CN106433303A - Quick-drying ink for clothing pattern printing - Google Patents
Quick-drying ink for clothing pattern printing Download PDFInfo
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- CN106433303A CN106433303A CN201610880936.7A CN201610880936A CN106433303A CN 106433303 A CN106433303 A CN 106433303A CN 201610880936 A CN201610880936 A CN 201610880936A CN 106433303 A CN106433303 A CN 106433303A
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- quick
- dry type
- pigment
- type ink
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- 238000007639 printing Methods 0.000 title claims abstract description 18
- 238000001035 drying Methods 0.000 title abstract description 7
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 36
- 239000000049 pigment Substances 0.000 claims abstract description 27
- 239000012046 mixed solvent Substances 0.000 claims abstract description 22
- -1 polysiloxane Polymers 0.000 claims abstract description 19
- 239000002270 dispersing agent Substances 0.000 claims abstract description 18
- 239000002318 adhesion promoter Substances 0.000 claims abstract description 17
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims abstract description 16
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 16
- 239000004014 plasticizer Substances 0.000 claims abstract description 11
- 239000002131 composite material Substances 0.000 claims abstract description 8
- 239000002952 polymeric resin Substances 0.000 claims abstract description 8
- 239000004094 surface-active agent Substances 0.000 claims abstract description 8
- 229920003002 synthetic resin Polymers 0.000 claims abstract description 8
- 230000000694 effects Effects 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims description 55
- 238000003801 milling Methods 0.000 claims description 28
- 239000004576 sand Substances 0.000 claims description 28
- 229920005989 resin Polymers 0.000 claims description 23
- 239000011347 resin Substances 0.000 claims description 23
- 229920000642 polymer Polymers 0.000 claims description 14
- 239000006185 dispersion Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 238000002360 preparation method Methods 0.000 claims description 9
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 8
- 239000005062 Polybutadiene Substances 0.000 claims description 7
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 7
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 7
- 239000012467 final product Substances 0.000 claims description 7
- 229920002857 polybutadiene Polymers 0.000 claims description 7
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 7
- 239000002904 solvent Substances 0.000 claims description 7
- AXDJCCTWPBKUKL-UHFFFAOYSA-N 4-[(4-aminophenyl)-(4-imino-3-methylcyclohexa-2,5-dien-1-ylidene)methyl]aniline;hydron;chloride Chemical group Cl.C1=CC(=N)C(C)=CC1=C(C=1C=CC(N)=CC=1)C1=CC=C(N)C=C1 AXDJCCTWPBKUKL-UHFFFAOYSA-N 0.000 claims description 6
- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical group [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 claims description 6
- JNXDCMUUZNIWPQ-UHFFFAOYSA-N trioctyl benzene-1,2,4-tricarboxylate Chemical compound CCCCCCCCOC(=O)C1=CC=C(C(=O)OCCCCCCCC)C(C(=O)OCCCCCCCC)=C1 JNXDCMUUZNIWPQ-UHFFFAOYSA-N 0.000 claims description 6
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical group CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 claims description 4
- MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 claims description 2
- 239000006229 carbon black Substances 0.000 claims description 2
- 239000001054 red pigment Substances 0.000 claims description 2
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical group C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims 2
- WZZBNLYBHUDSHF-DHLKQENFSA-N 1-[(3s,4s)-4-[8-(2-chloro-4-pyrimidin-2-yloxyphenyl)-7-fluoro-2-methylimidazo[4,5-c]quinolin-1-yl]-3-fluoropiperidin-1-yl]-2-hydroxyethanone Chemical group CC1=NC2=CN=C3C=C(F)C(C=4C(=CC(OC=5N=CC=CN=5)=CC=4)Cl)=CC3=C2N1[C@H]1CCN(C(=O)CO)C[C@@H]1F WZZBNLYBHUDSHF-DHLKQENFSA-N 0.000 claims 1
- 239000004952 Polyamide Substances 0.000 claims 1
- 150000001412 amines Chemical class 0.000 claims 1
- 239000001055 blue pigment Substances 0.000 claims 1
- 229920002313 fluoropolymer Polymers 0.000 claims 1
- 239000004811 fluoropolymer Substances 0.000 claims 1
- 229920002647 polyamide Polymers 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- 238000003860 storage Methods 0.000 abstract description 4
- 239000012975 dibutyltin dilaurate Substances 0.000 abstract 1
- HGAZMNJKRQFZKS-UHFFFAOYSA-N chloroethene;ethenyl acetate Chemical compound ClC=C.CC(=O)OC=C HGAZMNJKRQFZKS-UHFFFAOYSA-N 0.000 description 7
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 description 6
- 230000007613 environmental effect Effects 0.000 description 6
- 229920006122 polyamide resin Polymers 0.000 description 6
- 239000007787 solid Substances 0.000 description 5
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical class C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 235000012730 carminic acid Nutrition 0.000 description 2
- 231100000053 low toxicity Toxicity 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 238000003892 spreading Methods 0.000 description 2
- 238000009736 wetting Methods 0.000 description 2
- 238000010146 3D printing Methods 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000011538 cleaning material Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229960004756 ethanol Drugs 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/033—Printing inks characterised by features other than the chemical nature of the binder characterised by the solvent
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/108—Hydrocarbon resins
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention provides quick-drying ink for clothing pattern printing. The ink is prepared from the following components: 30-40 parts of composite polymer resin, 10-20 parts of pigments, 6-12 parts of polysiloxane, 3-8 parts of a curing agent, 2-5 parts of a plasticizer, 2-6 parts of a dispersing agent, 1-5 parts of an adhesion promoter, 1-2 parts of dibutyltin dilaurate, 1-2 parts of the surfactant Walloxen Tr50 with the concentration of 1%-5% and 25-45 parts of a mixed solvent. The prepared environment-friendly quick-drying ink is longer in storage time and better in stability, can be completely dried when dried at 70-80 DEG C for 3 min and avoids the negative effects of deformation, color change and the like of printing stock after high-temperature baking.
Description
Technical field
The present invention relates to clothing manufacture field, more particularly to a kind of quick-dry type for carrying out pattern printing on ready-made clothes
Ink.
Background technology
In order that the class of clothing improving product in appearance so as to more eye-catching and attractive in appearance, to obtain consumer
Favor and accreditation, reach the purpose for expanding production marketing, and ready-made clothes processing industry is provided with pattern in clothing surface.At present, exist
Clothing surface arranges pattern and comprises the following steps:1st, ready-made clothes processing industry provides AI shelves data and paper mold to manufacturer；2nd, manufacturer
Set up draft；3rd, ready-made clothes processing industry confirms sign-off draft；4th, manufacturer makes the web plate of basic code；5th, ready-made clothes processing industry
Confirm the web plate of sign-off basic code；6th, manufacturer sets up the draft of all-key；7th, ready-made clothes processing industry confirms the draft of sign-off all-key；
8th, manufacturer makes the web plate of all-key；9th, setting position region；10th, position beaten by web plate；11. brush coatings/scrape gasoline water；12nd, material is joined
Double；13rd, material placement positioning；14th, core set half tone；15th, cleaning material；16th, print；17th, material dries；18th, arrangement material is tidied up
Material；19th, web plate instrument is cleaned；20th, clothing surface arranges pattern and finishes.It is above-mentioned many step of setting pattern on ready-made clothes,
Complex procedures, high processing costs, its effect of pattern of printing is undesirable.Due to arranging the clothing price of pattern on ready-made clothes
Higher, ordinary consumer is beyond affordability, so, limit the development of ready-made clothes processing industry.Therefore, highly desirable one kind of people
On ready-made clothes, the method for three-dimensional printing pattern comes out.
However, on clothing requirement of the print pattern to pad-ink also more and more higher, traditional resistance to anti-boiling ink adopts
Polyurethane, vinyl chloride-vinyl acetate resin and chlorinated polypropylene etc. as binder, using the larger butanone of toxicity, dimethylbenzene etc. as solvent,
Serious environment pollution, while work the mischief to the health of printing worker.In terms of environmental conservation, presently the most urgent is environmental protection
The preparation of type high temperature steam endurance ink and use.In order to solve the pollution problem of traditional resistance to anti-boiling ink, water color ink meet the tendency of and
Raw.But as water color ink is difficult to wetting and spreading on plastic basis material, rate of drying is slow, can't be fully achieved and beat in performance
The use standard of printing ink.Alcohol-soluble printing ink adopts the alcohols of the low toxicity such as ethanol, isopropanol as solvent, can solve the problem that traditional oils
Ink injury health and problem of solvent residual, while can improve wetting and spreading performance of the ink on plastic basis material again.But its property existing
Can need to be improved, its stability, heat-resisting, quick-drying, harmless etc. be also short of, need to go further lifting.
Content of the invention
Present invention aim to a kind of a kind of environmental protection quick-dry type ink for clothing popularity printing is provided, its storage
Deposit time length, easily good stability, solidification and pollution-free, safety and environmental protection.
For achieving the above object, the present invention is achieved by the following scheme：
A kind of quick-dry type ink for clothing popularity printing, the ink is grouped into by following group：Composition polymer tree
30～40 parts of fat, 10～20 parts of pigment, 6～12 parts of polysiloxanes, 3～8 parts of firming agent, 2～5 parts of plasticizer, dispersant 2～6
Part, 1～5 part of adhesion promoter, 1～2 part of dibutyl tin laurate, the surfactant Walloxen of 0.1%-0.9%
TR501～2 part, 25～45 parts of mixed solvent；
Wherein, the composite polymeric resin is by organosilicon modified crylic acid resin, polybutadiene and polyamide resin
Fat is in mass ratio：1：0.2～0.4：0.5～0.8 composition；The mixed solvent is by dehydrated alcohol and water in mass ratio：1：0.2～
0.5 composition；
The preparation method of the quick-dry type ink comprises the steps：First by dispersant and mixed solvent mix homogeneously, stir
Mix under state after adding composition polymer mixed with resin uniform, pour in sand milling container；Then by pigment, polysiloxanes and plasticising
Agent is separately added in sand milling container, after pre-dispersed, and rotating speed is brought up to 2500 revs/min, and sand milling disperses 50 minutes, in sand milling
Dispersion completes front 4-7 minute and adds adhesion promoter；Firming agent, dibutyl tin laurate and surface is added after the completion of dispersion
Activating agent Walloxen TR50, after stirring, obtains final product.
Wherein, described pigment includes yellow, red, blue and black pigment, and wherein, yellow uitramarine is pigment Yellow 12, pigment yellow
13, one kind of pigment yellow 17 or its mixture；Red pigment is fuchsin 4B, fuchsin 6B, one kind of fuchsin 8B or its mixture；Blue
Color pigment is Phthalocyanine Blue BGS, one kind of phthalocyanine blue b or its mixture；Its black pigment is colour carbon black.
The firming agent is by polyvinyl alcohol and diethylenetriamine by weight 1：0.5～0.7 composition
The adhesion promoter is vinyl chloride-vinyl acetate resin.
The dispersant is nonionic type dispersant, and it is 7.0-8.0 that active component is 95%, pH, without alkyl phenol second
Epoxide compound, solvent and halogenide.
The plasticizer is the one kind in dioctyl phthalate, dibutyl phthalate or trioctyl trimellitate (TOTM)
Or several combinations.
The viscosity of the quick-dry type ink is 3.7-7.1CP/25 DEG C, and it is 36- that conductivity is 730-1890 μ S, surface tension
40dyn/cm, 20 DEG C.
The invention has the beneficial effects as follows：Obtained in the present invention, the environmental protection quick-dry type ink storage time is longer, and stability is relatively
Good, under 70-80 DEG C of environment, 3min can be completely dried, it is to avoid stock due to after high-temperature baking deformation, discoloration etc. bad after
Really；In addition, it is also an advantage of the present invention that its feature of environmental protection, the use alcohol of employing, water as solvent low toxic and environment-friendly, without benzene, ketone
Class solvent, other raw materials are also nontoxic to human body and environment or low toxicity composition；In addition the present invention is using composition polymer tree
Fat, the one-component resin for contrasting prior art has preferably printing adaptability and effect, and ink adhesion reaches 0.25-
0.45N/mm2, in addition, technical solution of the present invention is used as an entirety, the mutual coordinated of each group split-phase so that the ink tool of preparation
There are excellent wear-resisting, water-fast, resistance to chemical attack and good adhesive force, its quick drying capacity can avoid ink saturating
Print, greatly improves the quick-drying of ink using the combination of dibutyl tin laurate and surfactant Walloxen TR50
Performance, and the addition of polysiloxanes improves the toughness of ink, maintains the stability of ink, storage is never degenerated for 9-15 month.
Specific embodiment
Technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that described enforcement
Example is only a part of embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, this area is common
The every other embodiment obtained under the premise of creative work is not made by technical staff, belongs to the model of present invention protection
Enclose.
Embodiment 1
A kind of quick-dry type ink for clothing popularity printing, the ink is grouped into by following group：Composition polymer tree
30 parts of fat, 10 parts of pigment Phthalocyanine Blue BGS, 6 parts of polysiloxanes, 3 parts of firming agent, 2 parts of plasticizer phthalic acid dioctyl ester, non-
2 parts of ionic type dispersant, 1 part of adhesion promoter vinyl chloride-vinyl acetate resin, 1 part of dibutyl tin laurate, 0.1% surface activity
Agent Walloxen TR501 part, 25 parts of mixed solvent；
Wherein, the composite polymeric resin is by organosilicon modified crylic acid resin, polybutadiene and polyamide resin
Fat is in mass ratio：1：0.2：0.5 composition；The mixed solvent is by dehydrated alcohol and water in mass ratio：1：0.2 composition；Described solid
Agent is by polyvinyl alcohol and diethylenetriamine by weight 1：0.5 composition；
The preparation method of the quick-dry type ink comprises the steps：First by dispersant and mixed solvent mix homogeneously, stir
Mix under state after adding composition polymer mixed with resin uniform, pour in sand milling container；Then by pigment, polysiloxanes and plasticising
Agent is separately added in sand milling container, after pre-dispersed, and rotating speed is brought up to 2500 revs/min, and sand milling disperses 50 minutes, in sand milling
Dispersion completes first 4 minutes to add adhesion promoter；Firming agent, dibutyl tin laurate and surface is added to live after the completion of dispersion
Property agent Walloxen TR50, after stirring, obtains final product.
Embodiment 2
A kind of quick-dry type ink for clothing popularity printing, the ink is grouped into by following group：Composition polymer tree
40 parts of fat, 20 parts of pigment carmine 4B, 12 parts of polysiloxanes, 8 parts of firming agent, 5 parts of plasticizer phthalic acid dibutyl ester, non-from
6 parts of subtype dispersant, 5 parts of adhesion promoter vinyl chloride-vinyl acetate resin, 2 parts of dibutyl tin laurate, 0.9% surfactant
Walloxen TR502 part, 45 parts of mixed solvent；
Wherein, the composite polymeric resin is by organosilicon modified crylic acid resin, polybutadiene and polyamide resin
Fat is in mass ratio：1：0.4：0.8 composition；The mixed solvent is by dehydrated alcohol and water in mass ratio：1：0.5 composition；Described solid
Agent is by polyvinyl alcohol and diethylenetriamine by weight 1：0.7 composition；
The preparation method of the quick-dry type ink comprises the steps：First by dispersant and mixed solvent mix homogeneously, stir
Mix under state after adding composition polymer mixed with resin uniform, pour in sand milling container；Then by pigment, polysiloxanes and plasticising
Agent is separately added in sand milling container, after pre-dispersed, and rotating speed is brought up to 2500 revs/min, and sand milling disperses 50 minutes, in sand milling
Dispersion completes first 7 minutes to add adhesion promoter；Firming agent, dibutyl tin laurate and surface is added to live after the completion of dispersion
Property agent Walloxen TR50, after stirring, obtains final product.
Embodiment 3
A kind of quick-dry type ink for clothing popularity printing, the ink is grouped into by following group：Composition polymer tree
35 parts of fat, 15 parts of pigment yellow 13,9 parts of polysiloxanes, 5 parts of firming agent, 3 parts of plasticizer trioctyl trimellitate (TOTM), nonionic type
4 parts of dispersant, 3 parts of adhesion promoter vinyl chloride-vinyl acetate resin, 2 parts of dibutyl tin laurate, 0.5% surfactant
Walloxen TR501.5 part, 35 parts of mixed solvent；
Wherein, the composite polymeric resin is by organosilicon modified crylic acid resin, polybutadiene and polyamide resin
Fat is in mass ratio：1：0.3：0.6 composition；The mixed solvent is by dehydrated alcohol and water in mass ratio：1：0.4 composition；Described solid
Agent is by polyvinyl alcohol and diethylenetriamine by weight 1：0.6 composition；
The preparation method of the quick-dry type ink comprises the steps：First by dispersant and mixed solvent mix homogeneously, stir
Mix under state after adding composition polymer mixed with resin uniform, pour in sand milling container；Then by pigment, polysiloxanes and plasticising
Agent is separately added in sand milling container, after pre-dispersed, and rotating speed is brought up to 2500 revs/min, and sand milling disperses 50 minutes, in sand milling
Dispersion completes first 6 minutes to add adhesion promoter；Firming agent, dibutyl tin laurate and surface is added to live after the completion of dispersion
Property agent Walloxen TR50, after stirring, obtains final product.
Embodiment 4
A kind of quick-dry type ink for clothing popularity printing, the ink is grouped into by following group：Composition polymer tree
32 parts of fat, 12 parts of pigment phthalocyanine blue b, 8 parts of polysiloxanes, 4 parts of firming agent, 3 parts of plasticizer phthalic acid dioctyl ester, non-from
3 parts of subtype dispersant, 2 parts of adhesion promoter vinyl chloride-vinyl acetate resin, 1 part of dibutyl tin laurate, 0.4% surfactant
Walloxen TR501 part, 30 parts of mixed solvent；
Wherein, the composite polymeric resin is by organosilicon modified crylic acid resin, polybutadiene and polyamide resin
Fat is in mass ratio：1：0.2：0.6 composition；The mixed solvent is by dehydrated alcohol and water in mass ratio：1：0.3 composition；Described solid
Agent is by polyvinyl alcohol and diethylenetriamine by weight 1：0.6 composition；
The preparation method of the quick-dry type ink comprises the steps：First by dispersant and mixed solvent mix homogeneously, stir
Mix under state after adding composition polymer mixed with resin uniform, pour in sand milling container；Then by pigment, polysiloxanes and plasticising
Agent is separately added in sand milling container, after pre-dispersed, and rotating speed is brought up to 2500 revs/min, and sand milling disperses 50 minutes, in sand milling
Dispersion completes first 5 minutes to add adhesion promoter；Firming agent, dibutyl tin laurate and surface is added to live after the completion of dispersion
Property agent Walloxen TR50, after stirring, obtains final product.
Embodiment 5
A kind of quick-dry type ink for clothing popularity printing, the ink is grouped into by following group：Composition polymer tree
36 parts of fat, 16 parts of pigment carmine 8B, 10 parts of polysiloxanes, 7 parts of firming agent, 4 parts of plasticizer phthalic acid dibutyl ester, non-from
5 parts of subtype dispersant, 4 parts of adhesion promoter vinyl chloride-vinyl acetate resin, 2 parts of dibutyl tin laurate, 0.7% surfactant
Walloxen TR502 part, 38 parts of mixed solvent；
Wherein, the composite polymeric resin is by organosilicon modified crylic acid resin, polybutadiene and polyamide resin
Fat is in mass ratio：1：0.4：0.7 composition；The mixed solvent is by dehydrated alcohol and water in mass ratio：1：0.4 composition；Described solid
Agent is by polyvinyl alcohol and diethylenetriamine by weight 1：0.7 composition；
The preparation method of the quick-dry type ink comprises the steps：First by dispersant and mixed solvent mix homogeneously, stir
Mix under state after adding composition polymer mixed with resin uniform, pour in sand milling container；Then by pigment, polysiloxanes and plasticising
Agent is separately added in sand milling container, after pre-dispersed, and rotating speed is brought up to 2500 revs/min, and sand milling disperses 50 minutes, in sand milling
Dispersion completes first 6 minutes to add adhesion promoter；Firming agent, dibutyl tin laurate and surface is added to live after the completion of dispersion
Property agent Walloxen TR50, after stirring, obtains final product.
The present invention has carried out the test of respective performances to the ink of embodiment 1-5, the results are shown in Table 1：
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of spirit or essential attributes without departing substantially from the present invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of description is only that those skilled in the art should for clarity
Using description as an entirety, the technical scheme in each embodiment can also form those skilled in the art through appropriately combined
Understandable other embodiment.
Claims (7)
1. a kind of quick-dry type ink for clothing popularity printing, it is characterised in that the ink is grouped into by following group：Compound
30～40 parts of fluoropolymer resin, 10～20 parts of pigment, 6～12 parts of polysiloxanes, 3～8 parts of firming agent, 2～5 parts of plasticizer, point
2～6 parts of powder, 1～5 part of adhesion promoter, 1～2 part of dibutyl tin laurate, the surfactant of 0.1%-0.9%
WalloxenTR501～2 part, 25～45 parts of mixed solvent；
Wherein, the composite polymeric resin is pressed by organosilicon modified crylic acid resin, polybutadiene and polyamide
Mass ratio：1：0.2～0.4：0.5～0.8 composition；The mixed solvent is by dehydrated alcohol and water in mass ratio：1：0.2～0.5
Composition；
The preparation method of the quick-dry type ink comprises the steps：First by dispersant and mixed solvent mix homogeneously, shape is stirred
After adding composition polymer mixed with resin uniform under state, pour in sand milling container；Then pigment, polysiloxanes and plasticizer are divided
After pre-dispersed, rotating speed Jia Ru not brought up to 2500 revs/min in sand milling container, sand milling disperses 50 minutes, disperse in sand milling
Completing front 4-7 minute adds adhesion promoter；Firming agent, dibutyl tin laurate and surface activity is added after the completion of dispersion
Agent Walloxen TR50, after stirring, obtains final product.
2. quick-dry type ink according to claim 1, it is characterised in that described pigment includes yellow, red, blue and black face
Material, wherein, yellow uitramarine is pigment Yellow 12, pigment yellow 13, one kind of pigment yellow 17 or its mixture；Red pigment is fuchsin
4B, fuchsin 6B, one kind of fuchsin 8B or its mixture；Blue pigment is Phthalocyanine Blue BGS, one kind of phthalocyanine blue b or its mixture；
Its black pigment is colour carbon black.
3. quick-dry type ink according to claim 1, it is characterised in that the firming agent is by polyvinyl alcohol and divinyl three
Amine by weight 1：0.5～0.7 composition.
4. quick-dry type ink according to claim 1, it is characterised in that the adhesion promoter be.
5. quick-dry type ink according to claim 1, it is characterised in that the dispersant is nonionic type dispersant,
It is 7.0-8.0 that active component is 95%, pH, without alkylphenol ethoxylate, solvent and halogenide.
6. quick-dry type ink according to claim 1, it is characterised in that the plasticizer is dioctyl phthalate,
The combination of one or more in dibutyl phthalate or trioctyl trimellitate (TOTM).
7. quick-dry type ink according to claim 1, it is characterised in that the viscosity of the quick-dry type ink be
7.1CP/25 DEG C, it is 36-40dyn/cm that conductivity is 730-1890 μ S, surface tension, 20 DEG C.
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| CN201610880936.7A CN106433303A (en) | 2016-09-30 | 2016-09-30 | Quick-drying ink for clothing pattern printing |
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| CN201610880936.7A CN106433303A (en) | 2016-09-30 | 2016-09-30 | Quick-drying ink for clothing pattern printing |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113831799A (en) * | 2021-10-19 | 2021-12-24 | 黄明彦 | Quick-drying water-based paint |
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