CN106719727A - A kind of insecticide - Google Patents
A kind of insecticide Download PDFInfo
- Publication number
- CN106719727A CN106719727A CN201611148079.8A CN201611148079A CN106719727A CN 106719727 A CN106719727 A CN 106719727A CN 201611148079 A CN201611148079 A CN 201611148079A CN 106719727 A CN106719727 A CN 106719727A
- Authority
- CN
- China
- Prior art keywords
- parts
- diisobutylester
- insecticide
- polyethylene glycol
- active component
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000002917 insecticide Substances 0.000 title claims abstract description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 24
- MTXSIJUGVMTTMU-JTQLQIEISA-N (S)-anabasine Chemical compound N1CCCC[C@H]1C1=CC=CN=C1 MTXSIJUGVMTTMU-JTQLQIEISA-N 0.000 claims abstract description 12
- LXOFYPKXCSULTL-UHFFFAOYSA-N 2,4,7,9-tetramethyldec-5-yne-4,7-diol Chemical compound CC(C)CC(C)(O)C#CC(C)(O)CC(C)C LXOFYPKXCSULTL-UHFFFAOYSA-N 0.000 claims abstract description 12
- FIPWRIJSWJWJAI-UHFFFAOYSA-N Butyl carbitol 6-propylpiperonyl ether Chemical compound C1=C(CCC)C(COCCOCCOCCCC)=CC2=C1OCO2 FIPWRIJSWJWJAI-UHFFFAOYSA-N 0.000 claims abstract description 12
- FNELVJVBIYMIMC-UHFFFAOYSA-N Ethiprole Chemical compound N1=C(C#N)C(S(=O)CC)=C(N)N1C1=C(Cl)C=C(C(F)(F)F)C=C1Cl FNELVJVBIYMIMC-UHFFFAOYSA-N 0.000 claims abstract description 12
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 12
- 229930014345 anabasine Natural products 0.000 claims abstract description 12
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 12
- 239000001257 hydrogen Substances 0.000 claims abstract description 12
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims abstract description 12
- 229960005235 piperonyl butoxide Drugs 0.000 claims abstract description 12
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 12
- 229940124530 sulfonamide Drugs 0.000 claims abstract description 12
- 150000003456 sulfonamides Chemical class 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- ABBQHOQBGMUPJH-UHFFFAOYSA-M Sodium salicylate Chemical compound [Na+].OC1=CC=CC=C1C([O-])=O ABBQHOQBGMUPJH-UHFFFAOYSA-M 0.000 claims abstract description 10
- 229960004025 sodium salicylate Drugs 0.000 claims abstract description 10
- 239000004480 active ingredient Substances 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 8
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 240000000203 Salix gracilistyla Species 0.000 claims description 2
- 150000002148 esters Chemical class 0.000 claims description 2
- 241001440840 Mikania micrantha Species 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 4
- 241000238631 Hexapoda Species 0.000 abstract description 3
- 150000001875 compounds Chemical class 0.000 abstract description 2
- 238000013467 fragmentation Methods 0.000 abstract 1
- 238000006062 fragmentation reaction Methods 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 9
- 239000012467 final product Substances 0.000 description 3
- UWNADWZGEHDQAB-UHFFFAOYSA-N 2,5-dimethylhexane Chemical group CC(C)CCC(C)C UWNADWZGEHDQAB-UHFFFAOYSA-N 0.000 description 2
- 241001674044 Blattodea Species 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 241000254173 Coleoptera Species 0.000 description 1
- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 1
- 241000231739 Rutilus rutilus Species 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of insecticide, including following composition：56 60 parts of active component, 8 15 parts of N ethylperfluoro octyl group sulfonamide ethanol, 25 30 parts of tetramethyl decynediol, 30 40 parts of sodium salicylate, 80 100 parts of sulfosuccinic acid-diisobutylester-S-sodium salt, 15 28 parts of piperonyl butoxide, 35 46 parts of polyethylene glycol, 400 800 parts of water.Inventive compound is made up of double hydrogen mikanolides, anabasine, ethiprole, and ethiprole has stronger fragmentation effect to insect, then by double hydrogen mikanolides, the cooperation of anabasine, it is better.
Description
Technical field
The present invention relates to a kind of insecticide.
Background technology
Insecticide, the medicine usage histories that are mainly used in preventing and treating agricultural pests and urban health insect are long-range, consumption is big,
It is wide in variety.In 21st century, agriculture develops rapidly, and insecticide makes farm output rise higher.
But, nearly all insecticide all can seriously change the ecosystem, most of harmful, other meeting quilts
In concentrating on food chain.We must obtain balance in agricultural development and environment and health.
The content of the invention
It is an object of the present invention to provide a kind of insecticide, good disinsection effect, and it is safe efficient, drug degradation effect is good, residual
It is few.
The solution of the present invention is as follows：A kind of insecticide, it is characterised in that be made up of following raw material：
Active component 56-60 parts, 8-15 parts of N- ethylperfluoro octyl groups sulfonamide ethanol, tetramethyl decynediol 25-30 parts, bigcatkin willow
Sour sodium 30-40 parts, sulfosuccinic acid-diisobutylester-S-sodium salt 80-100 parts, piperonyl butoxide 15-28 parts, polyethylene glycol 35-46 parts, water
400-800 parts；
Described active ingredient is double hydrogen mikanolides, anabasine, ethiprole, and its weight ratio is 12-18：6-7：22-25.
Further, it is made up of following raw material：
58 parts of active component, 10 parts of N- ethylperfluoro octyl group sulfonamide ethanol, 26 parts of tetramethyl decynediol, sodium salicylate 34
Part, 89 parts of sulfosuccinic acid-diisobutylester-S-sodium salt, 21 parts of piperonyl butoxide, 40 parts of polyethylene glycol, 600 parts of water.
Further, it is made up of following raw material：
59 parts of active component, 9 parts of N- ethylperfluoro octyl group sulfonamide ethanol, 28 parts of tetramethyl decynediol, 33 parts of sodium salicylate,
96 parts of sulfosuccinic acid-diisobutylester-S-sodium salt, 26 parts of piperonyl butoxide, 38 parts of polyethylene glycol, 750 parts of water.
Further, it is made up of following raw material：
58 parts of active component, 12 parts of N- ethylperfluoro octyl group sulfonamide ethanol, 25 parts of tetramethyl decynediol, sodium salicylate 36
Part, 92 parts of sulfosuccinic acid-diisobutylester-S-sodium salt, 16 parts of piperonyl butoxide, 42 parts of polyethylene glycol, 680 parts of water.
Further, described active ingredient is double hydrogen mikanolides, anabasine, ethiprole, and its weight ratio is 15：6.3：
23
Inventive compound is made up of double hydrogen mikanolides, anabasine, ethiprole, and ethiprole has stronger killing to insect
Effect, then by double hydrogen mikanolides, the cooperation of anabasine, it is better.
Specific embodiment
With reference to embodiment, the present invention will be further described.
Embodiment 1
By 58 parts of active component, 10 parts of N- ethylperfluoro octyl group sulfonamide ethanol, 26 parts of tetramethyl decynediol, sodium salicylate 34
In part, 89 parts of sulfosuccinic acid-diisobutylester-S-sodium salt, 21 parts of piperonyl butoxide, 40 parts of polyethylene glycol, 600 parts of addition reactors of water,
Stir and be completely dissolved, obtain final product.
Double hydrogen mikanolides, anabasine, the weight ratio of ethiprole are 15 in active ingredient：6.3：23.
Embodiment 2
By active component 59g, N- ethylperfluoro octyl group sulfonamide ethanol 9g, tetramethyl decynediol 28g, sodium salicylate 33g, fourth
Diacid diisobutyl ester sodium sulfonate 96g, piperonyl butoxide 26g, polyethylene glycol 38g, water 750g are added in reactor, are stirred simultaneously
It is completely dissolved, obtains final product.
Double hydrogen mikanolides, anabasine, the weight ratio of ethiprole are 14 in active ingredient：6.5：24.
Embodiment 3
By active component 58g, N- ethylperfluoro octyl group sulfonamide ethanol 12g, tetramethyl decynediol 25g, sodium salicylate 36g,
Sulfosuccinic acid-diisobutylester-S-sodium salt 92g, piperonyl butoxide 16g, polyethylene glycol 42g, water 680g are added in reactor, are stirred
And be completely dissolved, obtain final product.
Double hydrogen mikanolides, anabasine, the weight ratio of ethiprole are 16 in active ingredient：6.7：25.
Comparative example 1
Compared with Example 1, at difference it is no double hydrogen mikanolides in active ingredient.
Comparative example 2
Compared with Example 1, it is do not have anabasine in active ingredient at difference.
Comparative example 3
Compared with Example 1, it is do not have ethiprole in active ingredient at difference.
Comparative example 4
Conventional insecticide.
Insecticidal test
200 cockroaches are put into closed room.Using insecticide to carrying out ultra-low volume spray in room.Apply observation post administration roach
Dung beetle knocks down number, continuous 30min.Then cockroach is moved to home and raises 24h, record death toll.
Respectively above-mentioned experiment is done using the insecticide of embodiment 1-3, comparative example 1-4.Result is as follows.
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | |
| Number is knocked down after dispenser 15min | 198 | 194 | 196 | 163 | 168 | 172 | 142 |
| Death toll after 24h | 200 | 200 | 200 | 168 | 175 | 179 | 148 |
Although detailed description being given to specific embodiment of the invention above and being illustrated, it should be noted that
We can carry out various equivalent changes and modification to above-mentioned implementation method according to conception of the invention, and the function produced by it is made
With still without departing from specification covered it is spiritual when, all should be within protection scope of the present invention.
Claims (5)
1. a kind of insecticide, it is characterised in that be made up of following raw material：
Active component 56-60 parts, 8-15 parts of N- ethylperfluoro octyl groups sulfonamide ethanol, tetramethyl decynediol 25-30 parts, bigcatkin willow
Sour sodium 30-40 parts, sulfosuccinic acid-diisobutylester-S-sodium salt 80-100 parts, piperonyl butoxide 15-28 parts, polyethylene glycol 35-46 parts, water
400-800 parts；
Described active ingredient is double hydrogen mikanolides, anabasine, ethiprole, and its weight ratio is 12-18：6-7：22-25.
2. a kind of insecticide according to claim 1, it is characterised in that be made up of following raw material：
58 parts of active component, 10 parts of N- ethylperfluoro octyl group sulfonamide ethanol, 26 parts of tetramethyl decynediol, sodium salicylate 34
Part, 89 parts of sulfosuccinic acid-diisobutylester-S-sodium salt, 21 parts of piperonyl butoxide, 40 parts of polyethylene glycol, 600 parts of water.
3. a kind of insecticide according to claim 1, it is characterised in that be made up of following raw material：
59 parts of active component, 9 parts of N- ethylperfluoro octyl group sulfonamide ethanol, 28 parts of tetramethyl decynediol, 33 parts of sodium salicylate,
96 parts of sulfosuccinic acid-diisobutylester-S-sodium salt, 26 parts of piperonyl butoxide, 38 parts of polyethylene glycol, 750 parts of water.
4. a kind of insecticide according to claim 1, it is characterised in that be made up of following raw material：
58 parts of active component, 12 parts of N- ethylperfluoro octyl group sulfonamide ethanol, 25 parts of tetramethyl decynediol, sodium salicylate 36
Part, 92 parts of sulfosuccinic acid-diisobutylester-S-sodium salt, 16 parts of piperonyl butoxide, 42 parts of polyethylene glycol, 680 parts of water.
5. a kind of insecticide according to claim 1, it is characterised in that described active ingredient is in double hydrogen Mikania micranthas
Ester, anabasine, ethiprole, its weight ratio are 15：6.3：23.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611148079.8A CN106719727A (en) | 2016-12-13 | 2016-12-13 | A kind of insecticide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611148079.8A CN106719727A (en) | 2016-12-13 | 2016-12-13 | A kind of insecticide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106719727A true CN106719727A (en) | 2017-05-31 |
Family
ID=58881123
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611148079.8A Withdrawn CN106719727A (en) | 2016-12-13 | 2016-12-13 | A kind of insecticide |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106719727A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1484646A (en) * | 2001-01-12 | 2004-03-24 | ��ѧ�о���Ӧ����ѯ��˾ | Mikanolide derivatives, their preparation and their therapeutic use |
| CN103283761A (en) * | 2012-02-27 | 2013-09-11 | 陕西韦尔奇作物保护有限公司 | Ethiprole-containing pesticidal composition |
| CN104341390A (en) * | 2014-11-04 | 2015-02-11 | 南开大学 | Asymmetric synthesis method for botanical pesticide nicotine and anabasine |
| CN104946698A (en) * | 2015-05-22 | 2015-09-30 | 南京泽朗医药科技有限公司 | Preparation method of anabasine |
-
2016
- 2016-12-13 CN CN201611148079.8A patent/CN106719727A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1484646A (en) * | 2001-01-12 | 2004-03-24 | ��ѧ�о���Ӧ����ѯ��˾ | Mikanolide derivatives, their preparation and their therapeutic use |
| CN103283761A (en) * | 2012-02-27 | 2013-09-11 | 陕西韦尔奇作物保护有限公司 | Ethiprole-containing pesticidal composition |
| CN104341390A (en) * | 2014-11-04 | 2015-02-11 | 南开大学 | Asymmetric synthesis method for botanical pesticide nicotine and anabasine |
| CN104946698A (en) * | 2015-05-22 | 2015-09-30 | 南京泽朗医药科技有限公司 | Preparation method of anabasine |
Non-Patent Citations (3)
| Title |
|---|
| 刘莉 等: "无叶假木贼杀虫有效部位的研究", 《农药》 * |
| 李君 等: "薇甘菊杀线虫活性成分及其对番茄生长的影响", 《广东农业科学》 * |
| 石华 等: "氟虫腈悬浮剂杀灭蟑螂实验室效果观察", 《中华卫生杀虫药械》 * |
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Application publication date: 20170531 |