CN106916658A - A kind of except mite soap and preparation method thereof - Google Patents
A kind of except mite soap and preparation method thereof Download PDFInfo
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- CN106916658A CN106916658A CN201710156496.5A CN201710156496A CN106916658A CN 106916658 A CN106916658 A CN 106916658A CN 201710156496 A CN201710156496 A CN 201710156496A CN 106916658 A CN106916658 A CN 106916658A
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- except mite
- soap
- saponification
- component
- mite
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- 239000000344 soap Substances 0.000 title claims abstract description 59
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 33
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 17
- 239000002280 amphoteric surfactant Substances 0.000 claims abstract description 16
- 239000000203 mixture Substances 0.000 claims abstract description 16
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 45
- 238000007127 saponification reaction Methods 0.000 claims description 40
- 230000002708 enhancing effect Effects 0.000 claims description 25
- 238000004140 cleaning Methods 0.000 claims description 21
- 239000003549 soybean oil Substances 0.000 claims description 16
- 235000012424 soybean oil Nutrition 0.000 claims description 16
- 239000004094 surface-active agent Substances 0.000 claims description 13
- 239000000341 volatile oil Substances 0.000 claims description 13
- 235000009024 Ceanothus sanguineus Nutrition 0.000 claims description 12
- 240000003553 Leptospermum scoparium Species 0.000 claims description 12
- 235000015459 Lycium barbarum Nutrition 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 11
- 229940119485 safflower extract Drugs 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 8
- ZVTDEEBSWIQAFJ-KHPPLWFESA-N 2-hydroxypropyl (z)-octadec-9-enoate Chemical group CCCCCCCC\C=C/CCCCCCCC(=O)OCC(C)O ZVTDEEBSWIQAFJ-KHPPLWFESA-N 0.000 claims description 7
- 235000019197 fats Nutrition 0.000 claims description 7
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 7
- -1 acyl diethanol amine Chemical compound 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 239000003240 coconut oil Substances 0.000 claims description 6
- 235000019864 coconut oil Nutrition 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- 239000002243 precursor Substances 0.000 claims description 6
- 239000012265 solid product Substances 0.000 claims description 6
- OYHQOLUKZRVURQ-HZJYTTRNSA-M 9-cis,12-cis-Octadecadienoate Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC([O-])=O OYHQOLUKZRVURQ-HZJYTTRNSA-M 0.000 claims description 4
- 229940043237 diethanolamine Drugs 0.000 claims description 4
- 239000003814 drug Substances 0.000 claims description 4
- 229940049918 linoleate Drugs 0.000 claims description 4
- 229940040452 linolenate Drugs 0.000 claims description 4
- DTOSIQBPPRVQHS-PDBXOOCHSA-M linolenate Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC([O-])=O DTOSIQBPPRVQHS-PDBXOOCHSA-M 0.000 claims description 4
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 claims description 3
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 3
- 238000001125 extrusion Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- ILRSCQWREDREME-UHFFFAOYSA-N lauric acid amide propyl betaine Natural products CCCCCCCCCCCC(N)=O ILRSCQWREDREME-UHFFFAOYSA-N 0.000 claims description 3
- 125000002252 acyl group Chemical group 0.000 claims description 2
- 238000004806 packaging method and process Methods 0.000 claims description 2
- YXJUEYDETJCBKA-UHFFFAOYSA-N bis(2-hydroxyethyl)azanium;dihydrogen phosphate Chemical compound OP(O)(O)=O.OCCNCCO YXJUEYDETJCBKA-UHFFFAOYSA-N 0.000 claims 1
- 239000006260 foam Substances 0.000 abstract description 6
- 210000002374 sebum Anatomy 0.000 abstract description 4
- 239000006229 carbon black Substances 0.000 abstract description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 2
- 239000003755 preservative agent Substances 0.000 abstract 1
- 230000002335 preservative effect Effects 0.000 abstract 1
- 239000002562 thickening agent Substances 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 19
- 238000005406 washing Methods 0.000 description 7
- 239000003599 detergent Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 4
- 206010020751 Hypersensitivity Diseases 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 230000000844 anti-bacterial effect Effects 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- 210000003491 skin Anatomy 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 201000004624 Dermatitis Diseases 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 230000000895 acaricidal effect Effects 0.000 description 2
- 230000003213 activating effect Effects 0.000 description 2
- 208000026935 allergic disease Diseases 0.000 description 2
- 208000030961 allergic reaction Diseases 0.000 description 2
- 230000007815 allergy Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 2
- 230000003129 miticidal effect Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- PPPFYBPQAPISCT-UHFFFAOYSA-N 2-hydroxypropyl acetate Chemical compound CC(O)COC(C)=O PPPFYBPQAPISCT-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 241000193880 Demodex folliculorum Species 0.000 description 1
- 241001127981 Demodicidae Species 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 208000006877 Insect Bites and Stings Diseases 0.000 description 1
- 102000016943 Muramidase Human genes 0.000 description 1
- 108010014251 Muramidase Proteins 0.000 description 1
- 108010062010 N-Acetylmuramoyl-L-alanine Amidase Proteins 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 230000000172 allergic effect Effects 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000037336 dry skin Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 210000004209 hair Anatomy 0.000 description 1
- 210000003780 hair follicle Anatomy 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000004325 lysozyme Substances 0.000 description 1
- 229960000274 lysozyme Drugs 0.000 description 1
- 235000010335 lysozyme Nutrition 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- JKQOBWVOAYFWKG-UHFFFAOYSA-N molybdenum trioxide Chemical compound O=[Mo](=O)=O JKQOBWVOAYFWKG-UHFFFAOYSA-N 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 210000003296 saliva Anatomy 0.000 description 1
- 210000001732 sebaceous gland Anatomy 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 239000008149 soap solution Substances 0.000 description 1
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
- 229910001948 sodium oxide Inorganic materials 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/21—Esters, e.g. nitroglycerine, selenocyanates
- A61K31/215—Esters, e.g. nitroglycerine, selenocyanates of carboxylic acids
- A61K31/22—Esters, e.g. nitroglycerine, selenocyanates of carboxylic acids of acyclic acids, e.g. pravastatin
- A61K31/23—Esters, e.g. nitroglycerine, selenocyanates of carboxylic acids of acyclic acids, e.g. pravastatin of acids having a carboxyl group bound to a chain of seven or more carbon atoms
- A61K31/231—Esters, e.g. nitroglycerine, selenocyanates of carboxylic acids of acyclic acids, e.g. pravastatin of acids having a carboxyl group bound to a chain of seven or more carbon atoms having one or two double bonds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/21—Esters, e.g. nitroglycerine, selenocyanates
- A61K31/215—Esters, e.g. nitroglycerine, selenocyanates of carboxylic acids
- A61K31/22—Esters, e.g. nitroglycerine, selenocyanates of carboxylic acids of acyclic acids, e.g. pravastatin
- A61K31/23—Esters, e.g. nitroglycerine, selenocyanates of carboxylic acids of acyclic acids, e.g. pravastatin of acids having a carboxyl group bound to a chain of seven or more carbon atoms
- A61K31/232—Esters, e.g. nitroglycerine, selenocyanates of carboxylic acids of acyclic acids, e.g. pravastatin of acids having a carboxyl group bound to a chain of seven or more carbon atoms having three or more double bonds, e.g. etretinate
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/286—Carthamus (distaff thistle)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/61—Myrtaceae (Myrtle family), e.g. teatree or eucalyptus
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/78—Neutral esters of acids of phosphorus
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/92—Sulfobetaines ; Sulfitobetaines
Landscapes
- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Medical Informatics (AREA)
- Botany (AREA)
- Alternative & Traditional Medicine (AREA)
- Emergency Medicine (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of except mite soap and preparation method thereof, its composition includes：The weight portion of nonionic surfactant 25, the weight portion of amphoteric surfactant 10 12, the weight portion of except mite agent 0.1 0.3, the weight portion of laundry care agent 25, the weight portion of preservative 0.2 0.3, the weight portion of thickener 13, the weight portion of small molecular alcohol 0.5 1 and the weight portion of essence 0.1 0.5.The except mite soap has excellent carbon black detergency, sebum detergency, foam performance, and except mite rate can reach more than 97%, the product of remote super prior art report.
Description
Technical field
The present invention relates to except mite soap field, and in particular to can be used for clothing or clean body except mite soap.
Background technology
Acarid cause it is allergic be common illness in clinical medicine, and have the trend being on the rise, this also draws
The concern of medical worker is played.Acarid, can be the parasite for being lodged in human body also known as follicle mites, mainly there is the compacted shape of hair follicle
Mite and sebaceous glands vermiform mite, the infection of vermiform mite is very common to have serious harm to health, and they both can directly sting
Sting skin and cause insect bite dermatitis, it is also possible to cause the inflammation of skin by its secretion such as excrement, saliva etc. for producing, if
Acarid living directly invades human body, can cause bigger internal organs internal diseases.
Acarid is widely distributed, in human epidermal, has presence on clothing and bed clothes.Human body clean in the prior art
Perfumed soap is generally the addition of plant extracts, Chinese prescription, the effect on driving birds is not good of its except mite, wherein not excessive add chemical synthesis class to remove
Mite agent is in order to avoid unnecessary allergic reaction；In cleaning supplies (liquid detergent, washing powder and fertilizer used by bed clothes, clothing
Soap) in except mite report it is common, but effect is also unsatisfactory, it is difficult to obtain the accreditation in market.In the prior art in detergent
Except mite agent have antibacterial and mouldproof drive mite agent MGU-350 (CN104694277A), antimildew and antibacterial liquid nm SKG (CN104450290A) with
And CN105886147A is disclosed removes acaricidal composition, wherein in washing powder it is specifically disclosed have Ambergris (CN105039016A),
Lysozyme (CN103540422A), but above-mentioned substance is used for reality in liquid detergent, washing powder and soap by inventor's trial
After border is attempted, all supported with different degrees of deficiency.By long-term research, inventor have studied a series of washing powder,
Liquid detergent and soaps cleaning supplies, it can realize good except mite effect, and cleaning, cleaning performance are also very excellent.
The content of the invention
In order to solve the above problems, the invention provides a kind of except mite soap with high-efficient washing and except mite function.This hair
Outside ensureing to have excellent carbon black detergency, sebum detergency, foam performance is excellent, and except mite rate can reach for bright except mite soap
More than 97%, its excellent combination property is far superior to prior art it has been reported that the soaps with except mite function.Meanwhile, the except mite
Soap is also satisfactory for human epidermal except mite effect, without bad allergic reaction.
The concrete technical scheme for reaching above-mentioned technique effect is：
(1) a kind of except mite soap, is made up of saponification component, clean enhancing component and except mite traditional Chinese medicinal components：Saponification component is big
The saponification resultant of soya-bean oil, lard and NaOH；Cleaning enhancing component be nonionic surfactant, amphoteric surfactant and
The mixture of except mite agent；Except mite traditional Chinese medicinal components are the mixtures of tea tree ethereal oil and safflower extract.
(2) the except mite soap according to (1), the quality in the soybean oil, lard and sodium hydroxide saponification course of reaction
Than being 5:1:1.
(3) the except mite soap according to (1), the nonionic surfactant is coconut oil fat acyl diethanol amine phosphoric acid
One or two mixture in ester, coconut oil fat acyl diethanol amine.
(4) according to the except mite soap described in (1), the amphoteric surfactant be dodecyl ethyoxyl sulfobetaines,
One or more mixture in dodecyl dimethyl hydroxypropyl sulfobetaines, dodecanamide propyl amine-oxides.
(5) the except mite soap according to (1), the except mite agent is propylene glycol mono-oleate, propane diols list linoleate, third
One or more mixture in glycol list linolenate.
(6) ratio of the except mite soap according to (1), the nonionic surfactant and amphoteric surfactant is 3-
5:2, except mite agent consumption is the 3-8% of surfactant total amount in clean enhancing component.
(7) the weight ratio of the except mite soap according to (1), the tea tree ethereal oil and safflower extract is 1-8:1.
(8) the except mite soap according to (1), the weight of the saponification component, clean enhancing component and except mite traditional Chinese medicinal components
Than being 100:5-10:2-5.
(9) the except mite soap according to (1), the weight of the saponification component, clean enhancing component and except mite traditional Chinese medicinal components
Than being 100:8:2, wherein the mass ratio in the soybean oil, lard and sodium hydroxide saponification course of reaction is 5:1:1；It is described non-
The ratio of ionic surface active agent and amphoteric surfactant is 4:2, except mite agent consumption is surface-active in clean enhancing component
The 5% of agent total amount；The weight ratio of the tea tree ethereal oil and safflower extract is 4:1.
(10) method for preparing any except mite soap in (1)-(9), preparation process includes：1. the soybean oil, lard and hydrogen
Sodium oxide molybdena obtains solid product by saponification, and soap powder is obtained by crushing, grinding；2. by cleaning enhancing component and except mite
Traditional Chinese medicinal components are well mixed with soap powder successively, obtain except mite soap precursor；3. except mite soap precursor is packed by heating, extrusion molding,
.
Saponification component
Saponification component of the present invention is the saponification resultant of soybean oil, lard and NaOH, which employs soybean oil and lard
A compound lard as raw material because soybean oil is used alone, final saponification resultant is softer, it is difficult to meet actually used
High request, adds a small amount of lard, improves the hardness of saponification resultant, and the final performance of saponification component is not influenceed.Institute
It is 5 to state the mass ratio in soybean oil, lard and sodium hydroxide saponification course of reaction:1:1.It should be noted that the unsuitable addition of NaOH
It is excessive, cross conference and cause saponification resultant alkalescence by force, opponent has damage in clothing, bed clothes cleaning process, is carrying out skin cleaning
During cause dry skin.
The basic step of saponification does not have a particular/special requirement, and parameter common in the art, process choice are suitable for
It is prepared by saponification resultant of the invention.
Cleaning enhancing component
Cleaning enhancing component be in order to make up traditional saponification resultant cleaning effect it is not in place the reason for, and assign soaps to remove
Mite effect, it is mainly and is made up of surfactant and except mite agent, is introduced separately below.
The selection of surfactant
Except mite soap of the invention employs two kinds of surfactants, and respectively nonionic surfactant and amphoteric surface is lived
Property agent, above two surfactant is used in mixed way and is much better than using individually a kind of.Wherein nonionic surfactant selection has
There are backbone, the specially one kind or two in coconut oil fat acyl diethanol amine phosphate, coconut oil fat acyl diethanol amine
The mixture planted.Amphoteric surfactant equally uses encourage honesty structure, specially dodecyl ethyoxyl sulfobetaines, 12
One or more mixture in alkyl dimethyl hydroxypropyl sulfobetaines, dodecanamide propyl amine-oxides.
Improve to long-chain moiety to the affinity of grease using the surfactant with backbone, meanwhile, to mite
The oily matter on worm surface also has preferable affinity, in soaps when using, can quickly be removed grease and acarid, washes
Wash middle cooperation and rub better energetically.There is substantial amounts of ion surfactant better than saponification resultant, nonionic table is used in the present invention
Face activating agent is more slightly larger than regular meeting.The ratio of the nonionic surfactant and amphoteric surfactant is 3-5:2.Nonionic table
If face activating agent is excessive, its dirt-removing power that can reduce the soap bubble later stage, for weight dirty clothing, bed clothes cleansing power not
Foot；If amphoteric surfactant is using excessive, one is to cause the cost to increase, two be in saponification component surfactant it is steady
It is qualitative to have influenceed.
The selection of except mite agent
The mite-proof agent that the present invention is used is selected by characteristic, and the except mite agent is preferably propylene glycol mono-oleate, third
One or more mixture in glycol list linoleate, propane diols list linolenate.The except mite agent is much better than background
Species in technology.Propylene glycol mono-oleate, propane diols list linoleate, propane diols list linolenate all fat containing long-chain
Chain, this arrangement enhances dispersiveness and stability, without the material of aliphatic chain long, the reduction of except mite performance is a lot, and such as the third two
Alcohol monoacetate, propane diols mono-propionate are all unable to reach preferable except mite effect.Meanwhile, the except mite agent is nontoxic to human body, nothing
Excitant.Indices are all an advantage over several components with except mite effect introduced in background technology.
Except mite traditional Chinese medicinal components
Except mite traditional Chinese medicinal components are the mixtures of tea tree ethereal oil and safflower extract, and its combination also has a certain degree of except mite
Effect, is a supplement to except mite agent, can within the specific limits reduce the usage amount of except mite agent, is further reduced possible
Allergy risk.Meanwhile, tea tree ethereal oil has bactericidal action, and safflower extract has certain detumescence effect, can reduce acarid
Damage to skin, fast quick-recovery.Above-mentioned essential oil and extract all have certain fragrance, can assign the smell of except mite soap.
The addition of same component has reached three kinds of different effects, and covert reduces cost.The tea tree ethereal oil and safflower extract
Weight ratio be 1-8:1.Can be selected according to two kinds of different emphasis of material, if not within the range, it is difficult to send out
Both common effects are waved, the original intentions of two kinds of materials of use of the invention are run counter to.
The selection of consumption
Basic consumption in foregoing introduction to each component is described.The saponification component, clean enhancing group
Divide and total weight ratio of except mite traditional Chinese medicinal components is 100:5-10:2-5.As most preferred technical scheme, the saponification component,
The weight ratio of cleaning enhancing component and except mite traditional Chinese medicinal components is 100:8:2, wherein the soybean oil, lard and sodium hydroxide saponification
Mass ratio in course of reaction is 5:1:1；The ratio of the nonionic surfactant and amphoteric surfactant is 4:2, remove
Mite agent consumption is 5% of surfactant total amount in clean enhancing component；The weight ratio of the tea tree ethereal oil and safflower extract
It is 4:1.
Beneficial technique effect
The present invention by the basis of traditional saponification component, it is comprehensive using a certain proportion of nonionic surfactant and
Amphoteric surfactant, particular kind of mite-proof agent enhance except mite and cleaning effect and further supplemented with traditional Chinese medicinal components, assign
Except mite soap has been given with except mite, sterilized and detumescence resultant effect, and with certain fragrance.Meanwhile, the adjustment of each component consumption
Outside obtaining with excellent carbon black detergency, sebum detergency, foam performance is excellent, and except mite rate can reach more than 96%.This
The except mite soap of invention is also satisfactory for human epidermal except mite effect, anti-without bad allergy
With reference to specific embodiment, the invention will be further described.
Specific embodiment
Can be so that the present invention will be further elaborated, however, the scope of the present invention not office by the following examples
It is limited to following embodiments.Those skilled in the art are it can be appreciated that in the premise without departing substantially from the spirit and scope of the present invention
Under, various change and modification can be carried out to the present invention.The present invention to used in experiment to material and test method enter
Row is general and/or specifically describes.Although to realize that many materials that the object of the invention used and operating method are abilities
Known to domain, but the present invention still makees description as detailed as possible herein.
Preparation example：
Saponification component A：The weight portion of soybean oil 75, the weight portion of lard 15, the weight portion of NaOH 15, by saponification,
Solid product is obtained, by crushing, grinding, is obtained final product.
Saponification component B：The weight portion of soybean oil 90, the weight portion of NaOH 15, by saponification, obtains solid product,
By crushing, grinding, obtain final product.
Saponification component C：The weight portion of soybean oil 45, the weight portion of lard 45, the weight portion of NaOH 15, by saponification,
Solid product is obtained, by crushing, grinding, is obtained final product.
Cleaning enhancing component A：The weight portion of nonionic surfactant 40, the weight portion of amphoteric surfactant 20, except mite agent
The weight portion of propylene glycol mono-oleate 3.
Cleaning enhancing component B：The weight portion of nonionic surfactant 60, the weight portion of except mite agent propylene glycol mono-oleate 3.
Cleaning enhancing component C：The weight portion of amphoteric surfactant 60, the weight portion of except mite agent propylene glycol mono-oleate 3.
Cleaning enhancing component D：The weight portion of nonionic surfactant 40, the weight portion of amphoteric surfactant 20, except mite agent
The weight portion of Propylene glycol monoacetate 3.
Cleaning enhancing component E：The weight portion of nonionic surfactant 40, the weight portion of amphoteric surfactant 20.
Except mite traditional Chinese medicinal components A：The weight portion of tea tree ethereal oil 40, the weight portion of safflower extract 10.
Except mite traditional Chinese medicinal components B：The weight portion of tea tree ethereal oil 50.
Embodiment
All preparation processes are identical in embodiment, and 1. the soybean oil, lard and NaOH are obtained by saponification
Solid product, soap powder is obtained by crushing, grinding；2. cleaning enhancing component and except mite traditional Chinese medicinal components are mixed with soap powder successively
It is even, obtain except mite soap precursor；3. except mite soap precursor is by heating, extrusion molding, packaging, you can.Each component consumption, corresponding test
Data are referring to following table：
-- expression does not carry out mite killing test
Method of testing：
Foaming power is tested：The soap sample 2.5g for preparing is weighed, is dissolved with 150mg/L hard water, be transferred to 1000mL volumetric flasks
In, and scale is diluted to, shake up, then be aged during solution is put into (40 ± 0.5) DEG C water bath with thermostatic control, the total time since being dissolved in water
It is 30min.Then, with Roche foam Instrument measuring.Specifically refer to GB/13173-2008《Surfactant detergent is tested
Method》Carry out.
Acaricidal rate is tested：
The except mite of except mite soap sample is tested according to GB13917.2-92《Agriculture chemical registration hygienic insecticide indoor harmacological effect is determined
The indoor harmacological effect assay method of method aerosol》Carry out.Specially：Acarid is inserted into transparent organic glass cylinder bottom, sky is tested
Adjust device except mite soap solution (1g except mite soaps are dissolved in 100g deionized waters) respectively wound packages on electronic spraying controller frame trestle,
Electronic spraying controller rack post is laid flat, at the time of regulation electronic controller time control button to spray usage amount medicament, is pressed
Dynamic operation button, clogs (it is 0.1g that culture dish surface contacts dose), immediately timing, and open with plug by circular hole immediately after spraying
Begin record, takes out culture dish after 30 minutes, is placed in 26 DEG C of incubators, and miticidal effect was observed when 24 hours, as a result takes three
Secondary average value.
Sebum detergency：
The detergency test of except mite soap sample is with reference to GB/T13174-2008《Dress material detergent detergency and circulation washing
The measure of performance》Carry out, due to the sample in the prior art without standard except mite soap, therefore with the standard washing powder of same quality
Test result is compared.
By experimental data in form it can be found that except mite soap of the invention is all obtained with optimal proportion and rational environs
Good grease detergency, timely foam, 5min foams and good miticidal effect are arrived.The above results are all an advantage over existing
Technology commercially available prod, belongs to top standard in the industry.
Claims (10)
1. a kind of except mite soap, it is characterised in that：It is made up of saponification component, clean enhancing component and except mite traditional Chinese medicinal components：Saponification group
Point it is the saponification resultant of soybean oil, lard and NaOH；Cleaning enhancing component is nonionic surfactant, amphoteric surface's work
Property agent and the mixture of except mite agent；Except mite traditional Chinese medicinal components are the mixtures of tea tree ethereal oil and safflower extract.
2. except mite soap according to claim 1, it is characterised in that：The reaction of the soybean oil, lard and sodium hydroxide saponification
During mass ratio be 5:1:1.
3. except mite soap according to claim 1, it is characterised in that：The nonionic surfactant is coconut oil fat acyl
One or two mixture in diethanol amine phosphate, coconut oil fat acyl diethanol amine.
4. except mite soap according to claim 1, it is characterised in that：The amphoteric surfactant is dodecyl ethyoxyl
In sulfobetaines, dodecyl dimethyl hydroxypropyl sulfobetaines, dodecanamide propyl amine-oxides one or two with
On mixture.
5. except mite soap according to claim 1, it is characterised in that：The except mite agent is propylene glycol mono-oleate, propane diols
One or more mixture in single linoleate, propane diols list linolenate.
6. except mite soap according to claim 1, it is characterised in that：The nonionic surfactant and amophoteric surface active
The ratio of agent is 3-5:2, except mite agent consumption is the 3-8% of surfactant total amount in clean enhancing component.
7. except mite soap according to claim 1, it is characterised in that：The weight ratio of the tea tree ethereal oil and safflower extract is
1-8:1。
8. except mite soap according to claim 1, it is characterised in that：In the saponification component, clean enhancing component and except mite
The weight ratio of medicine component is 100:5-10:2-5.
9. except mite soap according to claim 1, it is characterised in that：In the saponification component, clean enhancing component and except mite
The weight ratio of medicine component is 100:8:2, wherein the mass ratio in the soybean oil, lard and sodium hydroxide saponification course of reaction is
5:1:1；The ratio of the nonionic surfactant and amphoteric surfactant is 4:2, except mite agent consumption is clean enhancing group
The 5% of surfactant total amount in point；The weight ratio of the tea tree ethereal oil and safflower extract is 4:1.
10. the method for preparing any except mite soap in claim 1-9, it is characterised in that：Preparation process includes：
（1）The soybean oil, lard and NaOH obtain solid product by saponification, and soap is obtained by crushing, grinding
Powder；
（2）Cleaning enhancing component and except mite traditional Chinese medicinal components are well mixed with soap powder successively, except mite soap precursor is obtained；
（3）Except mite soap precursor is by heating, extrusion molding, packaging, you can.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710156496.5A CN106916658A (en) | 2017-03-15 | 2017-03-15 | A kind of except mite soap and preparation method thereof |
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| CN201710156496.5A CN106916658A (en) | 2017-03-15 | 2017-03-15 | A kind of except mite soap and preparation method thereof |
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ID=59460310
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| CN201710156496.5A Pending CN106916658A (en) | 2017-03-15 | 2017-03-15 | A kind of except mite soap and preparation method thereof |
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| WO2021164994A1 (en) | 2020-02-20 | 2021-08-26 | Unilever Ip Holdings B.V. | A soap composition |
| CN116751638A (en) * | 2023-06-09 | 2023-09-15 | 南风化工(运城)集团有限公司 | A kind of mite-removing washing powder and preparation method thereof |
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Application publication date: 20170704 |