CN106753787A - A kind of cigarette quick-fried pearl lemon-mint essential oil and its preparation method and application - Google Patents

Abstract

The invention provides a lemon mint essential oil for cigarettes and a preparation method thereof. The lemon peppermint essential oil for cigarettes is made from fruit essence, mint essence and essence diluent according to the ratio of weight ratio 1-5:10-60:35-89, mix evenly and add Span 80, then continue to stir for 0.5-1h, Obtained after standing still with foam disappearing. The fruity essence is prepared by mixing lemon oil, geranial and Brazilian sweet orange oil, and the mint essence is composed of L-menthol, peppermint oil, N,2,3-trimethyl-2-isopropyl Butanamide (WS-23) and absolute ethanol are mixed and prepared, and the essence diluent is prepared by mixing 24-degree palm oil and caprylic acid glycerin according to the mass ratio of 1-5:1-5. The invention can well adapt to the physical and chemical properties of the puffed bead rubber, and when used in the puffed puffed bead of cigarettes, it can make the cool taste of mint lasting and uniform, and the fragrance is full, unique in style, and has the fragrance of lemon. In the stick, the pumping experience from low cooling to high cooling is realized.

Description

A kind of poppear lemon mint essential oil for cigarettes and its preparation method and application

technical field

The invention relates to the field of flavors and fragrances for tobacco, in particular to an essential oil formula used for popping pearls containing lemon and mint flavors and a preparation method thereof.

Background technique

Cigarette flavoring additives are widely used and play an important role in cigarette flavor compensation. The traditional way of adding flavors and fragrances is accompanied by the burning of cigarettes. Flavors and fragrances participate in the combustion. While losing effective aromatizing substances, new harmful substances may be produced, which will have a greater impact on the flavoring effect of cigarettes. Cigarette popping beads are soft capsules wrapped with functional additives, placed in cigarette filter rods, and the contents of the popping beads can be released by consumers at their own discretion when smoking. The influence of air temperature plays a role, does not participate in combustion, can effectively improve product quality, enrich and improve product style characteristics, improve cigarette smoking safety, and ensure the stability of product functions.

Menthol and related cooling compounds can act on the body's temperature sensors, making people feel cool through the cold sensors. In the prior art, the Chinese patent with the patent number CN201310744007.X discloses a mint-type cigarette cooling flavor composition, including the following components and weight ratio: trimenthyl monoethyl titanate 65--85; salicylic acid methyl Esters 1--3; Lemon oil 0--0.5; Peppermint oil 0.2-0.3; Essence 6-11. The Chinese patent with the patent number CN201410338450.1 discloses a preparation method and application of a cool mint cigarette filter rod additive, which consists of the following components: L-menthol, sorbitol, glycerol, propylene glycol, peppermint oil , spearmint oil. The combination of the above flavors is used in filter rods or shredded tobacco. When smoking, the mint fragrance will rapidly weaken with the increase of the number of puffs, and the smoking feeling of uniform release of cool taste cannot be obtained, and there is a huge defect in the quality of smoking; The shelf life is relatively short, and the storage time is too long to cause menthol to volatilize and affect its stability. Mint is volatile.

The Chinese patent with the patent number CN201510027473.5 discloses a peppermint essence solvent used for cigarette dripping pills. The weight fractions of the raw materials of each component are as follows: menthol 1-40, olive oil 20-80, glyceryl caprylate 85-15, surfactant 0.1-1.5. Due to the low solubility of menthol in oils, this formula is difficult to achieve a high cooling product experience, and menthol is highly irritating. Its coolness lasts for a short time on human skin and mouth and has a strong instantaneous cooling effect, which makes people feel uncomfortable and uncomfortable. It has a bitter taste, which affects its use effect.

Contents of the invention

According to the deficiencies of the prior art, the present invention provides a kind of lemon peppermint essential oil for cigarettes and its preparation method. The present invention prepares the lemon peppermint essential oil together with the wrapping material into cigarette popping beads, and adds it to the cigarette tip stick. It satisfies consumers' immediate demand for fragrance substances, can bring fragrance substances in with the smoke, does not participate in combustion, does not produce new harmful substances, and has accurate quantification, long storage period, soft, delicate and irritating smoke It is small, and it has the characteristics of concentration and strength when drawn, and the aftertaste is clean and comfortable.

The technical solution provided by the present invention is: the lemon mint essential oil for cigarettes is characterized in that it is composed of the following components and raw materials in parts by weight:

The fruit flavor essence is mixed with the following substances by weight percentage: 50%-80% of lemon oil, 10%-30% of geranial, and 10%-20% of Brazilian sweet orange oil;

The mint flavor is mixed with the following substances in weight percentage: 65%-80% of L-menthol, 19%-22% of mint oil, N,2,3-trimethyl-2-isopropylbutanamide (WS-23) 1%-5%, absolute ethanol 0-8%;

The flavor diluent is prepared by mixing 24-degree palm oil and caprylic acid glycerin according to the mass ratio of 1-5:1-5.

The preferred technical scheme of the present invention is: when the peppermint essence content in the lemon peppermint essential oil is 10-20%, the mass ratio of 24 degree palm oil and glyceryl caprylate in the essence diluent is 5:1, so The amount of Span 80 added is 7‰-9‰ of the total weight of the lemon mint essential oil; when the peppermint essence content in the lemon peppermint essential oil is 21%-35%, the 24-degree palm oil and caprylic acid in the essence diluent The mass ratio of glycerides is 2:3, and the amount of Span 80 added is 4‰-6‰ of the total weight of the lemon peppermint essential oil; when the mint essence content in the lemon peppermint essential oil is 36%-60%, the essence diluent The mass ratio of medium 24 degree palm oil to caprylic acid glyceride is 1:5, and the added amount of Span 80 is 2‰-3‰ of the total weight of lemon mint essential oil.

A kind of preparation method of lemon peppermint essential oil provided by the invention is characterized in that the specific steps are as follows:

(1) Take the following substances in mass percentage: 50%-80% of lemon oil, 10%-30% of geranial, 10%-20% of Brazilian sweet orange oil, and mix the above-mentioned substances evenly to prepare fruit flavor essence;

(2) The following mass percentages are taken: L-menthol 65%-80%, peppermint oil 19%-22%, N,2,3-trimethyl-2-isopropylbutanamide 1%-5% , 0-8% absolute ethanol, stirring and dissolving the above-mentioned substances at room temperature until the solution is clear and transparent, then filtering, and the obtained filtrate is mint essence;

(3) Mix the fruity essence prepared in step (1), the mint essence prepared in step (2) and the essence diluent according to the ratio of 1-5:10-60:35-89 by weight, and stir at room temperature Evenly, then add Span 80 and continue to stir for 0.5-1h, and leave it to stand until the foam disappears to obtain lemon peppermint essential oil; Palm oil and glyceryl caprylate are mixed according to a mass ratio of 5:1, and the amount of Span 80 added is 7‰-9‰ of the total weight of lemon mint essential oil; when the mint essence content in lemon mint essential oil is 21 %-35%, the essence diluent is formed by mixing 24-degree palm oil and caprylic acid glycerin according to the mass ratio of 2:3, and the added amount of Span 80 is 4% of the total weight of lemon mint essential oil. ‰-6‰; when the mint flavor content in the lemon mint essential oil is 36%-60%, the flavor diluent is mixed with 24-degree palm oil and caprylic acid glyceride according to the mass ratio of 1:5 , the amount of Span 80 added is 2‰-3‰ of the total weight of lemon mint essential oil.

A method for using the lemon mint essential oil for cigarettes provided by the present invention is characterized in that: adding the lemon mint essential oil for cigarettes into the hopper of the dropping pill machine, adjusting the size of the discharge port, and then mixing with the The dripping pill wrapping material in the glue tank of the dripping pill machine and the curing agent placed in the pill container are made into popping beads for lemon mint cigarettes according to the preparation process of the dropping pills; during the forming process of the cigarette filter tow, the prepared The lemon menthol cigarettes are applied to filter rods with popping beads and made into cigarettes.

The method for the preparation of dripping pills in the present invention is the prior art. For details, see the publicly authorized Chinese patent. The application of pills; the patent specifically discloses the preparation method of dripping pills for cigarettes, as well as the wrapping material and curing agent of dripping pills for cigarettes. The wrapping material is composed of sodium alginate with a viscosity of 0.01-2 Pa.s, glycerin with a freezing force value of 100-250, and water according to a weight ratio of 1-8:0.5-5:85-100, and then placed in a heated In the interlayer reaction tank, stir at 70°C to melt the mixture, keep it warm for 1-2 hours, let it stand until the foam floats up, and filter it at 70°C. In addition to the wrapping material disclosed in the above-mentioned patents, other materials that meet the conditions of the wrapping material for cigarette dropping pills can also be used as the wrapping material for preparing the dropping pills for cigarettes in the present invention.

Beneficial effects of the present invention:

(1) The lemon peppermint essential oil of the present invention reduces the stimulation of menthol to the human oral cavity, and the cool taste lasts for a long time.

(2) The essence of the present invention can make the cool taste of mint lasting and uniform when used in cigarette popping beads, and the fragrance is full, unique in style, and has the fragrance of lemon.

(3) The essence formula of the present invention can well adapt to the physical and chemical properties of the pop-ball rubber, has good online production stability, low pop-ball eccentricity, and smaller cuts.

(4) The flavor prepared by the present invention and the puffed pearl rubber are made into puffed puffs for cigarettes, which are added to the cigarette tip stick to realize the smoking experience from low coolness to high coolness, and can bring flavor substances along with the smoke. It does not participate in combustion, does not produce new harmful substances, and has accurate quantification, long storage period, and has the characteristics of soft, delicate smoke, low irritation, moderate concentration and strength, and clean and comfortable aftertaste.

detailed description

The present invention will be further described in detail below in conjunction with specific examples, but they do not limit the present invention.

Embodiment 1, a kind of quick-fried pearl lemon mint essential oil for cigarettes, its specific preparation method is as follows:

Weigh 0.9 parts of lemon oil, 0.2 parts of geranial, and 0.4 parts of Brazilian sweet orange oil to mix to obtain a fruity essence; weigh 11.5 parts of L-menthol, 3 parts of peppermint oil, and mix with 0.5 parts of WS-23 Finally, stir and dissolve at room temperature until the solution is clear and transparent, filter, and the resulting filtrate is peppermint essence; take 70 parts of palm oil and 14 parts of glyceryl caprylate by weight, and mix them with the prepared fruit flavor essence and peppermint essence at room temperature. Stir evenly, and add 0.08 part of Span 80, continue to stir for 0.5-1h, and let it stand still until the foam disappears, and the lemon mint essential oil is obtained.

The above-mentioned lemon mint essential oil was prepared into pop-up beads for cigarettes by using the existing drop pill preparation method, and then added into cigarette filters, and seven smokers conducted sensory evaluation on them. The results of smoking evaluation show that: the cigarette samples added with popping pearl flavor have a touch of mint and lemon fruit aroma, and the smoke is naturally soft and less irritating.

Embodiment 2, a kind of quick-fried pearl lemon mint essential oil for cigarettes, its specific preparation method is as follows:

Take by weight 3 parts of lemon oil, 0.5 parts of geranial, and 1.5 parts of Brazilian sweet orange oil to mix to obtain fruit flavor essence; take by weight 20.4 parts of L-menthol, 6.6 parts of peppermint oil, 1 part of ws-23, After mixing 2 parts of absolute ethanol, stir and dissolve at room temperature until the solution is clear and transparent, filter, and the resulting filtrate is peppermint essence; take 26 parts of palm oil and 39 parts of glyceryl caprylate by weight, and mix with the prepared fruit flavor Mix the essence and peppermint essence, and stir evenly at room temperature, add 0.04 parts of Span 80, continue stirring for 0.5-1h, let it stand still until the foam disappears, and you can get lemon mint essential oil.

The above-mentioned lemon mint essential oil was prepared into pop-up beads for cigarettes by using the existing drop pill preparation method, and then added into cigarette filters, and seven smokers conducted sensory evaluation on them. The smoking evaluation results show that: the cigarette samples added with poppowder flavor have a strong cooling sensation and lemon fruit aroma in the mouth during smoking, which has a pleasant cooling effect, and the smoke has a slightly sweet feeling and a pleasant aftertaste.

Embodiment 3, a kind of quick-fried pearl lemon mint essential oil for cigarettes, its specific preparation method is as follows:

Take by weight 2.5 parts of lemon oil, 1.5 parts of geranial, and 1 part of Brazilian sweet orange oil to mix to obtain a fruity essence; take by weight 33.5 parts of L-menthol, 10 parts of peppermint oil, 2.5 parts of ws-23, Mix 4 parts of absolute ethanol at room temperature, stir and dissolve until the solution is clear and transparent, filter, and the resulting filtrate is peppermint essence; take 7.5 parts of palm oil and 37.5 parts of glyceryl caprylate by weight, mix with the prepared fruit flavor essence, peppermint Stir the essence evenly at room temperature, add 0.03 part of Span 80, continue to stir for 0.5-1 hour, let it stand still until the foam disappears, and you will get lemon mint essential oil.

The above-mentioned lemon mint essential oil was prepared into pop-up beads for cigarettes by using the existing drop pill preparation method, and then added into cigarette filters, and seven smokers conducted sensory evaluation on them. The results of smoking evaluation show that: the cigarette samples added with poppowder flavor have a strong mint aroma and fresh lemon fruit aroma in the mouth and throat during smoking, the aroma is long-lasting, and the impact is strong.

Comparative example: take by weight 83 parts of L-menthol, 3 parts of peppermint oil, 1 part of spearmint oil, 4 parts of propylene glycol, and 9 parts of glycerin, and mix the above-mentioned components uniformly at room temperature by weight to obtain common Mint flavor.

The mint essence in the above comparative example was added to the triglyceride at a ratio of 10%, and a mint-shaped cigarette filter rod was manufactured according to a conventional process, and the cigarettes made were sensory evaluated by 7 smokers. The smoking evaluation results show that the cigarette samples added with ordinary mint flavor have a weak mint aroma in smoking, the fragrance retention time is short, and the cool taste of the smoke decreases with the number of puffs.

It can be seen from the above comparative examples that the lemon mint essential oil prepared in the present invention is made into quick-fried beads and added to cigarettes after being smoked, the aroma is more durable, and the mint fragrance is more intense, the cooling taste is stronger and the impact force is stronger .

Claims (4)

1. a kind of cigarette is with quick-fried pearl lemon-mint essential oil, it is characterised in that be made up of the raw material of following components and weight portion：

The fruit essence is formed by the material mixing of following percentage by weight：Lemon oil 50%-80%, geranial 10%- 30%th, Brazilian orange oil 10%-20%；

The Mint Essence is formed by the material mixing of following percentage by weight：MENTHOL 65%-80%, peppermint oil dementholized 19%-22%, N, 2,3- trimethyl -2- butanamides 1%-5%, absolute ethyl alcohol 0-8%；

The essence diluent is according to mass ratio 1-5 by 24 degree of palm oils and Xin Kui acid glycerides:The ratio mixed configuration of 1-5 Form.

2. a kind of cigarette according to claim 1 is with quick-fried pearl lemon-mint essential oil, it is characterised in that：The lemon-mint essential oil When middle Mint Essence content is 10-20%, 24 degree of palm oils are with the mass ratio of pungent certain herbaceous plants with big flowers acid glyceride in the essence diluent 5:1, the addition of the Span 80 is the 7 ‰ -9 ‰ of lemon-mint essential oil gross weight；Mint Essence contains in the lemon-mint essential oil Measure during for 21%-35%, 24 degree of palm oils and the mass ratio of pungent certain herbaceous plants with big flowers acid glyceride are 2 in the essence diluent:3, the department 80 additions of class are the 4 ‰ -6 ‰ of lemon-mint essential oil gross weight；Mint Essence content is 36%- in the lemon-mint essential oil When 60%, 24 degree of palm oils and the mass ratio of pungent certain herbaceous plants with big flowers acid glyceride are 1 in essence diluent:5, the addition of the Span 80 is lemon The 2 ‰ -3 ‰ of lemon Peppermint essential oil gross weight.

3. the preparation method of quick-fried pearl lemon-mint essential oil of the cigarette described in a kind of claim 1, it is characterised in that specific steps are such as Under：

(1) material of following mass percent is taken：Lemon oil 50%-80%, geranial 10%-30%, Brazilian orange oil 10%- 20%, by the well mixed achievement of allocation essence of above-mentioned substance；

(2) material of following mass percent is taken：MENTHOL 65%-80%, peppermint oil dementholized 19%-22%, N, 2,3- front threes Base -2- butanamides 1%-5%, absolute ethyl alcohol 0-8%, by above-mentioned substance, stirring and dissolving is saturating to solution clarification at normal temperatures It is bright, then to filter, gained filtrate is Mint Essence；

(3) Mint Essence and essence diluent for being prepared in fruit essence, the step (2) that will be prepared in step (1) are according to weight Compare 1-5：10-60：The ratio mixing of 35-89, stirs at normal temperatures, is subsequently adding Span continuation after 80s and stirs 0.5-1h, Band lather collapse is stood, lemon-mint essential oil is obtained final product；It is described when Mint Essence content is 10-20% in lemon-mint essential oil Essence diluent is according to mass ratio 5 by 24 degree of palm oils with pungent certain herbaceous plants with big flowers acid glyceride:1 obtains ratio mixes, the Span 80 Addition is the 7 ‰ -9 ‰ of lemon-mint essential oil gross weight；When Mint Essence content is 21%-35% in lemon-mint essential oil, The essence diluent is according to mass ratio 2 by 24 degree of palm oils with pungent certain herbaceous plants with big flowers acid glyceride:3 obtain ratio mixes, the department 80 additions of class are the 4 ‰ -6 ‰ of lemon-mint essential oil gross weight；When Mint Essence content is 36%-60% in lemon-mint essential oil When, it by 24 degree of palm oils and pungent certain herbaceous plants with big flowers acid glyceride according to mass ratio is 1 that the essence diluent is:5 ratio is mixed, institute It is the 2 ‰ -3 ‰ of lemon-mint essential oil gross weight to state the addition of Span 80.

4. the application of quick-fried pearl lemon-mint essential oil of the cigarette described in a kind of claim 1 or 3, it is characterised in that：Above-mentioned cigarette is used Quick-fried pearl lemon-mint essential oil is added in the hopper of pill dripping machine, regulates the size of discharging opening, then be placed in pill dripping machine rubber cement tank In dripping pill lapping and be placed in the curing agent contained in ball device and be made lemon-mint cigarette with quick-fried according to the preparation technology of dripping pill Pearl；During cigarette filter wire-beam forming, the lemon-mint cigarette of preparation is positioned with quick-fried pearl and is applied in filter rod, and be made Cigarette.