstract description 2
- 238000000227 grinding Methods 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 210000000697 sensory organ Anatomy 0.000 abstract description 2
- 238000003786 synthesis reaction Methods 0.000 abstract description 2
- 239000003610 charcoal Substances 0.000 abstract 1
- 239000000571 coke Substances 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 12
- 230000006378 damage Effects 0.000 description 7
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 5
- 238000004939 coking Methods 0.000 description 5
- 230000003247 decreasing effect Effects 0.000 description 5
- 239000003546 flue gas Substances 0.000 description 5
- 235000005633 Chrysanthemum balsamita Nutrition 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- 239000003463 adsorbent Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
Landscapes
- Agronomy & Crop Science (AREA)
- Chemical & Material Sciences (AREA)
- Botany (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Materials Engineering (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of preparation methods of chu chrysanthemum flavored type cigarette filter, using nano-titanium dioxide as raw material, pass through hydro-thermal method synthesis of titanium dioxide nanotube in sodium hydroxide solution, then titania nanotube and chitosan solution are blended, chitosan is made to be carbonized to obtain chitosan charcoal titania nanotube sorbing material using hydro-thermal process, being sufficiently mixed with chu chrysanthemum oil makes chu chrysanthemum oil be supported in sorbing material, the chu chrysanthemum dry powder blend that remaining chrysanthemum slag drying and grinding obtains with extraction chu chrysanthemum oil uniformly obtains compound additive, compound additive is uniformly sprinkling upon on filter stick tow, it carries out processing and forming and chu chrysanthemum flavored type cigarette filter is made.Both there is cigarette filter produced by the present invention the excellent coke that subtracts to drop evil effect, and flavouring, the suction taste for improving cigarette can be played the role of, meet the sense organ needs of consumer, while the health-care efficacy also with anti-inflammatory fall fire, relieving mental strain and helping sleep while reducing and health is damaged.
Description
Technical field
The present invention relates to technical field of cigarettes more particularly to a kind of preparation methods of chu chrysanthemum flavored type cigarette filter.
Background technology
As people increasingly increase the concern of health problem, lowering harm and decreasing coking is carried out to cigarette and has become current development
Trend, cigarette industry also take many measures to reduce harm of the cigarette smoke to human body.Filter tip is in the lowering harm and decreasing coking of cigarette
In play the role of it is vital, wherein in filter tip add adsorbent can play good lowering harm and decreasing coking effect.But subtracting
While evil tar reduction, also accordingly bring cigarette flavor, inhale the negative effects such as taste decrease.Chu chrysanthemum is important Chinese medicine, main
Composition has nearly hundred kinds of flavonoids, volatile oil, amino acids and microelement kind etc..Document《The constituent analysis of chu chrysanthemum volatile oil
And its application in cigarette》Cigarette flavor can be enhanced, reduce flue gas irritation, improve and inhale taste by recording chu chrysanthemum absolute oil.In chu chrysanthemum
The ingredient contained also has the effect of flat liver removing toxic substances.But the waste that single chu chrysanthemum absolute oil not only causes resource is added into filter tip,
And it inhales taste and is easily interfered, and lowering harm and decreasing coking effect is bad by taste miscellaneous in flue gas.In order to give full play to chu chrysanthemum in cigarette
In beneficial effect, it is necessary to utilize the compound filter tip of the feature development of chu chrysanthemum.
Invention content
The object of the invention be exactly in order to make up prior art the defects of, provide a kind of lowering harm and decreasing coking effect it is good, improve inhale taste
It works well, and the preparation method of the chu chrysanthemum flavored type cigarette filter with health-care efficacy.
The present invention is achieved by the following technical solutions：
A kind of preparation method of chu chrysanthemum flavored type cigarette filter, includes the following steps：
（1）By nano-titanium dioxide and sodium hydroxide solution by weight 1：（10-20）It adds in after mixing closed
Insulation reaction 24-48h, cooling wash the distillation of obtained solid after filtering under the conditions of 120-160 DEG C in autoclave
It washs, dry, obtain titania nanotube；
（2）By step（1）Obtained titania nanotube is with chitosan, acetum by weight 1：（5-10）：
（500-1000）Then prior to 40-80 DEG C stirring 0.5-1h after mixing is added in closed autoclave in 150-200 DEG C of guarantor
Obtained solid, after cooling, filtering is washed with distilled water, dries, obtain chitosan charcoal-titanium dioxide and receive by temperature reaction 24-48h
Mitron sorbing material；
（3）It extracts chu chrysanthemum oil according to a conventional method from chrysanthemum, then washs the Daisy slag after extraction simultaneously with clear water
It is dry complete in 80-90 DEG C, and 100-200 mesh is ground to, obtained chu chrysanthemum dry powder is spare；
（4）By step（2）Obtained chitosan charcoal-titania nanotube sorbing material and step（3）Obtained chu chrysanthemum
Oil is by weight 1：（0.5-1）10-15min is mixed, adds step（3）Obtained chu chrysanthemum dry powder blend is uniformly answered
Additive is closed, then compound additive is uniformly sprinkling upon on filter stick tow, finally carries out processing and forming, chu chrysanthemum flavored type volume is made
Cigarette filter tip.
The nano-titanium dioxide is P25 type nano-titanium dioxides.
The concentration of sodium hydroxide solution is 8-10mol/L.
The acetum mass fraction is 4-8%.
The additive amount by compound additive is 10-15mg/10mm tow.
It is an advantage of the invention that：
The present invention passes through hydro-thermal method synthesis of titanium dioxide nanometer using nano-titanium dioxide as raw material in sodium hydroxide solution
Then titania nanotube and chitosan solution are blended, chitosan are made to be carbonized to obtain chitosan using hydro-thermal process by pipe
Charcoal-titania nanotube sorbing material, being sufficiently mixed with chu chrysanthemum oil makes chu chrysanthemum oil be supported in sorbing material, with extracting chu chrysanthemum
The chu chrysanthemum dry powder blend that the remaining chrysanthemum slag drying and grinding of oil obtains uniformly obtains compound additive, and compound additive is uniform
It is sprinkling upon on filter stick tow, carries out processing and forming and chu chrysanthemum flavored type cigarette filter is made.A part of nuisance when flue gas passes through filter tip
Matter is adsorbed by chu chrysanthemum dry powder and is retained, and a part is made when having the sorbing material of chu chrysanthemum oil through overload with flue gas by eluting
It is combined with sorbing material, while chu chrysanthemum oil wash is taken off, carried out flavoring while harmful substances in flue gas and miscellaneous gas is removed, have
Effect drop evil improves and inhales taste, and chu chrysanthemum oil can also play the role of anti-inflammatory fall fire, relieving mental strain and helping sleep.Cigarette filter produced by the present invention
Mouth both subtracted burnt drop evil effect with excellent, and can play the role of flavouring, the suction taste for improving cigarette, and human body is good for reducing
Health meets the sense organ needs of consumer, while the health-care efficacy also with anti-inflammatory fall fire, relieving mental strain and helping sleep while damage.
Specific embodiment
A kind of preparation method of chu chrysanthemum flavored type cigarette filter, includes the following steps：
（1）By nano-titanium dioxide and sodium hydroxide solution by weight 1：10 to add in closed high pressure after mixing anti-
It answers the interior insulation reaction under the conditions of 120 DEG C of kettle for 24 hours, obtained solid is washed with distilled water after cooling, filtering, is dried, is obtained
Titania nanotube；
（2）By step（1）Obtained titania nanotube is with chitosan, acetum by weight 1：5：500 mixing
Then prior to 40-80 DEG C stirring 0.5h afterwards is added in closed autoclave in 150 DEG C of insulation reactions for 24 hours, cooling, filtering
Obtained solid is washed with distilled water afterwards, is dried, obtains chitosan charcoal-titania nanotube sorbing material；
（3）It extracts chu chrysanthemum oil according to a conventional method from chrysanthemum, then washs the Daisy slag after extraction simultaneously with clear water
It is dry complete in 80 DEG C, and 100 mesh are ground to, obtained chu chrysanthemum dry powder is spare；
（4）By step（2）Obtained chitosan charcoal-titania nanotube sorbing material and step（3）Obtained chu chrysanthemum
Oil is by weight 1：0.5 is mixed 10min, adds step（3）Obtained chu chrysanthemum dry powder blend uniformly obtains compound addition
Then compound additive is uniformly sprinkling upon on filter stick tow by agent, finally carry out processing and forming, and the filter of chu chrysanthemum flavored type cigarette is made
Mouth.
The nano-titanium dioxide is P25 type nano-titanium dioxides.
The concentration of sodium hydroxide solution is 8mol/L.
The acetum mass fraction is 4%.
The additive amount by compound additive is 10mg/10mm tow.
Claims (5)
1. a kind of preparation method of chu chrysanthemum flavored type cigarette filter, which is characterized in that include the following steps：
（1）By nano-titanium dioxide and sodium hydroxide solution by weight 1：（10-20）Closed high pressure is added in after mixing
The interior insulation reaction 24-48h under the conditions of 120-160 DEG C of reaction kettle, be washed with distilled water obtained solid after cooling, filtering,
It is dry, obtain titania nanotube；
（2）By step（1）Obtained titania nanotube is with chitosan, acetum by weight 1：（5-10）：（500-
1000）Then prior to 40-80 DEG C stirring 0.5-1h after mixing is added in anti-in 150-200 DEG C of heat preservation in closed autoclave
24-48h is answered, obtained solid is washed with distilled water after cooling, filtering, is dried, obtains chitosan charcoal-titania nanotube
Sorbing material；
（3）It extracts chu chrysanthemum oil according to a conventional method from chrysanthemum, then washs the chrysanthemum slag after extraction and in 80- with clear water
90 DEG C of dryings are complete, and are ground to 100-200 mesh, and obtained chu chrysanthemum dry powder is spare；
（4）By step（2）Obtained chitosan charcoal-titania nanotube sorbing material and step（3）Obtained chu chrysanthemum oil by
Weight ratio 1：（0.5-1）10-15min is mixed, adds step（3）Obtained chu chrysanthemum dry powder blend uniformly obtains compound add
Add agent, then compound additive is uniformly sprinkling upon on filter stick tow, finally carry out processing and forming, the filter of chu chrysanthemum flavored type cigarette is made
Mouth.
2. the preparation method of a kind of chu chrysanthemum flavored type cigarette filter according to claim 1, which is characterized in that described receives
Rice titanium dioxide is P25 type nano-titanium dioxides.
A kind of 3. preparation method of chu chrysanthemum flavored type cigarette filter according to claim 1, which is characterized in that the hydrogen
A concentration of 8-10mol/L of sodium hydroxide solution.
A kind of 4. preparation method of chu chrysanthemum flavored type cigarette filter according to claim 1, which is characterized in that the vinegar
Acid solution mass fraction is 4-8%.
5. the preparation method of a kind of chu chrysanthemum flavored type cigarette filter according to claim 1, which is characterized in that described compound
The additive amount of additive is 10-15mg/10mm tow.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710530558.4A CN107136558B (en) | 2017-06-29 | 2017-06-29 | A kind of preparation method of chu chrysanthemum flavored type cigarette filter |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710530558.4A CN107136558B (en) | 2017-06-29 | 2017-06-29 | A kind of preparation method of chu chrysanthemum flavored type cigarette filter |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107136558A CN107136558A (en) | 2017-09-08 |
| CN107136558B true CN107136558B (en) | 2018-06-26 |
Family
ID=59785369
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710530558.4A Active CN107136558B (en) | 2017-06-29 | 2017-06-29 | A kind of preparation method of chu chrysanthemum flavored type cigarette filter |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107136558B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109864342B (en) * | 2019-04-11 | 2021-09-28 | 滁州卷烟材料厂 | Composite filter tip additive material for reducing heavy metals in cigarette smoke |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102178348A (en) * | 2011-04-18 | 2011-09-14 | 福州大学 | Filter tip additional material capable of reducing harmful ingredients as well as preparation method and application thereof |
| CN103693681A (en) * | 2013-12-11 | 2014-04-02 | 贵州中烟工业有限责任公司 | Method for preparing super-long titanate micro/nanotubes |
| CN106263023A (en) * | 2016-11-18 | 2017-01-04 | 江西中烟工业有限责任公司 | A kind of cigarette filter compositions that can effectively reduce tar and content of nitrosamines |
| CN106376968A (en) * | 2016-09-22 | 2017-02-08 | 内蒙古昆明卷烟有限责任公司 | Cigarette with recreated cut tobacco leaves and cut stems as cut tobacco and filter tip containing nano granular material |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8118035B2 (en) * | 2005-12-13 | 2012-02-21 | Philip Morris Usa Inc. | Supports catalyst for the combustion of carbon monoxide formed during smoking |
-
2017
- 2017-06-29 CN CN201710530558.4A patent/CN107136558B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102178348A (en) * | 2011-04-18 | 2011-09-14 | 福州大学 | Filter tip additional material capable of reducing harmful ingredients as well as preparation method and application thereof |
| CN103693681A (en) * | 2013-12-11 | 2014-04-02 | 贵州中烟工业有限责任公司 | Method for preparing super-long titanate micro/nanotubes |
| CN106376968A (en) * | 2016-09-22 | 2017-02-08 | 内蒙古昆明卷烟有限责任公司 | Cigarette with recreated cut tobacco leaves and cut stems as cut tobacco and filter tip containing nano granular material |
| CN106263023A (en) * | 2016-11-18 | 2017-01-04 | 江西中烟工业有限责任公司 | A kind of cigarette filter compositions that can effectively reduce tar and content of nitrosamines |
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| Publication number | Publication date |
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| CN107136558A (en) | 2017-09-08 |
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Address after: 239000 No. 1436 Qingliu East Road, Chuzhou economic and Technological Development Zone, Anhui Province Patentee after: Chuzhou Cigarette Material Factory Address before: 239000 No. 1436 Qingliu East Road, Chuzhou economic and Technological Development Zone, Anhui Province Patentee before: CHUZHOU CIGARETTE MATERIALS FACTORY |
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